CN103505398B - Forsythia leaf facial mask - Google Patents
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- CN103505398B CN103505398B CN201310483650.1A CN201310483650A CN103505398B CN 103505398 B CN103505398 B CN 103505398B CN 201310483650 A CN201310483650 A CN 201310483650A CN 103505398 B CN103505398 B CN 103505398B
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Abstract
The invention belongs to the technical field of cosmetics, and particularly relates to a facial mask comprising traditional Chinese medicinal ingredients. The technical problem to be solved is to provide a forsythia leaf extract and traditional Chinese medicinal ingredients compatible facial mask which has the effects of resisting against bacteria, diminishing inflammation, expelling toxin, rejuvenating the face, and resisting against oxidation, and can treat facial skin diseases such as acne. The facial mask in the technical scheme comprises functional ingredients including forsythia leaf extract, traditional Chinese medicines mixed extract of endive, umbellate rock jasmine, radix scutellariae, Chinese mugwort leaf, madder and radix astragali, and water-soluble pearl powder. The forsythia leaf extract accounts for 1-30% of the total weight of the facial musk; the traditional Chinese medicines mixed extract accounts for 1-15% of the total weight of the facial mask; the water-soluble pearl powder accounts for 1-5% of the total weight of the facial mask. The forsythia leaf facial mask can be widely applied to the technical field of the mask.
Description
Technical field
The invention belongs to cosmetic technical field, be specifically related to a kind of facial film containing Chinese medicine ingredients and preparation method thereof.
Background technology
Fructus Forsythiae is one of Chinese tradition Chinese medicine, has another name called Hemerocallis citrina Baroni bar, Fructus Forsythiae, green grass or young crops stick up, falls to sticking up, Huang Qidan etc.Pharmacopoeia of the People's Republic of China version in 2010 Fructus Forsythiae recorded be Oleaceae (
oleaceae) Forsythia (
forsythia) plant Fructus Forsythiae (
forsythia suspensa(Thunb.) Vahl) dry fruit.In recent ten years, people have carried out again new exploratory development to Folium Forsythiae.
Folium Forsythiae is containing 17 seed amino acids of needed by human, the glycoside such as phillyrin, Fructus Forsythiae ester glycoside, the Flavonoid substances such as rutin, and be rich in the trace element such as selenium, calcium, potassium, zinc, ferrum, not only there is good health-care effect and there is certain medical value, thus there is higher value of exploiting and utilizing.Forsythia suspense leaves tea of drinking among the people is with a long history, also has the pharmacological action of many scholar's research Folium Forsythiae extracts in recent years.Hou Gaixia etc. are by measuring myocardium antioxidase, lipid peroxidation product discussion Forsythia suspense leaves tea extract to the protective effect of hyperlipemia in mice heart; find that this extract can delay hyperlipemia in mice body weight rate of increase; reduce the abnormal rising of its cardiac index etc., to its heart, there is certain protective role.Yang Jianxiong etc. adopt Forsythia suspense leaves tea or Folium Forsythiae extract to carry out every research, and result shows that it has antibacterial, hepatoprotective, blood fat reducing, antioxidation, defying age and regulates the effects such as non-specific immunity.
Existing Folium Forsythiae is all do tea-drinking with Ye Weizhu, and we find by studying and consult documents and materials, composition contained by Folium Forsythiae is based on phillyrin and Fructus Forsythiae ester glycoside, it exceeds 30% than fruit content, these content have very large Development volue, have good curative effect and effect to antiinflammatory pathogenic fire purging, the breeding of suppression mushroom, antioxidation.
Acne is commonly called as comedo, is chronic inflammation hair follicle sebum gland disease, is one of modal disease of department of dermatologry.Pathogenesis of acne is main and sex hormone level, sebaceous gland are secreted in a large number, propionibacterium acnes is bred, and the factors such as the dyskeratosis of pilosebaceous duct and inflammation are correlated with.During adolescence, the hormone meeting stimulating hair growth in body, promote smegma more heavy wool fat, therefore hair and sebaceous gland pile up many materials, make oils and fats and bacterial adhesion, cause the reaction of red swelling of the skin.Have a kind of propionibacterium acnes in the hair follicle blocked, support one's family with sebum, normal presence is in skin, and when sebum blocks hair follicle, pathogenic bacteria Fast-propagation, produces harmful chemical substance, makes hair follicle and inflammation around thereof.Be mainly in hebetic masculinity and femininity, male is slightly more than women, but women's morbidity is early than male.Have the teenager of 80-90% to suffer from acne, few patients also can extend to more than 30 years old.Acne causes no small impact to youngster quality of life, causes certain stress and financial burden, especially sends out the acne in face, their self-confidence can be caused to decline, lack self-esteem, awkward etc.Acne can be divided into acne, pimple, pustule, cyst tuberosity etc.
Summary of the invention
The present invention, in order to overcome the deficiencies in the prior art, provides one to have inhibiting bacteria and diminishing inflammation, eliminating toxin and beautifying the skin, antioxidation, can be used for Folium Forsythiae extract and the drug matching facial film of the facial skin diseases such as Acne treatment.
In order to solve the problems of the technologies described above, the technical solution used in the present invention is: a kind of forsythia leaf facial mask, by functional components, deionized water, xanthan gum and flexibilizer composition, described functional components is by Folium Forsythiae extract, form containing the Chinese medicine mixed extract of Herba Sonchi Arvensis, Herba Androsaces umbellatae, Radix Scutellariae, Folium Artemisiae Argyi, Radix Rubiae and the Radix Astragali and water soluble Margarita ultrafine powder, and the 1-15% that Folium Forsythiae extract accounts for the 1-30% of facial film gross weight, Chinese medicine mixed extract accounts for facial film gross weight, water soluble Margarita ultrafine powder account for the 1-5% of facial film gross weight;
The preparation method of described Folium Forsythiae extract is:
Get ripe Folium Forsythiae after cleaning is dried, be ground into coarse powder, cross 40 mesh sieves; Add the ethanol of concentration of volume percent 50% wherein, mix thoroughly, stewing 10-16 hour, loads percolate pot, add the ethanol of the concentration of volume percent 60% of 1-6 times of volume, leave standstill percolation after 20-24 hour, flow 40-60 drips per minute, percolation 40-50 hour, filters and obtains filtrate and filtering residue; At 60 DEG C, reclaim ethanol, the concentrated solution A being condensed into relative density 1.1-1.3 is for subsequent use; Be the ethanol of 90% by the concentration of volume percent adding 1-6 times of volume in described filtering residue, reflux 5-10 hour at 80 DEG C, gets supernatant and carry out secondary filter, at 60 DEG C, reclaim ethanol, and the concentrated solution B being condensed into relative density 1.1-1.3 is for subsequent use; Merged by concentrated solution A and concentrated solution B, removing residue, centrifugalize, after separating medium is carried out drying, namely obtains Folium Forsythiae extract;
The preparation method of described Chinese medicine mixed extract is:
By Herba Sonchi Arvensis, Herba Androsaces umbellatae, Radix Scutellariae, Folium Artemisiae Argyi, Radix Rubiae and the Radix Astragali according to weight portion be Herba Sonchi Arvensis 1-9 part, Herba Androsaces umbellatae 1-15 part, Radix Scutellariae 1-10 part, Folium Artemisiae Argyi 1-9 part, Radix Rubiae 1-8 part, the Radix Astragali 1-7 part proportioning mixing, add water and soak half an hour at 60 DEG C, described Herba Sonchi Arvensis, Herba Androsaces umbellatae, Radix Scutellariae, Folium Artemisiae Argyi, Radix Rubiae and Radix Astragali mixing are 1:8 with the weight part ratio of water, rear decoction twice, 1.5 hours first times, second time 1 hour, merges and boils liquid, filters; Filtrate reduced in volume, to the extractum of relative density 1.25-1.4, after cooling, adds the alcohol settling of concentration of volume percent 60%, leave standstill 12 hours, after leaching supernatant, reclaim ethanol, at 60 DEG C, be concentrated into the extractum of relative density 1.05-1.1, drying obtains Chinese medicine mixed extract.
The beneficial effect that the present invention compared with prior art has is:
1, in the mountain forest of Folium Forsythiae growth more than 1500 meters, belong to natural crude drugs, pollution-free nuisanceless, the local common people make Folium Camelliae sinensis by Folium Forsythiae, drink at ordinary times, clearing away heat-fire, promoting pus discharge and removing toxic substances, local person " life-prolonging tea ", Folium Forsythiae can mix prepare cold dishes edible, dampness detoxify, clearly tasty and refreshing.Folium Forsythiae extract phillyrin and Fructus Forsythiae ester glycoside are the effective ingredient that in Folium Forsythiae, content is the highest, have important medical value with the facial film that it is made; Folium Forsythiae extract has the effect of heat-clearing and toxic substances removing, eliminating carbuncle eliminating stagnation, inducing diuresis and reducing edema, evacuation of pus of invigorating blood circulation, and may be used for Acne treatment, eliminating toxin and beautifying the skin, antiinflammatory antibacterial etc.Utilize Folium Forsythiae extract, and compatibility Chinese medicine mixed extract, water soluble Margarita ultrafine powder make facial film, there is synergistic function, the effect having heat-clearing and toxic substances removing, eliminating carbuncle eliminating stagnation, eliminating toxin and beautifying the skin, expelling pus and promoting granulation, evacuation of pus of invigorating blood circulation, antioxidation and enhance metabolism, has good curative effect for skin of face problem.
2, the present invention makes facial film with Folium Forsythiae extract and can treat facial skin disease, eliminating toxin and beautifying the skin.Characteristic part is that Folium Forsythiae extract has stronger antibacterial and antioxidation, can use, without the need to additionally adding artificial preservative as natural antiseptic agent.
3, mostly facial skin disease is because the reason such as germ reproduction, accumulation causes, and the bacteriostasis of Folium Forsythiae extract, germ reproduction can be suppressed, in addition the clearing away heat-fire of Folium Forsythiae extract, effect of promoting pus discharge and removing toxic substances, has good effect to dermatosis such as Acne treatments, pure natural has no side effect, and the Chinese medicine mixed extract obtained with the plurality of Chinese such as Herba Sonchi Arvensis, Folium Artemisiae Argyi, the Radix Astragali and Margarita powder compatibility use, and have the effect of Synergistic, can better improve skin of face problem.
4, the Fructus Forsythiae extract used in general production mostly is Fructus Forsythiae extract, and the present invention utilizes Folium Forsythiae extract, can make full use of resource, reduces production cost.There is a large amount of Folium Forsythiae not to be utilized every year, become fallen leaves all over the mountains and plains.By the research and development to Folium Forsythiae, make it turn waste into wealth, can increase farmers' income.
5, the present invention is widely used, adaptation population's large contingent, can be used for industrialization large-scale production.
Extract in Folium Forsythiae containing phillyrin, Fructus Forsythiae ester glycoside and rutin etc., can eliminating stagnation pathogenic fire purging, detumescence and apocenosis, relieve the pain diuretic.Modern pharmacology shows, phillyrin and Fructus Forsythiae ester glycoside have antioxidation, antibacterial, antiviral, protect the liver the antipyretic effect of antiinflammatory.
We study Folium Forsythiae effective ingredient in recent years, show that FSE can prevent hepatocellular damage with Folium Forsythiae extract (FSE) to mouse stomach test, and its effect is not second to Fructus Forsythiae.Can improve the ability of liver organization defence oxidative damage, improve liver superoxide dismutase (SOD) and cholinesterase (CHE) vigor, the exception reducing alanine aminotransferase (ALT) raises, and alleviates the hepatic injury that free radical causes.FSE can suppress malonaldehyde (MDA) to be accumulated in liver, has slow down aging and anti-stress ability, and all has inhibitory action to staphylococcus aureus, escherichia coli and Candida albicans.The effects such as its antiinflammatory, antibacterial, antioxidation obviously.Herba Sonchi Arvensis and Herba Androsaces umbellatae belong to antipyretic and antidotal type Chinese herbal medicine, and Herba Sonchi Arvensis main component, containing oils and fats, ceryl alcohol, choline, Nulomoline, tartaric acid, contains oxidase, rubber, mannitol, left-handed vitriol alcohol and bitter principle etc. in its milk.Herba Androsaces umbellatae tool heat-clearing and toxic substances removing, effect of reducing swelling and alleviating pain.Radix Scutellariae can heat clearing and damp drying, toxin expelling diuretic.Folium Artemisiae Argyi, Rubia blood-regulating drug, Folium Artemisiae Argyi nature and flavor are pungent, bitter, temperature, can contribute to disease such as treatment skin pruritus, decortication etc.Radix Rubiae has effect of promoting the circulation of blood hemostasis, dredge the meridian passage, toxin expelling.The effect that the Radix Astragali has expelling pus and promoting granulation, enhances metabolism.
Folium Forsythiae extract facial film of the present invention, in its formula, each constituent mass percentage ratio is: Folium Forsythiae extract 1-30%, Chinese medicine mixed extract 1-15%, water soluble Margarita ultrafine powder 1-5%, deionized water 20-80%, xanthan gum 1-5%, flexibilizer 5-10%.Also aromatic can be added in formula, as essence, quintessence oil 0-1%.
Wherein flexibilizer is calcium hydroxide or sodium bicarbonate.
Aromatic can select Peppermint essential oil, Herba Lysimachiae foenum-graeci quintessence oil, sandalwood essential oil etc.
Facial film preparation process of the present invention comprises: any method can be used Folium Forsythiae extract, Chinese medicine mixed extract and water soluble Margarita ultrafine powder to be mixed with suitable facial film film forming matrix, fixing shaping prepares facial film finished product.
Facial film preparation method of the present invention:
1. successively Folium Forsythiae extract, Chinese medicine mixed extract, water soluble Margarita ultrafine powder, aromatic, xanthan gum be slowly added to the water and constantly stir, fully mixing;
2. add flexibilizer after mixture heating being also constantly stirred and heated to 80-90 DEG C, stir;
3., by glue Slow cooling, when temperature is down to 75 DEG C, glue is injected mould, cooling forming, be prepared into facial film finished product.
Detailed description of the invention
Below in conjunction with specific embodiment, the invention will be further described.
Embodiment 1
A kind of forsythia leaf facial mask, by functional components, deionized water, xanthan gum and flexibilizer composition, described functional components by Folium Forsythiae extract, form containing the Chinese medicine mixed extract of Herba Sonchi Arvensis, Herba Androsaces umbellatae, Radix Scutellariae, Folium Artemisiae Argyi, Radix Rubiae and the Radix Astragali and water soluble Margarita ultrafine powder, Folium Forsythiae extract account for facial film gross weight 30%, Chinese medicine mixed extract account for facial film gross weight 15%, water soluble Margarita ultrafine powder accounts for 5% of facial film gross weight;
The preparation method of described Folium Forsythiae extract is:
Get ripe Folium Forsythiae after cleaning is dried, be ground into coarse powder, cross 40 mesh sieves; Add the ethanol of concentration of volume percent 50% wherein, mix thoroughly, stewing 16 hours, load percolate pot, add the ethanol of the concentration of volume percent 60% of 6 times of volumes, leave standstill percolation after 24 hours, flow 60 is per minute, percolation 50 hours, filters and obtains filtrate and filtering residue; At 60 DEG C, reclaim ethanol, the concentrated solution A being condensed into relative density 1.1-1.3 is for subsequent use; Be the ethanol of 90% by the concentration of volume percent adding 6 times of volumes in described filtering residue, reflux 10 hours at 80 DEG C, get supernatant and carry out secondary filter, at 60 DEG C, reclaim ethanol, the concentrated solution B being condensed into relative density 1.1-1.3 is for subsequent use; Merged by concentrated solution A and concentrated solution B, removing residue, centrifugalize, after separating medium is carried out drying, namely obtains Folium Forsythiae extract;
The preparation method of described Chinese medicine mixed extract is:
Be Herba Sonchi Arvensis 9 parts, Herba Androsaces umbellatae 15 parts, Radix Scutellariae 10 parts, Folium Artemisiae Argyi 9 parts, 8 parts, Radix Rubiae, the mixing of the Radix Astragali 7 parts of proportionings by Herba Sonchi Arvensis, Herba Androsaces umbellatae, Radix Scutellariae, Folium Artemisiae Argyi, Radix Rubiae and the Radix Astragali according to weight portion, add water and soak half an hour at 60 DEG C, described Herba Sonchi Arvensis, Herba Androsaces umbellatae, Radix Scutellariae, Folium Artemisiae Argyi, Radix Rubiae and Radix Astragali mixing are 1:8 with the weight part ratio of water, rear decoction twice, 1.5 hours first times, second time 1 hour, merges and boils liquid, filters; Filtrate reduced in volume, to the extractum of relative density 1.25-1.4, after cooling, adds the alcohol settling of concentration of volume percent 60%, leave standstill 12 hours, after leaching supernatant, reclaim ethanol, at 60 DEG C, be concentrated into the extractum of relative density 1.05-1.1, drying obtains Chinese medicine mixed extract.
Embodiment 2
A kind of forsythia leaf facial mask, by functional components, deionized water, xanthan gum and flexibilizer composition, described functional components by Folium Forsythiae extract, form containing the Chinese medicine mixed extract of Herba Sonchi Arvensis, Herba Androsaces umbellatae, Radix Scutellariae, Folium Artemisiae Argyi, Radix Rubiae and the Radix Astragali and water soluble Margarita ultrafine powder, Folium Forsythiae extract account for facial film gross weight 1%, Chinese medicine mixed extract account for facial film gross weight 1%, water soluble Margarita ultrafine powder accounts for 1% of facial film gross weight;
The preparation method of described Folium Forsythiae extract is:
Get ripe Folium Forsythiae after cleaning is dried, be ground into coarse powder, cross 40 mesh sieves; Add the ethanol of concentration of volume percent 50% wherein, mix thoroughly, stewing 10 hours, load percolate pot, add the ethanol of the concentration of volume percent 60% of 1 times of volume, leave standstill percolation after 20 hours, flow 40 is per minute, percolation 40 hours, filters and obtains filtrate and filtering residue; At 60 DEG C, reclaim ethanol, the concentrated solution A being condensed into relative density 1.1-1.3 is for subsequent use; Be the ethanol of 90% by the concentration of volume percent adding 1 times of volume in described filtering residue, reflux 5 hours at 80 DEG C, get supernatant and carry out secondary filter, at 60 DEG C, reclaim ethanol, the concentrated solution B being condensed into relative density 1.1-1.3 is for subsequent use; Merged by concentrated solution A and concentrated solution B, removing residue, centrifugalize, after separating medium is carried out drying, namely obtains Folium Forsythiae extract;
The preparation method of described Chinese medicine mixed extract is:
Be Herba Sonchi Arvensis 1 part, Herba Androsaces umbellatae 1 part, Radix Scutellariae 1 part, Folium Artemisiae Argyi 1 part, 1 part, Radix Rubiae, the mixing of the Radix Astragali 1 part of proportioning by Herba Sonchi Arvensis, Herba Androsaces umbellatae, Radix Scutellariae, Folium Artemisiae Argyi, Radix Rubiae and the Radix Astragali according to weight portion, add water and soak half an hour at 60 DEG C, described Herba Sonchi Arvensis, Herba Androsaces umbellatae, Radix Scutellariae, Folium Artemisiae Argyi, Radix Rubiae and Radix Astragali mixing are 1:8 with the weight part ratio of water, rear decoction twice, 1.5 hours first times, second time 1 hour, merges and boils liquid, filters; Filtrate reduced in volume, to the extractum of relative density 1.25-1.4, after cooling, adds the alcohol settling of concentration of volume percent 60%, leave standstill 12 hours, after leaching supernatant, reclaim ethanol, at 60 DEG C, be concentrated into the extractum of relative density 1.05-1.1, drying obtains Chinese medicine mixed extract.
Embodiment 3
A kind of forsythia leaf facial mask, by functional components, deionized water, xanthan gum and flexibilizer composition, described functional components by Folium Forsythiae extract, form containing the Chinese medicine mixed extract of Herba Sonchi Arvensis, Herba Androsaces umbellatae, Radix Scutellariae, Folium Artemisiae Argyi, Radix Rubiae and the Radix Astragali and water soluble Margarita ultrafine powder, Folium Forsythiae extract account for facial film gross weight 15%, Chinese medicine mixed extract account for facial film gross weight 9%, water soluble Margarita ultrafine powder accounts for 2% of facial film gross weight;
The preparation method of described Folium Forsythiae extract is:
Get ripe Folium Forsythiae after cleaning is dried, be ground into coarse powder, cross 40 mesh sieves; Add the ethanol of concentration of volume percent 50% wherein, mix thoroughly, stewing 12 hours, load percolate pot, add the ethanol of the concentration of volume percent 60% of 3 times of volumes, leave standstill percolation after 22 hours, flow 45 is per minute, percolation 45 hours, filters and obtains filtrate and filtering residue; At 60 DEG C, reclaim ethanol, the concentrated solution A being condensed into relative density 1.1-1.3 is for subsequent use; Be the ethanol of 90% by the concentration of volume percent adding 3 times of volumes in described filtering residue, reflux 8 hours at 80 DEG C, get supernatant and carry out secondary filter, at 60 DEG C, reclaim ethanol, the concentrated solution B being condensed into relative density 1.1-1.3 is for subsequent use; Merged by concentrated solution A and concentrated solution B, removing residue, centrifugalize, after separating medium is carried out drying, namely obtains Folium Forsythiae extract;
The preparation method of described Chinese medicine mixed extract is:
Be Herba Sonchi Arvensis 6 parts, Herba Androsaces umbellatae 3 parts, Radix Scutellariae 5 parts, Folium Artemisiae Argyi 5 parts, 6 parts, Radix Rubiae, the mixing of the Radix Astragali 4 parts of proportionings by Herba Sonchi Arvensis, Herba Androsaces umbellatae, Radix Scutellariae, Folium Artemisiae Argyi, Radix Rubiae and the Radix Astragali according to weight portion, add water and soak half an hour at 60 DEG C, described Herba Sonchi Arvensis, Herba Androsaces umbellatae, Radix Scutellariae, Folium Artemisiae Argyi, Radix Rubiae and Radix Astragali mixing are 1:8 with the weight part ratio of water, rear decoction twice, 1.5 hours first times, second time 1 hour, merges and boils liquid, filters; Filtrate reduced in volume, to the extractum of relative density 1.25-1.4, after cooling, adds the alcohol settling of concentration of volume percent 60%, leave standstill 12 hours, after leaching supernatant, reclaim ethanol, at 60 DEG C, be concentrated into the extractum of relative density 1.05-1.1, drying obtains Chinese medicine mixed extract.
Embodiment 4
A kind of forsythia leaf facial mask, by functional components, deionized water, xanthan gum and flexibilizer composition, described functional components by Folium Forsythiae extract, form containing the Chinese medicine mixed extract of Herba Sonchi Arvensis, Herba Androsaces umbellatae, Radix Scutellariae, Folium Artemisiae Argyi, Radix Rubiae and the Radix Astragali and water soluble Margarita ultrafine powder, Folium Forsythiae extract account for facial film gross weight 22%, Chinese medicine mixed extract account for facial film gross weight 3%, water soluble Margarita ultrafine powder accounts for 2% of facial film gross weight;
The preparation method of described Folium Forsythiae extract is:
Get ripe Folium Forsythiae after cleaning is dried, be ground into coarse powder, cross 40 mesh sieves; Add the ethanol of concentration of volume percent 50% wherein, mix thoroughly, stewing 15 hours, load percolate pot, add the ethanol of the concentration of volume percent 60% of 5 times of volumes, leave standstill percolation after 21 hours, flow 55 is per minute, percolation 44 hours, filters and obtains filtrate and filtering residue; At 60 DEG C, reclaim ethanol, the concentrated solution A being condensed into relative density 1.1-1.3 is for subsequent use; Be the ethanol of 90% by the concentration of volume percent adding 5 times of volumes in described filtering residue, reflux 6 hours at 80 DEG C, get supernatant and carry out secondary filter, at 60 DEG C, reclaim ethanol, the concentrated solution B being condensed into relative density 1.1-1.3 is for subsequent use; Merged by concentrated solution A and concentrated solution B, removing residue, centrifugalize, after separating medium is carried out drying, namely obtains Folium Forsythiae extract;
The preparation method of described Chinese medicine mixed extract is:
Be Herba Sonchi Arvensis 8 parts, Herba Androsaces umbellatae 14 parts, Radix Scutellariae 2 parts, Folium Artemisiae Argyi 7 parts, 3 parts, Radix Rubiae, the mixing of the Radix Astragali 5 parts of proportionings by Herba Sonchi Arvensis, Herba Androsaces umbellatae, Radix Scutellariae, Folium Artemisiae Argyi, Radix Rubiae and the Radix Astragali according to weight portion, add water and soak half an hour at 60 DEG C, described Herba Sonchi Arvensis, Herba Androsaces umbellatae, Radix Scutellariae, Folium Artemisiae Argyi, Radix Rubiae and Radix Astragali mixing are 1:8 with the weight part ratio of water, rear decoction twice, 1.5 hours first times, second time 1 hour, merges and boils liquid, filters; Filtrate reduced in volume, to the extractum of relative density 1.25-1.4, after cooling, adds the alcohol settling of concentration of volume percent 60%, leave standstill 12 hours, after leaching supernatant, reclaim ethanol, at 60 DEG C, be concentrated into the extractum of relative density 1.05-1.1, drying obtains Chinese medicine mixed extract.
Embodiment 5
A kind of forsythia leaf facial mask, by functional components, deionized water, xanthan gum and flexibilizer composition, described functional components by Folium Forsythiae extract, form containing the Chinese medicine mixed extract of Herba Sonchi Arvensis, Herba Androsaces umbellatae, Radix Scutellariae, Folium Artemisiae Argyi, Radix Rubiae and the Radix Astragali and water soluble Margarita ultrafine powder, Folium Forsythiae extract account for facial film gross weight 8%, Chinese medicine mixed extract account for facial film gross weight 12%, water soluble Margarita ultrafine powder accounts for 4% of facial film gross weight;
The preparation method of described Folium Forsythiae extract is:
Get ripe Folium Forsythiae after cleaning is dried, be ground into coarse powder, cross 40 mesh sieves; Add the ethanol of concentration of volume percent 50% wherein, mix thoroughly, stewing 13 hours, load percolate pot, add the ethanol of the concentration of volume percent 60% of 3 times of volumes, leave standstill percolation after 22 hours, flow 47 is per minute, percolation 42 hours, filters and obtains filtrate and filtering residue; At 60 DEG C, reclaim ethanol, the concentrated solution A being condensed into relative density 1.1-1.3 is for subsequent use; Be the ethanol of 90% by the concentration of volume percent adding 2 times of volumes in described filtering residue, reflux 7 hours at 80 DEG C, get supernatant and carry out secondary filter, at 60 DEG C, reclaim ethanol, the concentrated solution B being condensed into relative density 1.1-1.3 is for subsequent use; Merged by concentrated solution A and concentrated solution B, removing residue, centrifugalize, after separating medium is carried out drying, namely obtains Folium Forsythiae extract;
The preparation method of described Chinese medicine mixed extract is:
Be Herba Sonchi Arvensis 5 parts, Herba Androsaces umbellatae 11.5 parts, Radix Scutellariae 9 parts, Folium Artemisiae Argyi 3 parts, 3 parts, Radix Rubiae, the mixing of the Radix Astragali 4.5 parts of proportionings by Herba Sonchi Arvensis, Herba Androsaces umbellatae, Radix Scutellariae, Folium Artemisiae Argyi, Radix Rubiae and the Radix Astragali according to weight portion, add water and soak half an hour at 60 DEG C, described Herba Sonchi Arvensis, Herba Androsaces umbellatae, Radix Scutellariae, Folium Artemisiae Argyi, Radix Rubiae and Radix Astragali mixing are 1:8 with the weight part ratio of water, rear decoction twice, 1.5 hours first times, second time 1 hour, merges and boils liquid, filters; Filtrate reduced in volume, to the extractum of relative density 1.25-1.4, after cooling, adds the alcohol settling of concentration of volume percent 60%, leave standstill 12 hours, after leaching supernatant, reclaim ethanol, at 60 DEG C, be concentrated into the extractum of relative density 1.05-1.1, drying obtains Chinese medicine mixed extract.
Embodiment 6
1. formula: the raw material of every 100g product consists of: Folium Forsythiae extract 10g, Chinese medicine mixed extract 3g, water soluble Margarita ultrafine powder 2g, xanthan gum 1.5 g, calcium hydroxide 1g, all the other are deionized water.
2. preparation technology:
A.(1) get ripe Folium Forsythiae after pre-treatment, shatter into coarse powder (crossing 40 mesh sieves);
(2) add concentration of volume percent 50% appropriate amount of ethanol, mix thoroughly, stewing 12 hours, load percolate pot, concentration of volume percent 60% ethanol adding 5 times of volumes leaves standstill 24 hours, and start percolation, flow-control per minute is dripped at 40-60,48 hours percolation time, collect solution, filter;
(3) reclaiming ethanol, be concentrated into relative density 1.1-1.3(60 DEG C) extractum is for subsequent use.
B.(1) the Folium Forsythiae coarse powder after percolation is loaded multi-function extractor, add concentration of volume percent 90% alcohol solvent of 5 times of volumes, ethanol hot reflux is carried out in temperature control 80 DEG C, 8 hours time, gets supernatant and filters;
(2) reclaim ethanol, be concentrated into relative density 1.1-1.3(60 DEG C) extractum and a extractum merge;
(3) be separated by extractum, removing residue, gets separating medium;
(4) after separating medium being carried out vacuum drying (60 DEG C) or spraying dry, by broken for the dried cream powder of drying, cross 180 order dusting covers, obtain Folium Forsythiae extract.
C. each 3 parts of mixing of Herba Sonchi Arvensis, Herba Androsaces umbellatae, Radix Scutellariae, Folium Artemisiae Argyi, Radix Rubiae and the Radix Astragali, add water warm macerating half an hour (60 DEG C), rear decoction twice, 1.5 hours first times, and second time 1 hour merges and boils liquid, filters.Filtrate reduced in volume, to the extractum of relative density 1.25-1.4, after cooling, adds concentration of volume percent 60% alcohol settling, leave standstill 12 hours, elimination supernatant, reclaim ethanol, be concentrated into 1.05-1.1(60 DEG C) extractum, drying under reduced pressure or spraying dry, obtain Chinese medicine mixed extract.
D.(1) successively Folium Forsythiae extract, Chinese medicine mixed extract, water soluble Margarita ultrafine powder, xanthan gum be slowly added to the water and constantly stir, fully mixing;
(2) add calcium hydroxide after mixture heating being also constantly stirred and heated to 80-90 DEG C, stir;
(3) by glue Slow cooling, when temperature is down to 75 DEG C, glue is injected mould, cooling forming, be prepared into facial film finished product.
Embodiment 7
1. formula: the raw material of every 100g product consists of: Folium Forsythiae extract 15 g, Chinese medicine mixed extract 5g, water soluble Margarita ultrafine powder 2g, xanthan gum 1.2 g, calcium hydroxide 0.8g, Peppermint essential oil 0.1 g, all the other are deionized water.
2. preparation technology:
A.(1) get ripe Folium Forsythiae after pre-treatment, shatter into coarse powder (crossing 40 mesh sieves);
(2) add concentration of volume percent 50% appropriate amount of ethanol, mix thoroughly, stewing 12 hours, load percolate pot, concentration of volume percent 60% ethanol adding 5 times of volumes leaves standstill 24 hours, and start percolation, flow-control per minute is dripped at 40-60,48 hours percolation time, collect solution, filter;
(3) reclaiming ethanol, be concentrated into relative density 1.1-1.3(60 DEG C) extractum is for subsequent use.
B.(1) the Folium Forsythiae coarse powder after percolation is loaded multi-function extractor, add concentration of volume percent 90% alcohol solvent of 5 times of volumes, ethanol hot reflux is carried out in temperature control 80 DEG C, 8 hours time, gets supernatant and filters;
(2) reclaim ethanol, be concentrated into relative density 1.1-1.3(60 DEG C) extractum and a extractum merge;
(3) be separated by extractum, removing residue, gets separating medium;
(4) after separating medium being carried out vacuum drying (60 DEG C) or spraying dry, by broken for the dried cream powder of drying, cross 180 order dusting covers, obtain Folium Forsythiae extract.
C. Herba Sonchi Arvensis 4 parts, Herba Androsaces umbellatae 5 parts, Radix Scutellariae 3 parts, Folium Artemisiae Argyi 2.5 parts, 3.5 parts, Radix Rubiae and the Radix Astragali 2 parts mixing, add water warm macerating half an hour (60 DEG C), rear decoction twice, 1.5 hours first times, and second time 1 hour merges and boils liquid, filters.Filtrate reduced in volume, to the extractum of relative density 1.25-1.4, after cooling, adds concentration of volume percent 60% alcohol settling, leave standstill 12 hours, elimination supernatant, reclaim ethanol, be concentrated into 1.05-1.1(60 DEG C) extractum, drying under reduced pressure or spraying dry, obtain Chinese medicine mixed extract.
D.(1) successively Folium Forsythiae extract, Chinese medicine mixed extract, water soluble Margarita ultrafine powder, Peppermint essential oil, xanthan gum be slowly added to the water and constantly stir, fully mixing;
(2) add calcium hydroxide after mixture heating being also constantly stirred and heated to 80-90 DEG C, stir;
(3) by glue Slow cooling, when temperature is down to 75 DEG C, glue is injected mould, cooling forming, be prepared into facial film finished product.
The Folium Forsythiae extract of interpolation various dose is prepared facial film and is carried out bacteriostatic test:
1. test strain is staphylococcus aureus, escherichia coli, bacillus pyocyaneus and Candida albicans strain suspension;
2. test method: by strain inoculation in suitable culture medium, staphylococcus aureus, escherichia coli, bacillus pyocyaneus are at 37 DEG C of constant temperature culture 24 h, and Candida albicans, at 30 DEG C of constant temperature culture 48 h, makes strain concentration 10
8more than cfu/g, then antibacterial decile being mixed into concentration is 10
6the bacteria suspension of cfu/g.Sample facial film is carried out controlled trial according to different Folium Forsythiae extract addition.The facial film glue of uncolled shaping is selected for examination facial film.The content of microorganisms adopting plate dilution method to detect sample respectively at the 7th, 14,21 and 28 day.
3. criterion: the initial inoculum antibacterial 10 of sample
6cfu/g:(1) the 28th day time, containing antibacterial > 10 in sample
3cfu/g, this sample is not tested by the challenge of microorganism attack; When (2) the 28th days, contain antibacterial in sample 10
2cfu/g ~ 10
3cfu/g, this sample conditional pass challenge is tested, namely when protein in product or other animals and plants material compositions are not high especially, the hygienic conditions of simultaneously producing meet the requirements, when secondary pollution not easily occurs packing material, this protective system can use, otherwise can not use; When (3) the 28th days, contain antibacterial in sample in 10 cfu/g ~ 10
2cfu/g, shows that the protective system of this sample has stronger bactericidal effect to microorganism, and by challenge test, product is not easy to be subject to microbial contamination when producing, preserving and using; Within (4) the 7th days, rise, antibacterial < 10 cfu/g in sample, the 14th, 21,28 days, bacterial content unlike more than the 7th day time, the protective system of this sample has the bactericidal action of extra-heavy to microorganism, by challenge experiment, product is not easy microbial contamination when producing, preserving and using.
Bacteria Detection tables of data (n=3) in facial film
Analysis is shown, what find to have in 4 kinds of facial films antibacterial, bactericidal effect is Folium Forsythiae extract (0.3%) facial film, Folium Forsythiae extract (0.5%) facial film and Folium Forsythiae extract (1%) facial film, and wherein the antiseptic effect of Folium Forsythiae extract (1%) facial film is the strongest.Along with in Folium Forsythiae extract facial film, the increase of Folium Forsythiae extract addition, antiseptic effect strengthens.Therefore the anticorrosion dosage of Folium Forsythiae extract can be 0.3%-1% in facial film, minimum addition should be not less than 0.3%.
Product sensory describes:
Product is a kind of gluey shaping pad pasting.Color and luster: canescence.Fragrance: conform with the regulations fragrance.Figure: lamellar, bubble-free, homogeneous.
The present invention can summarize with other the concrete form without prejudice to spirit of the present invention or principal character.Therefore, no matter from that, above-mentioned embodiment of the present invention all can only be thought explanation of the present invention and can not limit invention, claims indicate scope of the present invention, and scope of the present invention is not pointed out in above-mentioned explanation, therefore, any change in the implication suitable with claims of the present invention and scope, all should think to be included in the scope of claims.
Claims (1)
1. a forsythia leaf facial mask, by functional components, deionized water, xanthan gum and flexibilizer composition, it is characterized in that described functional components is by Folium Forsythiae extract, form containing the Chinese medicine mixed extract of Herba Sonchi Arvensis, Herba Androsaces umbellatae, Radix Scutellariae, Folium Artemisiae Argyi, Radix Rubiae and the Radix Astragali and water soluble Margarita ultrafine powder, the 1-15% that Folium Forsythiae extract accounts for the 1-30% of facial film gross weight, Chinese medicine mixed extract accounts for facial film gross weight, water soluble Margarita ultrafine powder account for the 1-5% of facial film gross weight;
The preparation method of described Folium Forsythiae extract is:
Get ripe Folium Forsythiae after cleaning is dried, be ground into coarse powder, cross 40 mesh sieves; Add the ethanol of concentration of volume percent 50% wherein, mix thoroughly, stewing 10-16 hour, loads percolate pot, add the ethanol of the concentration of volume percent 60% of 1-6 times of volume, leave standstill percolation after 20-24 hour, flow 40-60 drips per minute, percolation 40-50 hour, filters and obtains filtrate and filtering residue; At 60 DEG C, reclaim ethanol, the concentrated solution A being condensed into relative density 1.1-1.3 is for subsequent use; Be the ethanol of 90% by the concentration of volume percent adding 1-6 times of volume in described filtering residue, reflux 5-10 hour at 80 DEG C, gets supernatant and carry out secondary filter, at 60 DEG C, reclaim ethanol, and the concentrated solution B being condensed into relative density 1.1-1.3 is for subsequent use; Merged by concentrated solution A and concentrated solution B, removing residue, centrifugalize, after separating medium is carried out drying, namely obtains Folium Forsythiae extract;
The preparation method of described Chinese medicine mixed extract is:
By Herba Sonchi Arvensis, Herba Androsaces umbellatae, Radix Scutellariae, Folium Artemisiae Argyi, Radix Rubiae and the Radix Astragali according to weight portion be Herba Sonchi Arvensis 1-9 part, Herba Androsaces umbellatae 1-15 part, Radix Scutellariae 1-10 part, Folium Artemisiae Argyi 1-9 part, Radix Rubiae 1-8 part, the Radix Astragali 1-7 part proportioning mixing, add water and soak half an hour at 60 DEG C, described Herba Sonchi Arvensis, Herba Androsaces umbellatae, Radix Scutellariae, Folium Artemisiae Argyi, Radix Rubiae and Radix Astragali mixing are 1:8 with the weight part ratio of water, rear decoction twice, 1.5 hours first times, second time 1 hour, merges and boils liquid, filters; Filtrate reduced in volume, to the extractum of relative density 1.25-1.4, after cooling, adds the alcohol settling of concentration of volume percent 60%, leave standstill 12 hours, after leaching supernatant, reclaim ethanol, at 60 DEG C, be concentrated into the extractum of relative density 1.05-1.1, drying obtains Chinese medicine mixed extract.
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| CN1279940A (en) * | 1999-07-07 | 2001-01-17 | 王淑贞 | Beautifying wet coating face mask capable of curing acne and seborrheic diseases |
| CN1840070A (en) * | 2006-01-18 | 2006-10-04 | 蒋其锟 | Application of a medicinal composition in preparation of acne-treating medicine |
| CN101406547A (en) * | 2008-11-11 | 2009-04-15 | 孙立华 | Facial mask for treating comedo |
| CN101732422A (en) * | 2008-11-11 | 2010-06-16 | 耿静 | Mask for treating adolescent acne |
| CN101757177A (en) * | 2008-11-18 | 2010-06-30 | 姜晓宇 | Medicament for treating facial severe acne |
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2013
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1279940A (en) * | 1999-07-07 | 2001-01-17 | 王淑贞 | Beautifying wet coating face mask capable of curing acne and seborrheic diseases |
| CN1840070A (en) * | 2006-01-18 | 2006-10-04 | 蒋其锟 | Application of a medicinal composition in preparation of acne-treating medicine |
| CN101406547A (en) * | 2008-11-11 | 2009-04-15 | 孙立华 | Facial mask for treating comedo |
| CN101732422A (en) * | 2008-11-11 | 2010-06-16 | 耿静 | Mask for treating adolescent acne |
| CN101757177A (en) * | 2008-11-18 | 2010-06-30 | 姜晓宇 | Medicament for treating facial severe acne |
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