CN109771326B - Composition for whitening and repairing mask - Google Patents
Composition for whitening and repairing mask Download PDFInfo
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- CN109771326B CN109771326B CN201910216867.3A CN201910216867A CN109771326B CN 109771326 B CN109771326 B CN 109771326B CN 201910216867 A CN201910216867 A CN 201910216867A CN 109771326 B CN109771326 B CN 109771326B
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Abstract
The invention relates to the technical field of cosmetics, in particular to a composition for a whitening and repairing mask and a preparation method thereof. The invention provides a composition for a whitening and repairing mask, which is prepared from a raw material comprising a component A, a component B and water; wherein, the component A comprises magnesium ascorbyl phosphate, humectant, xanthan gum, dipotassium glycyrrhizinate, sodium hyaluronate, biogel-1, mushroom dextran, hydrated silica, hydrolyzed sodium hyaluronate and potassium citrate, and the component B comprises 1.2-hexanediol and p-hydroxyacetophenone.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to a composition for a whitening and repairing mask and a preparation method thereof.
Background
With the improvement of living standard, beauty and skin care are more and more emphasized, the requirements of people on the efficacy and safety of skin care products are higher and higher, and facial color spots and facial roughness caused by heredity, ultraviolet irradiation or other reasons also become problems which plague people of all ages.
The facial mask is convenient to use, can integrate cleaning, nursing and nutrition into a whole, is popular with consumers, inhibits sebum secretion and sweat evaporation to increase the temperature of the skin by blocking the contact between the skin and the air, thereby promoting the blood circulation of the facial skin; the skin can be ruddy and glossy due to the accelerated blood circulation, and after the skin absorbs more moisture, nutrient essence and various effective components, the skin can effectively improve the water shortage and dullness of the skin, reduce the generation of fine wrinkles, delay the skin aging and play the roles of removing freckles and acnes to a certain extent; the facial mask can soften cutin, dilate pores, promote sweat gland secretion, and remove epidermal cell metabolite, thereby achieving the effects of cleaning and caring skin.
However, the existing facial masks with whitening effect on the market also have potential defects and hazards, for example, most facial masks contain irritant chemical components, and the skin becomes sensitive after long-term use, so that the phenomena of obturator, acne generation, allergy, aging and the like are more easily caused; when some facial masks are used, the absorption of skin is less, and the utilization rate is low; some mask components or systems are unstable in environment, harsh in storage condition, short in period and easy to deteriorate, so that the preparation of the safe and efficient multifunctional whitening mask is very important.
Disclosure of Invention
In order to solve the technical problems, the invention provides a composition for a whitening and repairing mask, which is prepared from a raw material comprising a component A, a component B and water; wherein, the component A comprises magnesium ascorbyl phosphate, humectant, xanthan gum, dipotassium glycyrrhizinate, sodium hyaluronate, biogel-1, mushroom dextran, hydrated silica, hydrolyzed sodium hyaluronate and potassium citrate, and the component B comprises 1.2-hexanediol and p-hydroxyacetophenone.
In a preferred embodiment of the present invention, the component a further comprises niacinamide and allantoin.
As a preferable technical scheme of the invention, the pH value of the composition is 7.5-7.8.
In a preferable embodiment of the present invention, the weight ratio of nicotinamide, allantoin, magnesium ascorbyl phosphate and potassium citrate is (0.5-10): (0.1-1.0): (0.5-7.0): (0.1-8.0).
As a preferable technical scheme of the invention, the weight ratio of the component A to the component B is (3-65): (0.2-4.0).
According to a preferable technical scheme of the invention, the preparation raw materials comprise, by weight, 0.5-7.0% of magnesium ascorbyl phosphate, 0.5-10% of nicotinamide, 0.4-18% of a humectant, 0.1-1.0% of xanthan gum, 0.1-1.0% of allantoin, 0.1-1.0% of dipotassium glycyrrhizinate, 0.01-0.5% of sodium hyaluronate, 0.1-6.0% of bioglycan-1, 0.1-6.0% of mushroom dextran, 0.1-3.0% of hydrated silica, 0.01-0.5% of hydrolyzed sodium hyaluronate, 0.1-8.0% of potassium citrate, 0.1-3.0% of 1.2-hexanediol, 0.1-3.0% of p-hydroxyacetophenone and the balance of water.
The preferable technical scheme of the invention is that the weight average molecular weight of the hydrolyzed sodium hyaluronate is 500-10000.
The preferable technical scheme of the invention is that the weight average molecular weight of the sodium hyaluronate is 60000-500000.
The second aspect of the invention provides a preparation method of the composition, phase A component is added into water and stirred evenly; stirring and uniformly stirring the component B; and mixing them uniformly to obtain the invented facial mask composition.
In a third aspect of the present invention, there is provided a whitening and repairing mask comprising the composition of the repairing mask.
Compared with the prior art, the invention has the following beneficial effects: the composition provided by the invention can effectively improve the whitening effect and moisturizing effect of skin, and components of the composition can be well absorbed by the skin in the using process, so that the generation of white substances on the surface of the skin due to incomplete absorption is avoided; also is beneficial to promoting wound healing, treating inflammation, removing acne marks and resisting wrinkles; on the other hand, the composition can effectively avoid the generation of allergic phenomena such as erythra and the like, and the application range of the product is expanded.
Detailed Description
In order to solve the technical problems, the invention provides a composition for a whitening and repairing mask, which is prepared from a raw material comprising a component A, a component B and water; wherein, the component A comprises magnesium ascorbyl phosphate, humectant, xanthan gum, dipotassium glycyrrhizinate, sodium hyaluronate, biogel-1, mushroom dextran, hydrated silica, hydrolyzed sodium hyaluronate and potassium citrate, and the component B comprises 1.2-hexanediol and p-hydroxyacetophenone.
In one embodiment, the a component further comprises niacinamide and allantoin.
Preferably, in one embodiment, the pH of the composition is from 7.5 to 7.8.
Preferably, in one embodiment, the weight ratio of the nicotinamide, the allantoin, the magnesium ascorbyl phosphate and the potassium citrate is (0.5-10): (0.1-1.0): (0.5-7.0): (0.1 to 8.0); more preferably, the weight ratio of the nicotinamide, the allantoin, the magnesium ascorbyl phosphate and the potassium citrate is (2-8): (0.3-0.8): (2.0-5.0): (2.0-6.0); more preferably, the weight ratio of nicotinamide, allantoin, magnesium ascorbyl phosphate and potassium citrate is 6.0: 0.5: 3.5: 4.5.
in one embodiment, the weight ratio of the component A to the component B is (3-65): (0.2-4.0).
Preferably, the composition is prepared from 0.5-7.0% of magnesium ascorbyl phosphate, 0.5-10% of nicotinamide, 0.4-18% of humectant, 0.1-1.0% of xanthan gum, 0.1-1.0% of allantoin, 0.1-1.0% of dipotassium glycyrrhizinate, 0.01-0.5% of sodium hyaluronate, 0.1-6.0% of bioglycan-1, 0.1-6.0% of mushroom dextran, 0.1-3.0% of hydrated silica, 0.01-0.5% of hydrolyzed sodium hyaluronate, 0.1-8.0% of potassium citrate, 0.1-3.0% of 1.2-hexanediol, 0.1-3.0% of p-hydroxyacetophenone and the balance of water by weight; preferably, the raw materials for preparing the composition comprise 2.0-5.0% of magnesium ascorbyl phosphate, 2-8% of nicotinamide, 5-10% of humectant, 0.3-0.8% of xanthan gum, 0.3-0.8% of allantoin, 0.3-0.8% of dipotassium glycyrrhizinate, 0.1-0.3% of sodium hyaluronate, 2.0-4.0% of biogan gum-1, 2.0-4.0% of mushroom dextran, 1.0-2.0% of hydrated silica, 0.1-0.4% of hydrolyzed sodium hyaluronate, 2.0-6.0% of potassium citrate, 1.0-2.0% of 1.2-hexanediol, 1.0-2.0% of p-hydroxyacetophenone and the balance of water; more preferably, the composition is prepared from 3.5% magnesium ascorbyl phosphate, 6.0% niacinamide, 13.5% humectant, 0.55% xanthan gum, 0.5% allantoin, 0.55% dipotassium glycyrrhizinate, 0.25% sodium hyaluronate, 3.0% biogan-1, 3.5% mushroom dextran, 1.5% hydrated silica, 0.3% hydrolyzed sodium hyaluronate, 4.5% potassium citrate, 2.0% 1.2-hexanediol, 1.5% p-hydroxyacetophenone, and the balance water.
In one embodiment, the humectant is selected from any one or combination of more of panthenol, 1, 3-butanediol, glycerin, erythritol, 1, 2-hexanediol; preferably, the moisturizer comprises panthenol, 1, 3-butylene glycol, glycerin, and erythritol; further preferably, the weight ratio of panthenol, 1, 3-butanediol, glycerol and erythritol is 1: (1-3): (1-3): (1-3); more preferably, the weight ratio of panthenol, 1, 3-butanediol, glycerol, and erythritol is 1: 2: 1.5: 1.5.
magnesium ascorbyl phosphate:
the magnesium ascorbyl phosphate is a white or yellowish powder of formula C12H12O18P2Mg3.10H2O; it can inhibit tyrosinase activity, inhibit melanin formation, and reduce melanin, thereby reducing pigment accumulation, and removing speckle and whitening skin; can eliminate oxygen free radicals after entering into body, thereby having wrinkle removing and antiaging effects.
The composition is not reactive with active substances such as oxygen radicals in vitro, so that the stability of the composition system can be improved, when the composition penetrates into skin, the composition can be decomposed into ascorbic acid and generate antioxidant activity, and the skin is protected from being influenced by free radicals, so that the anti-aging and whitening effects of the composition are improved; on the other hand, the vitamin E has a synergistic effect with vitamin E, so that the antioxidant capacity of the composition is improved; probably because vitamin E is lipophilic, it acts mainly on the cell membrane of cells; the ascorbic acid is hydrophilic and mainly acts on aqueous cell sap or extracellular space, and can comprehensively improve the antioxidant capacity of the composition under the combined action of the ascorbic acid and vitamin E.
Nicotinamide:
the most important effect of niacinamide on skin anti-aging is to reduce and prevent dullness, yellowing, and sallowness of skin color during early aging. Of course, niacinamide contributes far more than this to the skin and can also repair the damaged stratum corneum lipid barrier, increasing skin resistance. The skin care product containing the niacinamide has strong water locking and moisturizing effects; topical niacinamide reduces the production of fatty acids and triglycerides in sebum, thereby narrowing pores and reducing the severity of acne when it occurs.
However, in general, nicotinamide is most stable in a solution with a pH value of 6; in solutions with a pH above or below 6, it will hydrolyze to form niacin, which can cause skin irritation. Therefore, nicotinamide-containing formulations are typically controlled to a pH of between 5 and 7 to reduce niacin formation.
Panthenol:
panthenol is also called panthenol, is a transparent, slightly red and moisture-absorbing liquid and has a little special smell; is easily soluble in water, and is soluble in chloroform and diethyl ether; panthenol can be converted into pantothenic acid in skin and hair, and has effects of keeping moisture, resisting inflammation, and stimulating cell division.
Xanthan gum:
xanthan gum is an extracellular microbial multi-pool produced by fermentation of saccharides with xanthomonas sp. Due to the special structure and colloid characteristics of macromolecules, the modified starch has multiple functions, can be used as an emulsifier, a stabilizer, a gel thickener, a sizing agent, a film forming agent and the like, and is widely applied to various fields of national economy.
Xanthan gum is a pale yellow to white flowable powder with little off-flavor. It is easily dissolved in cold and hot water, has neutral solution, is resistant to freezing and thawing, and is insoluble in ethanol. Dispersing and emulsifying in water to obtain stable hydrophilic viscous colloid.
Allantoin:
allantoin, also known as 5-ureylethanolamide, ureidoacetolactam, ureidohydantoin and uretidione, is a hydantoin derivative; at present, the annual production capacity of allantoin in the world is about 5 million tons, the market demand is mainly three fields of medicine, cosmetics and agriculture, and the traditional process for extracting natural allantoin from natural animals and plants is low in content, complex in process and high in cost, so that the allantoin cannot be applied in a large scale.
The pure allantoin is a non-toxic, tasteless, non-irritant and non-allergenic white crystal, and is crystallized in water into a prism or colorless crystalline powder; can be dissolved in hot water, hot alcohol and dilute sodium hydroxide solution; water and alcohol which are slightly soluble at normal temperature are difficult to dissolve in organic solvents such as ether and chloroform; the saturated aqueous solution (concentration is 0.6%) is slightly acidic; the pH was 5.5; is stable in aqueous solution with pH value of 4-9, and also stable in non-aqueous solvent and dry air; can be decomposed by boiling in strong alkaline solution and exposing in sunlight.
In the medical aspect: allantoin has physiological functions of promoting cell growth, accelerating wound healing, softening keratin and the like, and is a good healing agent and an anti-ulcer agent for skin wounds; can be used for relieving and treating xeroderma, scaling skin diseases, skin ulcer, digestive tract ulcer and inflammation, and has good therapeutic effect on osteomyelitis, diabetes, liver cirrhosis, and acne.
In the aspect of cosmetics: the allantoin is an amphoteric compound, can be combined with various substances to form a double salt, has the effects of shading light, sterilizing, preventing corrosion, relieving pain and resisting oxidation, can keep the skin moisture, moisten and soften, is a special additive of cosmetics such as beauty and hairdressing, and is widely used as an additive of freckle cream, acne liquid, shampoo, perfumed soap, toothpaste, shaving lotion, hair conditioner, astringent, anti-sweat deodorant lotion and the like; the cosmetic containing allantoin has tissue protecting, hydrophilic, water absorbing, and moisture diffusion preventing effects; hair cream, hair cream and shampoo containing allantoin can protect hair and prevent hair from bifurcation and break hair; the lipstick and the face cream added with the allantoin can make the skin and the lips soft and elastic and have beautiful luster; allantoin promotes tissue growth, cell metabolism, and softens stratum corneum protein.
In agriculture: allantoin is an excellent plant growth regulator, can stimulate plant growth, has obvious yield increasing effect on wheat, orange, rice, vegetable, soybean and the like, and has the functions of fruit fixing and early maturing.
Experiments show that when the nicotinamide is added into a composition system, the anti-aging property and the moisture retention property of the mask can be effectively improved, and the phenomena of obturator and acne can be reduced, but the skin can sometimes generate an allergic phenomenon, which is probably because the nicotinamide is hydrolyzed in vivo to form nicotinic acid, the content of the nicotinic acid is higher, the vasodilatation is promoted, the flow of moisture is promoted, and the erythra is generated; the phenomenon can be weakened when allantoin is added into the composition, and probably because the allantoin can fix formed nicotinic acid, the flowing and the action of the nicotinic acid in the skin are reduced, the moisture retention performance of the system is improved, the diffusion of water is reduced, the absorption of the components by the skin is promoted, and the generation of erythema is reduced.
Dipotassium glycyrrhizinate:
the dipotassium glycyrrhizinate is white or white-like fine powder, has the purity of 98 percent, has special sweet taste, good water solubility and pure mouthfeel; the dipotassium glycyrrhizinate has multiple effects of bacteriostasis, inflammation diminishing, detoxification, anti-allergy, deodorization and the like; has wide application in the industries of medicine, cosmetics, daily chemicals, food and the like.
Dipotassium glycyrrhizinate has the effects of resisting inflammation, resisting allergy, preserving moisture and the like, and can be used for eye drops and ointment for stomatitis in the pharmaceutical industry; in the cosmetic industry, the product can be used for preventing sunburn, whitening skin, relieving itching, regulating sebum, promoting hair growth, caring hair, etc.; can be used for preventing dermatitis, xerosis cutis, sunburn, erythra, and throat moistening, and also can be used as speckle removing agent and antiallergic agent; can be used for antiallergic, sunscreen, skin care lotion, speckle removing cream, and lotion, and can be used in skin care products and face cream; in the daily chemical industry, the toothpaste can be used; in the food industry, the potassium replenishing agent can be used as a potassium replenishing agent, a sweetening agent, an antistaling agent and a flavoring agent for sports drinks.
Hyaluronic acid sodium salt&Hydrolysis of sodium hyaluronate:
the sodium hyaluronate can keep skin moist, smooth, fine, tender and elastic, and has the effects of preventing wrinkle, resisting wrinkle, beautifying, protecting health and recovering physiological functions of skin; the sodium hyaluronate can lock water on the surface of skin, replenish water and nourish cuticle.
The hydrolyzed sodium hyaluronate can keep moisture of skin and hair, moisten skin and hair, increase luster, and prevent chapped skin and wrinkle.
In one embodiment, the sodium hyaluronate has a weight average molecular weight of 60000 to 500000; preferably, the weight average molecular weight of the sodium hyaluronate is 100000-200000; more preferably, the weight average molecular weight of the sodium hyaluronate is 150000-160000.
In one embodiment, the hydrolyzed sodium hyaluronate has a weight average molecular weight of 500 to 10000; preferably, the weight average molecular weight of the hydrolyzed sodium hyaluronate is 3000-7000; more preferably, the weight average molecular weight of the hydrolyzed sodium hyaluronate is 5000-6000.
Experiments show that the sodium hyaluronate and the hydrolyzed sodium hyaluronate with certain molecular weights added into a composition system can effectively improve the moisturizing, anti-wrinkle and whitening performances of the composition, and the hydrolyzed sodium hyaluronate with small molecular weight can be quickly absorbed through skin and directly reach epidermis layers and dermis layers to achieve the effects of deep moisturizing, muscle bottom repairing and anti-wrinkle; hydrolyzed sodium hyaluronate is used as scalp absorption promoter to improve deep water replenishing effect; the sodium hyaluronate cross-linked polymer has the effect of 24-hour super-long-term moisture retention, and can reduce the water loss of skin as a biological protective net.
Erythritol:
erythritol has strong moisturizing and hygroscopic properties, can be used as a humectant for cosmetics like glycerin, but does not have a greasy and sticky feeling like glycerin; erythritol absorbs heat when dissolved in water, and a powdery cosmetic containing erythritol as a main active ingredient is mixed with water before application, has a strong cool feeling on the skin, is suitable for summer use, and is convenient for storage.
Polysaccharide gum-1:
the biopolysaccharide gum-1 is a biopolysaccharide derived from Bohai sea area of China, and is commonly called fucosan "Fucoidan" because of the presence of a large amount of fucose (L-fucose) in its molecule. Is a novel humectant, wrinkle removing agent, skin repairing agent and skin feeling regulator in the cosmetic industry; the skin care product can preserve moisture, improve skin feel and relieve skin, and brings soft, smooth and pleasant skin feel to the skin; the skin care product can be widely applied to the fields of moisturizing cream, body lotion, eye gel, makeup remover, toner, sun cream, shampoo and the like.
Mushroom glucan:
increasing Epidermal Growth Factor (EGF) on aged skin and wrinkled skin can promote increase of collagen and elastin in skin, thereby improving skin appearance and removing wrinkles; the sun-screening agent has the sun-screening effect, can reduce pain and inflammation, and can enhance the immunity of the skin; it also has significant anti-inflammatory and anti-allergic activities, and can help the skin to resist various exogenous mechanical and chemical stimuli.
Potassium citrate:
potassium citrate (Potassium citrate), also known as Potassium citrate, tripotassium citrate; the potassium citrate is a citrate with a molecular formula of C6H5K3O7Molecular weight 306.39500, which is a white crystalline powder slightly hygroscopic, odorless, tasteless, readily soluble in water, slowly soluble in glycerol, insoluble in alcohol, salty and cool in taste, used as a stabilizer, pH buffer, etc. The food can be used for various foods according to the national regulations, and is used in a proper amount according to the production requirements; in medical treatment, it can be used for controlling uric acid or cystine from kidney stone, and preventing and treating hypokalemia and alkalized urine.
Experiments show that the addition of magnesium ascorbyl phosphate into the facial mask system can effectively improve the whitening, wrinkle-removing and anti-aging performances of the facial mask system, but white substances are separated out on the surface of skin after use, which is probably that magnesium salts are separated out in the absorption process of the facial mask composition; in addition, the applicant also unexpectedly finds that when potassium citrate is added into the system, the whitening, wrinkle-removing and anti-aging performances of the mask system can be further improved, and the precipitation phenomenon of white substances on the surface of the skin can be eliminated, which is probably favorable for stabilizing the pH value of the system after the potassium citrate is added, so that the absorption and permeability of the system of the composition are stabilized, and the activity of the anti-oxidation substances is also favorably maintained; on the other hand, the addition of potassium citrate can improve the intercellular space of the stratum corneum and the pore size of the stratum corneum cells, so that the absorption of magnesium salts is improved, and meanwhile, the original acid-base balance can be broken through due to the addition of potassium citrate, the pH value of the original system is improved, and the absorption of magnesium salts by the skin is promoted.
P-hydroxyacetophenone:
p-Hydroxyacetophenone (English name p-Hydroxyacetophenone) is also known as 4-Hydroxyacetophenone (4-Hydroxyacetophenone), 4-Acetylphenol (4-Acetylphenol), p-Acetylphenol (p-Acetylphenol), 4-hydroxyphenylmethyl ketone (4-hydroxyphenylmethyl ketone), commonly known as pinicol, is white needle-shaped crystal at normal temperature, is combustible and easily soluble in hot water, methanol, ethanol, ether, acetone and benzene, and is difficultly soluble in petroleum ether; is naturally present in stems and leaves of Artemisia scoparia of Compositae, and roots of Artemisia capillaris, Heteropappus japonica of Asclepiadaceae, etc. The product can be used for preparing choleretic drug and other organic synthetic materials; animal experiments show that the product can increase the secretion of bile of rats, increase the discharge amount of solid matters, cholic acid and bilirubin in the bile, has the same effect on liver injury caused by carbon tetrachloride, is clinically used for treating hepatitis, has a certain curative effect on jaundice treatment, is harmful to swallowing the product and has stimulation effect on eyes, respiratory systems and skin.
Firstly, in the experimental process, it is unexpectedly found that the aging resistance and the whitening performance of the mask system can be effectively improved by adding a certain amount of nicotinamide and potassium citrate into the composition system, and probably because the nicotinamide can effectively avoid the oxidation problem after the magnesium ascorbyl phosphate is hydrolyzed to form ascorbic acid while maintaining the pH stability of the system, the action time and the action efficiency of the mask are prolonged.
The potassium citrate can adjust the pH value of the system and maintain the pH value of the system to be 7.5-7.8, so that a formed alkalescent system is strong in surface activity, good in permeability and strong in dissolving power, and can easily participate in a series of biochemical activities of cells, alkalescent water can neutralize acidic products of cell metabolism to a certain extent, and the cleaning capability and the whitening effect of the mask system are improved; but also easily dry the skin, and can dry, tighten and even itch the skin; however, the applicant has found that the composition system provided by the present invention does not have such a problem, and may form a dense network structure on the skin surface under the synergistic effect of the above substances, so as to have good moisture retention property, and simultaneously form a hydrophobic layer on the skin surface, so as to reduce moisture diffusion.
The second aspect of the invention provides a preparation method of the composition, namely, the phase A component is added into water and stirred uniformly; stirring and uniformly stirring the component B; and mixing them uniformly to obtain the invented facial mask composition.
Preferably, the preparation method of the composition comprises the following steps:
(1) heating water to 80-85 ℃, and then cooling to room temperature;
(2) sequentially adding ascorbic acid phosphate magnesium, nicotinamide, humectant, xanthan gum, allantoin, dipotassium glycyrrhizinate, sodium hyaluronate, biogel-1, mushroom dextran, hydrated silica, hydrolyzed sodium hyaluronate and potassium citrate in the phase A, and stirring uniformly;
(3) stirring the phase B component at 45 ℃ fully, and then cooling to room temperature;
(4) and uniformly mixing the phase B component with the uniformly mixed phase A to obtain the mask composition.
The third aspect of the invention provides a whitening repairing mask which contains the composition of the repairing mask.
Example 1
Example 1 of the present invention provides a composition for a whitening and repairing mask, which is prepared from, by weight, 3.5% magnesium ascorbyl phosphate, 6.0% niacinamide, 13.5% humectant, 0.55% xanthan gum, 0.5% allantoin, 0.55% dipotassium glycyrrhizinate, 0.25% sodium hyaluronate, 3.0% bioglycan-1, 3.5% mushroom dextran, 1.5% hydrated silica, 0.3% sodium hyaluronate, 4.5% potassium citrate, 2.0% 1, 2-hexanediol, 1.5% p-hydroxyacetophenone, and the balance water;
the humectant comprises panthenol, 1, 3-butanediol, glycerol and erythritol, wherein the weight ratio of the panthenol to the 1, 3-butanediol to the glycerol to the erythritol is 1: 2: 1.5: 1.5;
the weight average molecular weight of the sodium hyaluronate is 150000-160000;
the weight average molecular weight of the hydrolyzed sodium hyaluronate is 5000-6000;
the preparation method of the composition comprises the following steps:
(1) heating water to 80-85 ℃, and then cooling to room temperature;
(2) sequentially adding ascorbic acid phosphate magnesium, nicotinamide, humectant, xanthan gum, allantoin, dipotassium glycyrrhizinate, sodium hyaluronate, biogel-1, mushroom dextran, hydrated silica, hydrolyzed sodium hyaluronate and potassium citrate in the phase A, and stirring uniformly;
(3) stirring the phase B component at 45 ℃ fully, and then cooling to room temperature;
(4) and uniformly mixing the phase B component with the uniformly mixed phase A to obtain the mask composition.
Example 2
Embodiment 2 of the present invention provides a composition for a whitening and repairing mask, which is prepared from 0.5% magnesium ascorbyl phosphate, 0.5% niacinamide, 0.4% humectant, 0.1% xanthan gum, 0.1% allantoin, 0.1% dipotassium glycyrrhizinate, 0.01% sodium hyaluronate, 0.1% biogan-1, 0.1% mushroom dextran, 0.1% hydrated silica, 0.01% hydrolyzed sodium hyaluronate, 0.1% potassium citrate, 0.1% 1, 2-hexanediol, 0.1% p-hydroxyacetophenone, and the balance water;
the humectant comprises panthenol, 1, 3-butanediol, glycerol and erythritol, wherein the weight ratio of the panthenol to the 1, 3-butanediol to the glycerol to the erythritol is 1: 1: 1: 1;
the weight average molecular weight of the sodium hyaluronate is 150000-160000;
the weight average molecular weight of the hydrolyzed sodium hyaluronate is 5000-6000;
the preparation method of the composition comprises the following steps:
(1) heating water to 80-85 ℃, and then cooling to room temperature;
(2) sequentially adding ascorbic acid phosphate magnesium, nicotinamide, humectant, xanthan gum, allantoin, dipotassium glycyrrhizinate, sodium hyaluronate, biogel-1, mushroom dextran, hydrated silica, hydrolyzed sodium hyaluronate and potassium citrate in the phase A, and stirring uniformly;
(3) stirring the phase B component at 45 ℃ fully, and then cooling to room temperature;
(4) and uniformly mixing the phase B component with the uniformly mixed phase A to obtain the mask composition.
Example 3
Embodiment 3 of the present invention provides a composition for a whitening and repairing mask, which is prepared from 7.0% magnesium ascorbyl phosphate, 10% niacinamide, 18% humectant, 1.0% xanthan gum, 1.0% allantoin, 1.0% dipotassium glycyrrhizinate, 0.5% sodium hyaluronate, 6.0% biogan-1, 6.0% mushroom dextran, 3.0% hydrated silica, 0.5% hydrolyzed sodium hyaluronate, 8.0% potassium citrate, 3.0% 1, 2-hexanediol, 3.0% p-hydroxyacetophenone, and the balance water;
the humectant comprises panthenol, 1, 3-butanediol, glycerol and erythritol, wherein the weight ratio of the panthenol to the 1, 3-butanediol to the glycerol to the erythritol is 1: 3: 3: 3;
the weight average molecular weight of the sodium hyaluronate is 150000-160000;
the weight average molecular weight of the hydrolyzed sodium hyaluronate is 5000-6000;
the preparation method of the composition comprises the following steps:
(1) heating water to 80-85 ℃, and then cooling to room temperature;
(2) sequentially adding ascorbic acid phosphate magnesium, nicotinamide, humectant, xanthan gum, allantoin, dipotassium glycyrrhizinate, sodium hyaluronate, biogel-1, mushroom dextran, hydrated silica, hydrolyzed sodium hyaluronate and potassium citrate in the phase A, and stirring uniformly;
(3) stirring the phase B component at 45 ℃ fully, and then cooling to room temperature;
(4) and uniformly mixing the phase B component with the uniformly mixed phase A to obtain the mask composition.
Example 4
Example 4 of the present invention provides a composition for a whitening and repairing mask, which is similar to example 1, except that the content of the component B is 0.
Example 5
Example 5 of the present invention provides a composition for a whitening and repairing mask, which is similar to example 1 except that the amount of niacinamide is 0.
Example 6
Example 6 of the present invention provides a composition for a whitening and repairing mask, which is substantially the same as example 1, except that the allantoin content is 0.
Example 7
Example 7 of the present invention provides a composition for a whitening and repairing mask, which is similar to example 1, except that the amounts of niacinamide and allantoin are 0.
Example 8
Example 8 of the present invention provides a composition for a whitening and repairing mask, which is the same as example 1 except that the content of potassium citrate is 0.
Example 9
Example 9 of the present invention provides a composition for a whitening and repairing mask, which is substantially the same as example 1, except that magnesium ascorbyl phosphate is replaced with trisodium ascorbyl palmitate phosphate.
Example 10
Example 10 of the present invention provides a composition for a whitening and repairing mask, which is substantially the same as example 1, except that magnesium ascorbyl phosphate is contained in an amount of 0.
Example 11
Example 11 of the present invention provides a composition for a whitening and repairing mask, which is substantially the same as in example 1, except that panthenol is contained in an amount of 0.
Example 12
Example 12 of the present invention provides a composition for a whitening and repairing mask, which is the same as example 1 in the specific embodiment except that the content of biosaccharide gum-1 is 0.
Example 13
Example 13 of the present invention provides a composition for a whitening and repairing mask, which is prepared according to the following specific embodiment with the exception that the composition is prepared from 3.5% magnesium ascorbyl phosphate, 12% niacinamide, 13.5% moisturizer, 0.55% xanthan gum, 0.5% allantoin, 0.55% dipotassium glycyrrhizinate, 0.25% sodium hyaluronate, 3.0% biogum-1, 3.5% mushroom dextran, 1.5% hydrated silica, 0.3% hydrolyzed sodium hyaluronate, 10% potassium citrate, 2.0% 1, 2-hexanediol, 1.5% p-hydroxyacetophenone, and the balance water.
Example 14
Example 14 of the present invention provides a composition for a whitening and repairing mask, which is the same as example 1 except that the content of sodium hyaluronate is 0.
Example 15
Example 15 of the present invention provides a composition for a whitening and repairing mask, which is the same as example 1 except that the content of hydrolyzed sodium hyaluronate is 0.
Example 16
Example 16 of the present invention provides a composition for a whitening and repairing mask, which is substantially the same as example 1, except that the content of hydrated silica is 0.
Example 17
Example 17 of the present invention provides a composition for a whitening and repairing mask, which is the same as example 1 except that the content of mushroom glucan is 0.
Performance evaluation:
1. 850 female volunteers 35-40 years old with skin surface with light spots are selected and randomly divided into 17 groups, 50 persons in each group use the composition prepared in examples 1-17 under normal external conditions, and the proportion of red rash and white substances appearing on the skin surface of the volunteers is observed in sequence; observing the proportion of obvious skin whitening in the volunteers when in use, wherein the standard of obvious whitening is that the skin surface of a tester has no spot fading, and the test result is shown in table 1;
2. the moisture retention was tested using a KSN skin tester. In each example, 50 testers are selected, the simulated experiment environment is 20 +/-1 ℃ at room temperature, the humidity is 10 +/-1%, the percentage of the moisture retention of the composition is calculated to be more than 90% after the composition is used for 15 hours, and the test results are shown in table 1.
Table 1 results of performance testing
The experimental results show that the composition provided by the invention can effectively improve the whitening effect and moisturizing effect of the skin, and the components of the composition can be well absorbed by the skin in the using process, so that the generation of white substances on the surface of the skin due to incomplete absorption is avoided; on the other hand, the composition can effectively avoid the generation of allergic phenomena such as erythra and the like, and the application range of the product is expanded.
It should be noted that the above mentioned embodiments are only preferred embodiments of the present invention, but the scope of the present invention is not limited thereto, and any changes or substitutions that can be easily conceived by those skilled in the art within the technical scope of the present invention are included in the scope of the present invention.
Claims (6)
1. The composition for the whitening and repairing mask is characterized in that raw materials for preparing the composition contain a component A, a component B and water;
wherein the component A contains magnesium ascorbyl phosphate, humectant, xanthan gum, dipotassium glycyrrhizinate, sodium hyaluronate, biogel-1, mushroom dextran, hydrated silica, hydrolyzed sodium hyaluronate, potassium citrate, nicotinamide and allantoin; the component B contains 1, 2-hexanediol and p-hydroxyacetophenone;
the weight percentage of the preparation raw materials is as follows: 2.0-5.0% magnesium ascorbyl phosphate, 2-8% nicotinamide, 5-10% humectant, 0.3-0.8% xanthan gum, 0.3-0.8% allantoin, 0.3-0.8% dipotassium glycyrrhizinate, 0.1-0.3% sodium hyaluronate, 2.0-4.0% biogan gum-1, 2.0-4.0% mushroom dextran, 1.0-2.0% hydrated silica, 0.1-0.4% hydrolyzed sodium hyaluronate, 2.0-6.0% potassium citrate, 1.0-2.0% 1.2-hexanediol, 1.0-2.0% p-hydroxyacetophenone, and the balance water;
the weight ratio of the nicotinamide, the allantoin, the magnesium ascorbyl phosphate and the potassium citrate is (0.5-10): (0.1-1.0): (0.5-7.0): (0.1 to 8.0);
the humectant contains panthenol, 1, 3-butanediol, glycerol and erythritol; the weight ratio of the panthenol, the 1, 3-butanediol, the glycerol and the erythritol is 1: (1-3): (1-3): (1-3).
2. The mask pack repairing composition according to claim 1, wherein the composition has a pH of 7.5 to 7.8.
3. The mask pack repairing composition according to claim 1, wherein the hydrolyzed sodium hyaluronate has a weight average molecular weight of 500 to 10000.
4. The mask pack repairing composition according to claim 1, wherein the sodium hyaluronate has a weight average molecular weight of 60000 to 500000.
5. A method for preparing the composition of any one of claims 1 to 4, wherein the phase A component is added to water and stirred uniformly; then uniformly stirring the component B; and mixing them uniformly to obtain the invented facial mask composition.
6. A whitening repair mask characterized by containing the composition of the repair mask according to any one of claims 1 to 4.
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| CN201910216867.3A CN109771326B (en) | 2019-03-20 | 2019-03-20 | Composition for whitening and repairing mask |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910216867.3A CN109771326B (en) | 2019-03-20 | 2019-03-20 | Composition for whitening and repairing mask |
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| CN109771326B true CN109771326B (en) | 2021-08-17 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112057356A (en) * | 2019-05-25 | 2020-12-11 | 陈超 | Skin care facial mask with natural extract composition as basic component |
| CN113662882B (en) * | 2021-10-09 | 2022-11-08 | 上海新高姿化妆品有限公司 | Whitening, spot-fading and tightening essence and preparation method thereof |
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| CN103349617A (en) * | 2013-07-17 | 2013-10-16 | 中山德尚伟业生物科技有限公司 | Transparent alginate mask powder capable of being peeled off wholly |
| CN104473812A (en) * | 2014-11-28 | 2015-04-01 | 海南海之润生物工程有限公司 | Biological fiber facial mask |
| CN104814918A (en) * | 2015-05-13 | 2015-08-05 | 朱敏 | Moisturizing facial mask solution, preparation method of moisturizing facial mask solution and moisturizing facial mask |
| KR20160067472A (en) * | 2014-12-04 | 2016-06-14 | (주)헵틸와이 | Biocompatible fibrous matrix, mask pack containing the same and manufacturing method thereof |
| KR20170012735A (en) * | 2015-07-23 | 2017-02-03 | (주)뷰티화장품 | Method for preparing hydrogel pack containing even porous silica particle for skin whitening and anti-wrinkle |
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2019
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103349617A (en) * | 2013-07-17 | 2013-10-16 | 中山德尚伟业生物科技有限公司 | Transparent alginate mask powder capable of being peeled off wholly |
| CN104473812A (en) * | 2014-11-28 | 2015-04-01 | 海南海之润生物工程有限公司 | Biological fiber facial mask |
| KR20160067472A (en) * | 2014-12-04 | 2016-06-14 | (주)헵틸와이 | Biocompatible fibrous matrix, mask pack containing the same and manufacturing method thereof |
| CN104814918A (en) * | 2015-05-13 | 2015-08-05 | 朱敏 | Moisturizing facial mask solution, preparation method of moisturizing facial mask solution and moisturizing facial mask |
| KR20170012735A (en) * | 2015-07-23 | 2017-02-03 | (주)뷰티화장품 | Method for preparing hydrogel pack containing even porous silica particle for skin whitening and anti-wrinkle |
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