CN111346031A - Functional slow-release lipstick and preparation method thereof - Google Patents
Functional slow-release lipstick and preparation method thereof Download PDFInfo
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/738—Cyclodextrins
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
- A61Q1/06—Lipsticks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/56—Compounds, absorbed onto or entrapped into a solid carrier, e.g. encapsulated perfumes, inclusion compounds, sustained release forms
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
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- A61K2800/782—Enzyme inhibitors; Enzyme antagonists
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Abstract
The invention relates to a functionalized sustained-release lipstick and a preparation method thereof, wherein the functionalized sustained-release lipstick comprises, by weight, 15-20 parts of beeswax, 5-15 parts of candelilla wax, 30-50 parts of olive oil, 15-25 parts of sweet almond oil, 5-30 parts of β -cyclodextrin-natural pigment inclusion compound, 0-10 parts of color-mixing natural pigment, 0.1-1 part of vitamin E, 0.1-0.5 part of natural perfume, one, any two, any three, any four or five compositions of tea pigment, seabuckthorn polysaccharide, rhodiola rosea extract, gynostemma pentaphylla extract and astragalus extract.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to a functional slow-release lipstick and a preparation method thereof.
Background
Human lips, as exposed skin, not only face the health problems caused by environmental pollution, but also as food passage organs, are subjected to stimulation of different ingredients such as sourness, sweetness, bitterness, spiciness, saltiness, and the like. With the improvement of the living standard of human beings, the requirement and quality requirement of lip care for human beings, especially women, are continuously increased. Traditional nursing products such as lipstick and lipstick contain high amount of heavy metals such as lead and cadmium, and are easy to cause problems such as anemia, bellyache and acute renal failure after long-term use. Generally, the lip care product is frequently used in the daytime, and is a peak period when people drink and eat water, substances harmful to health on the lip care product easily enter human bodies along with eating, and after lipstick is smeared, the color gradually becomes shallow along with the time due to the oxidation of air and the absorption of skin, and the functional nourishing components cannot play a role in nourishing the lips for a long time.
The invention patent 201810656511.7 discloses a jasmine flower lipstick and a preparation method thereof, and specifically relates to a jasmine flower lipstick which is prepared by applying jasmine flower hydrosol to a lipstick formula and has the advantages of safety, no side effect, lip nourishing and natural fragrance of jasmine flowers; the invention patent 201811396814.6 discloses a lipstick with repairing effect and a preparation method thereof, and particularly relates to a functional lipstick with repairing and anti-inflammatory effects, which is developed by introducing C10-30 acid cholesterol/lanosterol mixed ester into a lipstick formula, so that with the development of science and technology, natural and environment-friendly materials and even natural materials with health care and repairing functions become the first choice of cosmetic raw materials.
Disclosure of Invention
The invention aims to provide a lip nourishing lipstick which is safe, has no side effect, is antibacterial, antioxidant and anti-aging and has a slow release function.
The invention also aims to provide a preparation method of the functional sustained-release lipstick.
The functional slow-release lipstick is prepared from the following raw materials, by weight, 15-20 parts of beeswax, 5-15 parts of candelilla wax, 30-50 parts of olive oil, 15-25 parts of sweet almond oil, 5-30 parts of β -cyclodextrin-natural pigment inclusion compound, 0-10 parts of color-mixing natural pigment, 0.1-1 part of vitamin E, 0.1-0.5 part of natural perfume, one, two, three, four or five of tea pigment, hippophae rhamnoides polysaccharide, rhodiola rosea extract, gynostemma pentaphylla extract and astragalus membranaceus extract.
Preferably, the extraction of tea pigments: weighing tea leaves, adding deionized water, refluxing for 1h at 40-60 ℃, filtering to remove the tea leaves, adjusting the pH of the liquid to 6.5-7, condensing to one tenth of the original liquid, adjusting the pH to 4-6, adding absolute ethyl alcohol according to the volume ratio of 1:1, refluxing, adjusting the pH to 6.5-7, distilling to remove the solvent, and drying the remainder in an oven to obtain the tea.
Preferably, the extraction of the hippophae rhamnoides polysaccharide: adding deionized water into defatted fructus Hippophae powder without monosaccharide and oligosaccharide, refluxing at 70-80 deg.C for 2-3 hr, filtering, concentrating the filtrate to one tenth of the original liquid, adding 95% ethanol to precipitate polysaccharide, storing at 0-5 deg.C for 48 hr, filtering, washing with anhydrous ethanol, and vacuum drying at-80 deg.C to-100 deg.C.
Preferably, the extraction of the rhodiola rosea extract: adding 50% ethanol water solution into radix Rhodiolae, refluxing at 80-90 deg.C for 2-3 hr, filtering, concentrating the filtrate, and vacuum drying at-80 deg.C to-100 deg.C to obtain the final product.
Preferably, the extraction of the gynostemma pentaphyllum extract is as follows: weighing dried herba Gynostemmatis, adding anhydrous ethanol, refluxing at 90-95 deg.C for 2-3 hr, vacuum filtering, removing residue, concentrating the liquid to paste, and vacuum drying at-80 deg.C to-100 deg.C.
Preferably, the extraction of the astragalus extract: weighing dried radix astragali, adding anhydrous ethanol, refluxing at 90 deg.C for 2-3 hr, vacuum filtering, discarding residue, concentrating to one tenth of stock solution, and vacuum drying at-80 deg.C to-100 deg.C.
Preferably, the β -natural pigment and toning pigment included by cyclodextrin are one or a mixture of any more of paprika red pigment, tomato red pigment, rose juice extract, safflower yellow pigment, mulberry red pigment, sorghum red pigment, peanut skin red pigment, β -carotene and corn yellow pigment.
Preferably, the natural perfume is one or a mixture of any more of rose essential oil, bergamot essential oil, mint essential oil, sweet osmanthus essential oil, rosemary essential oil, nardostachys chinensis essential oil, lemon essential oil, cinnamon essential oil, lavender essential oil, jasmine essential oil and rose oil.
A method for preparing functional sustained-release lipstick comprises the following steps:
β -preparation of cyclodextrin-natural pigment clathrate compound, which comprises dissolving β -cyclodextrin in distilled water at 80 deg.C, dissolving appropriate amount of natural pigment in ethanol or water, mixing the two solutions slowly for clathration for 2-3h, standing overnight, washing with anhydrous ethanol, and drying to obtain β -cyclodextrin-natural pigment clathrate compound;
grinding β -cyclodextrin-natural pigment inclusion compound, toning natural pigment, one, any two, any three or four of sea buckthorn polysaccharide, rhodiola rosea extract, gynostemma pentaphylla extract and astragalus extract for 1h to obtain a uniform mixture;
heating and melting beeswax, candelilla wax, olive oil, sweet almond oil and vitamin E at 80-90 ℃, adding the mixture obtained in the step (2) and natural perfume, stirring uniformly, and cooling for later use;
and (4) pouring the mixture obtained in the step (3) into a mold, cooling and shaping the filled mold at the temperature of 2-5 ℃ for 10-30min, and demolding to obtain the functional slow-release lipstick.
The invention has the beneficial effects that: the functional sustained-release lipstick which has the sustained-release function and can prolong the shelf life and the service time of the lipstick and improve the effective nourishing time and the shelf life is developed by fully utilizing the physiological effects of the effective components of the natural components of the tea pigment, the hippophae rhamnoides polysaccharide, the rhodiola rosea, the gynostemma pentaphylla and the astragalus and combining the sustained-release function of the cyclodextrin structure to prepare the pigment and the nourishing components into the sustained-release material.
β -truncated cone cylinder cavity of cyclodextrin can envelop various object molecules and is used as sustained release agent of object by people, so that effective ingredients are enveloped in the cavity, effective ingredients are released slowly, and use effect is improved
Tea pigment is a water-soluble phenolic pigment extracted from tea leaves, and the tea pigment is a main component of the tea pigment, has pharmacological actions of resisting lipid peroxidation, enhancing immunity, reducing blood fat, bidirectionally regulating blood pressure and blood fat, resisting atherosclerosis, reducing blood viscosity, improving microcirculation, inhibiting experimental tumors and the like, and is known as 'green gold in medicine'.
The sea buckthorn polysaccharide has various activities, such as antibacterial, antioxidant and anti-aging effects, and also has the effects of resisting tumors, preventing and treating cardiovascular and cerebrovascular system diseases and the like in the aspect of medicine.
Modern pharmacological and clinical researches find that the rhodiola rosea has the tonifying effect similar to that of ginseng, and has the effects of resisting anoxia, cold, fatigue, radiation and viruses and inhibiting the growth of cancer cells.
Gynostemma pentaphyllum has antiaging, antifatigue, anticancer, endocrine regulating, stress tolerance and immunity improving, cholesterol and transaminase reducing, tumor preventing, and ulcer inhibiting effects.
Radix astragali can improve immunity and delay cell aging process.
Detailed Description
The formulation and preparation method of the functional sustained-release lipstick of the present invention are further described in detail by the following specific examples.
Example 1
A functional sustained-release lipstick is prepared from (by weight parts) Cera flava 10, candelilla wax 10, oleum Olivarum 45, sweet almond oil 15, β -cyclodextrin-lycopene clathrate 25, natural pigment with color matching 0-10, vitamin E0.2, rose essential oil 0.2, fructus Hippophae polysaccharide 6, and radix Rhodiolae extract 2.
Wherein, the extraction of tea pigment: weighing 50g of tea leaves, adding 2L of deionized water, refluxing for 1h at 40 ℃, filtering to remove the tea leaves, adjusting the pH of the liquid to 6.5, condensing to one tenth of the original liquid, adjusting the pH to 4, adding absolute ethyl alcohol according to the volume ratio of 1:1, refluxing, adjusting the pH to 6.5, distilling to remove the solvent, and drying the remainder in an oven to obtain the tea leaf.
Extracting the sea buckthorn polysaccharide: adding 50g of defatted, monosaccharide-removed and oligosaccharide-removed sea buckthorn powder into 2L of deionized water, refluxing at 70 ℃ for 2h, filtering, concentrating the filtrate to one tenth of the original liquid, adding 95% ethanol to precipitate polysaccharide, storing at 0-5 ℃ for 48h, filtering, washing with absolute ethanol, and drying at-80 ℃ in vacuum.
Extracting the rhodiola root extract: adding 50g radix Rhodiolae into 1L50% ethanol water solution, refluxing at 85 deg.C for 2 hr, filtering, concentrating the filtrate, and vacuum drying the concentrated solution-80-100.
Extracting the gynostemma pentaphylla extract: weighing 50g of dried gynostemma pentaphylla, adding 1L of absolute ethyl alcohol, refluxing for 2h at 90 ℃, carrying out vacuum filtration, removing residues, concentrating the liquid into paste, and drying at-80 ℃ in vacuum to obtain the gynostemma pentaphylla extract.
Extracting the astragalus extract: weighing 50g of dried radix astragali, adding 1L of anhydrous ethanol, refluxing at 90 deg.C for 2h, vacuum filtering, discarding residue, concentrating the liquid to one tenth of the original liquid, and vacuum drying at-80 deg.C.
The preparation method comprises the following steps:
β -preparation of cyclodextrin-lycopene inclusion compound, which comprises the steps of dissolving β -cyclodextrin 30 parts in distilled water 100 parts at 80 ℃, dissolving lycopene 5 parts in ethanol, slowly mixing the two solutions for inclusion for 2-3h, standing overnight, washing with absolute ethanol, and drying to obtain β -cyclodextrin-lycopene inclusion compound.
β -cyclodextrin-tomato red pigment clathrate 25 parts, toning tomato red pigment 5 parts, seabuckthorn polysaccharide 6 parts and rhodiola rosea extract 2 parts, grinding for 1h to obtain a uniform mixture.
And (3) heating and melting 10 parts of beeswax, 10 parts of candelilla wax, 45 parts of olive oil, 15 parts of sweet almond oil and 0.2 part of vitamin E at 90 ℃, adding the mixture obtained in the step (2) and 0.2 part of rose essential oil, stirring uniformly, and cooling for later use.
And (4) pouring the mixture obtained in the step (3) into a mold, cooling and shaping the filled mold at 4 ℃ for 15min, and demolding to obtain the functional sustained-release lipstick.
Wherein the extraction of tea pigment, the extraction of sea buckthorn polysaccharide, the extraction of rhodiola rosea extract, the extraction of gynostemma pentaphylla extract and the extraction of astragalus extract are the same as in example 1.
Example 2
A functional slow-release lipstick is composed of, by weight, 15 parts of beeswax, 10 parts of candelilla wax, 45 parts of olive oil, 20 parts of sweet almond oil, 20 parts of β -cyclodextrin-tomato red pigment inclusion compound, 5 parts of color-mixing capsanthin, 0.2 part of vitamin E, 0.2 part of jasmine essential oil, 3 parts of tea pigment and 3 parts of sea buckthorn polysaccharide.
Wherein the extraction of tea pigment, the extraction of sea buckthorn polysaccharide, the extraction of rhodiola rosea extract, the extraction of gynostemma pentaphylla extract and the extraction of astragalus extract are the same as in example 1.
The preparation method comprises the following steps:
β -preparation of cyclodextrin-lycopene inclusion compound, which comprises dissolving β -cyclodextrin in 100 parts of distilled water at 80 ℃, dissolving lycopene 3 parts in ethanol, mixing the two solutions slowly for inclusion for 2-3h, standing overnight, washing with absolute ethanol, and drying to obtain β -cyclodextrin-lycopene inclusion compound;
β -cyclodextrin-tomato red pigment inclusion compound 20 parts, color-mixing capsanthin 5 parts, tea pigment 3 parts and sea buckthorn polysaccharide 3 parts, and grinding for 1 hour to obtain a uniform mixture;
heating and melting 15 parts of beeswax, 10 parts of candelilla wax, 45 parts of olive oil, 20 parts of sweet almond oil and 0.2 part of vitamin E at 85 ℃, adding the mixture obtained in the step (2) and 0.2 part of jasmine essential oil, stirring uniformly, and cooling for later use;
and (4) pouring the mixture obtained in the step (3) into a mold, cooling and shaping the filled mold at 2 ℃ for 20min, and demolding to obtain the functional sustained-release lipstick.
Wherein the extraction of tea pigment, the extraction of sea buckthorn polysaccharide, the extraction of rhodiola rosea extract, the extraction of gynostemma pentaphylla extract and the extraction of astragalus extract are the same as in example 1.
Example 3
A functional sustained-release lipstick is composed of, by weight, 15 parts of beeswax, 10 parts of candelilla wax, 40 parts of olive oil, 20 parts of sweet almond oil, 25 parts of β -cyclodextrin-sorghum red pigment inclusion compound, β parts of toning-carotene 3 parts, 0.5 part of vitamin E, 0.15 part of a mixture of rose essential oil and sweet osmanthus essential oil, 3 parts of tea pigment, 3 parts of sea buckthorn polysaccharide and 3 parts of rhodiola rosea extract.
Wherein the extraction of tea pigment, the extraction of sea buckthorn polysaccharide, the extraction of rhodiola rosea extract, the extraction of gynostemma pentaphylla extract and the extraction of astragalus extract are the same as in example 1.
The preparation method comprises the following steps:
β -preparation of a cyclodextrin-sorghum red pigment clathrate compound, namely dissolving β -cyclodextrin in 100 parts of distilled water at 80 ℃, dissolving 8 parts of sorghum red pigment in ethanol, slowly mixing the two solutions for inclusion for 2-3 hours, standing overnight, washing with absolute ethanol, and drying to obtain a β -cyclodextrin-sorghum red pigment clathrate compound;
β -cyclodextrin-sorghum red pigment inclusion compound 25 parts, toning β -carotene 3 parts, tea pigment 3 parts, seabuckthorn polysaccharide 3 parts and rhodiola rosea 3 parts are ground for 1 hour to obtain a uniform mixture;
heating and melting 15 parts of beeswax, 10 parts of candelilla wax, 40 parts of olive oil, 20 parts of sweet almond oil and 0.5 part of vitamin E at 90 ℃, adding the mixture obtained in the step (2) and 0.15 part of the mixture of rose essential oil and sweet osmanthus essential oil, stirring uniformly, and cooling for later use;
and (4) pouring the mixture obtained in the step (3) into a mold, cooling and shaping the filled mold at 2 ℃ for 15min, and demolding to obtain the functional slow-release lipstick.
Wherein the extraction of tea pigment, the extraction of sea buckthorn polysaccharide, the extraction of rhodiola rosea extract, the extraction of gynostemma pentaphylla extract and the extraction of astragalus extract are the same as in example 1.
Example 4
A functional sustained-release lipstick is composed of, by weight, 15 parts of beeswax, 15 parts of candelilla wax, 45 parts of olive oil, 20 parts of sweet almond oil, 30 parts of β -cyclodextrin-capsanthin inclusion compound, 3 parts of color-mixing corn yellow pigment, 0.7 part of vitamin E, 0.1 part of rose essential oil and rose flower oil, 2 parts of sea buckthorn polysaccharide, 3 parts of gynostemma pentaphylla extract and 2 parts of astragalus extract.
Wherein the extraction of tea pigment, the extraction of sea buckthorn polysaccharide, the extraction of rhodiola rosea extract, the extraction of gynostemma pentaphylla extract and the extraction of astragalus extract are the same as in example 1.
The preparation method comprises the following steps:
β -preparation of cyclodextrin-capsanthin clathrate compound, which comprises dissolving β -cyclodextrin 30 parts in distilled water 100 parts at 80 deg.C, dissolving capsanthin 6 parts in ethanol, mixing the two solutions slowly for clathration for 2-3h, standing overnight, washing with anhydrous ethanol, and drying to obtain β -cyclodextrin-capsanthin clathrate compound;
grinding β -cyclodextrin-capsanthin inclusion compound 30 parts, toning corn yellow pigment 3 parts, sea buckthorn polysaccharide 2 parts, gynostemma pentaphylla extract 3 parts and astragalus root extract 2 parts for 1 hour to obtain a uniform mixture;
heating and melting 15 parts of beeswax, 15 parts of candelilla wax, 45 parts of olive oil, 20 parts of sweet almond oil and 0.7 part of vitamin E at 90 ℃, adding the mixture obtained in the step (2), rose essential oil and 0.1 part of rose oil, uniformly stirring, and cooling for later use;
and (4) pouring the mixture obtained in the step (3) into a mold, cooling and shaping the filled mold at 3 ℃ for 20min, and demolding to obtain the functional sustained-release lipstick.
Example 5
A functional sustained-release lipstick is composed of, by weight, 15 parts of beeswax, 15 parts of candelilla wax, 50 parts of olive oil, 15 parts of sweet almond oil, 30 parts of β -cyclodextrin-sorghum red pigment-corn yellow pigment inclusion compound, 3 parts of color-mixing sorghum red pigment, 0.6 part of vitamin E, 0.3 part of rose essential oil, 4 parts of sea buckthorn polysaccharide, 2 parts of rhodiola rosea extract, 2 parts of gynostemma pentaphylla extract and 2 parts of astragalus extract.
Wherein the extraction of tea pigment, the extraction of sea buckthorn polysaccharide, the extraction of rhodiola rosea extract, the extraction of gynostemma pentaphylla extract and the extraction of astragalus extract are the same as in example 1.
The preparation method comprises the following steps:
β -preparation of a cyclodextrin-sorghum red pigment-corn yellow pigment clathrate compound, which is to dissolve β parts of cyclodextrin into 100 parts of distilled water at 80 ℃, dissolve 5 parts of sorghum red pigment and 2 parts of corn yellow pigment into ethanol, slowly mix the two solutions for inclusion for 2-3h, stand overnight, wash with absolute ethyl alcohol, and dry to obtain a β -cyclodextrin-sorghum red pigment-corn yellow pigment clathrate compound;
grinding β -cyclodextrin-sorghum red pigment-corn yellow pigment clathrate 30 parts, hippophae rhamnoides polysaccharide 4 parts, rhodiola rosea extract 2 parts, gynostemma pentaphylla extract 2 parts and astragalus root extract 2 parts for 1 hour to obtain a uniform mixture;
heating and melting 15 parts of beeswax, 15 parts of candelilla wax, 50 parts of olive oil, 15 parts of sweet almond oil and 0.6 part of vitamin E at 90 ℃, adding the mixture obtained in the step (2) and 0.3 part of rose essential oil, stirring uniformly, and cooling for later use;
and (4) pouring the mixture obtained in the step (3) into a mold, cooling and shaping the filled mold at 2 ℃ for 15min, and demolding to obtain the functional slow-release lipstick.
Compared with the lipstick which is not subjected to pigment inclusion and does not have a slow release function, the color retention time and the nourishing time of the lipstick can be effectively improved by using β -cyclodextrin to perform inclusion on the pigment, the lipstick is prevented from being dried and cracked in the storage process, and the quality guarantee period and the service life of the lipstick are prolonged.
It should be noted that the above-mentioned embodiments illustrate rather than limit the invention, and that those skilled in the art will be able to design alternative embodiments without departing from the scope of the appended claims. In the claims, any reference signs placed between parentheses shall not be construed as limiting the claim. The word "comprising" does not exclude the presence of elements or operations not listed in a claim.
Claims (9)
1. A functional sustained-release lipstick is characterized by comprising, by weight, 15-20 parts of beeswax, 5-15 parts of candelilla wax, 30-50 parts of olive oil, 15-25 parts of sweet almond oil, 5-30 parts of β -cyclodextrin-natural pigment inclusion compound, 0-10 parts of color-mixing natural pigment, 0.1-1 part of vitamin E, 0.1-0.5 part of natural spice, and 1-10 parts of a composition of one, any two, any three, any four or five of tea pigment, hippophae rhamnoides polysaccharide, rhodiola rosea extract, gynostemma pentaphylla extract and astragalus root extract.
2. The functionalized sustained-release lipstick according to claim 1, wherein said extraction of tea pigments: weighing tea leaves, adding deionized water, refluxing for 1h at 40-60 ℃, filtering to remove the tea leaves, adjusting the pH of the liquid to 6.5-7, condensing to one tenth of the original liquid, adjusting the pH to 4-6, adding absolute ethyl alcohol according to the volume ratio of 1:1, refluxing, adjusting the pH to 6.5-7, distilling to remove the solvent, and drying the remainder in an oven to obtain the tea.
3. The functionalized sustained-release lipstick according to claim 1, wherein: the extraction of the sea buckthorn polysaccharide is carried out by adding the sea buckthorn powder after degreasing and removing monosaccharide and oligosaccharide into deionized water, refluxing for 2-3h at 70-80 ℃, filtering, concentrating the filtrate to one tenth of the original liquid, adding 95% ethanol to precipitate the polysaccharide, storing for 48h at 0-5 ℃, filtering, washing with absolute ethanol, and drying at-80-100 ℃ in vacuum.
4. The functionalized sustained-release lipstick according to claim 1, wherein: extracting the rhodiola rosea extract: adding 50% ethanol water solution into radix Rhodiolae, refluxing at 80-90 deg.C for 2-3 hr, filtering, concentrating the filtrate, and vacuum drying at-80 deg.C to-100 deg.C to obtain the final product.
5. The functionalized sustained-release lipstick according to claim 1, wherein: extracting the gynostemma pentaphylla extract: weighing dried herba Gynostemmatis, adding anhydrous ethanol, refluxing at 90-95 deg.C for 2-3 hr, vacuum filtering, removing residue, concentrating the liquid to paste, and vacuum drying at-80 deg.C to-100 deg.C.
6. The functionalized sustained-release lipstick according to claim 1, wherein: extracting the astragalus extract: weighing dried radix astragali, adding anhydrous ethanol, refluxing at 90 deg.C for 2-3 hr, vacuum filtering, discarding residue, concentrating to one tenth of stock solution, and vacuum drying at-80 deg.C to-100 deg.C.
7. The functional slow-release lipstick according to claim 1, wherein the natural pigment and the color-adjusting natural pigment of the β -cyclodextrin-natural pigment inclusion compound are one or a mixture of any more of paprika red pigment, tomato red pigment, rose juice extract, safflower yellow pigment, mulberry red pigment, sorghum red pigment, peanut skin red pigment, β -carotene and corn yellow pigment.
8. The functional sustained-release lipstick according to claim 1, wherein the natural perfume is one or a mixture of any of rose essential oil, bergamot essential oil, mint essential oil, sweet osmanthus essential oil, rosemary essential oil, nardostachys chinensis essential oil, lemon essential oil, cinnamon essential oil, lavender essential oil, jasmine essential oil and rose oil.
9. A process for preparing a functionalized sustained release lipstick according to any one of claims 1 to 8, comprising the steps of:
β -preparation of cyclodextrin-natural pigment clathrate compound, which comprises dissolving β -cyclodextrin in distilled water at 80 deg.C, dissolving appropriate amount of natural pigment in ethanol or water, mixing the two solutions slowly for clathration for 2-3h, standing overnight, washing with anhydrous ethanol, and drying to obtain β -cyclodextrin-natural pigment clathrate compound;
grinding β -cyclodextrin-natural pigment inclusion compound, toning natural pigment, one, any two, any three or four of sea buckthorn polysaccharide, rhodiola rosea extract, gynostemma pentaphylla extract and astragalus extract for 1h to obtain a uniform mixture;
heating and melting beeswax, candelilla wax, olive oil, sweet almond oil and vitamin E at 80-90 ℃, adding the mixture obtained in the step (2) and natural perfume, stirring uniformly, and cooling for later use;
and (4) pouring the mixture obtained in the step (3) into a mold, cooling and shaping the filled mold at the temperature of 2-5 ℃ for 10-30min, and demolding to obtain the functionalized sustained-release lipstick.
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| CN113876654A (en) * | 2021-10-13 | 2022-01-04 | 齐鲁工业大学 | Edible wolfberry lipstick and preparation method thereof |
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