CN104958196B - The application of golden camellia tea extract, whitening and skin-protecting composition and preparation method thereof - Google Patents

The application of golden camellia tea extract, whitening and skin-protecting composition and preparation method thereof Download PDF

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CN104958196B
CN104958196B CN201510266489.1A CN201510266489A CN104958196B CN 104958196 B CN104958196 B CN 104958196B CN 201510266489 A CN201510266489 A CN 201510266489A CN 104958196 B CN104958196 B CN 104958196B
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skin
whitening
golden camellia
oil
camellia tea
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CN104958196A (en
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李晓宇
罗新星
徐永平
贺栋业
张萍
王丽丽
李淑英
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Dalian University of Technology
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Dalian University of Technology
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Abstract

The invention discloses application of the golden camellia tea extract in the cosmetics or health food with white-skinned face function, and whitening and skin-protecting composition is provided, mainly it is made up of disodium ethylene diamine tetraacetate, Sodium Hyaluronate, glycerine, pyrrolidone sodium carboxylate, Phenoxyethanol, methyl hydroxybenzoate, golden camellia tea water extract, L-vitamin C, SIMMONDSIA CHINENSIS SEED OIL, vitamin E, emulsifying agent, essential oil.The present invention has the function that skin whitening by suppressing tyrosinase activity, suppressing B16 cell, reduction environmental stimuli, anti-oxidant, antibacterial, six approach of moisturizing.Compared with existing product the present invention have the advantages that it is safer, gentle it is non-stimulated, without rebounding.

Description

The application of golden camellia tea extract, whitening and skin-protecting composition and preparation method thereof
Technical field
The present invention's is related to daily living article technical field, the more particularly to application of golden camellia tea extract, whitening shield Skin composition and preparation method thereof.
Background technology
Camellia nitidissima (Camellia nitidissima Chi) is described as " tea race queen " " plant kingdom giant panda " " " Dongfang " magic Tea " etc., belong to Theaceae Camellia Camellia Section Chrysantha, be high about 2~5 meters of evergreen shrubs or dungarunga.And China is great certainly Right resources advantage, because having known that Camellia Section Chrysantha has 34 kinds and 5 mutation in global range, NATURAL DISTRIBUTION removes North Vietnam 4 kinds and Yunnan Province of China, Guizhou, Sichuan respectively produce a kind it is outer, remaining 27 kinds originate in China's south Guangxi and the west and south with 5 mutation.
Camellia nitidissima is Zhuang nationality in Guangxi traditional medication among the people,《Guangxi Chinese medicine standard》《Guangxi ethnic drug short course》《Extensively Western medicinal garden medicinal plant register》《Modern Compendium of Materia Medica》《Medicinal Plants of Guangxi register》In it is on the books.Golden camellia tea Traditional medical value is clearing heat and detoxicating, inducing diuresis to remove edema, sphagitis, ephritis, dysentery, oedema, urinary tract infections, treats hypertension, in advance Preventing tumor (be decocted in water for oral dose or work as tea-drinking), flower are used to have blood in stool, irregular menstruation.The modern study of Camellia nitidissima medicinal material started from for 20th century 60 years In generation, it is related to the pharmacognosy identification of Camellia nitidissima medicinal material, the artificial culture of medicinal material, chemical composition, pharmacological activity etc..It has been investigated that The chemical composition of Camellia nitidissima mainly has flavones, Tea Polyphenols, tea polysaccharide, saponin(e, trace element, amino acid and fiber fat etc., existing Show for pharmaceutical research, Camellia nitidissima has significant antibacterial, antioxidation activity, anticancer, reducing blood lipid and hypoglycemic and other effects.
Ursin, VC derivatives, kojic acid and licorice licoflavone are more normal in current skin-lightening cosmetic both at home and abroad The whitening additive used.But ursin, kojic acid, radix glycyrrhizae are respectively provided with CDCC, it is thin can also to increase ovary for wherein kojic acid Born of the same parents' chromosome interchange and the probability of chromosome aberration, and these whitening active ingredients for being formulated use are synthesis chemicals, Action effect is limited, easily bounce-back.In recent years, as the aging of population, environmental pollution, global warning, increasing people go out Existing skin pigmentation disorder disease.Find safer Novel external skin-whitening and speckle eliminating agent be current cosmetics study hotspot it One.Modern study, which is proved golden camellia tea, has the general green tea of toxicity ratio of significantly antibacterial and antioxidation and Camellia nitidissima more It is low, and golden camellia tea can be used as safe whitening and skin-protecting raw material, have no document report.
The content of the invention
The purpose of the present invention aim to provide it is a kind of there is whitening function and safer plant source raw material, be cosmetics and guarantor The whitening direction of strong conduct industry provides new raw material, enriches market, while increases the market profit of the peculiar resource in this China of Camellia nitidissima With.
To achieve the above object, the technical solution adopted by the present invention is as follows:
The present invention provides application of the golden camellia tea extract in the cosmetics or health food with white-skinned face function.
Preferably, the golden camellia tea extract is the water extract of golden camellia tea.
It is further preferred that the water extract of the golden camellia tea is to mix golden camellia tea with water, through boiling extraction, mistake Filter, freeze-drying obtain.It is freeze-dried obtained powder and is easy to quantitative, storage;Freeze-drying can prevent active component by broken Bad, its main function is:Antibacterial, removing free radical, suppress tyrosinase activity, suppress B16 cell.
It is highly preferred that the boiling extraction is carried out three times, first time, second, the golden camellia tea and water of third time extraction Weight ratio respectively 1:20、1:14、1:14.
The present invention also provides whitening and skin-protecting composition, containing above-mentioned golden camellia tea extract, by weight percentage, by Following raw material composition:
Golden camellia tea has the function that anti-oxidant, suppression tyrosinase activity, suppresses B16 cell, contains in Camellia nitidissima Abundant Tea Polyphenols, Tea Polyphenols have the function that to absorb ultraviolet, radiation proof etc..
L-vitamin C is functional components, has anti-oxidant white-skinned face function.
Vitamin E is functional components, has whitening antioxidation effect.
The effect of essential oil is to diminish inflammation, skin of releiving.
The effect of glycerine, pyrrolidone sodium carboxylate is efficient moisture-retention, is moistened, and strengthens the dispersiveness of active component with promoting Osmotic absorption.
Sodium Hyaluronate is efficient physiology NMF, strengthens skin moisture-retaining capacity.
Phenoxyethanol is safe preservative.
Methyl hydroxybenzoate is antioxidant.
Disodium ethylene diamine tetraacetate is ion chelating agent, protection activity composition, promotes product effect.
Emulsifying agent can emulsify oil phase at normal temperatures, obtain the emulsion of fine and smooth temperature.
It is oily based on SIMMONDSIA CHINENSIS SEED OIL;Can unimpeded pore, adjust the fat secretion of oiliness or Combination skin, and improve hair Scorching skin, eczema, chronic eczema, pimples etc..There is the effect of suitable with releiving to allergic skin, wrinkled for Dry Hair and dryness Line skin can make its gloss that rejuvenates, and be the base oil that various skin properties can use.
Preferably, described whitening and skin-protecting composition, by weight percentage, it is made up of following raw material:
Preferably, by weight percentage, it is made up of following raw material:
Preferably, by weight percentage, it is made up of following raw material:
Preferably, the essential oil is at least one of tea tree ethereal oil, osmanthus essential oil, jasmine essential oil.
Further preferably, essential oil is 1 by weight part ratio:1:1 tea tree ethereal oil, osmanthus essential oil and jasmine essential oil composition.
The present invention also provides the preparation method of the whitening and skin-protecting composition, comprises the following steps:
(1) prepared by aqueous phase:By deionized water, disodium ethylene diamine tetraacetate, Sodium Hyaluronate, it is well mixed;Add sweet Oil, pyrrolidone sodium carboxylate, it is well mixed;Phenoxyethanol, methyl hydroxybenzoate are added, is well mixed;Golden camellia tea is added to carry Take thing, left-handed Vc to be well mixed, obtain aqueous phase liquid;
(2) prepared by oil phase:SIMMONDSIA CHINENSIS SEED OIL is taken, adds vitamin E, is well mixed, adds emulsifying agent, is well mixed, adds Enter essential oil, be well mixed, obtain oil phase feed liquid;
(3) aqueous phase oil phase mixes:The obtained aqueous phase liquid of step (1) is slowly added into the oil phase feed liquid of step (2) preparation In, it is evenly stirred until that emulsion is moist.
The primary efficacy of the golden flower tea extractions of the offer of the present invention is skin whitening, and main lightening mechanism has:
1. golden camellia tea extract, VC, B16 cell can be suppressed.Pass through intracellular melanin assay (measure side Method referring to:Mesh, Yan Zemin, Zhu Shaojuan, Fu Tingzhi are opened, whitening function research [J] balsamics of several Chinese medicines of section star are refined Cosmetic .2009, (1) 33-36), it is thin to melanin B16 when the concentration for finding golden camellia tea extract is 10,100,500 μ g/ml The B16 cell inhibiting rate of born of the same parents is respectively (2.48 ± 0.710) %, (11.78 ± 0.968) %, (41.86 ± 2.326) %;
The obscure mainly melanin deposition of skin, so the first step of whitening is to suppress the synthesis of melanin in cell;
2. golden camellia tea extract, VC, VE, tyrosinase activity can be suppressed.Pass through the life of tyrosinase activity in cell Change zymetology method (assay method referring to:Song Qiru, Huang Lei, the biochemical-Enzymic method measure of tyrosinase activity in golden tin roc cells [J] daily chemical industries .2001,31 (4):When the concentration for 52-53) measuring golden camellia tea extract is 10,100,500 μ g/ml Relative to blank control group to the inhibiting rate of total tyrosinase activity to be respectively (2.96 ± 8.060) %, (16.50 ± 5.214) %, (46.60 ± 11.028) %;
Tyrosinase is the important enzyme related to synthesis of melanin, when suppressing tyrosinase activity, controls synthesis of melanin Reaction speed, reach the effect of whitening;
3. golden camellia tea extract, VC, VE, there is anti-oxidation efficacy.By FRAP methods (assay method referring to:Gong Jin inflammation Research [D] .2010. of the skin-protecting function factor in bamboo exocuticle), measuring the TAC of golden camellia tea extract is The 20% of 99.5%VC;By DPPH methods (assay method referring to:The research of the skin-protecting function factor in Gong Jin inflammation bamboo exocuticles [D] .2010.) to measure golden camellia tea extract be the 25% of 99.5%VC to DPPH Scavenging activity;
Control the source of B16 cell:The synthesis of melanin is in fact an oxidizing process, can after removing free radical To slow down the reaction speed of synthesis of melanin;
4. containing abundant natural active matter such as Tea Polyphenols, polysaccharide, flavones etc. in Camellia nitidissima, and Tea Polyphenols has absorption The effect of ultraviolet, radiation proof etc..
Influenceed by living environment and natural environment, the environmental stimuli that people touch such as ultraviolet, radiation include Mobile phone, computer etc. are more and more, seriously endanger the skin of people, and contain several physiological active substances in golden flower tea extractions Such as golden flower Tea Polyphenols, polysaccharide, ultraviolet, radiation-screening can be absorbed, a natural cover for defense is provided for skin;
5. golden camellia tea extract, tea tree ethereal oil have anti-inflammatory efficacy,《Modern Compendium of Materia Medica》Described in golden camellia tea soup With antiinflammatory action.
Often after skin suffers from inflammation, there is pigment deposition.Anti-inflammatory can reinforce skin defence line, skin is not susceptible to suffer from inflammation Or there is fast quick-recovery after inflammation, it will not grow in intensity, cause large area pigment deposition;
6. glycerine, pyrrolidone sodium carboxylate, Sodium Hyaluronate have moisturizing effect
Moisture abundance can strengthen the metabolism of cell in Skin Cell, reduce the deposition of melanin;
Compared with existing product, the present invention provides plant source whitening active ingredients golden camellia tea extract, lightening compositions Also containing chemical synthesis active components such as VE, VC, product effectively can be used no dependence for a long time safely, keep its quick again The feature to take effect, while also adapt to the relatively small number of present situation of plant resources.
Compared with prior art, emulsion process need to only be carried out at normal temperatures and pressures, and production operation is simple, device simple, right The holding of active component physiologically active is also significant.
Brief description of the drawings
The width of accompanying drawing 1 of the present invention, Fig. 1 are preparation technology flow chart of the present invention.
Embodiment
Following non-limiting examples can make one of ordinary skill in the art be more fully understood the present invention, but not with Any mode limits the present invention.
Emulsifying agent is from the import 305 for originating in Guangzhou Yu Tai Chemical Industry Science Co., Ltd.
Aqueous Phase Raw Material:Deionized water, disodium ethylene diamine tetraacetate, Sodium Hyaluronate, glycerine, pyrrolidone sodium carboxylate, benzene Oxyethanol, methyl hydroxybenzoate, golden camellia tea water extract, L-vitamin C.
Oil phase raw material:SIMMONDSIA CHINENSIS SEED OIL, vitamin E, emulsifying agent, essential oil.
Embodiment 1
Whitening and skin-protecting composition, by weight percentage, it is made up of following raw material:
1 preparation technology flow of this implementation case is as shown in figure 1, concrete operation step is as follows:
(1) golden camellia tea is extracted:The water extract of the golden camellia tea is by golden camellia tea (preferably Camellia nitidissima dried leaf powder End) mix with water, through boiling extraction three times, filtering, freeze-drying obtain, for the first time, second, the Camellia nitidissima extracted for the third time The weight ratio respectively 1 of leaf and water:20、1:14、1:14.
(2) prepared by aqueous phase:By deionized water, disodium ethylene diamine tetraacetate, Sodium Hyaluronate, it is well mixed;Add sweet Oil, pyrrolidone sodium carboxylate, it is well mixed;Phenoxyethanol, methyl hydroxybenzoate are added, is well mixed;Golden camellia tea is added to carry Take thing, L-vitamin C to be well mixed, obtain aqueous phase liquid;
(3) prepared by oil phase:SIMMONDSIA CHINENSIS SEED OIL is taken, adds vitamin E, is well mixed, adds emulsifying agent, is well mixed, adds Enter essential oil, be well mixed, obtain oil phase feed liquid;
(4) aqueous phase oil phase mixes:The obtained aqueous phase liquid of step (1) is slowly added into the oil phase feed liquid of step (2) preparation In, stir while adding, until the smooth exquisiteness of emulsion.
Embodiment 2
Whitening and skin-protecting composition, by weight percentage, it is made up of following raw material:
Preparation technology is the same as embodiment 1.
Embodiment 3
Whitening and skin-protecting composition, by weight percentage, it is made up of following raw material:
Preparation technology is the same as embodiment 1.

Claims (7)

1. whitening and skin-protecting composition, it is characterised in that containing golden camellia tea extract, by weight percentage, by following raw material Composition:
The golden camellia tea extract is the water extract of golden camellia tea, is to mix golden camellia tea with water, through boiling extraction, mistake Filter, freeze-drying obtain.
2. whitening and skin-protecting composition according to claim 1, it is characterised in that the boiling extraction is carried out three times, and first The weight ratio respectively 1 of golden camellia tea and water secondary, extract for the second time, for the third time:20、1:14、1:14.
3. whitening and skin-protecting composition according to claim 1, it is characterised in that by weight percentage, by following raw material Composition:
4. whitening and skin-protecting composition according to claim 1, it is characterised in that by weight percentage, by following raw material group Into:
5. whitening and skin-protecting composition according to claim 1, it is characterised in that by weight percentage, by following raw material group Into:
6. according to the whitening and skin-protecting composition described in claim 1-5 any one, it is characterised in that the essential oil is tea tree essence At least one of oil, osmanthus essential oil, jasmine essential oil.
7. the preparation method of whitening and skin-protecting composition, comprises the following steps described in claim 1-6 any one:
(1) prepared by aqueous phase:By deionized water, disodium ethylene diamine tetraacetate, Sodium Hyaluronate, it is well mixed;Add glycerine, pyrrole Pyrrolidone carboxylic acid's sodium, it is well mixed;Phenoxyethanol, methyl hydroxybenzoate are added, is well mixed;Add golden camellia tea extract, L-vitamin C is well mixed, and obtains aqueous phase liquid;
(2) prepared by oil phase:SIMMONDSIA CHINENSIS SEED OIL is taken, adds vitamin E, is well mixed, adds emulsifying agent, is well mixed, adds essence Oil, it is well mixed, obtains oil phase feed liquid;
(3) aqueous phase oil phase mixes:Step (1) is made into aqueous phase liquid to be slowly added into the oil phase feed liquid of step (2) preparation, stirred Mix moist to emulsion.
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CN105997716A (en) * 2016-07-08 2016-10-12 柯湘 Golden camellia bath salt and preparation method thereof
CN107213057A (en) * 2017-06-06 2017-09-29 安徽吉乃尔电器科技有限公司 A kind of preparation method of Camellia nitidissima whitening emulsion
CN110051571A (en) * 2018-09-18 2019-07-26 广州青岚生物科技有限公司 A kind of pharmaceutical composition of sun-proof reparation

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