CN109157489A - A kind of preparation method of skin care compositions and facial mask with antibacterial functions - Google Patents

A kind of preparation method of skin care compositions and facial mask with antibacterial functions Download PDF

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Publication number
CN109157489A
CN109157489A CN201811089059.7A CN201811089059A CN109157489A CN 109157489 A CN109157489 A CN 109157489A CN 201811089059 A CN201811089059 A CN 201811089059A CN 109157489 A CN109157489 A CN 109157489A
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China
Prior art keywords
care compositions
skin care
antibacterial functions
facial mask
film forming
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Chinese (zh)
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梅淑婕
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Individual
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/41Amines
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/55Phosphorus compounds
    • A61K8/553Phospholipids, e.g. lecithin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P31/00Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
    • A61P31/04Antibacterial agents
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions

Abstract

The invention discloses the preparation methods of a kind of skin care compositions with antibacterial functions and facial mask.The raw material of the skin care compositions is made of Radix et Caulis Opuntiae Dillenii extract, nutgall extractive, lecithin, Phenoxyethanol, triethanolamine etc..The above-mentioned skin care compositions with antibacterial functions can be facial mask, preparation method is specifically that film forming agent is added in deionized water, insulated and stirred to film forming agent is completely dissolved after heating, obtain base soln, again by triethanolamine, hydroxyethyl cellulose, talcum powder, polysorbate alcohol -80, Sodium Hyaluronate, glycerol, alchlor, which is added in base soln, carries out insulated and stirred, Radix et Caulis Opuntiae Dillenii extract is added after solution cooling, nutgall extractive, lecithin, Phenoxyethanol, essence, preservative stirring, pH is adjusted again, finally move to stirring and emulsifying in mulser, it is filling after the screen to filtrate, obtain finished product facial mask.This has the effect of that the skin care compositions of antibacterial functions has and effectively inhibits the breeding of skin surface harmful bacteria, uses suitable for the crowd with bacterial dermatitis.

Description

A kind of preparation method of skin care compositions and facial mask with antibacterial functions
Technical field
The present invention relates to cosmetic technical fields, more particularly to a kind of skin care compositions and facial mask with antibacterial functions Preparation method.
Background technique
The principle of facial mask is temporarily isolating extraneous air and pollution, improves exactly using the of short duration time for being covered on face Skin temperature, the pore expansion of skin, promotes sweat gland secretion and metabolism, increase the oxygen content of skin, be conducive to skin The product of epidermal cell metabolism and the oil substances of accumulation are excluded, the moisture in facial mask penetrates into the cutin of skin epidermis Layer, skin become soft, increase elasticity.Skin is naturally bright flexible, and aerobic color is presented.Facial mask is one kind of face beautifying health keeping product Carrier, using fexible film as basic material, with contained thereon nourishing ingredient and direct facial contact, thus when reaching long Between maintaining skin purpose.Since the face pack prescription of the prior art contains certain organic components, rear face hair is used Kong Zhongyi residual organic matter increases microorganism in this case and colonizes risk.If staphylococcus aureus is exactly a kind of skin The common bacterium in skin surface, this bacterium can cause a variety of diseases, for example, it be skin and Soft Tissue Abscess: An Experimental, furuncle and The first cause of cellulitis.
Summary of the invention
The problem of not still being able to satisfy consumer demand the effect of inhibiting in terms of skin surface bacterium based on contemporary skin care product, The present invention provides the preparation method of a kind of skin care compositions with antibacterial functions and facial mask.
A kind of skin care compositions with antibacterial functions, the raw material of the skin care compositions is by Radix et Caulis Opuntiae Dillenii extract, five times Seed extract, lecithin, Phenoxyethanol, triethanolamine, hydroxyethyl cellulose, talcum powder, polysorbate alcohol -80, hyaluronic acid Sodium, glycerol, alchlor, essence, film forming agent, preservative, deionized water composition.
The above-mentioned skin care compositions with antibacterial functions contain be made of Radix et Caulis Opuntiae Dillenii extract, nutgall extractive it is natural The functional components such as effective component and lecithin, Phenoxyethanol, triethanolamine, each component are giving full play to respective basic function , can be synergistic except effect, effectively adjust human endocrine.The skin care compositions with antibacterial functions, which has, effectively to be inhibited The effect of skin surface harmful bacteria breeding, uses suitable for the crowd with bacterial dermatitis.
In one of the embodiments, the raw material of the skin care compositions according to parts by weight, concrete composition are as follows:
Radix et Caulis Opuntiae Dillenii extract 1.5~2.5%
Nutgall extractive 0.8~2.2%
Lecithin 0.08~0.3%
Phenoxyethanol 0.6~3.0%
Triethanolamine 0.2~0.8%
Hydroxyethyl cellulose 0.4~2.5%
Talcum powder 0.08~1.2%
Polysorbate alcohol -801.5~3.0%
Sodium Hyaluronate 2.0~3.0%
Glycerol 2.5~8.5%
Alchlor 0.06~0.12%
Essence 0.05~0.09%
Film forming agent 5.0~7.5%
Preservative 0.3~1.0%
Deionized water surplus.
The raw material of the skin care compositions according to parts by weight, specifically comprises in one of the embodiments,
Radix et Caulis Opuntiae Dillenii extract 2.0%
Nutgall extractive 1.5%
Lecithin 0.19%
Phenoxyethanol 1.6%
Triethanolamine 0.5%
Hydroxyethyl cellulose 1.5%
Talcum powder 0.8%
Polysorbate alcohol -802.2%
Sodium Hyaluronate 2.5%
Glycerol 5.5%
Alchlor 0.09%
Essence 0.07%
Film forming agent 6.3%
Preservative 0.7%
Deionized water surplus.
The film forming agent is in polyvinyl alcohol, dextrin, hydroxymethyl cellulose, carragheen in one of the embodiments, One or more.
The preservative is in ethylparaben, Nipasol, triclosan, sorbic acid in one of the embodiments, One or more.
The skin care compositions is facial mask in one of the embodiments,.
The present invention also provides the preparation methods of the above-mentioned facial mask with antibacterial functions, comprise the steps of:
(1) film forming agent is added in deionized water, solution is then heated to 80~85 DEG C, keep the temperature 20~30 minutes, and Being stirred according to 250~350 revs/min of rate to solution is completely dissolved film forming agent, obtains base soln;
(2) by triethanolamine, hydroxyethyl cellulose, talcum powder, polysorbate alcohol -80, Sodium Hyaluronate, glycerol, trichlorine Change aluminium to be added in step (1) resulting base soln, solution temperature is maintained 65~75 DEG C, according to 250~350 revs/min The rate of clock stirs 25~35 minutes;
(3) step (2) resulting solution is cooled to 40~50 DEG C, Radix et Caulis Opuntiae Dillenii extract, nutgall extractive, ovum is added Phosphatide, Phenoxyethanol, essence, preservative stir 15~20 minutes according to 250~350 revs/min of rates, by mixture PH is adjusted to 6~8, obtains intermediate solution;
(4) step (3) resulting intermediate solution is transferred in mulser, stirring and emulsifying 45 minutes, after the screen to filtrate It is filling, obtain finished product facial mask.
The preparation method of the above-mentioned facial mask with antibacterial functions, raw material is easy to get, simple process, is suitable for heavy industrialization Production.
The sodium hydroxide solution that concentration is 8% is selected to adjust mixture in the step (3) in one of the embodiments, PH.
The rate of stirring and emulsifying is 1500~2500 revs/min in the step (4) in one of the embodiments,.
The present invention also provides application of the skin care compositions with antibacterial functions in mask product preparation.
Specific embodiment
In order to make the foregoing objectives, features and advantages of the present invention clearer and more comprehensible, below in conjunction with specific embodiment, The present invention will be described in further detail.It should be appreciated that the specific embodiments described herein are only used to explain this hair It is bright, it is not intended to limit the present invention.
Unless otherwise defined, all technical and scientific terms used herein and belong to technical field of the invention The normally understood meaning of technical staff is identical.Term as used herein in the specification of the present invention is intended merely to description tool The purpose of the embodiment of body, it is not intended that in the limitation present invention.Term " and or " used herein includes one or more Any and all combinations of relevant listed item.
Raw materials used and reagent is commercially available common raw material and reagent in following embodiment.
A kind of skin care compositions with antibacterial functions, the raw material of the skin care compositions is by Radix et Caulis Opuntiae Dillenii extract, five times Seed extract, lecithin, Phenoxyethanol, triethanolamine, hydroxyethyl cellulose, talcum powder, polysorbate alcohol -80, hyaluronic acid Sodium, glycerol, alchlor, essence, film forming agent, preservative, deionized water composition.
Wherein, fleshy stem protein rich in, minerals, cellulose and the vitamin C etc. of cactus plumpness, simultaneously The various actives functional components such as SOD, flavonoids and polysaccharide rich in.Radix et Caulis Opuntiae Dillenii extract may penetrate into skin inner layer, It improves the anti-oxidant of skin and promotes moisturizing, dispel melanin, keep skin surface brilliant white.
Wherein, Chinese gall is parasitic times Aphidiadae insect horned gall aphid on the trees such as Anacardiaceae plant Chinese sumac, potanin sumac, redpunjab sumac root Or the insect gall formed after berry-gall aphid.Chinese gall main component is tannic acid, to staphylococcus aureus, streptococcus, pneumococcus And typhoid bacillus, paratyphosum Bacterium, shigella dysenteriae, bacillus anthracis, corynebacterium diphtheriae, Pseudomonas aeruginosa etc. have it is apparent antibacterial or Bactericidal effect.Chinese gall has astringing lung-QI fall fire, relieving diarrhea with astringents, astringent sperm contracting urine, hidroschesis, hemostasis, removing toxic substances, sore as traditional Chinese medicine Etc. various clinicals effect.
Wherein, lecithin, also known as lecithin are known as " third nutrient " arranged side by side with protein, vitamin.Lecithin Rouge is the indispensable substance of each cell of human body, if lacked, will reduce the power of regeneration of Skin Cell, lead to skin It is coarse, have wrinkle.As can suitably absorbing lecithin, skin regeneration vigor can be ensured, along with lecithin is good hydrophilic Property and lipophilicity, skin are able to maintain gloss.
Wherein, Phenoxyethanol is a kind of fine chemical product and organic synthesis intermediate, and a kind of higher boiling, low volatility are molten Agent, but be a kind of low sensitization, efficiently, the anticorrosion and bactericidal agent of wide spectrum.It is in the industrial applications frequency such as light industry, daily use chemicals, pesticide, medicine It is higher and higher, there is very high realistic meaning and economic benefit.
The above-mentioned skin care compositions with antibacterial functions contain be made of Radix et Caulis Opuntiae Dillenii extract, nutgall extractive it is natural The functional components such as effective component and lecithin, Phenoxyethanol, triethanolamine, each component are giving full play to respective basic function , can be synergistic except effect, effectively adjust human endocrine.The skin care compositions with antibacterial functions, which has, effectively to be inhibited The effect of skin surface harmful bacteria breeding, uses suitable for the crowd with bacterial dermatitis.
In a preferred embodiment, the raw material of the skin care compositions according to parts by weight, concrete composition are as follows:
Radix et Caulis Opuntiae Dillenii extract 1.5~2.5%
Nutgall extractive 0.8~2.2%
Lecithin 0.08~0.3%
Phenoxyethanol 0.6~3.0%
Triethanolamine 0.2~0.8%
Hydroxyethyl cellulose 0.4~2.5%
Talcum powder 0.08~1.2%
Polysorbate alcohol -801.5~3.0%
Sodium Hyaluronate 2.0~3.0%
Glycerol 2.5~8.5%
Alchlor 0.06~0.12%
Essence 0.05~0.09%
Film forming agent 5.0~7.5%
Preservative 0.3~1.0%
Deionized water surplus.
In one more preferably embodiment, the raw material of the skin care compositions according to parts by weight, is specifically comprised
Radix et Caulis Opuntiae Dillenii extract 2.0%
Nutgall extractive 1.5%
Lecithin 0.19%
Phenoxyethanol 1.6%
Triethanolamine 0.5%
Hydroxyethyl cellulose 1.5%
Talcum powder 0.8%
Polysorbate alcohol -802.2%
Sodium Hyaluronate 2.5%
Glycerol 5.5%
Alchlor 0.09%
Essence 0.07%
Film forming agent 6.3%
Preservative 0.7%
Deionized water surplus.
In a preferred embodiment, the film forming agent is selected from polyvinyl alcohol, dextrin, hydroxymethyl cellulose, carragheen One or more of.
In a preferred embodiment, the preservative is selected from ethylparaben, Nipasol, triclosan, sorbic acid One or more of.
In a preferred embodiment, the skin care compositions is facial mask.
The present invention also provides the preparation methods of the above-mentioned facial mask with antibacterial functions, comprise the steps of:
(1) film forming agent is added in deionized water, solution is then heated to 80~85 DEG C, keep the temperature 20~30 minutes, and Being stirred according to 250~350 revs/min of rate to solution is completely dissolved film forming agent, obtains base soln;
(2) by triethanolamine, hydroxyethyl cellulose, talcum powder, polysorbate alcohol -80, Sodium Hyaluronate, glycerol, trichlorine Change aluminium to be added in step (1) resulting base soln, solution temperature is maintained 65~75 DEG C, according to 250~350 revs/min The rate of clock stirs 25~35 minutes;
(3) step (2) resulting solution is cooled to 40~50 DEG C, Radix et Caulis Opuntiae Dillenii extract, nutgall extractive, ovum is added Phosphatide, Phenoxyethanol, essence, preservative stir 15~20 minutes according to 250~350 revs/min of rates, by mixture PH is adjusted to 6~8, obtains intermediate solution;
(4) step (3) resulting intermediate solution is transferred in mulser, stirring and emulsifying 45 minutes, after the screen to filtrate It is filling, obtain finished product facial mask.
In a preferred embodiment, the Radix et Caulis Opuntiae Dillenii extract, nutgall extractive the preparation method comprises the following steps: by corresponding Vegetable raw material pulverize and sieve, obtained powder is added separately in ethanol solution, is filtered after ultrasonic treatment, by collection Filtrate decompression distillation, obtains corresponding extract.
In a preferred embodiment, the sodium hydroxide solution that concentration is 8% is selected to adjust mixing in the step (3) The pH of object.
In a preferred embodiment, the rate of stirring and emulsifying is 1500~2500 revs/min in the step (4).
The present invention also provides application of the above-mentioned skin care compositions with antibacterial functions in mask product preparation
Below by embodiment, the present invention is furture elucidated.It should be pointed out that the present invention is not intended to be limited to the reality Apply example.
Embodiment 1
The face pack prescription with antibacterial functions of the present embodiment is as follows:
Radix et Caulis Opuntiae Dillenii extract 2.0%
Nutgall extractive 1.5%
Lecithin 0.19%
Phenoxyethanol 1.6%
Triethanolamine 0.5%
Hydroxyethyl cellulose 1.5%
Talcum powder 0.8%
Polysorbate alcohol -802.2%
Sodium Hyaluronate 2.5%
Glycerol 5.5%
Alchlor 0.09%
Essence 0.07%
Film forming agent 6.3%
Preservative 0.7%
Deionized water surplus.
The facial mask with antibacterial functions of the present embodiment is prepared in accordance with the following methods:
(1) film forming agent is added in deionized water, solution is then heated to 80 DEG C, keep the temperature 20 minutes, and according to 250 Rev/min rate solution be stirred be completely dissolved film forming agent, obtain base soln;
(2) by triethanolamine, hydroxyethyl cellulose, talcum powder, polysorbate alcohol -80, Sodium Hyaluronate, glycerol, trichlorine Change aluminium to be added in step (1) resulting base soln, solution temperature is maintained 65 DEG C, is stirred according to 250 revs/min of rate It mixes 25 minutes;
(3) step (2) resulting solution is cooled to 40 DEG C, Radix et Caulis Opuntiae Dillenii extract, nutgall extractive, lecithin is added Rouge, Phenoxyethanol, essence, preservative stir 15 minutes according to 250 revs/min of rates, the sodium hydroxide for being 8% with concentration Solution adjusts the pH of mixture to 6, obtains intermediate solution;
(4) step (3) resulting intermediate solution is transferred in mulser, stirs cream according to 1500 revs/min of rates Change 45 minutes, it is filling after the screen to filtrate, finished product facial mask is obtained, S1 is denoted as.
Embodiment 2
The face pack prescription with antibacterial functions of the present embodiment is as follows:
Radix et Caulis Opuntiae Dillenii extract 2.0%
Nutgall extractive 1.5%
Lecithin 0.19%
Phenoxyethanol 1.6%
Triethanolamine 0.5%
Hydroxyethyl cellulose 1.5%
Talcum powder 0.8%
Polysorbate alcohol -802.2%
Sodium Hyaluronate 2.5%
Glycerol 5.5%
Alchlor 0.09%
Essence 0.07%
Film forming agent 6.3%
Preservative 0.7%
Deionized water surplus.
The facial mask with antibacterial functions of the present embodiment is prepared in accordance with the following methods:
(1) film forming agent is added in deionized water, solution is then heated to 83 DEG C, keep the temperature 25 minutes, and according to 300 Rev/min rate solution be stirred be completely dissolved film forming agent, obtain base soln;
(2) by triethanolamine, hydroxyethyl cellulose, talcum powder, polysorbate alcohol -80, Sodium Hyaluronate, glycerol, trichlorine Change aluminium to be added in step (1) resulting base soln, solution temperature is maintained 70 DEG C, is stirred according to 300 revs/min of rate It mixes 25~35 minutes;
(3) step (2) resulting solution is cooled to 45 DEG C, Radix et Caulis Opuntiae Dillenii extract, nutgall extractive, lecithin is added Rouge, Phenoxyethanol, essence, preservative stir 18 minutes according to 300 revs/min of rates, the sodium hydroxide for being 8% with concentration Solution adjusts the pH of mixture to 7, obtains intermediate solution;
(4) step (3) resulting intermediate solution is transferred in mulser, stirs cream according to 2000 revs/min of rates Change 45 minutes, it is filling after the screen to filtrate, finished product facial mask is obtained, S2 is denoted as.
Embodiment 3
The face pack prescription with antibacterial functions of the present embodiment is as follows:
Radix et Caulis Opuntiae Dillenii extract 2.0%
Nutgall extractive 1.5%
Lecithin 0.19%
Phenoxyethanol 1.6%
Triethanolamine 0.5%
Hydroxyethyl cellulose 1.5%
Talcum powder 0.8%
Polysorbate alcohol -802.2%
Sodium Hyaluronate 2.5%
Glycerol 5.5%
Alchlor 0.09%
Essence 0.07%
Film forming agent 6.3%
Preservative 0.7%
Deionized water surplus.
The facial mask with antibacterial functions of the present embodiment is prepared in accordance with the following methods:
(1) film forming agent is added in deionized water, solution is then heated to 85 DEG C, keep the temperature 30 minutes, and according to 350 Rev/min rate solution be stirred be completely dissolved film forming agent, obtain base soln;
(2) by triethanolamine, hydroxyethyl cellulose, talcum powder, polysorbate alcohol -80, Sodium Hyaluronate, glycerol, trichlorine Change aluminium to be added in step (1) resulting base soln, solution temperature is maintained 75 DEG C, is stirred according to 350 revs/min of rate It mixes 35 minutes;
(3) step (2) resulting solution is cooled to 50 DEG C, Radix et Caulis Opuntiae Dillenii extract, nutgall extractive, lecithin is added Rouge, Phenoxyethanol, essence, preservative stir 20 minutes according to 350 revs/min of rates, the sodium hydroxide for being 8% with concentration Solution adjusts the pH of mixture to 8, obtains intermediate solution;
(4) step (3) resulting intermediate solution is transferred in mulser, stirs cream according to 2500 revs/min of rates Change 45 minutes, it is filling after the screen to filtrate, finished product facial mask is obtained, S3 is denoted as.
Comparative example 1
Substantially with embodiment 2, difference is the formula and preparation method of the facial mask of this comparative example, does not add cactus and mentions Object is taken, final facial mask obtained is denoted as C1.
Comparative example 2
Substantially with embodiment 2, difference is the formula and preparation method of the facial mask of this comparative example, does not add Chinese gall and mentions Object is taken, final facial mask obtained is denoted as C2.
Comparative example 3
Substantially with embodiment 2, difference is the formula and preparation method of the facial mask of this comparative example, does not add lecithin, Final facial mask obtained is denoted as C3.
Comparative example 4
Substantially with embodiment 1, difference is the formula and preparation method of the facial mask of this comparative example, does not add benzene oxygen second Alcohol, final facial mask obtained are denoted as C4.
Performance test
The present embodiment carries out using effect test to facial mask prepared by Examples 1 to 3 and comparative example 1~4.
(1) experimental group: the selection age, the crowd with bacterial dermatitis was test object at 20~40 years old, random point It is 7 groups, every group of 10 people, each group there are no significant in terms of skin health, organism endocrine difference, the 1st~7 group Facial mask C1~C4 that the facial mask S1~S3 and comparative example 1~4 being prepared respectively using Examples 1 to 3 are prepared.
(2) application method of facial mask:
It is primary respectively at morning, evening each face mask film daily, 30 minutes every time.
(3) test result:
Comprehensive score is carried out using investigation point system.Every group of crowd is used continuously 3 months, fills in grade form on probation.Scoring Every using effect total score is 10 points in table, and 9~10 points of expression effects are optimal;6~8 points of expression effects are preferable;4~5 points of expressions Effect is general;3 points of following presentation effects are poor, and every using effect average situation is as shown in table 1:
Table 1
Test result is as shown above, and the facial mask of embodiment S1~S3 group is compared with the facial mask of comparative example C1~C4 group, tool There is effect that is significantly more antibacterial and improving skin health.Illustrate the skin care compositions with antibacterial functions of the invention Material composition between there is the facilitation that mutually cooperates with.
The embodiments described above only express several embodiments of the present invention, and the description thereof is more specific and detailed, but simultaneously It cannot therefore be construed as limiting the scope of the patent.It should be pointed out that coming for those of ordinary skill in the art It says, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to protection of the invention Range.

Claims (10)

1. a kind of skin care compositions with antibacterial functions, which is characterized in that the raw material of the skin care compositions is mentioned by cactus Take object, nutgall extractive, lecithin, Phenoxyethanol, triethanolamine, hydroxyethyl cellulose, talcum powder, polysorbate alcohol -80, Sodium Hyaluronate, glycerol, alchlor, essence, film forming agent, preservative, deionized water composition.
2. the skin care compositions according to claim 1 with antibacterial functions, which is characterized in that the skin care compositions Raw material according to parts by weight, concrete composition are as follows:
Radix et Caulis Opuntiae Dillenii extract 1.5~2.5%
Nutgall extractive 0.8~2.2%
Lecithin 0.08~0.3%
Phenoxyethanol 0.6~3.0%
Triethanolamine 0.2~0.8%
Hydroxyethyl cellulose 0.4~2.5%
Talcum powder 0.08~1.2%
Polysorbate alcohol -80 1.5~3.0%
Sodium Hyaluronate 2.0~3.0%
Glycerol 2.5~8.5%
Alchlor 0.06~0.12%
Essence 0.05~0.09%
Film forming agent 5.0~7.5%
Preservative 0.3~1.0%
Deionized water surplus.
3. the skin care compositions according to claim 2 with antibacterial functions, which is characterized in that the skin care compositions Raw material according to parts by weight, specifically comprises
Radix et Caulis Opuntiae Dillenii extract 2.0%
Nutgall extractive 1.5%
Lecithin 0.19%
Phenoxyethanol 1.6%
Triethanolamine 0.5%
Hydroxyethyl cellulose 1.5%
Talcum powder 0.8%
Polysorbate alcohol -80 2.2%
Sodium Hyaluronate 2.5%
Glycerol 5.5%
Alchlor 0.09%
Essence 0.07%
Film forming agent 6.3%
Preservative 0.7%
Deionized water surplus.
4. described in any item skin care compositions with antibacterial functions according to claim 1~3, which is characterized in that it is described at Film is selected from one or more of polyvinyl alcohol, dextrin, hydroxymethyl cellulose, carragheen.
5. described in any item skin care compositions with antibacterial functions according to claim 1~3, which is characterized in that described anti- Rotten agent is selected from one or more of ethylparaben, Nipasol, triclosan, sorbic acid.
6. described in any item skin care compositions with antibacterial functions according to claim 1~3, which is characterized in that the shield Skin composition is facial mask.
7. a kind of preparation method of the facial mask with antibacterial functions as claimed in claim 6, which is characterized in that by following steps Composition:
(1) film forming agent is added in deionized water, solution is then heated to 80~85 DEG C, keep the temperature 20~30 minutes, and according to 250~350 revs/min of rate, which is stirred solution, is completely dissolved film forming agent, obtains base soln;
(2) by triethanolamine, hydroxyethyl cellulose, talcum powder, polysorbate alcohol -80, Sodium Hyaluronate, glycerol, alchlor It is added in step (1) resulting base soln, solution temperature is maintained 65~75 DEG C, according to 250~350 revs/min Rate stirs 25~35 minutes;
(3) step (2) resulting solution is cooled to 40~50 DEG C, Radix et Caulis Opuntiae Dillenii extract, nutgall extractive, lecithin is added Rouge, Phenoxyethanol, essence, preservative stir 15~20 minutes according to 250~350 revs/min of rates, by the pH of mixture It adjusts to 6~8, obtains intermediate solution;
(4) step (3) resulting intermediate solution is transferred in mulser, it is stirring and emulsifying 45 minutes, filling after the screen to filtrate, Obtain finished product facial mask.
8. the preparation method of the facial mask according to claim 7 with antibacterial functions, which is characterized in that the step (3) The middle pH for selecting the sodium hydroxide solution that concentration is 8% to adjust mixture.
9. the preparation method of the facial mask according to claim 7 with antibacterial functions, which is characterized in that the step (4) The rate of middle stirring and emulsifying is 1500~2500 revs/min.
10. described in any item skin care compositions with antibacterial functions are in mask product preparation according to claim 1~5 Using.
CN201811089059.7A 2018-09-18 2018-09-18 A kind of preparation method of skin care compositions and facial mask with antibacterial functions Pending CN109157489A (en)

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