CN113116753B - Rose essential oil face cream and preparation method thereof - Google Patents

Abstract

The invention discloses rose essential oil face cream and a preparation method thereof, and the rose essential oil face cream comprises the following raw materials in parts by weight: 12-15 parts of rose essential oil, 8-12 parts of salvia miltiorrhiza extract, 8-10 parts of astragalus extract, 5-7 parts of potassium laureth phosphate, 4-6 parts of polyethylene glycol, 2-4 parts of madecassoside, 3-5 parts of triglyceride, 0.1-0.3 part of arbutin, 2-5 parts of fibroin, 4-7 parts of polysorbate, 2-6 parts of polydimethylsiloxane, 6-9 parts of poria extract, 4-7 parts of ethyl methoxycinnamate, 6-8 parts of glycerol, 3-5 parts of sodium hyaluronate, 0.5-1 part of triethanolamine, 2-5 parts of sodium alginate, 3-5 parts of safflower extract, 2-5 parts of propylene glycol, 2-6 parts of tocopherol, 0.8-1 part of sodium polyacrylate, 25-37 parts of deionized water and the like. The invention has the functions of continuously whitening, compounding and moisturizing, and also has the effects of resisting itch and inhibiting bacteria.

Description

Rose essential oil face cream and preparation method thereof

Technical Field

The invention relates to the technical field of daily necessities, in particular to rose essential oil face cream and a preparation method thereof.

Background

Skin health and skin-like coagulated fat are always good wishes of oriental women. Due to the deterioration of environmental pollution and the continuous increase of working pressure, adverse conditions such as dry skin, dark yellow skin, sensitivity, pigmentation and the like have serious adverse effects on the physiology and psychology of human beings.

Skin care products with whitening efficacy are always hot concerns of researchers, suppliers and consumers all over the world, and early skin care product components for whitening mainly use some whitening agents, such as heavy metal elements containing mercury and lead, hydroquinone whitening agents, hydroquinone and the like, but the components have large toxic and side effects and are eliminated by the market at present. At present, the global research focus is to search product components with multiple-effect and synergistic whitening effects.

Lightening, in terms of skin microstructure, is to reduce pigmentation, production, and block the activity of enzymes required to induce pigment expression.

From the aspect of skin anatomy, the skin is composed of an epidermal layer, a dermal layer and a subcutaneous tissue from the outside to the inside. The epidermal layer is further divided into a horny layer and a clear layer (partial structure containing), a granular layer, a spinous layer and a basal layer, and melanin is a blackish brown pigment present in animal skin or hair, which is produced by and stored in a special cell, i.e., melanocyte. It is the presence of melanin that the skin has a color. Melanin cannot be formed for some reason, and pigment loss is caused, thereby forming white spots.

Melanin is essentially an amino acid derivative, which is found in the body of everyone. 20-25 years of age is the active phase of melanin precipitate formation. They are present in the middle of the cells of the basal layer of the skin, but are a substance called "melanogenic substance", also called "chromoplast". The melanoblast secretes Maillarin pigment, when ultraviolet rays (B wave and A wave) irradiate the skin (the B wave, namely UVB acts on the basal layer of the skin), the skin is in a self-protection state, namely the Maillarin pigment is stimulated by the ultraviolet rays, and the activity of tyrosinase is activated, so that the skin cells are protected. Dopa is in fact the precursor of melanin, which is oxidized by tyrosine to release melanin. Melanin moves layer by layer through cell metabolism, and forms freckles, sunburn and black spots on the skin epidermis.

Abundant water content is the basis of skin health, the whitening and maintaining effect is closely related to the skin moisture, the moisturizing work is better, the nursing effect is more obvious, the moisture of the skin is most easily dehydrated, the water of the skin mainly comes from the body, the protective effect of a sebum membrane is weakened or damaged along with the growth of age and the change of the external environment, the natural moisturizing factor of the cuticle is lost, the cuticle of the skin is easily in a water shortage state, the cuticle metabolism is easily caused, impurities and metabolites in cells cannot be removed in time, the phenomenon of so-called 'thick cuticle' is generated, the color of the skin is influenced, the skin looks dark and dull, and meanwhile, the permeation of maintenance products is also hindered. Even with whitening care, the effect is limited. Therefore, after 25 years of age, any skin should be constantly moisturized.

Whitening components usually have certain hygroscopicity, a large amount of moisture in the skin can be consumed when the skin absorbs the components, if the moisture is not supplemented in time, the skin is easy to lack water and dry, and the nursing effect is not ideal, which is also the reason that the high-efficiency moisture preservation environment is often emphasized in the professional whitening nursing process.

In conclusion, the wet healing environment is closely related to skin whitening, and the facial cream with the slow-release whitening and composite moisturizing effects is very difficult and expensive.

Chinese patent document CN108113920A discloses a sustained-release whitening composite moisturizing cream matrix and a preparation method and application thereof. Wherein the cream matrix comprises alpha-arbutin, nicotinamide, licoflavone, sodium hyaluronate, algal polysaccharide, polyquaternium-73, azelaic acid, lecithin, microcrystalline wax, lanolin alcohol, paraffin and water; wherein the alpha-arbutin, the nicotinamide, the licoflavone, the sodium hyaluronate, the algal polysaccharide, the polyquaternium-73, the azelaic acid and the lecithin are as follows by mass percent: 1 to 8 percent of alpha-arbutin, 6 to 11 percent of nicotinamide, 6 to 11 percent of licoflavone, 1 to 10 percent of sodium hyaluronate, 1 to 10 percent of algal polysaccharide, 1 to 10 percent of polyquaternium-73, 1 to 5 percent of azelaic acid and 1 to 10 percent of lecithin. The sustained-release whitening and moisturizing cream disclosed by the invention can obviously improve the skin state after being used continuously.

Chinese patent document CN108309874A discloses a whitening and moisturizing cream which is prepared from the following raw materials in parts by weight: 100 parts of water, 2-6 parts of glycerol, 2-4 parts of 1, 3-butanediol, 0.2-0.8 part of isopropyl palmitate, 0.2-0.6 part of bletilla striata root extract, 0.2-0.6 part of ampelopsis japonica root extract, 0.2-0.6 part of bighead atractylodes rhizome root extract, 0.2-0.8 part of isononyl isononanoate, 0.1-0.3 part of magnesium ascorbyl phosphate, 0.2-0.8 part of PEG-100 stearate, 0.04-0.08 part of dipotassium glycyrrhizinate, 0.1-0.3 part of tocopherol acetate and 0.1-0.3 part of propyl hydroxybenzoate. The whitening and moisturizing cream disclosed by the invention can generate a long-lasting and continuous water-locking and moisturizing effect on skin all day long, can brighten skin color and promote complexion, is used for a long time, can improve skin quality, achieves the whitening and moisturizing effect on the whole, enables people to be refreshed and more self-believes.

Chinese patent document CN107233236A discloses an fair and bright white cream and a preparation method thereof, wherein the fair and bright white cream comprises ethylhexyl methoxycinnamate, ethylhexyl carboxystearate, PPG-15 stearyl ether, octyl polymethylsiloxane, isononyl isononanoate, C12-15 alcohol benzoate, hydroxyethyl urea, propylene glycol, titanium dioxide, polydimethylsiloxane, glyceryl stearate \ PEG-100 stearate, cetearyl alcohol \ cetearyl glucoside, butyl methoxydibenzoylmethane, tocopheryl acetate, 4-butylresorcinol, peony whitening essence, apple seed extract, arbutin, thyme extract, sodium bisulfite, polyhydroxystearic acid, triethyl citrate, xanthan gum, disodium EDTA, water and the like. The fair and transparent whitening cream disclosed by the invention is natural and safe, good in permeability and easy to absorb, and has good effects of moisturizing, whitening and tendering skin.

In order to further meet the demand of people on the diversification of the face cream products, the inventor carries out deep research on the face cream products and pays creative labor to obtain the face cream.

Disclosure of Invention

In view of the above, the invention aims to provide a rose essential oil facial cream and a preparation method thereof, and the rose essential oil facial cream has the functions of continuous whitening, compound moisturizing, anti-itching and bacteriostasis.

The adopted technical scheme is as follows:

the invention relates to rose essential oil face cream which is prepared from the following raw materials in parts by weight:

further, the polysorbate is polysorbate-60.

The invention relates to a preparation method of rose essential oil face cream, which comprises the following steps:

s1, putting deionized water, potassium laureth phosphate, madecassoside, arbutin, fibroin, polydimethylsiloxane, sodium hyaluronate and tocopherol into a reaction kettle according to a ratio, heating to 70-80 ℃, and fully stirring and uniformly mixing all the components and completely dissolving the components;

s2, putting triglyceride, polysorbate, ethyl methoxycinnamate, polyethylene glycol, glycerol and propylene glycol into the reaction kettle according to the proportion, maintaining the temperature at 70-80 ℃, fully stirring and uniformly mixing all the components, fully dissolving the components, homogenizing for 8-10 minutes, and stirring and cooling;

s3, cooling to 45-50 ℃, adding rose essential oil, the red sage root extract, the astragalus root extract, the poria cocos extract and the safflower extract according to the proportion, fully stirring and uniformly mixing;

s4, cooling to 30-35 ℃, adding triethanolamine, sodium alginate, sodium polyacrylate, essence, p-hydroxyacetophenone and hydroxyethyl cellulose according to the proportion, and fully stirring and uniformly mixing.

Further, the preparation method also comprises the following steps:

and S5, discharging, after being inspected to be qualified, filling and warehousing.

In the above-mentioned technical solution,

the rose essential oil is essential oil extracted from roses, has good beautifying and skin-care effects, can make skin tender and white, and is a main component of the invention.

The main component of Saviae Miltiorrhizae radix extract is phenanthrenequinone derivative. The red sage root extract has excellent effect of promoting collagen proliferation, and thus can strengthen the metabolism of skin corium layer and has also antioxidant effect.

The astragalus extract has the main function of viscosity control and is used as an emulsion stabilizer. In the astragalus extract, the skin compatibility is good, the polysaccharide content is high, and the astragalus extract is a good film forming component.

The poria extract is mainly used as a skin conditioner, has the function of promoting proliferation of integrin and the like, the integrin can reflect the proliferation condition of fibroblasts and the adhesion condition between cells and between fibrin, and the proliferation of the integrin can reduce the diameter and the volume of collagen wrapped by the fibroblasts, so that the poria extract has a contraction effect and is used for tightening skin and fine wrinkles; the antibacterial agent has antibacterial property and has good inhibition effect on various bacteria and fungi; it also has anti-inflammatory and moisture keeping effects.

The Carthami flos extract has effects of promoting blood circulation, resisting inflammation, resisting oxidation, whitening skin, preventing sunburn, and resisting aging by improving skin blood circulation, promoting skin metabolism, scavenging free radicals, inhibiting melanin deposition, accelerating speckle and decolorizing, and absorbing ultraviolet, and can be used for treating contact dermatitis, seborrheic dermatitis, pruritus, and neurodermatitis.

The potassium laureth phosphate is mainly used as a cleaning agent and an emulsifier.

Polyethylene glycol, preferably polyethylene glycol-800, is used as humectant.

The madecassoside has the main functions of an antioxidant, a whitening and freckle-removing and skin conditioning agent, has the effect of promoting the activity of scar fibroblasts, has the effect of removing scars, has a good polymerization effect with phospholipid substances, and has a remarkable effect of removing acnes; has effect in inhibiting glucuronidase.

The main function of triglycerides is a emollient, which has good hydrolytic stability.

Glycerol has certain moisturizing effect.

Arbutin has the main functions of an antioxidant, whitening and freckle removing and skin conditioner, can obviously inhibit the accumulation of tyrosinase in the cortex, has the whitening effect on the skin, can be used for preventing skin stains and freckles, and has stronger effect than kojic acid and ascorbic acid.

The fibroin is a natural high molecular fibrin extracted from silk, accounts for 70-80% of the silk, contains 18 amino groups, and can be used as a moisturizing agent, a skin conditioner and an antistatic agent in cream.

The main function of polysorbates is as emulsifiers.

The polydimethylsiloxane mainly acts as a softening agent and a film forming agent. The polydimethylsiloxane has good lubricating property, and after the polydimethylsiloxane is used for the face cream, a layer of uniform protective film with water resistance can be formed after the face cream is coated on the skin, but no sticky or greasy feeling exists, and the glossiness is good. The performance of resisting ultraviolet radiation is good. It is not oxidized and deteriorated under ultraviolet rays to cause skin irritation. The antistatic performance is good. Has the slow-release and fragrance-fixing effects on the essence, so that the fragrance-retaining period is longer, the stability is high, the chemical inertness is realized, no adverse effect is caused on other components of the face cream, and the matching property is good.

Ethyl methoxycinnamate absorbs UVB in sunlight and protects the skin from damage.

The sodium hyaluronate plays a role in moisturizing and replenishing water, and can achieve the effect of quickly replenishing water.

Triethanolamine is mainly used as a pH regulator to adjust the pH value of the cream.

The main function of sodium alginate is as a binder. Sodium alginate is a byproduct after iodine and mannitol are extracted from brown algae such as kelp or gulfweed, the molecule of sodium alginate is formed by connecting beta-D-mannuronic acid (beta-D-mannuronic, M) and alpha-L-guluronic acid (alpha-L-guluronic acid, G) according to a (1 → 4) bond, and the sodium alginate is a natural polysaccharide and has stability, solubility, viscosity and safety.

The main function of propylene glycol is as a humectant. Propylene glycol is one of polyhydric alcohols, has no greasy feeling, is completely dissolved in water, and also has antiseptic effect. Propylene glycol helps the other ingredients of the cream spread and penetrate the skin surface.

The main role of tocopherol is as a humectant and antioxidant.

The main functions of sodium polyacrylate are film forming agent and adsorbent.

The essence improves the fragrance of the product and gives the product a pleasant feeling in the sense.

The p-hydroxyacetophenone has the function of preserving the product.

Hydroxyethyl cellulose is used as a thickener.

The invention has the beneficial effects that:

in the rose essential oil cream, after the rose essential oil, the salvia miltiorrhiza extract, the astragalus extract, the poria cocos extract and the safflower extract are combined according to respective parts by weight, the medicinal effects of the rose essential oil, the salvia miltiorrhiza extract, the astragalus extract, the poria cocos extract and the safflower extract are mutually promoted and supplemented, so that the rose essential oil cream has a continuous whitening and composite moisturizing effect and also has an anti-itching and bacteriostatic effect.

Detailed Description

The present invention is described in detail below with reference to specific examples, but the use and purpose of these exemplary embodiments are merely to exemplify the present invention, and do not set forth any limitation on the actual scope of the present invention in any form, and the scope of the present invention is not limited thereto.

The components of the following examples and comparative examples are contained in parts by weight unless otherwise specified.

Example 1

The rose essential oil facial cream provided by the embodiment comprises the following raw materials in parts by weight:

the preparation method of the rose essential oil cream comprises the following steps:

s1, putting deionized water, potassium laureth phosphate, madecassoside, arbutin, fibroin, polydimethylsiloxane, sodium hyaluronate and tocopherol into a reaction kettle according to a ratio, heating to 70-80 ℃, and fully stirring and uniformly mixing all the components and completely dissolving the components;

s2, putting triglyceride, polysorbate, ethyl methoxycinnamate, polyethylene glycol, glycerol and propylene glycol into the reaction kettle according to the proportion, maintaining the temperature at 70-80 ℃, fully stirring and uniformly mixing all the components, fully dissolving the components, homogenizing for 8-10 minutes, and stirring and cooling;

s3, cooling to 45-50 ℃, adding rose essential oil, the red sage root extract, the astragalus root extract, the poria cocos extract and the safflower extract according to the proportion, fully stirring and uniformly mixing;

s4, cooling to 30-35 ℃, adding triethanolamine, sodium alginate, sodium polyacrylate, essence, p-hydroxyacetophenone and hydroxyethyl cellulose according to the proportion, fully stirring and uniformly mixing.

And S5, discharging, filling and warehousing after the materials are qualified through inspection.

Example 2

Referring to example 1, unlike example 1, the rose essential oil cream of this example is composed of the following raw materials in parts by weight:

the preparation method is as in example 1.

Example 3

Referring to example 1, unlike example 1, the rose essential oil cream of this example is composed of the following raw materials in parts by weight:

the preparation method is as in example 1.

Comparative example 1

Referring to example 2, unlike example 2, the rose essential oil cream of this comparative example was 38 parts deionized water without adding poria extract.

Test and test:

test 1

The moisturizing effect of the rose essential oil creams of examples 1-3 was tested.

50 healthy female subjects of 20-40 years old without skin disease were randomly selected, skin was coated with the rose essential oil cream obtained in examples 1-3, and the moisture content of the right forearm was measured in an environment where the test environment temperature was 25 ℃ and the relative humidity was 60%, while the subjects were allowed to remain calm. 2 square test areas of 4cm × 4cm were drawn on the right forearm as a test area of the rose essential oil cream, and the moisture content of the skin was measured 1 hour, 2 hours, and 3 hours after bathing with a skin moisture meter, respectively, and the results were recorded.

Specific results are shown in table 1.

TABLE 1 moisturizing effect test results of rose essential oil cream

Test 2

The bacteriostatic effect of the rose essential oil creams of examples 1-3 was tested.

The specific results are shown in Table 2.

Table 2 table of the bacteriostatic effect test results of the rose essential oil cream.

	Total number of colonies, cfu/g
		Example 1	25
Example 2	23
		Example 3	27
Comparative example 1	41

Example 2 compared with comparative example 1, in example 2, the antibacterial effect is significantly improved by adding the poria cocos extract.

The above-listed detailed description is only a specific description of possible embodiments of the present invention, and they are not intended to limit the scope of the present invention, and equivalent embodiments or modifications made without departing from the technical spirit of the present invention should be included in the scope of the present invention.

Claims (4)

1. The rose essential oil face cream is characterized by comprising the following raw materials in parts by weight:

2. the rose essential oil cream of claim 1, wherein the polysorbate is polysorbate-60.

3. A method of preparing a rose essential oil cream according to any one of claims 1 to 2, comprising the steps of:

s1, putting deionized water, potassium laureth phosphate, madecassoside, arbutin, fibroin, polydimethylsiloxane, sodium hyaluronate and tocopherol into a reaction kettle according to a ratio, heating to 70-80 ℃, and fully stirring and uniformly mixing all the components and completely dissolving;

s2, putting triglyceride, polysorbate, ethyl methoxycinnamate, polyethylene glycol, glycerol and propylene glycol into the reaction kettle according to the proportion, maintaining the temperature at 70-80 ℃, fully stirring and uniformly mixing all the components, fully dissolving the components, homogenizing for 8-10 minutes, and stirring and cooling;

s3, cooling to 45-50 ℃, adding rose essential oil, the red sage root extract, the astragalus root extract, the poria cocos extract and the safflower extract according to the proportion, fully stirring and uniformly mixing;

s4, cooling to 30-35 ℃, adding triethanolamine, sodium alginate, sodium polyacrylate, essence, p-hydroxyacetophenone and hydroxyethyl cellulose according to the proportion, fully stirring and uniformly mixing.

4. The method for preparing the rose essential oil cream according to claim 3, further comprising:

and S5, discharging, filling and warehousing after the materials are qualified through inspection.