CN106420516A - Red onion extract containing skin-care product and application thereof - Google Patents
Red onion extract containing skin-care product and application thereof Download PDFInfo
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- CN106420516A CN106420516A CN201610513885.4A CN201610513885A CN106420516A CN 106420516 A CN106420516 A CN 106420516A CN 201610513885 A CN201610513885 A CN 201610513885A CN 106420516 A CN106420516 A CN 106420516A
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- skin care
- ethyl acetate
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
Abstract
The invention belongs to the technical field of daily cosmetics, and particularly discloses a red onion extract containing skin-care product and application thereof. The red onion extract containing skin-care product comprises the following components in percent by weight: 3-15% of a red onion ethyl acetate extract, 1-5% of a cactus extract, 1-3% of a centella extract and 78-95% of an auxiliary material. The red onion extract containing skin-care product provided by the invention has a remarkable skin-care effect, can effectively improve facial skin, resist bacteria, eliminate inflammation, remove free radicals, delay aging and promote skin microcirculation, has acne-removing and whitening efficacy, has a good moisturizing effect and is safe and non-irritant to skin.
Description
Technical field
The present invention relates to daily cosmetics technical field, in particular it relates to a kind of skin care item containing red Herba Alii fistulosi extract and
Purposes.
Background technology
Red allium, in herbaceous plant, is Iridaceae（Iridaceae）Red allium（Eleutherineamericana
Merr.et K.Heyne）Plant.The red green onion of Iridaceae is southwest especially the Dai nationality of Yunnan Province, the Yi nationality, distributed over Yunnan, Sichuan and Guizhou, De'ang nationality and local Han nationality
The herbal medicine commonly used Deng various nationalities, another name among the people is numerous, such as little red garlic, Herba Gynurae Divaricatae, ten thousand mas (Deang Praenomen), Lou Zicong, fearness ripple
Bright (Dai Nationality's language) etc..Red green onion originates in the ground such as the West Indies, America, and China is as far back as Yunnan introducing among the people cultigen.Its bulb
Oval, diameter about 2.5 centimetres, scale is plump, and aubergine is coated without film quality.Leaf width lanceolar or wide bar shaped, 4-5 bar longitudinal vein
Parallel and prominent, make leaf surface present obvious gauffer.
Red green onion has effect of clearing heat and cooling blood, promoting blood circulation to remove blood stasis, promoting urination and removing dampness, subdhing swelling and detoxicating, and clinic is mainly used in treating crown
Atherosclerotic heart disease, gynecological disease and the cancer of the stomach such as irregular menstruation, dysmenorrhoea, amenorrhoea and uterine bleeding.At present in red green onion
Isolate the main chemical compositions such as anthraquinone, naphthols, naphthoquinones and derivative thereof, have antibacterial, anti-oxidant, antitumor and AntiHIV1 RT activity is sick
The effects such as poison.Existing document reports the campylobacter to the mankind and bird for the red green onion ethanol extract obvious inhibitory effect, red
Green onion methanolic extract is several to staphylococcus aureus and Glorosprium musarum Cookeet Mass, lily anthrax bacteria, botrytis cinerea etc.
Phytopathogen has good inhibiting effect, three primary pharmacological activity composition eleutherols in red green onion, eleutherin and different red
Green onion A prime, also has significant antibacterial action.Red green onion crude extract has scavenging action to DPPH and OH, has people as a kind of sky
Right food additives are applied in pork, are the food antioxidants of a kind of potential new type natural anti-lipid peroxidation.Red
Green onion ethanol extract can be obviously enhanced SOD activity and GSH-Px activity in blood, moreover it is possible to effectively suppresses the activity of tyrosinase.
Eleutherin can suppress melanin to be formed, and eleutherol is applied to feature whitening and skin-protecting as the whitening factor by Japanese enterprises
It in the middle of product, it is seen that red Herba Alii fistulosi extract contains skin-whitening active functional component, is that a kind of vegetable active having very much market prospects becomes
Divide raw material.
With the raising of people's living standard, the foods and cosmetics of " natural " " organic " is increasingly favored, red green onion
There is integration of drinking and medicinal herbs, with red green onion for new resources food processing, functional food, plant feed additive, functional cosmetics,
The aspects such as botanical drug substance have good application prospect.But its exploitation have very big region limitation, therefore, with safety
Premised on property, exploitation natural plants is main composition, to improve the face skin of people, delays senility, and promotes that skin is micro-
Circulation, is very significant for the purpose of anti-inflammation.At present, there is no red green onion ethyl acetate extract part and be applied to cosmetics
Report.Content of the invention
The present invention is directed to the deficiencies in the prior art, provide a kind of skin care item containing red Herba Alii fistulosi extract, this skin care item can be effectively improved
Face skin, removes free radical, promotes skin microcirculation, has anti-inflammation, delay senility, the effect of skin whitening, moisturizing and anti-acne
Really.
For achieving the above object, the present invention gives to realize by below scheme：
A kind of skin care item containing red Herba Alii fistulosi extract, each component containing following percetage by weight：Red green onion ethyl acetate extract 3～
15%, Radix et Caulis Opuntiae Dillenii extract 1～5%, Gotu Kola P.E 1～3%, auxiliary material 78～95%.
In red green onion, three primary pharmacological activity compositions are eleutherol, eleutherin and different eleutherol, have significantly anti-
Bacterium effect.Eleutherin can suppress melanin to be formed, and eleutherol, as a kind of whitening factor, can improve skin function.Red
Green onion, possibly together with multiple naphthoquinones, naphthols, anthraquinone, glucoside compounds, can promote skin blood circulation, the work of suppression tyrosinase
Property, desalinate melanin；Inflammation part, anti-inflammatory disease, only distending pain can be rapidly permeated into；Free radical can be removed, strengthen skin elasticity
The activity of flesh；Radix et Caulis Opuntiae Dillenii extract has effect that is anti-oxidant and that delay senility；Gotu Kola P.E can compact epidermis with true
Skin coupling part, can make skin limber up, improve cutis laxa, make skin smooth flexible, promotes collagen in skin corium
Formed, make fibrin regenerate, make skin reach smooth effect of compacting.Also assist in impaired organization healing and consolidation flesh
Skin.
Preferably, the formulation of described skin care item be face cream, emulsion, facial mask, Essence, mildy wash, toner, toner/smoothing toner,
Firming lotion, nutrition toner, muffin, body dew or body lotion.
Being preferably face cream with skin care item prepared by red green onion ethyl acetate extract, face cream contains each of following percetage by weight
Component：Red green onion ethyl acetate extract 3～15%, Radix et Caulis Opuntiae Dillenii extract 1～5%, Gotu Kola P.E 1～3%, base oil 5～
15%, NMF 3～10%, emulsifying agent 3 ~ 10%, transdermal enhancer 0.5～1%, excipient 0.1～1%, antioxidant 0.1 ~ 1%, anticorrosion
Agent 0.1～0.6%, essence 0.01～0.05%, water surplus.
Preferably, face cream can also add the sun-screening agent of 0.1～0.5%.Described sun-screening agent is 4-methyl
Benzylidene camphor.
Being preferably emulsion with skin care item prepared by red green onion ethyl acetate extract, emulsion contains each of following percetage by weight
Component：Red green onion ethyl acetate extract 3～15%, Radix et Caulis Opuntiae Dillenii extract 1～5%, Gotu Kola P.E 1～3%, base oil 3～
10%, NMF 3～10%, emulsifying agent 5～10%, antioxidant 0.1～0.5%, keratolytic 0.1～0.3%, preservative 0.1
～0.6%, immunomodulator 1～3%, essence 0.01～0.05%, water surplus.
It is highly preferred that described emulsion contains each component of following percetage by weight：Red green onion ethyl acetate extract 3～15%,
Radix et Caulis Opuntiae Dillenii extract 1～5%, Gotu Kola P.E 1～3%, base oil 3～5%, NMF 5～8%, emulsifying agent 5～8%, antioxygen
Agent 0.1～0.5%, keratolytic 0.1%, preservative 0.5～0.6%, immunomodulator 1～2%, essence 0.01～0.05%,
Water surplus.
Preferably, emulsion can also add the transdermal enhancer of 0.1～1%.
It is highly preferred that the immunomodulator in emulsion is Sensor Chip CM 5.
Being preferably facial mask with skin care item prepared by red green onion ethyl acetate extract, facial mask contains each of following percetage by weight
Component：Red green onion ethyl acetate extract 3～15%, Radix et Caulis Opuntiae Dillenii extract 1～5%, Gotu Kola P.E 1～3%, NMF 3～
15%, emulsifying agent 1～5%, keratolytic 0.1～0.3%, antioxidant 0.1～0.5%, preservative 0.1～0.6%, essence
0.01～0.05%, water surplus.
It is highly preferred that described facial mask, each component containing following percetage by weight：Red green onion ethyl acetate extract 3～
15%, Radix et Caulis Opuntiae Dillenii extract 1～5%, Gotu Kola P.E 1～3%, NMF 5～10%, emulsifying agent 1～2%, keratolytic
0.1～0.2%, antioxidant 0.3～0.5%, preservative 0.1～0.3%, essence 0.01～0.05%, water surplus.
It is highly preferred that described facial mask can also add the transdermal enhancer of 0.1～0.2%.
It is highly preferred that described facial mask can also add the excipient of 0.2～0.5%.
Being preferably Essence with skin care item prepared by red green onion ethyl acetate extract, Essence contains following percetage by weight
Each component：Red green onion ethyl acetate extract 3～15%, Radix et Caulis Opuntiae Dillenii extract 1～5%, Gotu Kola P.E 1～3%, NMF 3
～15%, emulsifying agent 1～5%, preservative 0.1～0.6%, essence 0.01～0.05%, water surplus.
It is highly preferred that described Essence contains each component of following percetage by weight：Red green onion ethyl acetate extract 3～
15%, Radix et Caulis Opuntiae Dillenii extract 1～5%, Gotu Kola P.E 1～3%, NMF 5～13%, emulsifying agent 1～2%, and antioxidant 0.1 ~
1%, preservative 0.5%, essence 0.01～0.05%, water surplus.
It is highly preferred that described Essence can also add the transdermal enhancer of 0.1～1%；The base oil of 1～5%；0.1～
The keratolytic of 0.3%；The complexing agent of 0.01～0.05%.Described complexing agent is EDETATE SODIUM.
Most preferably, the emulsifying agent described in above face cream, emulsion, facial mask, Essence is selected from hydrolecithin, cetanol
With cetearyl glucoside, octanoic acid/certain herbaceous plants with big flowers acid glycerol three ester, stearine, cetearyl alcohol alcohol ether-21, the smooth tristearin of sorb
One or more in acid esters, laureth, glycerin monostearate or polyvinyl alcohol.
Most preferably, the NMF described in above face cream, emulsion, facial mask, Essence selected from phytosterin ester, 1,3-fourth
Glycol, polyethylene glycol-6, glycerine, hyaluronic acid, ceramide, triethanolamine, isopropyl myristate, trehalose, trimethyl are sweet
In propylhomoserin, propane diols, hexadecanol, dipropylene glycol, sucrose, isohexadecane, PCA sodium or dipotassium glycyrrhizinate one
Plant or multiple.
Most preferably, the base oil described in above face cream, emulsion, facial mask, Essence is selected from shea butter, dimethyl-silicon
One in oxygen alkane, cyclomethicone, dimethyl silicone polymer, ring five dimethyl silicone polymer, saualane or apricot kernel oil or
Multiple.
Most preferably, the antioxidant described in above face cream, emulsion, facial mask, Essence is Butylated Hydroxytoluene or tocopherol
Acetic acid esters.
Most preferably, the preservative described in above face cream, emulsion, facial mask, Essence is selected from methyl hydroxybenzoate, Nipasol
Or one or more in Phenoxyethanol.
Most preferably, the transdermal enhancer described in above face cream, emulsion, facial mask, Essence is selected from Cremophor RH40.
Most preferably, the keratolytic described in above emulsion, facial mask, Essence is allantoin.
It is highly preferred that one or more that the above excipient is xanthan gum or carbomer.
It is highly preferred that the preparation method of red green onion ethyl acetate extract described above is：
S1. taking and being dried red green onion block, add 60% ethanol, extract twice, extract 1h every time, extract merges, filters twice；
S2. the filtrate after filtering toward S1 adds activated carbon decolorizing, bleaching temperature 85 DEG C, filters to the inactive charcoal of solution clarification；
S3. filtrate in S2 is extracted with ethyl acetate, ethyl acetate extract liquid rotary evaporation recycling design；
S4. by recovered solvent concentrate drying in S3, red green onion ethyl acetate extract is obtained.
Compared with prior art, the invention have the advantages that：
The skin effect that the present invention provides is notable, can be effectively improved face skin, anti-inflammation, remove free radical, delay senility,
Promoting skin microcirculation, having effect of pox-eliminating whitening concurrently, moistening effect is good, non-stimulated to skin safe.
Brief description
Fig. 1 is that red green onion ethyl acetate extract part thing is to staphylococcus aureus ATCC25923 bacteriostatic activity.
Fig. 2 is that red green onion ethyl acetate extract part thing is to Escherichia coli ATCC25922 bacteriostatic activity.
Fig. 3 is that red green onion ethyl acetate extract part thing is to salmonella typhimurium ATCC 14028 bacteriostatic activity.
Fig. 4 is that red green onion ethyl acetate extract part thing is to epidermis staphylococcus aureus ATCC11827 bacteriostatic activity.
Fig. 5 is that red green onion ethyl acetate extract part thing is to propionibacterium acnes ATCC6919 bacteriostatic activity.
Fig. 6 is the Scavenging activity to DPPH for the red green onion ethyl acetate extract part thing.
Fig. 7 is the Scavenging activity to OH for the red green onion ethyl acetate extract part thing.
Detailed description of the invention
Below in conjunction with Figure of description and specific embodiment the present invention made and elaborating further, described embodiment
It is served only for explaining the present invention, be not intended to limit the scope of the present invention.Test method used in following embodiment is as without spy
Different explanation, is conventional method；The material that used, reagent etc., if no special instructions, for the reagent commercially obtaining
And material.
The preparation of embodiment 1 red green onion ethyl acetate extract part
Taking and being dried red green onion block 500g, add 60% ethanol 4L, extract twice, each 1h, extract filters, and merging filtrate adds
100g activated carbon decolorizing, bleaching temperature 85 DEG C, to filter to the inactive charcoal of solution clarification, filtrate is extracted by equal-volume ethyl acetate,
Ethyl acetate extract extract 55～65 DEG C of recycling design of Rotary Evaporators, concentrate drying i.e. obtains red green onion ethyl acetate extraction unit
Position.
The preparation of embodiment 2 red Herba Alii fistulosi extract face cream 1
A phase：Hydrolecithin 35g, shea butter 20g, phytosterin ester 8g, dimethyl siloxane 30g, cyclomethicone
20g, cetanol and cetearyl glucoside 10g, octanoic acid/certain herbaceous plants with big flowers acid glycerol three ester 40g, Butylated Hydroxytoluene 2g, PEG-40 hydrogenate castor
Sesame oil 5g, Nipasol 0.1g.
B phase：Carbomer 4g, 1,3-BDO 20g, polyethylene glycol-6 2g, xanthan gum 1g, glycerine 30g, hyaluronic acid
0.5g, methyl hydroxybenzoate 1g, balance of deionized water（In terms of 1000g）.
C phase：Ceramide 0.2g, triethanolamine 2g, red green onion ethyl acetate extract 35g, Radix et Caulis Opuntiae Dillenii extract 10g, long-pending
Snow grass extract 20g.
D phase：Phenoxyethanol 4g, essence 0.3g.
Preparation：By A heat phase to 85 DEG C so that it is be completely dissolved, by B heat phase to 85 DEG C, dispersed with stirring is uniform, by A, B
Mixing homogeneous stirring mutually, adding triethanolamine while hot, when temperature drops to less than 40 DEG C, addition C phase, D is equal and stirs 20 points
Clock and get final product.
The preparation of embodiment 3 red Herba Alii fistulosi extract face cream 2
A phase：Octanoic acid/certain herbaceous plants with big flowers acid glycerol three ester 20g, ethylhexyl palmitate 20g, isopropyl myristate 20g, stearine
10g, shea butter 20g, cetearyl alcohol alcohol ether-21 10g, cyclomethicone 20g, cetanol and cetearyl glucoside
10g, phytosterin ester 8g, 4 methyl benzylidene camphor 3g, Butylated Hydroxytoluene 5g, Nipasol 0.2g, Cremophor RH40
10 g.
B phase：Glycerine 30g, trehalose 10g, 1,3-BDO 20g, xanthan gum 1g, hyaluronic acid 0.5g, methyl hydroxybenzoate 1g,
Balance of deionized water（In terms of 1000g）.
C phase：Ceramide 0.2g, red green onion ethyl acetate extract 50g, Radix et Caulis Opuntiae Dillenii extract 20g, Gotu Kola P.E
15g.
D phase：Phenoxyethanol 4g, essence 0.5g.
Preparation：By A heat phase to 85 DEG C so that it is be completely dissolved, by B heat phase to 85 DEG C, dispersed with stirring is uniform, by A, B
Mixing homogeneous stirring mutually, when temperature drops to less than 40 DEG C, addition C phase, D is equal and stirs 20 minutes and get final product.
The preparation of embodiment 4 red Herba Alii fistulosi extract face cream 3
A phase：Shea butter 25g, octanoic acid/certain herbaceous plants with big flowers acid glycerol three ester 30g, sorb smooth stearate 20g, phytosterin ester 10g, diformazan
Radical siloxane 30g, cyclomethicone 10g, cetanol and cetearyl glucoside 20g, isopropyl palmitate 20g, fourth hydroxyl
Toluene 2g, Nipasol 0.1g.
B phase：Glycerine 60g, 1,3-BDO 20g, polyethylene glycol-63g, xanthan gum 1.5g, hyaluronic acid 0.5g, oxybenzene first
Ester 2g, balance of deionized water（In terms of 1000g）.
C phase：Ceramide 0.2g, red green onion ethyl acetate extract 45g, Radix et Caulis Opuntiae Dillenii extract 20g, Gotu Kola P.E
20g.
D phase：Phenoxyethanol 3g, essence 0.1g.
Preparation：By A heat phase to 85 DEG C so that it is be completely dissolved, by B heat phase to 85 DEG C, dispersed with stirring is uniform, by A, B
Mixing homogeneous stirring mutually, when temperature drops to less than 40 DEG C, addition C phase, D is equal and stirs 20 minutes and get final product.
The preparation of embodiment 5 red Herba Alii fistulosi extract facial treatment milk 1
A phase：Cetanol and cetearyl glucoside 25g, octanoic acid/certain herbaceous plants with big flowers acid glycerol three ester 30g, ring five dimethyl silicone polymer
20g, sorb smooth stearate 10g, saualane 20g, Sensor Chip CM 5 15g, cyclomethicone 15g, trimethylglycine
10g, laureth 2g, Cremophor RH40 8g, Butylated Hydroxytoluene 3g,.
B phase：1,3 butanediol 30g, propane diols 20g, hyaluronic acid 0.5g, allantoin 1g, methyl hydroxybenzoate 2g, balance of go
Ionized water（In terms of 1000g）.
C phase：Red green onion ethyl acetate extract 40g, Radix et Caulis Opuntiae Dillenii extract 20g, Gotu Kola P.E 20g.
D phase：Phenoxyethanol 4g, essence 0.2g.
Preparation：By A heat phase to 85 DEG C so that it is be completely dissolved, by B heat phase to 85 DEG C, dispersed with stirring is uniform, by A, B
Mixing homogeneous stirring mutually, when temperature drops to less than 40 DEG C, addition C phase, D is equal and stirs 20 minutes and get final product.
The preparation of embodiment 6 red Herba Alii fistulosi extract facial treatment milk 2
A phase：Hydrolecithin 20g, cetanol and cetearyl glucoside 10g, octanoic acid/certain herbaceous plants with big flowers acid glycerol three ester 35g, ring five gathers
Dimethyl siloxane 30g, glycerin monostearate 15g, Sensor Chip CM 5 20g, cyclomethicone 15g, the sweet ammonia of trimethyl
Acid 10g, laureth 2g, Nipasol 0.1g.
B phase：1,3 butanediol 30g, hexadecanol 15g, hyaluronic acid 1g, allantoin 1g, methyl hydroxybenzoate 0.5g, balance of go
Ionized water（In terms of 1000g）.
C phase：Red green onion ethyl acetate extract 50g, Radix et Caulis Opuntiae Dillenii extract 20g, Gotu Kola P.E 30g, tocopheryl acetate
Ester 5g.
D phase：Phenoxyethanol 5g, essence 0.3g.
Preparation：By A heat phase to 85 DEG C so that it is be completely dissolved, by B heat phase to 85 DEG C, dispersed with stirring is uniform, by A, B
Mixing homogeneous stirring mutually, when temperature drops to less than 40 DEG C, addition C phase, D is equal and stirs 20 minutes.
The preparation of embodiment 7 red Herba Alii fistulosi extract facial mask 1
A phase：1,3 butanediol 50g, propane diols 20g, polyvinyl alcohol 10g, xanthan gum 1.5g, hyaluronic acid 0.5g, allantoin 1g.
B phase：Tocopherol acetate 4g, dipropylene glycol 10g, red green onion ethyl acetate extract 30g, Radix et Caulis Opuntiae Dillenii extract 10g,
Gotu Kola P.E 15g, Phenoxyethanol 2g, methyl hydroxybenzoate 0.5g, essence 0.4g, remaining is deionized water（In terms of 1000g）.
Preparation：A phase heats 30min under conditions of 85 DEG C, then stirs under conditions of certain rotating speed, treats that temperature is cooled to
It when less than 40 DEG C, is sequentially added into B phase, until stirring, Essence being poured into equipped with in the facial mask bag of face paper, treats Essence
Being sufficiently submerged in face paper, sealing i.e. obtains the facial mask containing natural component.
The preparation of embodiment 8 red Herba Alii fistulosi extract facial mask 2
A phase：Glycerine 40g, propane diols 30g, Acritamer 940 5g, sucrose 2g, allantoin 1.5g.
B phase：Triethanolamine 2g, Cremophor RH40 2g, tocopherol acetate 4g, red green onion ethyl acetate extract
20g, Radix et Caulis Opuntiae Dillenii extract 15g, Gotu Kola P.E 10g, Phenoxyethanol 2g, methyl hydroxybenzoate 0.5g, essence 0.2g, remaining is for going
Ionized water（In terms of 1000g）.
Preparation：A phase heats 30min under conditions of 85 DEG C, then stirs under conditions of certain rotating speed, treats that temperature is cooled to
It when less than 40 DEG C, is sequentially added into B phase, until stirring, Essence being poured into equipped with in the facial mask bag of face paper, treats Essence
Being sufficiently submerged in face paper, sealing i.e. obtains the facial mask containing natural component.
The preparation of embodiment 9 red Herba Alii fistulosi extract Essence 1
A phase：Saualane 20g, apricot kernel oil 30g, isohexadecane 30g, cetearyl glucoside 20g, Nipasol 0.5g.
B phase：Glycerine 60g, dipropylene glycol 30g, allantoin 1g, EDETATE SODIUM 0.2g, methyl hydroxybenzoate 1g, remaining is deionization
Water（In terms of 1000g）.
C phase：PCA sodium 2g, red green onion ethyl acetate extract 40g, Radix et Caulis Opuntiae Dillenii extract 20g, centella carries
Take thing 10g, Butylated Hydroxytoluene 2g, Phenoxyethanol 4g, essence 0.3g.
Preparation：A, B phase heats 30min, while hot homogeneous 3min under conditions of 85 DEG C, then stirs under conditions of certain rotating speed
Mixing, when temperature is cooled to below 40 DEG C, being sequentially added into C phase, until stirring.
The preparation of embodiment 10 red Herba Alii fistulosi extract Essence 2
A phase：1,3 butanediol 20g, dipropylene glycol 30g, Acritamer 940 5g, hydroxyethyl cellulose 5g, dipotassium glycyrrhizinate 1g.
B phase：Triethanolamine 4g, tocopherol acetate 5g, red green onion ethyl acetate extract 60g, Radix et Caulis Opuntiae Dillenii extract 15g,
Gotu Kola P.E 10g, Phenoxyethanol 4g, methyl hydroxybenzoate 1g, essence 0.1g, remaining is deionized water（In terms of 1000g）.
Preparation：A phase heats 30min under conditions of 85 DEG C, then stirs under conditions of certain rotating speed, treats that temperature is cooled to
It when less than 40 DEG C, is sequentially added into B phase, until stirring.
Antibacterial and the Antioxidative Activity Determination of embodiment 11 red green onion ethyl acetate extract part thing
Antibacterial and the antioxidation activity of red green onion ethyl acetate extract part thing is measured, with staphylococcus aureus
ATCC25923, Escherichia coli ATCC25922, salmonella typhimurium ATCC14028, epidermis staphylococcus aureus
ATCC11827, propionibacterium acnes ATCC6919 are for for examination bacterium, measuring 6 mass concentrations of red green onion ethyl acetate extract part
To the bacteriostatic activity for examination bacterium, result shows, red green onion ethyl acetate extract part is golden yellow to staphylococcus aureus and epidermis
Staphylococcus inhibitory activity is the strongest, and when mass concentration is 50mg/mL, antibacterial circle diameter is respectively 27mm and 26mm, next to that husky
Door Salmonella, maximum antibacterial circle diameter is 16mm, the most weak (see Fig. 1～5) to Escherichia coli and propionibacterium acnes bacteriostasis.
The antioxidation of embodiment 12 red green onion ethyl acetate extract part thing
Red Herba Alii fistulosi extract ethyl acetate layer, n-butanol layer, chloroform layer, ethanol carry layer, 5 opposed polarity positions of petroleum ether layer all have
Antioxidation activity, the antioxidation at opposed polarity position is different, the selective effect to different types of free radical.Wherein with
Ethyl acetate phase and n-butanol activity mutually is relatively strong, and chloroform phase is taken second place, and the antioxidation activity of petroleum ether phase and ethanol extract is low.Always
Resistance to oxidation (TAC) is strong and weak carries a layer ＞ petroleum ether layer, ethyl acetate for ethyl acetate layer ＞ n-butanol layer ＞ chloroform layer ＞ ethanol
Layer extract in DPPH removing system, when mass concentration is 0.04～0.4 mg/mL, reach 60% to DPPH clearance rate～
88%, when mass concentration is 2～4 mg/mL, reach 73%～86% (see Fig. 6～7) to OH clearance rate.
Claims (10)
1. the skin care item containing red Herba Alii fistulosi extract, it is characterised in that each component containing following percetage by weight：Red green onion acetic acid
Ethyl ester extract 3～15%, Radix et Caulis Opuntiae Dillenii extract 1～5%, Gotu Kola P.E 1～3%, auxiliary material 78～95%.
2. skin care item according to claim 1, it is characterised in that the formulation of described skin care item be face cream, emulsion, facial mask,
Essence, mildy wash, toner, toner/smoothing toner, firming lotion, nutrition toner, muffin, body dew or body lotion.
3. skin care item according to claim 2, it is characterised in that described skin care item are face cream, face cream contains following weight
Each component of percentage：Red green onion ethyl acetate extract 3～15%, Radix et Caulis Opuntiae Dillenii extract 1～5%, Gotu Kola P.E 1～3%,
Base oil 5～15%, NMF 3～10%, emulsifying agent 3 ~ 15%, transdermal enhancer 0.5～1%, excipient 0.1～1%, antioxidant 0.1
~ 1%, preservative 0.1～0.6%, essence 0.01～0.05%, water surplus.
4. skin care item according to claim 2, it is characterised in that described skin care item are emulsion, emulsion contains following heavy
Each component of amount percentage：Red green onion ethyl acetate extract 3～15%, Radix et Caulis Opuntiae Dillenii extract 1～5%, Gotu Kola P.E 1～
3%, base oil 3～10%, NMF 3～10%, emulsifying agent 1～10%, antioxidant 0.1～0.5%, keratolytic 0.1～
0.3%, preservative 0.1～0.6%, immunomodulator 1～3%, essence 0.01～0.05%, water surplus.
5. skin care item according to claim 2, it is characterised in that described skin care item are facial mask, facial mask contains following heavy
Each component of amount percentage：Red green onion ethyl acetate extract 3～15%, Radix et Caulis Opuntiae Dillenii extract 1～5%, Gotu Kola P.E 1～
3%, NMF 3～15%, emulsifying agent 1～5%, keratolytic 0.1～0.3%, antioxidant 0.1～0.5%, preservative 0.1～
0.6%, essence 0.01～0.05%, water surplus.
6. skin care item according to claim 2, it is characterised in that described skin care item are Essence, Essence contain with
Each component of lower percetage by weight：Red green onion ethyl acetate extract 3～15%, Radix et Caulis Opuntiae Dillenii extract 1～5%, Gotu Kola P.E 1
～3%, NMF 3～15%, emulsifying agent 1～5%, antioxidant 0.1 ~ 1%, preservative 0.1～0.6%, essence 0.01～0.05%,
Water surplus.
7. the skin care item according to any one of claim 3 to 6, it is characterised in that described red green onion ethyl acetate extract
Preparation method is as follows：
S1. taking and being dried red green onion block, add 60% ethanol, extract twice, extract 1h every time, extract merges, filters twice；
S2. the filtrate after filtering toward S1 adds activated carbon decolorizing, bleaching temperature 85 DEG C, filters to the inactive charcoal of solution clarification；
S3. filtrate in S2 is extracted with ethyl acetate, ethyl acetate extract liquid rotary evaporation recycling design；
S4. by recovered solvent concentrate drying in S3, red green onion ethyl acetate extract is obtained.
8. the skin care item according to any one of claim 3 to 6, it is characterised in that described emulsifying agent selected from hydrolecithin,
Cetanol and cetearyl glucoside, octanoic acid/certain herbaceous plants with big flowers acid glycerol three ester, stearine, cetearyl alcohol alcohol ether-21, sorb
One or more in smooth stearate, laureth, glycerin monostearate or polyvinyl alcohol.
9. the skin care item according to any one of claim 3 to 6, it is characterised in that described NMF selected from phytosterin ester,
1,3-BDO, polyethylene glycol-6, glycerine, hyaluronic acid, ceramide, triethanolamine, isopropyl myristate, trehalose, three
Methylglycine, propane diols, hexadecanol, dipropylene glycol, sucrose, isohexadecane, PCA sodium or dipotassium glycyrrhizinate
In one or more.
10. the skin care item according to any one of claim 3 to 6, it is characterised in that described base oil selected from shea butter,
Dimethyl siloxane, cyclomethicone, dimethyl silicone polymer, ring five dimethyl silicone polymer, isopropyl palmitate, palm
One or more in acid Octyl Nitrite, saualane or apricot kernel oil.
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| CN201610513885.4A CN106420516A (en) | 2016-06-30 | 2016-06-30 | Red onion extract containing skin-care product and application thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610513885.4A CN106420516A (en) | 2016-06-30 | 2016-06-30 | Red onion extract containing skin-care product and application thereof |
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| CN106420516A true CN106420516A (en) | 2017-02-22 |
Family
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610513885.4A Pending CN106420516A (en) | 2016-06-30 | 2016-06-30 | Red onion extract containing skin-care product and application thereof |
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| CN109157489A (en) * | 2018-09-18 | 2019-01-08 | 梅淑婕 | A kind of preparation method of skin care compositions and facial mask with antibacterial functions |
| CN109718122A (en) * | 2019-03-15 | 2019-05-07 | 派能生物科技（深圳）有限公司 | A kind of anti-oxidant lightening compositions of skin and preparation method thereof |
| WO2019236935A1 (en) * | 2018-06-08 | 2019-12-12 | The Procter & Gamble Company | Topical skincare compositions comprising centella asiatica selected triterpenes |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107625661A (en) * | 2017-08-16 | 2018-01-26 | 佛山实瑞先导材料研究院（普通合伙） | A kind of anti-aging additive and its application |
| CN107998024A (en) * | 2017-12-20 | 2018-05-08 | 上海东晟源日化有限公司 | A kind of elite containing cactus has effects that the skincare product that depth is maintained |
| WO2019236935A1 (en) * | 2018-06-08 | 2019-12-12 | The Procter & Gamble Company | Topical skincare compositions comprising centella asiatica selected triterpenes |
| US10980851B2 (en) | 2018-06-08 | 2021-04-20 | The Procter & Gamble Company | Topical skincare compositions comprising Centella asiatica selected triterpenes |
| CN109157489A (en) * | 2018-09-18 | 2019-01-08 | 梅淑婕 | A kind of preparation method of skin care compositions and facial mask with antibacterial functions |
| CN109718122A (en) * | 2019-03-15 | 2019-05-07 | 派能生物科技（深圳）有限公司 | A kind of anti-oxidant lightening compositions of skin and preparation method thereof |
| CN109718122B (en) * | 2019-03-15 | 2021-10-22 | 派能生物科技（深圳）有限公司 | Skin antioxidant whitening composition and preparation method thereof |
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