CN107970293A - A kind of Chinese medicine composition for improving skin sub-health state and preparation method thereof, skin care item - Google Patents
A kind of Chinese medicine composition for improving skin sub-health state and preparation method thereof, skin care item Download PDFInfo
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- A61K36/03—Phaeophycota or phaeophyta (brown algae), e.g. Fucus
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- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
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- A61K36/18—Magnoliophyta (angiosperms)
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- A61K36/73—Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
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Abstract
The present invention relates to a kind of Chinese medicine composition for improving skin sub-health state and preparation method thereof, skin care item, belong to cosmetic technical field.The Chinese medicine composition of the present invention, is mainly made of the polar solvent extract of the medicinal raw material of following parts by weight：10~25 parts of Poria cocos, 10~15 parts of pot marigold, 10~15 parts of sargassum, 10~15 parts of high mallow, 10~15 parts of peach blossom.The Chinese medicine composition of the present invention, it is made with several drug matchings, it can effectively improve skin sub-health state, using the Poria cocos of clearing damp and promoting diuresis, the pot marigold of promoting blood circulation to remove blood stasis, peach blossom, clearing heat and detoxicating, qi-regulating dampness removing high mallow, the sargassum of clearing heat and eliminating phlegm, softening and resolving hard mass, five medicines share, the effect of playing eliminating toxic dampness and heat, heat-clearing disinfection altogether, can remove the phlegm wet for causing local qi and blood retardance, hemostasis well and remove qi and blood retardance, the caused metabolism deposit of failure of skin and muscle to be nourished, increase the moisture of skin, release skin sub-health state.
Description
Technical field
The present invention relates to a kind of Chinese medicine composition for improving skin sub-health state and preparation method thereof, skin care item, belong to
Cosmetic technical field.
Background technology
Skin is the organ of our human body maximums, and Nails focus on the whitening to skin, therefore the skin-protection product brightened
With it is more, but should more focus on while skin whitening the health of skin.From the perspective of medicine, healthy skin is to grow
Profit, the colour of skin are uniform, it is lineolate not have.In daily life, since skin is easily corroded by inside and outside, endured to the fullest extent in external environment condition
The problems such as pollution of environment, the radiation of computer, the accumulation of toxins in human body, can all influence the health status of skin.Undesirable life
Many undesirable elements in custom and living environment living can all cause skin histology underactivity, and hyaluronic acid contents are increasingly
Few, there is obstacle in cell metabolism, microcirculation, and cellular content is shunk, and viscosity declines, and ultimately results in skin and is chronically at Asia
Health status, shows as dry skin, water shortage, dark yellow, cuticula accumulation, the thick state of clogging of pores.If adjust not in time
Whole, exchanges of mass and energy is reduced between Skin tissue fluid and blood, the nutritional ingredient that Skin Cell cannot be sufficient, gradually old
Change simultaneously loss of function.Skin sub-health state is prevalent in crowd, and an investigation result of the World Health Organization is shown, yellow
In kind people, skin, which is in sub-health state person ratio, can reach 70%.Coarse, dry, intense darkness without light inferior health skin, becomes
The serious puzzlement of more and more women.
With advancing age, the old dead cuticula of skin cannot voluntarily come off in time, make pachylosis, intensely dark,
And the barrier for stopping moisture and absorption of nutrient ingredients is formed in skin surface.The characteristics of for inferior health skin quality, except needing to solve
Certainly the problem of the drying of skin, colour of skin inequality, microgroove, it is also necessary to remove old dead cutin, some chemical synthesis facial masks are although short
Phase positive effect, but side effect is big, it is impossible to fundamentally solve the problems, such as inferior health.
Skin care item are made of both effectiveness component and base starting material two parts, and both effectiveness component assigns the improvement of cosmetics uniqueness
The effect of skin main problem, the function that base starting material mainly assigns shape of product and protects product to stablize.Facial treatment milk pin
It is various to different skin Questions types, but between it is healthy with it is non-health between " gray zone " inferior health skin, it is difficult to
Fundamentally improve.Traditional Chinese medicine has unique advantage nursed one's health in all directions, and can improve the regulating power of skin itself, promotes
The secretion of cytohyalop lasm acid, and recover the vigor of epidermal cell, the health status of skin is assigned again, and reaching improves skin Asia
The purpose of health status.
The content of the invention
The object of the present invention is to provide a kind of Chinese medicine composition of the lasting improvement skin sub-health state of safety, effect,
It is capable of the sub-health state of across-the-board regulation skin as cosmetics the effect of property component, improves skin gloss, active cell is lived
Power.
Should present invention also offers the preparation method of the Chinese medicine composition of above-mentioned improvement skin sub-health state and use
The skin care item of Chinese medicine composition.
In order to realize the above object technical side used by the Chinese medicine composition of the improvement skin sub-health state of the present invention
Case is：
It is a kind of improve skin sub-health state Chinese medicine composition, mainly by following parts by weight medicinal raw material polarity
Solvent extractable matter forms：10~25 parts of Poria cocos, 10~15 parts of pot marigold, 10~15 parts of sargassum, 10~15 parts of high mallow, peach blossom 10
~15 parts.
Skin care item in the present invention improve the spy of each medicinal raw material used in the Chinese medicine composition of skin sub-health state
Property is as follows：
Poria cocos, slightly sweet flavor is mild-natured, enters the heart, lung, kidney channel, has the effect of clearing damp and promoting diuresis invigorating the spleen.《Sheng Nong's herbal classic》Say
It：" diuresis.Long term usage peace soul is reposed, not hungry, macrobiosis." illustrate that it there are anti-aging effects；《Compendium of Materia Medica》Think：" solar eclipse
One piece, macrobiosis of moistening to one hundred days human body ... is resistance to old, if face ruddy complexion." illustrate that it has the effect of beauty；Meanwhile it or ancient times
One of externally applied drug is often used in beauty, such as《Bencao Pinhui Jingyao》Record：" PORIA ALBA for end, close honey and, in surface application.The more Shao- in treatment face
Blister and the black blister of puerpera such as sparrow ovum." discovery is studied, tuckahoe extracts can reach the proliferation rate of integrin 109%, the increasing of integrin
The diameter and volume-diminished of the collagen that can make fiber tooth cell encapsulation are grown, so as to there is contractive effect, while can be effectively eliminated
Superoxide radical, SOD of the 1g dry products equivalent to 360 units；Skin is measured after the coating of Poria cocos water extract with conductive method, moisture
Rate of scattering and disappearing can reduce by 80%, therefore tuckahoe extracts can be used for Firm and desalination skin lines, and available for skin moisture-keeping, anti-
The nursing role such as bacterium and conditioning.In the experiment to rat, to the shrinking percentage of pore up to 49.64%, therefore, tuckahoe extracts
Can also effective pore refining effect, fine skin.The Poria cocos that the present invention uses refers to the dry sclerotia of Poria cocos.Poria cocos is carried out
During extraction, cold soaking or decoction can be used, the yield of the cold soaking extract of Poria cocos dry sclerotia water is up to 5%.
Pot marigold is pot marigold, and bitter cold, has the effect of promoting blood circulation to remove blood stasis, promoting the circulation of qi promoting menstruation.Pot marigold extract, mainly into
It is the compounds such as carotenoid to divide.The pot marigold that the present invention uses is dry pot marigold.Research shows, pot marigold extract
With antibacterial action, and the oxygen of hydroxyl radical free radical and singlet can effectively be quenched, play good antioxidation.50% wine
Essence extract in cell culture to the proliferation rate of epidermal cell up to 116.5%, it is reachable to the propagation promotion rate of dermal cell
To 283%, 17.5% can reach to the inhibiting rate of elastoser.Pot marigold extract is coated on skin, is surveyed with conductance method
Determine water content of stratum corneum, water content of stratum corneum increase is original 3 times.Therefore, pot marigold extract can effectively strengthen skin
Activity, plays inferior health skin good moistening effect, and can eliminate microgroove, improves the effect of colour of skin dimness.
Sargassum, bitter is salty, cold in nature, such as liver and kidney channel.With clearing heat and eliminating phlegm, the function of softening and resolving hard mass.In TCM Document often
For treating all kinds of tubercle lumps, such as《Sheng Nong's herbal classic》Saying it, " main goiter and tumor gas, core under neck, breaks dissipating bind gas." at present, also use
Go to live in the household of one's in-laws on getting married in treatment facial scar, acne, skin.The main component of horse hair algae extract is compound of polysaccharide sodium alginate and poly- isophthalic
The compound of triphenol.The sargassum that the present invention uses is dry full algae.The diagonal cell plastid of horse hair algae extract and fibroblast
Propagation promotion rate respectively reach 130% and 109%；The rate that is eliminated to singlet oxygen and hydroxyl radical free radical is reachable respectively
50% and 38%；The promotion rate of hyaluronic acid generation is acted on up to 104%, therefore with good skin-active and moisturizing, and energy
The effect of effective anti-ageing, moisturizing and adjustment skin-balance.
High mallow, taste saltiness are trembled with fear, and have the function of clearing heat and detoxicating, qi-regulating dampness removing.The high mallow that the present invention uses refers to high mallow.Gold
Sunflower extract can promote the generation of elastin laminin and collagen.High mallow is carried with the alcohol that volume fraction is 50%
Take, 193% and 117% can be respectively reached to the generation promotion rate of elastin laminin, collagen in cell culture, to hyalomitome
The promotion rate of acid generation can reach 171%；After extract applies 7d on the skin, with the increase of Means of Electrical Conductivity water content of stratum corneum
Nearly 4 times；Can 100% suppression Corynebacterium xerosis；53%, therefore, high mallow can be reached to the inhibiting rate for generating male sex hormone
Flower extract in cosmetics can effective conditioning skin itself protective layer, the effect such as microgroove, effective moisturizing and anti-inflammatory can be eliminated,
Also there is good preventive and therapeutic effect to acne at the same time.
Peach blossom, it is bitter, put down, there is promoting blood circulation and removing blood stasis, inducing diuresis for removing edema to act on.《Sheng Nong's herbal classic》Say that it " can kill note evil spirit, make us
Good color "《Ge Shi side》Record " peach blossom, melon seeds grade, and smash with surface application " and control face more or such as sparrow ovum color side.Illustrate that it has well
Beauty functions.Elimination of the Flos persicae extract to hydroxyl radical free radical, superoxide radical, NO free radicals is obvious；In particular by alcohol
Eradicating efficacy is more obvious during extraction, after alcoholic extract is applied skin, the water content increase for the cuticula that conductive method measures
3 times.Flos persicae extract can be to oxynitrides and free radical etc. generation there is Antioxidation, therefore to skin energy
Effective moisturizing, and microgroove and skin-active effect can be eliminated, it can be used as moisturizer and anatrophic.
The traditional Chinese medical science thinks, whether main and internal organs qi and blood prosperity and decline and local skin qi and blood are unobstructed related whether skin health." lung
Main fur, main gas ", " its China of the heart is in face, controlling blood and vessel ", qi and blood fills Sheng, and passages through which vital energy circulates is unobstructed, and skin must support, then skin is moistened.If by
Not smooth in body insufficiency of vital energy and blood or operation, skin loses nutrition, is easy for dried-up simple and unadorned, generation wrinkle, dim spot.Therefore, exist
Maintain in skin health, overall qi and blood fills Sheng and the QI-blood circulation of part is unobstructed all extremely important.《The Yellow Emperor's Canon of Internal Medicine》Say " clear sun
Send out space between skin and muscles ", " defending gas, warm boundary between muscles, fertile space between skin and muscles, take charge of folding ", if such as phlegm wet, hemostasis, exopathogen cause face due to various reasons
Portion channels and collaterals obstruction, qi and blood be obstructed, clear sun cannot be for skin, the various metabolins less easy-clear in skin is so pernicious
Circulation, not only skin cannot moisten foster but also stagnation of QI-blood, metabolin deposition, be easy for it is withered matt, occur it is various dim
Spot；Local qi and blood is strongly fragrant long, and being also easy to fire, produces acne etc..Therefore, in the skin care for improving skin sub-health state of the present invention
Product make use of the Poria cocos of clearing damp and promoting diuresis, the pot marigold of promoting blood circulation to remove blood stasis, peach blossom, clearing heat and detoxicating, qi-regulating dampness removing high mallow, heat-clearing
The sargassum of phlegm, softening and resolving hard mass, five medicines share, play altogether eliminating toxic dampness and heat, heat-clearing disinfection the effect of.Both can be very good removing causes
The phlegm wet of local qi and blood retardance, hemostasis, and qi and blood retardance, the caused metabolism deposit of failure of skin and muscle to be nourished can be removed.Each medicine at the same time
Material raw material acts synergistically, and increases the moisture of skin, releases skin sub-health state, allows skin to reach a kind of and moistens, is glossiness
Health status.
Active ingredient in the Chinese medicine composition of the present invention is the polar solvent extract of medicinal raw material, in traditional
Medicine extracting method carries out medicinal raw material the efficient exudation that extraction is to ensure that active ingredient in medicinal raw material.
Poria cocos, pot marigold, the polar solvent extract of high mallow and peach blossom are molten using mixing using water extraction and alcohol precipitation method or directly
Agent carries out extraction and is made；The polar solvent extract of sargassum carries out extraction using water and is made.What the water extraction and alcohol precipitation method used
Alcohol is ethanol；The mixed solvent is made of second alcohol and water.During the heavy method of water purification, precipitation is removed after alcohol precipitation.
The water extraction and alcohol precipitation method is first to be extracted that extracting solution is made with water, and ethanol is then added in extracting solution to the body of ethanol
Fraction is 40~70%, and separation of solid and liquid, takes liquid that polar solvent extract is made；The volume integral of the in the mixed solvent ethanol
Number is 40~70%.
Preferably, the polar solvent extract of Poria cocos is made using water extraction and alcohol precipitation method；The polarity of pot marigold, high mallow and peach blossom
Solvent extractable matter is made using mixed solvent extraction；The volume fraction of addition ethanol to ethanol is in extracting solution during water extract-alcohol precipitation
60~70%；The volume fraction of the in the mixed solvent ethanol is 40~60%.
Technical solution is used by the preparation method of the Chinese medicine composition of the present invention：
A kind of preparation method of above-mentioned Chinese medicine composition, comprises the following steps：By Poria cocos, pot marigold, sargassum, high mallow,
Peach blossom is extracted using polar solvent, then concentrates extracting solution, concentrate is made, to obtain the final product.
The preparation method of the Chinese medicine composition of the present invention, technique is simple, easy to application.
Preferably, a kind of preparation method of above-mentioned Chinese medicine composition, comprises the following steps：
1) Poria cocos is extracted using water, obtains extracting solution, ethanol is then added in extracting solution to the volume of ethanol
Fraction is 60~70%, and separation of solid and liquid, is concentrated after liquid is removed ethanol, obtain Poria cocos concentrate；Or Poria cocos is used
The mixed solution of second alcohol and water composition is extracted, and is concentrated after extracting solution is removed ethanol, obtains Poria cocos concentrate；It is described
The volume fraction of ethanol is 60~70% in mixed solution；
It will be extracted after sargassum broken wall with water, extracting solution concentrated, obtains sargassum concentrate；
Pot marigold, high mallow and peach blossom are extracted using mixed solvent, pot marigold extracting solution, high mallow extraction are made respectively
The mixed extract of liquid, peach blossom extracting solution or obtained pot marigold, high mallow and peach blossom；Then respectively by pot marigold extracting solution, high mallow
Extracting solution, peach blossom extracting solution will be concentrated after mixed extract removal ethanol, obtain pot marigold concentrate, high mallow concentration
Liquid, peach blossom concentrate or mixed concentrated liquid；The mixed solvent is made of second alcohol and water；The volume of the in the mixed solvent ethanol
Fraction is 40~60%；
2) by Poria cocos concentrate, sargassum concentrate and pot marigold concentrate, high mallow concentrate, peach blossom concentrate or by Fu
Siberian cocklebur concentrate, sargassum concentrate are mixed with mixed concentrated liquid, to obtain the final product.
The preparation method of above-mentioned Chinese medicine composition, according to the characteristics of different medicinal raw materials, is carried using different methods
Take, can effectively ensure that both effectiveness component fully proposes.
In step 1), it is first to be crushed Poria cocos that Poria cocos is carried out extraction with water, is then soaked, and is decocted, separation
Fried liquid, extracting solution is used as using fried liquid.Preferably, after adding ethanol in extracting solution, 1~3h is stood, then carries out solid-liquid point
From.After isolating fried liquid, again water can also be added to be decocted the dregs of a decoction, separation of solid and liquid, is incorporated as with previous fried liquid
Extracting solution.The dregs of a decoction can be decocted repeatedly, and the fried liquid repeatedly decocted is incorporated as extracting solution.During decoction, adopted per 1g Poria cocos
The volume of water is 15~20mL.The decoction is first to be boiled boiling with big fire, then uses and is cooked by slow fire 25~35min.Decoct
The time soaked before boiling is 20~100min.Decoct before to Poria cocos carry out fully immersion can Poria cocos soften, cell water suction
Expansion, that is, be conducive to being fully dissolved out for active principle, can also shorten decocting time.When being cooked by slow fire, water slightly boiling is kept.
When Poria cocos is extracted using the mixed solution, Poria cocos is soaked into 20~100min in the mixed solution,
Liquid is isolated, obtains extracting solution.The volume of the mixed solution used per 1g Poria cocos is 8~12mL.
Sargassum is subjected to broken wall treatment using colloidal mill, the time of broken wall treatment is 2min.Sargassum is carried out with water
During extraction, the volume of the water used per 1g sargassums is 10~20mL.It is to break that the sargassum after broken wall is carried out extraction with water
Sargassum after wall soaks 8~12h, separation of solid and liquid, using liquid as extracting solution in 70~90 DEG C of water.
It is molten using the mixing of 8~12mL per 1g medicinal raw materials when pot marigold, high mallow and peach blossom are extracted using mixed solvent
Agent is soaked 3~4 days, and separation of solid and liquid, takes liquid as extracting solution；Or added according to every 1g medicinal raw materials using the mixed solvent of 10mL
Heat reflux 2~3 times, the time being heated to reflux every time is 0.5~1.5h, and the phegma that merging is heated to reflux every time is used as and carries
Take liquid.
During extracting solution removes ethanol, there may be a small amount of ethanol residual because of the difference of technique, this is also to be permitted
Perhaps.In step 1), removing ethanol can use the method for vacuum distillation to carry out.Such as decompression steaming is carried out using Rotary Evaporators
Evaporate.
In step 1), when extracting solution is concentrated, 0.8~1.5mL concentrations are concentrated to give according to every 3g medicinal raw materials
The ratio of liquid is concentrated.When volume is less than aforementioned proportion after concentration, suitable water polishing can be added in concentrate.
Preferably, the water used when being extracted to each medicinal raw material can be super water.
The concentration is to be freezed liquid to be concentrated, then vacuumizes and is concentrated in freezing state.Vacuumized
Vacuumized conditions are controlled to remove partial solvent, it can be achieved that the purpose of concentration in journey.Such as can by control time for vacuumizing into
Row concentration.
Preferably, the temperature of the freezing is -60~-80 DEG C, and the time is 20~30h.
Desivac concentration can protect the effective both effectiveness due activity of component；Extract is only concentrated and is not exclusively frozen
It is dry to solve the problems, such as that lyophilized rear powder is insoluble when carrying out skin care item preparation or is insoluble in base starting material.
Technical solution is used by the skin care item of the present invention：
A kind of skin care item, are made of base starting material and above-mentioned Chinese medicine composition.The polarity of Chinese medicine composition traditional Chinese medicinal material raw materials
Solvent extractable matter is skin care item primary efficacy component.
The Chinese medicine composition of the present invention is added in base starting material facial treatment milk is made；Chinese medicine composition is added to and is contained
In the base starting material of silty raw material, body of paste washing facial treatment mask can be made.The skin care milk of Chinese medicine composition using the present invention
Liquid and facial treatment mask can be effectively improved inferior health skin quality.
The skin care item are facial treatment mask；The base starting material includes silty raw material；The silty raw material is Plant Soot, height
Ridge is native, at least one of green clay, bentonite；The mass ratio of the silty raw material and Poria cocos is 9~50:10~25.Silty
Raw material can effectively remove the old dead angle matter of skin, further promote absorption and profit of the skin to active ingredient in extraction concentrate
With.The mass ratio of silty raw material and Poria cocos refers to Poria cocos of the silty raw material with being used to prepare the Chinese medicine composition in base starting material
Mass ratio.
Plant Soot, pungent-warm, Return liver, lung, stomach, have the effect of disinfection dissipates fire hemostasis.Main component is carbon granules, is passed through for weeds
The cigarette ink deposited in the bottom of a pan or chimney is invested after burning, its is light thin, therefore the frost of meaning, pharmaceutically acceptable.TCM Document is recorded and can used
To treat bleeding, sore etc..Modern study finds that it mainly has suction-operated, except can effectively remove the old dead cutin of skin,
Also there is the function such as calmness, anti-inflammatory, antibacterial, anti-oxidant to skin.Plant Soot heat dissipation disinfection, coordinate Poria cocos, pot marigold, sargassum,
High mallow and peach blossom, six medicines share, can further enhance eliminating toxic dampness and heat, heat-clearing disinfection the effect of.
The skin care item are facial treatment mask, and the base starting material is mainly made of the component of following parts by weight：Powder is former
10~50 parts of material, 2.5~3.5 parts of polyvinyl alcohol, 1.5~2.5 parts of pyrrolidone sodium carboxylate, 0.8~1.3 part of propane diols, ethanol
0.4~0.6 part.When the skin care item are facial treatment mask, the base starting material further includes water.Facial treatment mask is by the Chinese medicine group
After compound, silty raw material, polyvinyl alcohol, pyrrolidone sodium carboxylate, propane diols, ethanol mixing, add water to 100 parts of mixings and be made.
The skin care item are skin care milk；The base starting material is mainly made of the component of following parts by weight：Lanolin 5~
7 parts, 1.5~2.5 parts of pyrrolidone sodium carboxylate, 1.5~2.5 parts of glycerine, 0.15~0.25 part of magnesium sulfate, methyl hydroxybenzoate 0.08
~0.13 part, 0.9~1.3 part of sorbierite, 0.8~1.3 part of butanediol, 0.6~1.0 part of niacinamide, five polydimethylsiloxanes of ring
0.4~0.6 part of alkane.The mass ratio of the lanolin and Poria cocos is 5~7:10~25.The mass ratio of lanolin and Poria cocos refers to base
The mass ratio of Poria cocos of the lanolin with being used to prepare Chinese medicine composition in matter raw material.
When the skin care item are facial treatment milk, the matrix further includes water.Skin care milk be by Chinese medicine composition, lanolin,
Pyrrolidone sodium carboxylate, glycerine, magnesium sulfate, methyl hydroxybenzoate, sorbierite, butanediol, niacinamide, ring five dimethyl silicone polymer
After mixing, add water to 100 parts of mixings and be made.
Preferably, the water in the base starting material is H2O or T2O。
Brief description of the drawings
Fig. 1 be embodiment 1 on probation facial treatment milk during the moisture of volunteer or so face, the contrast of pigment testing result；
Fig. 2 be embodiment 1 on probation facial treatment milk during volunteer or so face roughness, microgroove testing result pair
Than；
Fig. 3 be embodiment 4 on probation facial treatment milk during the moisture of volunteer or so face, the contrast of pigment testing result；
Fig. 4 be embodiment 4 on probation facial treatment milk during volunteer or so face roughness, microgroove testing result pair
Than；
Fig. 5 be embodiment 5 on probation facial treatment mask during the moisture of volunteer or so face, the contrast of pigment testing result；
Fig. 6 be embodiment 5 on probation facial treatment mask during volunteer or so face roughness, microgroove testing result pair
Than；
Fig. 7 be embodiment 7 on probation facial treatment mask during the moisture of volunteer or so face, the contrast of pigment testing result；
Fig. 8 be embodiment 7 on probation facial treatment mask during volunteer or so face roughness, microgroove testing result pair
Than.
Embodiment
Technical scheme is further described below in conjunction with embodiment.
Embodiment 1
The Chinese medicine composition of the improvement skin sub-health state of the present embodiment, mainly by the medicinal raw material of following parts by weight
Polar solvent extract composition：20 parts of Poria cocos, 10 parts of pot marigold, 12 parts of sargassum, 10 parts of high mallow, 10 parts of peach blossom.
The preparation method of the Chinese medicine composition of the present embodiment, comprises the following steps：
1) Poria cocos is crushed, 1h is soaked using the ratio of 20mL water according to every 1g Poria cocos, is boiled by fire, is changed and be cooked by slow fire
30min, separates fried liquid, and the dregs of a decoction boil 1 time according to preceding method again, merges 2 fried liquid, and filter centrifugation, takes supernatant to add ethanol and mix,
The volume fraction for making ethanol is about 65%, places 2h, centrifugation, takes supernatant to be rotated out under vacuum conditions using Rotary Evaporators
Ethanol, then stays overnight remaining liq after revolving in -80 DEG C of pre-freezes, then vacuumizes removal partial solvent with freeze drier and carry out
Concentration, is made Poria cocos concentrate；(after concentration such as not enough, the ratio for concentrating out 1mL concentrates during concentration according to every 3g Poria cocos carries out
With super water polishing)；
2) sargassum is subjected to broken wall treatment using colloidal mill, the time of broken wall treatment is 2min, then according to every 1g
Sargassum uses the ratio of 15mL water, and the sargassum after broken wall is extracted 10h in 80 DEG C of heating water baths, is filtered, centrifugation, takes
Clearly, by supernatant in -80 DEG C of pre-freeze 20h, then with freeze drier concentration is vacuumized, sargassum concentrate is made；Pressed during concentration
The ratio that 1mL concentrates are concentrated out according to every 3g sargassums carries out (as inadequate after concentration, with super water polishing)；
3) mixing medicinal material is obtained after mixing pot marigold, high mallow and peach blossom, then uses 10mL according to every 1g mixing medicinal material
Mixed solvent soaks mixing medicinal material 3 days, filter and remove residue, centrifugation, and supernatant Rotary Evaporators low pressure is evaporated, removes second
Alcohol, obtains extracting solution, and extracting solution is stayed overnight in -80 DEG C of pre-freezes, then vacuumizes concentration with freeze drier, obtains mixed concentrated liquid；It is dense
The ratio for concentrating out 1mL concentrates during contracting according to every 3g mixing medicinal material carries out (as inadequate after concentration, with super water polishing)；Adopted
Mixed solvent is made of second alcohol and water, and the volume fraction of in the mixed solvent ethanol is 50%；
4) Poria cocos concentrate, sargassum concentrate and mixed concentrated liquid are mixed, to obtain the final product.
The skin care item of the present embodiment are facial treatment milk, are made of the Chinese medicine composition and base starting material of the present embodiment, matrix
Raw material is made of the component of super water and following parts by weight：6 parts of lanolin, 2 parts of pyrrolidone sodium carboxylate, 2 parts of glycerine, sulfuric acid
0.2 part of magnesium, 0.1 part of methyl hydroxybenzoate, 70% 1.5 parts of sorbierite, 1 part of butanediol, 0.8 part of niacinamide, five poly dimethyl silicon of ring
0.5 part of oxygen alkane；The mass ratio of Poria cocos of the lanolin with being used to prepare Chinese medicine composition is 6:20.
The preparation method of the facial treatment milk of the present embodiment, comprises the following steps：By Chinese medicine composition, lanolin, pyrrolidines
Keto carboxylic acid sodium, glycerine, magnesium sulfate, methyl hydroxybenzoate, 70% sorbierite, butanediol, niacinamide, ring five dimethyl silicone polymer are mixed
Close, then plus super water ad pond om number is 100 parts, is mixed, to obtain the final product.
Embodiment 2
The Chinese medicine composition of the improvement skin sub-health state of the present embodiment, mainly by the medicinal raw material of following parts by weight
Polar solvent extract composition：10 parts of Poria cocos, 10 parts of pot marigold, 10 parts of sargassum, 10 parts of high mallow, 10 parts of peach blossom.
The preparation method of the Chinese medicine composition of the present embodiment, comprises the following steps：
1) Poria cocos is crushed, 100min is soaked using the ratio of 20mL water according to every 1g Poria cocos, is boiled by fire, changes text
Fire boils 25min, separates fried liquid, and the dregs of a decoction boil 1 time according to preceding method again, merges 2 fried liquid, filter centrifugation, takes supernatant to add ethanol
Mix, the volume fraction for making ethanol is 70%, places 1h, centrifugation, takes supernatant to be revolved under vacuum conditions using Rotary Evaporators
Ethanol is steamed, is then stayed overnight remaining liq after revolving in -80 DEG C of pre-freezes, then removal partial solvent is vacuumized with freeze drier
Concentrated, Poria cocos concentrate is made；The ratio for concentrating out 1mL concentrates during concentration according to every 3g Poria cocos carries out (after concentration such as
Not enough, with super water polishing)；
2) sargassum is subjected to broken wall treatment using colloidal mill, the time of broken wall treatment is 2min, then according to every 1g
Sargassum uses the ratio of 20mL water, and the sargassum after broken wall is extracted 8h in 70 DEG C of heating water baths, is filtered, and centrifugation, takes supernatant,
By supernatant in -80 DEG C of pre-freeze 30h, then with freeze drier concentration is vacuumized, sargassum concentrate is made；According to every during concentration
The ratio that 3g sargassums concentrate out 1mL concentrates carries out (as inadequate after concentration, with super water polishing)；
3) mixing medicinal material is obtained after mixing pot marigold, high mallow and peach blossom, then uses 12mL according to every 1g mixing medicinal material
Mixed solvent soaks mixing medicinal material 4 days, filter and remove residue, centrifugation, and supernatant Rotary Evaporators low pressure is evaporated, removes second
Alcohol, obtains extracting solution, and extracting solution is stayed overnight in -80 DEG C of pre-freezes, then vacuumizes concentration with freeze drier, obtains mixed concentrated liquid；It is dense
The ratio for concentrating out 1mL concentrates during contracting according to every 3g mixing medicinal material carries out (as inadequate after concentration, with super water polishing)；Adopted
Mixed solvent is made of second alcohol and water, and the volume fraction of in the mixed solvent ethanol is 60%；
4) Poria cocos concentrate, sargassum concentrate and mixed concentrated liquid are mixed, to obtain the final product.
The skin care item of the present embodiment are facial treatment milk, are made of the Chinese medicine composition and base starting material of the present embodiment, matrix
Raw material is made of the component of super water and following parts by weight：5 parts of lanolin, 2.5 parts of pyrrolidone sodium carboxylate, 1.5 parts of glycerine,
0.25 part of magnesium sulfate, 0.08 part of methyl hydroxybenzoate, 70% 1.3 parts of sorbierite, 1.3 parts of butanediol, 0.6 part of niacinamide, ring five are poly-
0.54 part of dimethyl siloxane；The mass ratio of Poria cocos of the lanolin with being used to prepare Chinese medicine composition is 6:10.
The preparation method of the facial treatment milk of the present embodiment, comprises the following steps：By Chinese medicine composition, lanolin, pyrrolidines
Keto carboxylic acid sodium, glycerine, magnesium sulfate, methyl hydroxybenzoate, 70% sorbierite, butanediol, niacinamide, ring five dimethyl silicone polymer are mixed
Close, then plus super water ad pond om number is 100 parts, is mixed, to obtain the final product.
Embodiment 3
The Chinese medicine composition of the improvement skin sub-health state of the present embodiment, mainly by the medicinal raw material of following parts by weight
Polar solvent extract composition：25 parts of Poria cocos, 15 parts of pot marigold, 15 parts of sargassum, 15 parts of high mallow, 15 parts of peach blossom.
The preparation method of the Chinese medicine composition of the present embodiment, comprises the following steps：
1) Poria cocos is crushed, 20min is soaked using the ratio of 15mL water according to every 1g Poria cocos, is boiled by fire, changes text
Fire boils 35min, separates fried liquid, and the dregs of a decoction boil 1 time according to preceding method again, merges 2 fried liquid, filter centrifugation, takes supernatant to add ethanol
Mix, the volume fraction for making ethanol is 60%, places 3h, centrifugation, takes supernatant to be revolved under vacuum conditions using Rotary Evaporators
Ethanol is steamed, remaining liq vacuumizes removal partial solvent in -80 DEG C of pre-freeze 24h, then with freeze drier after then rotating
Concentrated, Poria cocos concentrate is made；The ratio for concentrating out 1mL concentrates during concentration according to every 3g Poria cocos carries out (after concentration such as
Not enough, with water (H2O) polishing)；
2) sargassum is subjected to broken wall treatment using colloidal mill, the time of broken wall treatment is 2min, then according to every 1g
Sargassum uses the ratio of 10mL water, and the sargassum after broken wall is extracted 12h in 90 DEG C of heating water baths, is filtered, centrifugation, takes
Clearly, supernatant is stayed overnight in -80 DEG C of pre-freezes, then concentration is vacuumized with freeze drier, sargassum concentrate is made；Pressed during concentration
The ratio that 1mL concentrates are concentrated out according to every 3g sargassums is carried out (as inadequate after concentration, with water (H2O) polishing)；
3) mixing medicinal material is obtained after mixing pot marigold, high mallow and peach blossom, is then mixed according to every 1g mixing medicinal material using 8ml
Bonding solvent soaks mixing medicinal material 4 days, filter and remove residue, centrifugation, and supernatant Rotary Evaporators low pressure is evaporated, removes ethanol,
Extracting solution is obtained, extracting solution is stayed overnight in -80 DEG C of pre-freezes, then concentration is vacuumized with freeze drier, obtains mixed concentrated liquid；During concentration
The ratio that 1mL concentrates are concentrated out according to every 3g mixing medicinal material is carried out (as inadequate after concentration, with water (H2O) polishing)；Used
Mixed solvent be made of second alcohol and water, the volume fraction of in the mixed solvent ethanol is 40%；
4) Poria cocos concentrate, sargassum concentrate and mixed concentrated liquid are mixed, to obtain the final product.
The skin care item of the present embodiment are facial treatment milk, are made of the Chinese medicine composition and base starting material of the present embodiment, matrix
Raw material is by water (H2O) and following parts by weight component composition：7 parts of lanolin, 1.5 parts of pyrrolidone sodium carboxylate, glycerine 2.5
Part, 0.15 part of magnesium sulfate, 0.13 part of methyl hydroxybenzoate, 70% 1.8 parts of sorbierite, 0.8 part of butanediol, 1 part of niacinamide, ring five are poly-
0.6 part of dimethyl siloxane；The mass ratio of Poria cocos of the lanolin with being used to prepare Chinese medicine composition is 6:25.
The preparation method of the facial treatment milk of the present embodiment, comprises the following steps：By Chinese medicine composition, lanolin, pyrrolidines
Keto carboxylic acid sodium, glycerine, magnesium sulfate, methyl hydroxybenzoate, 70% sorbierite, butanediol, niacinamide, ring five dimethyl silicone polymer are mixed
Close, then add water (H2O) ad pond om number is 100 parts, is mixed, to obtain the final product.
Embodiment 4
The Chinese medicine composition of the improvement skin sub-health state of the present embodiment, mainly by the medicinal raw material of following parts by weight
Polar solvent extract composition：18 parts of Poria cocos, 12 parts of pot marigold, 10 parts of sargassum, 12 parts of high mallow, 12 parts of peach blossom.This implementation
The preparation method of the Chinese medicine composition of example is the same as embodiment 1.
The skin care item of the present embodiment are facial treatment milk, are made of the Chinese medicine composition and base starting material of the present embodiment, matrix
Raw material is made of the component of super water and following parts by weight：6 parts of lanolin, 2 parts of pyrrolidone sodium carboxylate, 2 parts of glycerine, sulfuric acid
0.2 part of magnesium, 0.1 part of methyl hydroxybenzoate, 70% 1.5 parts of sorbierite, 1 part of butanediol, 0.8 part of niacinamide, five poly dimethyl silicon of ring
0.5 part of oxygen alkane；The mass ratio of Poria cocos of the lanolin with being used to prepare Chinese medicine composition is 6:10.
The preparation method of the facial treatment milk of the present embodiment, comprises the following steps：By Chinese medicine composition, lanolin, pyrrolidines
Keto carboxylic acid sodium, glycerine, magnesium sulfate, methyl hydroxybenzoate, 70% sorbierite, butanediol, niacinamide, ring five dimethyl silicone polymer are mixed
Close, then plus super water ad pond om number is 100 parts, is mixed, to obtain the final product.
Embodiment 5
The skin care item of the present embodiment wash facial treatment mask for body of paste, by the Chinese medicine composition and base starting material of embodiment 1
Composition, base starting material are made of the component of super water and following parts by weight：30 parts of silty raw material, 2.5 parts of polyvinyl alcohol, pyrroles
2.5 parts of alkanone carboxylic acid sodium, 0.8 part of propane diols, 0.56 part of ethanol；The matter of Poria cocos of the silty raw material with being used to prepare Chinese medicine composition
Amount is than being 30:20；Used silty raw material is Plant Soot.
The preparation method of the facial treatment mask of the present embodiment, comprises the following steps：By Chinese medicine composition, silty raw material, poly- second
Enol, pyrrolidone sodium carboxylate, propane diols, ethanol mixing, then plus super water ad pond om number is 100 parts, is mixed, i.e.,
.
Embodiment 6
The skin care item of the present embodiment wash facial treatment mask for body of paste, by the Chinese medicine composition and base starting material of embodiment 2
Composition, base starting material are made of the component of super water and following parts by weight：9 parts of silty raw material, 3.5 parts of polyvinyl alcohol, pyrroles
1.5 parts of alkanone carboxylic acid sodium, 1.3 parts of propane diols, 0.4 part of ethanol；The matter of Poria cocos of the silty raw material with being used to prepare Chinese medicine composition
Amount is than being 9:10；Used silty raw material is Plant Soot.
The preparation method of the facial treatment mask of the present embodiment, comprises the following steps：By Chinese medicine composition, silty raw material, poly- second
Enol, pyrrolidone sodium carboxylate, propane diols, ethanol mixing, then plus super water ad pond om number is 100 parts, is mixed, i.e.,
.
Embodiment 7
The skin care item of the present embodiment wash facial treatment mask for body of paste, by the Chinese medicine composition and base starting material of embodiment 3
Composition, base starting material is by water (H2O) and following parts by weight component composition：25 parts of silty raw material, 3 parts of polyvinyl alcohol, pyrroles
2 parts of alkanone carboxylic acid sodium, 1 part of propane diols, 0.5 part of ethanol；The mass ratio of Poria cocos of the silty raw material with being used to prepare Chinese medicine composition
For 25:25；Used silty raw material is Plant Soot.
The preparation method of the facial treatment mask of the present embodiment, comprises the following steps：By Chinese medicine composition, silty raw material, poly- second
Enol, pyrrolidone sodium carboxylate, propane diols, ethanol mixing, then add water (H2O) ad pond om number is 100 parts, is mixed, i.e.,
.
Embodiment 8
The skin care item of the present embodiment wash facial treatment mask for body of paste, by the Chinese medicine composition and base starting material of embodiment 4
Composition, base starting material are made of the component of super water and following parts by weight：22 parts of silty raw material, 3 parts of polyvinyl alcohol, pyrrolidines
2 parts of keto carboxylic acid sodium, 1 part of propane diols, 0.5 part of ethanol；The mass ratio of Poria cocos of the silty raw material with being used to prepare Chinese medicine composition is
22:18；Used silty raw material is Plant Soot.
The preparation method of the facial treatment mask of the present embodiment, comprises the following steps：By Chinese medicine composition, silty raw material, poly- second
Enol, pyrrolidone sodium carboxylate, propane diols, ethanol mixing, then plus super water ad pond om number is 100 parts, is mixed, i.e.,
.
Embodiment 9
The Chinese medicine composition of the improvement skin sub-health state of the present embodiment, mainly by the medicinal raw material of following parts by weight
Polar solvent extract composition：20 parts of Poria cocos, 10 parts of pot marigold, 12 parts of sargassum, 10 parts of high mallow, 10 parts of peach blossom.This implementation
The preparation method of the Chinese medicine composition of example is the same as embodiment 1.
The skin care item of the present embodiment wash facial treatment mask for body of paste, by the Chinese medicine composition and base starting material of the present embodiment
Composition, base starting material are made of the component of super water and following parts by weight：30 parts of silty raw material, 3 parts of polyvinyl alcohol, pyrrolidines
2 parts of keto carboxylic acid sodium, 1 part of propane diols, 0.5 part of ethanol；The mass ratio of Poria cocos of the silty raw material with being used to prepare Chinese medicine composition is
30:20；Used silty raw material is kaolin.
The preparation method of the facial treatment mask of the present embodiment, comprises the following steps：By Chinese medicine composition, silty raw material, poly- second
Enol, pyrrolidone sodium carboxylate, propane diols, ethanol mixing, then plus super water ad pond om number is 100 parts, is mixed, i.e.,
.
Effect detection：
Experimental method and result：Effect detection be to the facial treatment milk of embodiment 1,4 and the facial treatment mask of embodiment 5,7 into
The detection of row using effect.
1) the skin-protection product moisture retention of embodiment 1,4,5 and 7 is detected, using the matrix of embodiment 1 as control
Group, the external weight method of detection use (reference Liu Wei, what Zhang Huailiang was compiled《Dermatology is evaluated with cosmetic industry》Employed in
Weight method), 10g products to be tested are uniformly applied on a culture dish bottle cap, is contrasted with base starting material, is put into constant temperature and humidity
In case, weigh once within every 15 minutes, nominal amount 5 times, calculates moisture-holding capacity=remaining quality/sample quality (%), the results are shown in Table
1。
Table 1 measures the result of moisture-holding capacity every time
| Number | For the first time | Second | For the third time | 4th time | 5th time |
| Embodiment 1 | 95.8 | 91.0 | 90.4 | 89.2 | 86.9 |
| Embodiment 4 | 93.4 | 89.9 | 88.6 | 85.8 | 80.5 |
| Embodiment 5 | 90.1 | 89.4 | 85.7 | 84.5 | 79.3 |
| Embodiment 7 | 90.4 | 87.8 | 86.3 | 79.8 | 76.1 |
| Base starting material | 21.1 | 15.5 | 10.7 | 8.8 | 6.7 |
As can be seen from Table 4, weighed by continuous five times, the moisture-holding capacity of facial treatment milk and facial mask is said more than 50%
Bright Water-saving effect is good, and water holding capacity is more preferable than matrix components.
2) experimental subjects is the individual of 12 different occupations no more than 40 years old, left half face of each volunteer is carried out real
Apply the on probation of the skin care item of example 1,4,5,7, right half face applies corresponding matrix at the same time, each one group of embodiment, every group of 3 people,
Pass through scientific and technological moisture, color of (Shenzhen Lang Dai industry developments Co., Ltd) the witch mirror LD6021 series skins analyzer to skin of bright enlightening
Five aspects such as element, microgroove, roughness carry out the comparative analysis of qualitative, quantitative.
Experimental period：Skin epidermis all renewals generally at 28 days or so, so test period is 28 days.
Subject Population：Because occurring in age less high crowd more than inferior health skin quality, age too high person, skin problem one
As than more serious, category of the skin problem such as wrinkle, color spot and aging beyond inferior health.Therefore, 12 ages are randomly selected
Different sexes, the volunteer of occupation carry out facial treatment mask actual effect test below 40 years old.Numbering, the gender of 12 volunteers
And the age is shown in Table 2.
The information for the volunteer that table 2 randomly selects
| Numbering | 1 | 2 | 3 | 4 | 5 | 6 | 7 | 8 | 9 | 10 | 11 | 12 |
| Gender | Female | Female | Female | Man | Female | Female | Man | Man | Female | Female | Man | Female |
| Age (year) | 21 | 40 | 37 | 40 | 31 | 25 | 26 | 35 | 33 | 19 | 32 | 36 |
1. the facial treatment milk of 1~No. 3 embodiment 1 on probation, the facial treatment milk of 4~No. 6 embodiments 4 on probation, applies sooner or later daily
Smear.Carry out moisture, pigment, roughness, the microgroove point of left and right face to each volunteer with witch mirror LD6021 skin analyzers weekly
Do not detect once, each item data of 3 people is averaged every time, the testing result being detected as the first time before uncoated, similarly hereinafter, test
It the results are shown in Table 3~4 and Fig. 1~4.
3 embodiment of table, 1 trial effect
4 embodiment of table, 4 trial effect
It can be seen that from 3 table 4 of table：Left face and right water for washing the face point increase the obvious ascendant trend of presentation with coating number,
Left face applies lotion, and the improvement degree of moisture of skin substantially becomes apparent from than right face；And the left and right such as pigment, roughness and microgroove face
There is different degrees of improvement, but left face coating lotion becomes apparent from than the degree that right face coated substrate improves, and illustrates to add Chinese medicine
The lotion of composition can effectively improve the sub-health status such as skin, the colour of skin be dry, obscure, coarse.
2. the facial treatment mask of the facial treatment mask of 7~No. 9 embodiments 5 on probation, 10~No. 12 embodiments 7 on probation, left face is weekly
Facial treatment mask, right face apply corresponding matrix twice for coating, clean within 20 minutes.It is every to use witch mirror LD6021 skins twice after cleaning
Analyzer detects the moisture of left and right face, pigment, roughness, microgroove, and three personal datas, are averaged by surrounding every time altogether, surveys
Test result is shown in Table 5~6 and Fig. 5~8.
5 embodiment of table, 5 trial effect
6 embodiment of table, 7 trial effect
It can be seen that from 5 table 6 of table：Left face and right water for washing the face point increase the obvious ascendant trend of presentation with coating number,
Left face applies facial mask, and the improvement degree of moisture of skin substantially becomes apparent from than right face coated substrate；And pigment, roughness and microgroove
There is different degrees of improvement Deng left and right face, but left face coating facial mask becomes apparent from than the degree that right face coated substrate improves, explanation
The facial mask for adding Chinese medicine composition also can effectively improve the sub-health status such as skin, the colour of skin be dry, obscure, coarse.
Claims (10)
- A kind of 1. Chinese medicine composition for improving skin sub-health state, it is characterised in that：Mainly by the medicinal material of following parts by weight The polar solvent extract composition of raw material：10~25 parts of Poria cocos, 10~15 parts of pot marigold, 10~15 parts of sargassum, high mallow 10~ 15 parts, 10~15 parts of peach blossom.
- 2. the Chinese medicine composition according to claim 1 for improving skin sub-health state, it is characterised in that：Poria cocos, golden small cup The polar solvent extract of flower, high mallow and peach blossom using mixed solvent extract obtained using water extraction and alcohol precipitation method or directly；Horse The polar solvent extract of tail algae carries out extraction using water and is made；The alcohol that the water extraction and alcohol precipitation method uses is ethanol；The mixing Solvent is made of second alcohol and water.
- 3. the Chinese medicine composition according to claim 2 for improving skin sub-health state, it is characterised in that：The water extracting alcohol Heavy method is first to be extracted that extracting solution is made with water, and the volume fraction that ethanol to ethanol are then added in extracting solution is 40~70%, Separation of solid and liquid, takes liquid that polar solvent extract is made；The volume fraction of the in the mixed solvent ethanol is 40~70%.
- 4. the Chinese medicine composition according to claim 3 for improving skin sub-health state, it is characterised in that：The polarity of Poria cocos Solvent extractable matter is made using water extraction and alcohol precipitation method；The polar solvent extract of pot marigold, high mallow and peach blossom is carried using mixed solvent Take obtained；The volume fraction for adding ethanol to ethanol during water extract-alcohol precipitation in extracting solution is 60~70%；The in the mixed solvent The volume fraction of ethanol is 40~60%.
- A kind of 5. preparation method of Chinese medicine composition as claimed in claim 1, it is characterised in that：Comprise the following steps：By Fu Siberian cocklebur, pot marigold, sargassum, high mallow, peach blossom are extracted using polar solvent, then concentrate extracting solution, concentrate are made, i.e., .
- 6. the preparation method of Chinese medicine composition according to claim 5, it is characterised in that：The concentration is by solution to be concentrated Body freezes, and then vacuumizes and is concentrated in freezing state.
- A kind of 7. skin care item, it is characterised in that：It is made of base starting material and Chinese medicine composition as claimed in claim 1.
- 8. skin care item according to claim 7, it is characterised in that：The skin care item are facial treatment mask；The base starting material Including silty raw material；The silty raw material is at least one of Plant Soot, kaolin, green clay, bentonite；The silty is former The mass ratio of material and Poria cocos is 9~50:10~25.
- 9. skin care item according to claim 8, it is characterised in that：The base starting material is mainly by the group of following parts by weight It is grouped into：10~50 parts of powder material, 2.5~3.5 parts of polyvinyl alcohol, 1.5~2.5 parts of pyrrolidone sodium carboxylate, propane diols 0.8 ~1.3 parts, 0.4~0.6 part of ethanol.
- 10. skin care item according to claim 7, it is characterised in that：The skin care item are facial treatment milk；The base starting material Mainly it is made of the component of following parts by weight：5~7 parts of lanolin, 1.5~2.5 parts of pyrrolidone sodium carboxylate, glycerine 1.5~ 2.5 parts, 0.15~0.25 part of magnesium sulfate, 0.08~0.13 part of methyl hydroxybenzoate, 0.9~1.3 part of sorbierite, butanediol 0.8~ 1.3 parts, 0.6~1.0 part of niacinamide, 0.4~0.6 part of ring five dimethyl silicone polymer.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113116753A (en) * | 2021-04-23 | 2021-07-16 | 厦门力嘉诚生物科技有限公司 | Rose essential oil face cream and preparation method thereof |
| CN113116801A (en) * | 2019-12-26 | 2021-07-16 | 华熙生物科技股份有限公司 | Composition for improving skin sub-health state and preparation method thereof |
| CN115590793A (en) * | 2022-09-08 | 2023-01-13 | 河南中医药大学（Cn） | Traditional Chinese medicine washing and caring liquid for improving sub-health state of scalp and hair and preparation method and application thereof |
-
2017
- 2017-12-16 CN CN201711355380.0A patent/CN107970293A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113116801A (en) * | 2019-12-26 | 2021-07-16 | 华熙生物科技股份有限公司 | Composition for improving skin sub-health state and preparation method thereof |
| CN113116753A (en) * | 2021-04-23 | 2021-07-16 | 厦门力嘉诚生物科技有限公司 | Rose essential oil face cream and preparation method thereof |
| CN113116753B (en) * | 2021-04-23 | 2022-06-03 | 厦门力嘉诚生物科技有限公司 | Rose essential oil face cream and preparation method thereof |
| CN115590793A (en) * | 2022-09-08 | 2023-01-13 | 河南中医药大学（Cn） | Traditional Chinese medicine washing and caring liquid for improving sub-health state of scalp and hair and preparation method and application thereof |
| CN115590793B (en) * | 2022-09-08 | 2023-09-15 | 河南中医药大学 | Traditional Chinese medicine washing and caring liquid for improving sub-health state of scalp and hair, and preparation method and application thereof |
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Application publication date: 20180501 |