CN111956573A - Infant water cream and preparation method thereof - Google Patents
Infant water cream and preparation method thereof Download PDFInfo
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- A61Q19/00—Preparations for care of the skin
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Abstract
The invention relates to an infant water cream which comprises the following components in parts by weight: the phase A component consists of PEG/PPG-20/15 dimethyl silicone polymer, isononyl isononanoate, cyclopentadecyl dimethyl silicone polymer, isostearyl alcohol (and) butanediol cocoyl ester; the phase B component comprises water, sodium chloride, glycerol, butanediol, xanthan gum, sodium hyaluronate, dipotassium glycyrrhizinate, trehalose, a chamomile extracting solution, a mallow flower extracting solution, a peony root extracting solution, a honeysuckle flower extracting solution, an extract of roots and rhizomes of dandelion, a Chinese violet extracting solution, echinaconine, a Chinese wolfberry fruit extract and an aloe barbadensis leaf extract; the phase C component consists of caprylyl hydroximic acid, ethylhexyl glycerin and 1, 2-hexanediol. According to the invention, the market demand is combined, the unique moisturizing mechanism of the natural green moisturizing agent Linlan moisturizing lotion is skillfully utilized, the moisture content of the skin is instantly and permanently improved from the outside to the inside, and the moisturizing composition is matched with other moisturizing combinations to achieve a better moisturizing effect through interaction.
Description
Technical Field
The invention relates to the technical field of infant products, in particular to infant water cream and a preparation method thereof.
Background
It is said that women are made of water, and the water content of the skin of normal people is 20-35 parts, and the water in the skin is a prerequisite for keeping the skin healthy, preventing the skin from aging, moistening and beautifying the skin. From the viewpoint of skin histology, the skin is a layered structure, which is composed of an epidermal layer, a basement membrane and a dermal layer from outside to inside, and the dermis and the epidermis are divided and connected by the basement membrane, which together constitute a skin moisturizing system. The dermis layer is the "water source", the basement membrane is the "canal", and the stratum corneum is the "dam". Problems occur in any link of the moisturizing system, and the skin can not finish self repair. The effective moisture-keeping nursing can delay the aging of normal skin, improve the tolerance degree of the skin to external stimulation and can prevent the occurrence of skin diseases.
The skin care products of the same type on the market are mostly poor in water replenishing capacity, poor in continuous water replenishing capacity and the like. At present, the natural moisturizer which is excellent in moisturizing performance and one dosage of natural moisturizers is not ideal, and most of the natural moisturizers are additives with a single moisturizing function, only can achieve the moisturizing effect, but cannot meet other skin care requirements of consumers such as skin elasticity enhancement, skin barrier enhancement, blood microcirculation promotion and the like.
In conclusion, the development of the infant high-moisture cosmetic with scientific moisturizing effect has practical significance and broad market prospect.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provides an infant water cream and a preparation method thereof.
The purpose of the invention is realized by the following technical scheme:
the infant water cream comprises the following components in parts by weight:
phase A component: 3.1-18 parts;
b phase component: 79-96.87 parts;
c phase component: 0.03-3 parts;
the phase A component consists of PEG/PPG-20/15 polydimethylsiloxane, isononyl isononanoate, cyclopentadecyldimethyl siloxane, isostearyl alcohol (and) butanediol cocoate;
the phase B component comprises water, sodium chloride, glycerol, butanediol, xanthan gum, sodium hyaluronate, dipotassium glycyrrhizinate, trehalose, a chamomile extracting solution, a mallow flower extracting solution, a peony root extracting solution, a honeysuckle flower extracting solution, an ohaiba rhizome and root extract solution, a Chinese violet extracting solution, a dendrobium nobile extracting solution, a sophora flavescens root extract, echinaconine, a Chinese wolfberry fruit extract and an aloe barbadensis leaf extract;
the phase C component consists of caprylyl hydroximic acid, ethylhexyl glycerin and 1, 2-hexanediol.
Further, the infant water cream comprises the following components in parts by weight:
phase A component: 0.1-2 parts of PEG/PPG-20/15 polydimethylsiloxane, 1-5 parts of isononyl isononanoate, 1-5 parts of cyclopentasiloxane and 1-6 parts of isostearyl alcohol (and) butanediol cocoate;
b phase component: adding water to 100 parts, sodium chloride 0.1-2 parts, glycerol 5-10 parts, butanediol 1-10 parts, xanthan gum 0.1-0.5 part, sodium hyaluronate 0.01-0.1 part, dipotassium glycyrrhizinate 0.1-5 parts, trehalose 0.1-5 parts, chamomile extract 0.1-2 parts, mallow flower extract 0.1-2 parts, radix Paeoniae extract 0.1-2 parts, flos Lonicerae extract 0.1-2 parts, herba Taraxaci rhizome and root extract 0.1-2 parts, herba Violae extract 0.1-2 parts, herba Dendrobii extract 0.1-2 parts, radix Sophorae Flavescentis extract 0.1-2 parts, Echinacea purpurea extract 0.1-2 parts, fructus Lycii extract 0.1-2 parts, and Aloe Barbadensis leaf extract 0.5-10 parts;
c phase component: 0.01-1 part of caprylyl hydroximic acid, 0.01-1 part of ethylhexyl glycerol and 0.01-1 part of 1, 2-hexanediol.
Further, the water is deionized water.
The preparation method of the infant water cream comprises the following steps:
s1, adding the materials of the phase B component into a water phase pot, stirring and heating to 80-85 ℃, keeping the temperature for 20-40min, sterilizing, stirring and cooling to 40 ℃, and taking the mixture as a water phase for later use;
s2, adding the phase A component into an emulsifying pot, and slowly pumping the water phase into the emulsifying pot under stirring;
s3, adding the phase C after uniformly stirring, and stirring and mixing for 3-5 min;
and S4, detecting to be qualified, and filtering and discharging the material by using a 200-mesh filter screen.
Further, in the step (1), the heating specifically comprises the following steps: firstly, heating the materials in the water phase pot at a heating speed of 2-4 ℃/min until the temperature in the water phase pot reaches 80-85 ℃.
Further, in the step (1), the cooling speed is 4-6 ℃/min during cooling.
Further, in the step (2), when the water phase is pumped, the total time of pumping the water phase is 2-3h, so that the water phase is completely wrapped by the oil phase.
Further, in the step (3), the stirring speed is 20-30 rpm.
The invention has the following advantages:
1. according to market demands, the unique moisturizing mechanism of the natural green moisturizing agent Linlan moisturizing lotion is skillfully applied, the moisture content of the skin is instantly and permanently improved from the outside to the inside, and the moisturizing composition is matched with other moisturizing combinations to achieve a better moisturizing effect through interaction.
2. The stability problem is well solved by adopting a double-gel emulsification technology, and the double-gel emulsification technology stabilizes the violent repulsion among liquid drops by the fact that ethyl cellulose exists in an oil-water two-phase interface, thereby preventing the liquid drops from aggregating and flocculating; the hardness of the dispersed particles formed by the hydrogel and oleogel may also reduce the tendency of the dispersion to flocculate.
3. The moisture-absorbing and moisture-retaining facial mask is lightly applied to the skin to release a large amount of moisture, instantly moisturizes and permanently retains moisture, is cool and comfortable in skin feel, is convenient to use and remarkable in effect, can bring cool and comfortable feeling to the skin due to the release of the moisture, can take away part of heat, and has the effect of improving silky and smooth feeling.
Detailed Description
The invention is further described below with reference to examples, but the scope of the invention is not limited to the following.
[ example 1 ]
The infant water cream comprises the following components in parts by weight:
phase A component: 0.1 part of PEG/PPG-20/15 dimethyl silicone polymer, 1 part of isononyl isononanoate, 1 part of cyclopentasiloxane and 1 part of isostearyl alcohol (and) butanediol cocoate;
b phase component: adding water to 34.27 parts, 2 parts of sodium chloride, 10 parts of glycerol, 10 parts of butanediol, 0.5 part of xanthan gum, 0.1 part of sodium hyaluronate, 5 parts of dipotassium glycyrrhizinate, 5 parts of trehalose, 2 parts of an extracting solution of chamomile, 2 parts of an extracting solution of malva sylvestris, 2 parts of an extracting solution of radix paeoniae alba, 2 parts of an extracting solution of honeysuckle flower, 2 parts of an extract solution of rhizomes and roots of dandelion, 2 parts of an extracting solution of herba violae, 2 parts of an extracting solution of dendrobium nobile, 2 parts of an extract of roots of sophora flavescens, 2 parts of echinacea purpurea, 2 parts of an extract of fruits of lycium barbarum and 10 parts of an extract of leaves of aloe barbadensi;
c phase component: 0.01 part of caprylyl hydroximic acid, 0.01 part of ethylhexyl glycerol and 0.01 part of 1, 2-hexanediol.
Further, the water is deionized water.
The preparation method of the infant water cream comprises the following steps:
s1, adding the materials of the phase B component into a water phase pot, heating to 85 ℃ with stirring at a heating speed of 4 ℃/min, keeping the temperature for 20min, sterilizing, cooling to 40 ℃ with stirring, and cooling to 6 ℃/min as a water phase for later use;
s2, adding the phase A component into an emulsifying pot, slowly pumping the water phase into the emulsifying pot under stirring, wherein when the water phase is pumped, the total time of pumping the water phase into the emulsifying pot is 2 hours, and ensuring that the water phase is completely wrapped by the oil phase;
s3, adding the phase C after stirring uniformly, stirring and mixing for 5min, wherein the stirring speed is 20 rpm;
and S4, detecting to be qualified, and filtering and discharging the material by using a 200-mesh filter screen.
Further, in the step (1), the heating specifically comprises the following steps: the materials in the water phase pot are heated until the temperature in the water phase pot reaches 85 ℃.
[ example 2 ]
The infant water cream comprises the following components in parts by weight:
phase A component: 1 part of PEG/PPG-20/15 polydimethylsiloxane, 3 parts of isononyl isononanoate, 3 parts of cyclopentasiloxane and 3.5 parts of isostearyl alcohol (and) butanediol cocoate;
b phase component: 53.65 parts of water, 1 part of sodium chloride, 7.5 parts of glycerol, 5.5 parts of butanediol, 0.3 part of xanthan gum, 0.05 part of sodium hyaluronate, 2.5 parts of dipotassium glycyrrhizinate, 2.5 parts of trehalose, 1 part of chamomile extract, 1 part of mallotus flower extract, 1 part of peony root extract, 1 part of honeysuckle flower extract, 1 part of dandelion rhizome and root extract, 1 part of Chinese violet extract, 1 part of dendrobium nobile extract, 1 part of sophora flavescens root extract, 1 part of echinacea purpurea, 1 part of lycium barbarum fruit extract and 5 parts of aloe barbadensis leaf extract;
c phase component: 0.5 part of caprylyl hydroximic acid, 0.5 part of ethylhexyl glycerol and 0.5 part of 1, 2-hexanediol.
Further, the water is deionized water.
The preparation method of the infant water cream comprises the following steps:
s1, adding the materials of the phase B component into a water phase pot, heating to 83 ℃ with stirring at a heating rate of 3 ℃/min, keeping the temperature for 30min, sterilizing, cooling to 40 ℃ with stirring, and cooling at a cooling rate of 5 ℃/min to obtain a water phase for later use;
s2, adding the phase A component into an emulsifying pot, slowly pumping the water phase into the emulsifying pot under stirring, wherein when the water phase is pumped, the total time of pumping the water phase into the emulsifying pot is 2.5 hours, and ensuring that the water phase is completely wrapped by the oil phase;
s3, adding the phase C after uniformly stirring, stirring and mixing for 3-5 min, wherein the stirring speed is 25 rpm;
and S4, detecting to be qualified, and filtering and discharging the material by using a 200-mesh filter screen.
Further, in the step (1), the heating specifically comprises the following steps: the materials in the water phase pot are heated until the temperature in the water phase pot reaches 83 ℃.
[ example 3 ]
The infant water cream comprises the following components in parts by weight:
phase A component: 2 parts of PEG/PPG-20/15 polydimethylsiloxane, 5 parts of isononyl isononanoate, 5 parts of cyclopentasiloxane and 6 parts of isostearyl alcohol (and) butanediol cocoate;
b phase component: adding water to 71.09 parts, sodium chloride 0.1 part, glycerol 5 parts, butanediol 1 part, xanthan gum 0.1 part, sodium hyaluronate 0.01 part, dipotassium glycyrrhizinate 0.1 part, trehalose 0.1 part, flos Matricariae Chamomillae extract 0.1 part, Mallotus flower extract 0.1 part, radix Paeoniae extract 0.1 part, flos Lonicerae extract 0.1 part, herba Taraxaci rhizome and root extract 0.1 part, herba Violae extract 0.1 part, herba Dendrobii extract 0.1 part, radix Sophorae Flavescentis extract 0.1 part, Echinacea purpurea extract 0.1 part, fructus Lycii extract 0.1 part and Aloe Barbadensis leaf extract 0.5 part;
c phase component: 1 part of caprylyl hydroximic acid, 1 part of ethylhexyl glycerol and 1, 2-hexanediol.
Further, the water is deionized water.
The preparation method of the infant water cream comprises the following steps:
s1, adding the materials of the phase B component into a water phase pot, heating to 80 ℃ with stirring at a temperature of 2 ℃/min, keeping the temperature for 40min, sterilizing, cooling to 40 ℃ with stirring, and cooling to 4 ℃/min as a water phase for later use;
s2, adding the phase A component into an emulsifying pot, slowly pumping the water phase into the emulsifying pot under stirring, wherein when the water phase is pumped, the total time for pumping the water phase into the emulsifying pot is 3 hours, and ensuring that the water phase is completely wrapped by the oil phase;
s3, adding the phase C after uniformly stirring, stirring and mixing for 3min, wherein the stirring speed is 30 rpm;
and S4, detecting to be qualified, and filtering and discharging the material by using a 200-mesh filter screen.
Further, in the step (1), the heating specifically comprises the following steps: the materials in the water phase pot are heated until the temperature in the water phase pot reaches 80 ℃.
Effect testing
1. Moisture retention test
The experimental environment is as follows: subjects were 30, and the experimental procedure controlled for relative humidity (30+5 parts) and temperature (25+1 ℃).
And (4) judging the standard: the moisture content of the skin was measured at 1h, 4h, and 8h, respectively.
The using method comprises the following steps: after the test subject sits still for 20min, the moisture content of the stratum corneum of the skin before application of the sample to the test area (T0) was tested, and then the test substance was applied in a prescribed amount, the moisture cream A, B of examples 1 and 2 and the moisture cream of comparative sample C, D were selected, gently applied to the inner skin surface of the arm of the test subject, and the test area was marked at 5, and randomly assigned to apply examples 1, 2, 3, and 4 and the control area without any product applied thereto. During the experiment, the forearm of the subject was exposed and left in the test condition to remain relaxed.
The smearing dosage of the product is as follows: coating area: 3cm × 3cm, application dose: 2mg/cm2。
The experimental result proves that the moisture content of the skin obviously rises after being smeared for 1 hour, the moisture content of the examples 1 and 2 slowly decreases along with the lapse of time, and a certain value can be kept after 8 hours and is higher than that of comparative group data, which shows that the moisture content of the skin can be obviously improved and the moisturizing effect is durable.
2. Stability test
The experimental environment is as follows: the refrigerator was adjusted to (-5 to-15 ℃). And (4) judging the standard: and (4) after the room temperature is recovered, comparing the samples with another sample, and observing whether phenomena such as thinning, color change, layering and the like exist or not to judge the cold resistance of the samples.
The test method comprises the following steps: the water cream A, B of examples 1 and 2 and the water cream of comparative sample C, D were selected, and each sample was taken in two portions, one portion was placed in a refrigerator for 24 hours and then taken out, and the other portion was placed at normal temperature.
The results of the experiment are as follows:
| time of day | A | B | C | D |
| 24h | △ | △ | △ | ▲ |
| 1 month | △ | △ | ▲ | ▲ |
| 2 months old | △ | △ | ▲ | ● |
| 3 months old | △ | △ | ● | ● |
Remarking: the triangle is stable, a little water is produced, and ● water is serious.
The experimental results demonstrate that the cold resistance stability of example 1 and example 2 is excellent. The cold resistance stability of the water cream can be enhanced by the invention.
In conclusion, the baby moisture cream prepared by the invention adopts a double-gel emulsification technology and a unique moisturizing idea, so that when a large amount of moisture is emitted after being applied, the moisture of the skin is instantly and permanently improved, the skin is cool and comfortable, and the skin is smooth, and the defect of lacking stability of the moisture cream on the market is well solved. The natural moisture-keeping components have high safety and safe and reliable use, and are suitable for infants.
In recent years, Chinese herbal medicine extracts serving as additives of beauty and skin care cosmetics have the advantages of stable and lasting drug effect, remarkable curative effect, mild skin effect, high safety and the like, so that consumers prefer a natural green moisturizing agent extracted from Chinese herbal medicines, and the natural green moisturizing agent has special skin care effect while moisturizing, and is safer and more reliable.
The invention utilizes the unique moisturizing mechanism of the natural green moisturizing agent, and the combination of various natural moisturizing agents has the exterior and interior, and can instantly and long-term improve the moisture content of the skin. A new idea of moisturizing: the mallow occidentalis is natural and moisture-retaining, has the functions of coordinating skin and helping to clean old waste cutin, and is added into cosmetics to enable the skin to be pure, fine and tender, so that the sensitive skin is relieved, and the pressure is relieved. The radix Paeoniae, the effective component of which is paeoniflorin, has inhibitory effect on some pathogenic bacteria and fungi, and can achieve bacteriostatic effect. The flos Lonicerae contains luteolin with antibacterial and antiinflammatory effects. The dandelion rhizome and root also have anti-inflammatory and antibacterial effects. Viola yedoensis Makino has the effects of clearing heat and removing toxicity, cooling blood and relieving swelling, and clearing heat and promoting diuresis. The flos Matricariae Chamomillae, i.e. flos Matricariae Chamomillae, contains volatile oil, flavonoid, amino acids, chlorogenic acid and microelements, etc., and the flos Chrysanthemi extract has biological activities of resisting bacteria, resisting oxidation, diminishing inflammation, relieving and resisting allergy, etc. The dendrobium stem extract has the effects of supplementing fluid and promoting the production of body fluid, and activates aquaporin AQP3 to express, so that a 'canal' is unblocked; the extract of the sophora flavescens roots can clear heat, inhibit fire, inhibit the activity of hyaluronidase and consolidate 'water source'; echinacea purpurea extract, water retention and screen protection, improvement of filaggrin FLG mRNA expression and sluice protein CLDN-1mRNA expression, and firm dam; the extract of the barbary wolfberry fruit, the aloe barbadensis leaf, has the effects of nourishing and moistening yin and immediately and long-acting smoothing fine lines and scraps.
Stem extract of dendrobium nobile: ming Li Shizhen (compendium of materia Medica, Caojiu, Dendrobii officinals): the roots of the bouquet of the Congsheng stone are tangled and frequently watered with water … …, which is not dead after years and is commonly called as millennium moistening. The ancient praise refers to the Chinese characters of 'Qianjin grass, Soft gold' and 'the head of the Chinese Jiudao Xiancao'. The effective substances of the dendrobium nobile can promote the expression of aquaporin AQP3 in epidermal keratinocytes (HaCaT cells), improve the activity of the keratinocytes, and effectively improve the moisture content of the skin and the expression of aquaporin AQP 3. Matched with mallow occidentalis, sophora flavescens root extract, echinacea purpurea extract, fructus lycii extract, aloe barbadensis leaf extract and the like, the hyaluronic acid enzyme activity is further inhibited, the expression of filaggrin FLG mRNA and the expression of sluice protein CLDN-1mRNA are further improved, and fine lines and scraps are smoothed instantly and in a long-acting manner.
After the water content of the water-in-oil moisture cream is increased, the water-in-oil moisture cream often has the defect of lacking stability, and the stability is improved in order to keep the original effect unchanged. The invention well solves the stability problem by utilizing the double-gel emulsification technology, and the double-gel emulsification technology stabilizes the violent repulsion among liquid drops by the existence of ethyl cellulose at an oil-water two-phase interface, thereby preventing the liquid drops from aggregating and flocculating; the hardness of the dispersed particles formed by the hydrogel and oleogel may also reduce the tendency of the dispersion to flocculate; the structure is different from the traditional emulsification system, and can better enhance the stability of the system.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (8)
1. An infant water cream, characterized in that: the composition comprises the following components in parts by weight:
phase A component: 3.1-18 parts;
b phase component: 79-96.87 parts;
c phase component: 0.03-3 parts;
the phase A component consists of PEG/PPG-20/15 polydimethylsiloxane, isononyl isononanoate, cyclopentadecyldimethyl siloxane, isostearyl alcohol (and) butanediol cocoate;
the phase B component comprises water, sodium chloride, glycerol, butanediol, xanthan gum, sodium hyaluronate, dipotassium glycyrrhizinate, trehalose, a chamomile extracting solution, a mallow flower extracting solution, a peony root extracting solution, a honeysuckle flower extracting solution, an ohaiba rhizome and root extract solution, a Chinese violet extracting solution, a dendrobium nobile extracting solution, a sophora flavescens root extract, echinaconine, a Chinese wolfberry fruit extract and an aloe barbadensis leaf extract;
the phase C component consists of caprylyl hydroximic acid, ethylhexyl glycerin and 1, 2-hexanediol.
2. An infant moisture cream as claimed in claim 1, wherein: the composition comprises the following components in parts by weight:
phase A component: 0.1-2 parts of PEG/PPG-20/15 polydimethylsiloxane, 1-5 parts of isononyl isononanoate, 1-5 parts of cyclopentasiloxane and 1-6 parts of isostearyl alcohol (and) butanediol cocoate;
b phase component: adding water to 100 parts, sodium chloride 0.1-2 parts, glycerol 5-10 parts, butanediol 1-10 parts, xanthan gum 0.1-0.5 part, sodium hyaluronate 0.01-0.1 part, dipotassium glycyrrhizinate 0.1-5 parts, trehalose 0.1-5 parts, chamomile extract 0.1-2 parts, mallow flower extract 0.1-2 parts, radix Paeoniae extract 0.1-2 parts, flos Lonicerae extract 0.1-2 parts, herba Taraxaci rhizome and root extract 0.1-2 parts, herba Violae extract 0.1-2 parts, herba Dendrobii extract 0.1-2 parts, radix Sophorae Flavescentis extract 0.1-2 parts, Echinacea purpurea extract 0.1-2 parts, fructus Lycii extract 0.1-2 parts, and Aloe Barbadensis leaf extract 0.5-10 parts;
c phase component: 0.01-1 part of caprylyl hydroximic acid, 0.01-1 part of ethylhexyl glycerol and 0.01-1 part of 1, 2-hexanediol.
3. An infant moisture cream as claimed in claim 2, wherein: the water is deionized water.
4. A method of preparing an infant moisture cream according to any one of claims 1 to 3, wherein: the method comprises the following steps:
s1, adding the materials of the phase B component into a water phase pot, stirring and heating to 80-85 ℃, keeping the temperature for 20-40min, sterilizing, stirring and cooling to 40 ℃, and taking the mixture as a water phase for later use;
s2, adding the phase A component into an emulsifying pot, and slowly pumping the water phase into the emulsifying pot under stirring;
s3, adding the phase C after uniformly stirring, and stirring and mixing for 3-5 min;
and S4, detecting to be qualified, and filtering and discharging the material by using a 200-mesh filter screen.
5. The method of claim 4, wherein the method comprises: in the step (1), the heating comprises the following specific operation steps: firstly, heating the materials in the water phase pot at a heating speed of 2-4 ℃/min until the temperature in the water phase pot reaches 80-85 ℃.
6. The method of claim 5, wherein the method comprises: in the step (1), the cooling speed is 4-6 ℃/min during cooling.
7. The infant water cream and the preparation method thereof according to claim 4, wherein the infant water cream comprises: in the step (2), when the water phase is pumped, the total time for pumping the water phase is 2-3h, and the water phase is completely wrapped by the oil phase.
8. The infant water cream and the preparation method thereof according to claim 4, wherein the infant water cream comprises: in the step (3), the stirring speed is 20-30 rpm.
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| CN114073657A (en) * | 2021-11-17 | 2022-02-22 | 广州市添姿彩精细化工有限公司 | Multi-effect cream for infants and preparation method thereof |
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Application publication date: 20201120 |