CN109453056A - A kind of moisture saver mask liquid and preparation method thereof - Google Patents
A kind of moisture saver mask liquid and preparation method thereof Download PDFInfo
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Abstract
The invention proposes a kind of moisture saver mask liquid, are prepared by following raw material according to parts by weight: 10-15 parts of casein antibacterial peptide, 50-70 parts of ceramide, 10-20 parts of 2-pyrrolidone-5-carboxylic acid, 10-20 parts of lactic acid, 30-50 parts of konjaku glucomannan, 1-5 parts of antioxidant, 1-3 parts of diethanol amine, 0.1-1 parts of EDETATE SODIUM, 1-2 parts of carbomer, 1-5 parts of plants essential oil, 10-15 parts of Chinese medicine moisturizing extract and 70-100 parts of deionized water.Moisture saver mask liquid prepared by the present invention has anti-inflammatory effect, anti-cell splitting action and itching-relieving action, can be used for healthy skin, can prevent skin disease, it may also be used for treatment skin disease has broad application prospects.
Description
Technical field
The present invention relates to cosmetic technical fields, and in particular to a kind of moisture saver mask liquid.
Background technique
The fundamental of healthy skin is smooth, full, high resilience.With the increase at age, in keratoderma
Moisturizing factor content gradually decreases, and the hydratability of skin is caused to decline, and shows as dry skin, corrugation, relaxation, aging is presented
Appearance.Skin water content gradually decrease be this aged appearance one of pathomechanism.The major reason of dry skin be because
It is lost to play the lipid of water lock moisture-keeping function in space between cells, cuticula moisture is reduced, and skin barrier is impaired.When cuticula
Water content is lower than 10%, and crack occur in dry skin, furfur, imbricate keratinocyte layer arranged in parallel.Therefore, skin is maintained
Water content, guarantee cuticula in moisture content be maintain skin emolliency and elasticity key factor, and improve looks most
Important basic means.
Facial mask is a kind of cosmetics and skincare product applied on the face, apply after by 15-25 minutes, will be formed one layer it is tight in face
On film, so referred to as facial mask.It integrates three kinds of cleaning, nursing, nutrition skin of face functions.Facial mask covers skin table
Face, air-isolation infiltrate, have softened cuticula, increase local skin temperature, pore and sweat gland mouth are expanded, to promote skin
The blood circulation of skin promotes the infiltration of active constituent in facial mask, promotes sweat gland secretion and metabolism, makes in the oxygen content of skin
It rises, is conducive to skin and excludes the product of epidermal cell metabolism and the oil substances of accumulation, the moisture in facial mask penetrates into flesh
The cuticula of skin epidermis, skin become soft, increase elasticity.Skin is naturally bright flexible, and aerobic color is presented.Facial mask type is numerous
More, effect is also different.According to the difference of production raw material, moisturizing, whitening, nti-freckle and other functional masks can be divided into.As relaxed
Slow skin, excludes skin toxin, improves skin quality, becoming brighter glossy using the rear colour of skin enhancing skin metabolic detoxification effect,
Improve the wax yellow, obscure of the colour of skin, dry puzzlement etc..It can also enhance or increase other effects, such as elastic force moisturizing compact mentions
Drawing, skin-moisturizing, skin, whitening despeckle, wrinkle resistant anti-aging, anti-inflammatory toxin expelling, prevention and treatment dark sore etc..Initial stage facial mask mostly uses greatly chemical synthesis
Product are as base stock, with the improvement of functional additive in formula, consumer to it is purer extraction, it is more natural, safer, more effective
Mask product have further pursuit.Face pack prescription composition uses natural plant extraction composition, active ingredient, day as far as possible
Right mineral composition etc..
State Intellectual Property Office discloses one entitled " a kind of moisture saver mask liquid ", and number of patent application is
201110103296.6 patent of invention, it is with deionized water, D-sorbite, Hydrolyzed Collagen, vitamin E, alginic acid
Potassium, hyaluronic acid, bi-imidazolidinyl urea and mulberry root extract are a kind of facial mask of raw material preparation, and there are some for the patent of the disclosure
In place of shortcomings and deficiencies: bi-imidazolidinyl urea is a kind of preservative being mainly used in cosmetics, it is to pass through slow release
Formaldehyde reaches corrosion-resistant purpose, its general additive amount is no more than 0.3%, and the additive amount of the displosure formula is 1-2%,
Therefore prepared product is that there are potentially hazardous to human body；The molecular weight of used Hydrolyzed Collagen does not explain；
The product efficacy of disclosed method preparation does not explain.
State Intellectual Property Office authorizes one entitled " collagen wet-retaining face mask liquid and preparation method thereof ", patent application
Number be 200610020676.2 patent of invention, it is with porcine collagen, cellulose derivative, starch, moisturizer and crosslinking
Agent is a kind of facial mask of raw material preparation, and collagen is a kind of good cosmetic material, it, which has, moisturizes the skin, delays to decline
Always, beauty, wrinkle-chasing and other effects, but the degree that collagen is absorbed by the body is critically important index, the collagen egg of small-molecular-weight
White (general requirement≤1000D) is easy to be rapidly absorbed by a human, and porcine collagen prepared by the patent of the disclosure does not have its molecular weight
It is illustrated.In addition, the patent of the disclosure is not explained with regard to the effect of product, with the method converted products of the displosure, there is also works
In place of the deficiencies of skill step is more, complicated for operation.
For the deficiency of existing Moisturizer, exploitation is a safely and effectively, does not stimulate naturally, the guarantor that pure plant is extracted
Wet facial mask liquid will will receive liking for numerous female friends.
Summary of the invention
In order to solve the above technical problems, the present invention provides a kind of moisture saver mask liquid and preparation method thereof, and purpose exists
In, a kind of moisture saver mask liquid is provided, by add Chinese medicine moisturizing extract component, do not stimulate naturally, moistening effect is good, facilitates skin
Skin is protected in the reparation and holding of skin natural barrier, is enhanced humidity of skin, is kept the glossy water of skin tender.
The present invention provides a kind of moisture saver mask liquid, is prepared from the following materials: casein antibacterial peptide, ceramide, pyrrole
Pyrrolidone carboxylic acid, lactic acid, konjaku glucomannan, antioxidant, diethanol amine, EDETATE SODIUM, carbomer, plants essential oil, Chinese medicine are protected
Wet extract and deionized water.
As further improvement of the invention, it is prepared by following raw material according to parts by weight: casein antibacterial peptide 10-15
Part, 50-70 parts of ceramide, 10-20 parts of 2-pyrrolidone-5-carboxylic acid, 10-20 parts of lactic acid, 30-50 parts of konjaku glucomannan, antioxidant
1-5 parts, 1-3 parts of diethanol amine, 0.1-1 parts of EDETATE SODIUM, 1-2 parts of carbomer, 1-5 parts of plants essential oil, Chinese medicine moisturizing extract
10-15 parts and deionized water 70-100 parts.
As further improvement of the invention, it is prepared by following raw material according to parts by weight: casein antibacterial peptide 12-14
Part, 55-65 parts of ceramide, 12-17 parts of 2-pyrrolidone-5-carboxylic acid, 14-17 parts of lactic acid, 35-47 parts of konjaku glucomannan, antioxidant
2-4 parts, 2-3 parts of diethanol amine, 0.2-0.6 parts of EDETATE SODIUM, 1.2-1.8 parts of carbomer, 2-4 parts of plants essential oil, Chinese medicine moisturizing
12-14 parts and deionized water 80-90 parts of extract.
As further improvement of the invention, it is prepared by following raw material according to parts by weight: 13 parts of casein antibacterial peptide,
2 parts of Cer AP, 16 parts of 2-pyrrolidone-5-carboxylic acid, 15 parts of lactic acid, 42 parts of konjaku glucomannan, 3 parts of antioxidant, diethanol amine 2.5
Part, 0.4 part of EDETATE SODIUM, 1.5 parts of carbomer, 3 parts of plants essential oil, 13 parts of Chinese medicine moisturizing extract and 87 parts of deionized water.
As further improvement of the invention, the Chinese medicine moisturizing extract is prepared in accordance with the following methods:
(1) 25 parts of gynostemma pentaphylla, 25 parts of Poria cocos, 20 parts of Radix Angelicae Sinensis, 20 parts of Siraitia grosvenorii, 15 parts of lily, red is weighed according to parts by weight
10 parts of red-spotted stonecrop, 5 parts of honey and 5 parts of the bletilla striata, will other Chinese medicines are dry in addition to honey, beat powder, obtain traditional Chinese medicine powder；
(2) extractor is added in traditional Chinese medicine powder, deionized water is added by solid-to-liquid ratio 1:(20-40), be heated to 100 DEG C of boilings,
After return stirring extracts 5h, filtering, filter residue discards after extracting 1 time repeatedly, combined extract, and being concentrated into density is 1-1.5g/
Cm3 is added honey, stirs evenly, obtain Chinese medicine moisturizing extract.
As further improvement of the invention, the speed of agitator is 300-500r/min.
As further improvement of the invention, the antioxidant is selected from 2,6- three-level butyl -4- methylphenol, bis- (3,5-
Three-level butyl -4- hydroxy phenyl) it is thioether, four (β-(3,5- three-level butyl -4- hydroxy phenyl) propionic acid) pentaerythritol esters, three pungent
Ester, three last of the ten Heavenly stems esters, three (Lauryl Alcohol) esters, one in three (16 carbon alcohol) ester, potassium sorbate, sorbic acid, sodium lactate and tea polyphenols
Kind is several.
As further improvement of the invention, the plants essential oil is selected from lavender oil, lemon oil, bergamot oil, cloves
One or more of oil, peppermint oil, cinnamon oil, attar of rose, rosemary oil and thyme linaloe oil.
The present invention further protects a kind of preparation method of above-mentioned moisture saver mask liquid, which is characterized in that in accordance with the following methods
Preparation:
(1) ceramide, 2-pyrrolidone-5-carboxylic acid, lactic acid, konjaku glucomannan and Chinese medicine moisturizing extract are added and are reacted
Device, moderate-speed mixer obtain viscous fluid A to being uniformly mixed；
(2) antioxidant, diethanol amine, EDETATE SODIUM and carbomer are uniformly mixed, are added in viscous fluid A, side original speed is stirred
Mix side be added 1/5 deionized water, be warming up to 60 DEG C, continue to stir, after 30min be added 1/5 deionized water, wait go from
It after sub- water adds, after high-speed stirred 20min, is cooled to room temperature, mixing speed is reduced to middling speed, plants essential oil and junket egg is added
White antibacterial peptide obtains moisture saver mask liquid after mixing evenly.
As further improvement of the invention, the moderate-speed mixer revolving speed is 300-500r/min, and the high-speed stirred turns
Speed is 500-700r/min.
The invention has the following beneficial effects:
1, present invention preparation is added to Chinese medicine moisturizing extract component, does not stimulate naturally, moistening effect is good, facilitates skin day
The reparation and holding of right barrier, protect skin, enhance humidity of skin, keep the glossy water of skin tender；
2, the present invention is added to ceramide, 2-pyrrolidone-5-carboxylic acid, lactic acid, their moisture-keeping functions are much better than glycerol, and
And not that sticky sense of glycerol, enhance the comfort of moisture saver mask liquid, so that the facial more water applied after facial mask is tender, moistens
It is sliding, have the function of good reparation epidermal barrier, there is fabulous moisture retention, safety, water solubility and permeability, there are also anti-
Inflammation, anti-cell division and antipruritic effect；
3, moisture saver mask liquid prepared by the present invention has anti-inflammatory effect, anti-cell splitting action and itching-relieving action, Ke Yiyong
In healthy skin, skin disease can be prevented, it may also be used for treatment skin disease.
Detailed description of the invention
Fig. 1 is the preparation technology figure of moisture saver mask liquid.
Specific embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the invention is clearly and completely described,
Obviously, the embodiment described is the embodiment of part of representative of the invention, rather than whole embodiments, this field are general
Other all embodiments obtained belong to protection of the invention to logical technical staff without making creative work
Range.
Embodiment 1
Raw material forms (parts by weight): 10 parts of casein antibacterial peptide, 50 parts of ceramide, 10 parts of 2-pyrrolidone-5-carboxylic acid, lactic acid
10 parts, 30 parts of konjaku glucomannan, 1 part of three monooctyl ester, 1 part of diethanol amine, 0.1 part of EDETATE SODIUM, 1 part of carbomer, lemon oil 1
Part, 10 parts of Chinese medicine moisturizing extract and 70 parts of deionized water；
The Chinese medicine moisturizing extract is prepared in accordance with the following methods:
(1) 25 parts of gynostemma pentaphylla, 25 parts of Poria cocos, 20 parts of Radix Angelicae Sinensis, 20 parts of Siraitia grosvenorii, 15 parts of lily, red is weighed according to parts by weight
10 parts of red-spotted stonecrop, 5 parts of honey and 5 parts of the bletilla striata, will other Chinese medicines are dry in addition to honey, beat powder, obtain traditional Chinese medicine powder；
(2) extractor is added in traditional Chinese medicine powder, deionized water is added by solid-to-liquid ratio 1:20, be heated to 100 DEG C of boilings, reflux is stirred
It mixes and extracts 5h, speed of agitator 300r/min, filtering, filter residue discards after extracting 1 time repeatedly, and combined extract is concentrated into density
For 1.0g/cm3, honey is added, stirs evenly, obtains Chinese medicine moisturizing extract.
The preparation method of the moisture saver mask liquid, which is characterized in that prepare in accordance with the following methods:
(1) ceramide, 2-pyrrolidone-5-carboxylic acid, lactic acid, konjaku glucomannan and Chinese medicine moisturizing extract are added and are reacted
Device, for moderate-speed mixer to being uniformly mixed, speed of agitator 300r/min obtains viscous fluid A；
(2) three monooctyl esters, diethanol amine, EDETATE SODIUM and carbomer are uniformly mixed, are added in viscous fluid A, side original speed is stirred
Mix side be added 1/5 deionized water, be warming up to 60 DEG C, continue to stir, after 30min be added 1/5 deionized water, wait go from
After sub- water adds, high-speed stirred 20min, speed of agitator 500r/min are cooled to room temperature, mixing speed are reduced to middling speed,
Speed of agitator is 300r/min, and lemon oil is added and casein antibacterial peptide obtains moisture saver mask liquid after mixing evenly.
Embodiment 2
Raw material forms (parts by weight): 15 parts of casein antibacterial peptide, 70 parts of ceramide, 20 parts of 2-pyrrolidone-5-carboxylic acid, lactic acid
20 parts, 50 parts of konjaku glucomannan, 5 parts of tea polyphenols, 3 parts of diethanol amine, 1 part of EDETATE SODIUM, 2 parts of carbomer, 5 parts of attar of rose,
15 parts and 100 parts of deionized water of Chinese medicine moisturizing extract；
The Chinese medicine moisturizing extract is prepared in accordance with the following methods:
(1) 25 parts of gynostemma pentaphylla, 25 parts of Poria cocos, 20 parts of Radix Angelicae Sinensis, 20 parts of Siraitia grosvenorii, 15 parts of lily, red is weighed according to parts by weight
10 parts of red-spotted stonecrop, 5 parts of honey and 5 parts of the bletilla striata, will other Chinese medicines are dry in addition to honey, beat powder, obtain traditional Chinese medicine powder；
(2) extractor is added in traditional Chinese medicine powder, deionized water is added by solid-to-liquid ratio 1:40, be heated to 100 DEG C of boilings, reflux is stirred
It mixes and extracts 5h, speed of agitator 500r/min, filtering, filter residue discards after extracting 1 time repeatedly, and combined extract is concentrated into density
For 1.5g/cm3, honey is added, stirs evenly, obtains Chinese medicine moisturizing extract.
The preparation method of the moisture saver mask liquid, which is characterized in that prepare in accordance with the following methods:
(1) ceramide, 2-pyrrolidone-5-carboxylic acid, lactic acid, konjaku glucomannan and Chinese medicine moisturizing extract are added and are reacted
Device, for moderate-speed mixer to being uniformly mixed, speed of agitator 500r/min obtains viscous fluid A；
(2) tea polyphenols, diethanol amine, EDETATE SODIUM and carbomer are uniformly mixed, are added in viscous fluid A, side original speed is stirred
Mix side be added 1/5 deionized water, be warming up to 60 DEG C, continue to stir, after 30min be added 1/5 deionized water, wait go from
After sub- water adds, high-speed stirred 20min, speed of agitator 700r/min are cooled to room temperature, mixing speed are reduced to middling speed,
Speed of agitator is 500r/min, and attar of rose is added and casein antibacterial peptide obtains moisture saver mask liquid after mixing evenly.
Embodiment 3
Raw material forms (parts by weight): 12 parts of casein antibacterial peptide, 55 parts of ceramide, 12 parts of 2-pyrrolidone-5-carboxylic acid, lactic acid
14 parts, 35 parts of konjaku glucomannan, 2 parts of sorbic acid, 2 parts of diethanol amine, 0.2 part of EDETATE SODIUM, 1.2 parts of carbomer, rosemary
2 parts of oil, 12 parts of Chinese medicine moisturizing extract and 80 parts of deionized water；
The Chinese medicine moisturizing extract is prepared in accordance with the following methods:
(1) 25 parts of gynostemma pentaphylla, 25 parts of Poria cocos, 20 parts of Radix Angelicae Sinensis, 20 parts of Siraitia grosvenorii, 15 parts of lily, red is weighed according to parts by weight
10 parts of red-spotted stonecrop, 5 parts of honey and 5 parts of the bletilla striata, will other Chinese medicines are dry in addition to honey, beat powder, obtain traditional Chinese medicine powder；
(2) extractor is added in traditional Chinese medicine powder, deionized water is added by solid-to-liquid ratio 1:25, be heated to 100 DEG C of boilings, reflux is stirred
It mixes and extracts 5h, speed of agitator 350r/min, filtering, filter residue discards after extracting 1 time repeatedly, and combined extract is concentrated into density
For 1.2g/cm3, honey is added, stirs evenly, obtains Chinese medicine moisturizing extract.
The preparation method of the moisture saver mask liquid, which is characterized in that prepare in accordance with the following methods:
(1) ceramide, 2-pyrrolidone-5-carboxylic acid, lactic acid, konjaku glucomannan and Chinese medicine moisturizing extract are added and are reacted
Device, for moderate-speed mixer to being uniformly mixed, speed of agitator 350r/min obtains viscous fluid A；
(2) sorbic acid, diethanol amine, EDETATE SODIUM and carbomer are uniformly mixed, are added in viscous fluid A, side original speed is stirred
Mix side be added 1/5 deionized water, be warming up to 60 DEG C, continue to stir, after 30min be added 1/5 deionized water, wait go from
After sub- water adds, high-speed stirred 20min, speed of agitator 550r/min are cooled to room temperature, mixing speed are reduced to middling speed,
Speed of agitator is 350r/min, and rosemary oil is added and casein antibacterial peptide obtains moisture saver mask liquid after mixing evenly.
Embodiment 4
Raw material forms (parts by weight): 14 parts of casein antibacterial peptide, 5 parts of Cer AP, 17 parts of 2-pyrrolidone-5-carboxylic acid, lactic acid
17 parts, 47 parts of konjaku glucomannan, 4 parts of sodium lactate, 3 parts of diethanol amine, 0.6 part of EDETATE SODIUM, 1.8 parts of carbomer, bergamot
4 parts of oil, 14 parts of Chinese medicine moisturizing extract and 90 parts of deionized water；
The Chinese medicine moisturizing extract is prepared in accordance with the following methods:
(1) 25 parts of gynostemma pentaphylla, 25 parts of Poria cocos, 20 parts of Radix Angelicae Sinensis, 20 parts of Siraitia grosvenorii, 15 parts of lily, red is weighed according to parts by weight
10 parts of red-spotted stonecrop, 5 parts of honey and 5 parts of the bletilla striata, will other Chinese medicines are dry in addition to honey, beat powder, obtain traditional Chinese medicine powder；
(2) extractor is added in traditional Chinese medicine powder, deionized water is added by solid-to-liquid ratio 1:35, be heated to 100 DEG C of boilings, reflux is stirred
It mixes and extracts 5h, speed of agitator 450r/min, filtering, filter residue discards after extracting 1 time repeatedly, and combined extract is concentrated into density
For 1.4g/cm3, honey is added, stirs evenly, obtains Chinese medicine moisturizing extract.
The preparation method of the moisture saver mask liquid, which is characterized in that prepare in accordance with the following methods:
(1) ceramide, 2-pyrrolidone-5-carboxylic acid, lactic acid, konjaku glucomannan and Chinese medicine moisturizing extract are added and are reacted
Device, for moderate-speed mixer to being uniformly mixed, speed of agitator 450r/min obtains viscous fluid A；
(2) sodium lactate, diethanol amine, EDETATE SODIUM and carbomer are uniformly mixed, are added in viscous fluid A, side original speed is stirred
Mix side be added 1/5 deionized water, be warming up to 60 DEG C, continue to stir, after 30min be added 1/5 deionized water, wait go from
After sub- water adds, high-speed stirred 20min, speed of agitator 650r/min are cooled to room temperature, mixing speed are reduced to middling speed,
Speed of agitator is 450r/min, and bergamot oil is added and casein antibacterial peptide obtains moisture saver mask liquid after mixing evenly.
Embodiment 5
Raw material forms (parts by weight): 13 parts of casein antibacterial peptide, 2 parts of Cer AP, 16 parts of 2-pyrrolidone-5-carboxylic acid, lactic acid
15 parts, 42 parts of konjaku glucomannan, three 3 parts of (Lauryl Alcohol) esters, 2.5 parts of diethanol amine, 0.4 part of EDETATE SODIUM, carbomer 1.5
Part, 3 parts of caryophyllus oil, 13 parts of Chinese medicine moisturizing extract and 87 parts of deionized water；
The Chinese medicine moisturizing extract is prepared in accordance with the following methods:
(1) 25 parts of gynostemma pentaphylla, 25 parts of Poria cocos, 20 parts of Radix Angelicae Sinensis, 20 parts of Siraitia grosvenorii, 15 parts of lily, red is weighed according to parts by weight
10 parts of red-spotted stonecrop, 5 parts of honey and 5 parts of the bletilla striata, will other Chinese medicines are dry in addition to honey, beat powder, obtain traditional Chinese medicine powder；
(2) extractor is added in traditional Chinese medicine powder, deionized water is added by solid-to-liquid ratio 1:30, be heated to 100 DEG C of boilings, reflux is stirred
It mixes and extracts 5h, speed of agitator 400r/min, filtering, filter residue discards after extracting 1 time repeatedly, and combined extract is concentrated into density
For 1.3g/cm3, honey is added, stirs evenly, obtains Chinese medicine moisturizing extract.
The preparation method of the moisture saver mask liquid, which is characterized in that prepare in accordance with the following methods:
(1) ceramide, 2-pyrrolidone-5-carboxylic acid, lactic acid, konjaku glucomannan and Chinese medicine moisturizing extract are added and are reacted
Device, for moderate-speed mixer to being uniformly mixed, speed of agitator 400r/min obtains viscous fluid A；
(2) three (Lauryl Alcohol) esters, diethanol amine, EDETATE SODIUM and carbomer are uniformly mixed, are added in viscous fluid A,
1/5 deionized water is added in former speed stirring, is warming up to 60 DEG C, continues to stir, 1/5 deionization is added after 30min
Water, after deionized water adds, high-speed stirred 20min, speed of agitator 600r/min are cooled to room temperature, mixing speed are dropped
Down to middling speed, speed of agitator 400r/min, is added caryophyllus oil and casein antibacterial peptide obtains moisture saver mask after mixing evenly
Liquid.
1 patch test of test example
1. tested material: moisture saver mask liquid prepared by embodiment 5
2. negative control: deionized water
3. subject: totally 30 people, male 0 people, 30 people of female the age 21-48 years old, meet subject and volunteer inclusion criteria.
4. patch method: selecting qualified spot tester, with enclosed patch test method, about by tested material and negative control
0.020mL-0.025mL (semifluid) is dripped in spot tester, and external application special adhesive tape is pasted on subject back, removes after 24 hours
Tested material, observation dermoreaction in 0.5,24,48 hour after removing respectively, by skin in " cosmetics health specification " (version in 2007)
Reaction grade scale records its result.Test result is shown in Table 1:
1 human skin patch test result of table
Human skin patch test result is shown: 0 there is skin adverse reaction in 30 people；Illustrate moisturizing face of the invention
Film liquid uses safe.
The experiment of 2 moistening effect of test example
1. sample sets: moisture saver mask liquid prepared by embodiment 5
2. control group: commercially available moisture saver mask liquid
3. subject: totally 30 people, male 0 people, 30 people of female the age 30-55 years old, meet subject and volunteer inclusion criteria health shape
Condition.
4. selecting tested position: because in contrast four limbs do not have individual differences, being selected as tested position, choose examinee
Left and right inner forearm 3cm × 3cm area as tested area.Trial target is covered in left and right inner forearm at random.
5. test condition is in 20 ± 2 DEG C of room temperature hereinafter, 50 ± 5% or less relative humidity (RH).
6. instrument and reagent: Corneometer is a set of, Hygrothermograph one.
7. short term tests: when determining the moistening effect intensity of moisturizing cosmetic, be suitable for make to terminate in the short time it is primary
Test is sticked, i.e. performance of keeping humidity is tested.It is sticked in measurement cuticula moisture content test with moisture saver mask liquid short-term 1 time plus life
Object cuticlar water load test, can parse moistening effect.This law is mainly used for selecting to determine that it is when moisturizer in formula
No to have moisture retention, moisturizer determines optimum concentration compared with matrix.Before facial mask sticks, the cuticlar water at tested position is measured
Divide content.Sample is sticked with latex finger cot；Measurement trial target sticks after 15min immediately, after 15,30,45,60,75,90 minutes
Cuticula moisture content；The cuticula moisture content for respectively being tested position takes the average value of 5 measured values；Measurement result is shown in Table 1.
The raising degree of skin hydration degree=(skin hydration degree (when test)-skin hydration degree (before sticking))/skin water
Right (before sticking) × 100%
The skin hydration degree of 1 different time of table
| Group | Before sticking | 0min | 15min | 30min | 45min | 60min | 75min | 90min |
| Embodiment 5 | 25.7 | 90.5 | 7.3 | 65.2 | 59.7 | 54.2 | 50.5 | 48.1 |
| Control group | 26.9 | 89.2 | 60.4 | 51.7 | 46.5 | 40.3 | 37.8 | 35.4 |
As can be seen from Table 1, facial mask is significantly improved to the hydrauture of skin, especially after use 0-75min
In time range, with the extension of time, moistening effect decreases, but the 90min skin hydration degree within the testing time
It is still significantly improved, higher than the skin hydration degree before sticking, it is bright to illustrate that the moisture saver mask liquid of the preparation of the embodiment of the present invention 5 has
The raising degree of aobvious moistening effect, skin hydration degree is up to 252%.
8. long-term effect is tested: being suitable for making to observe organism angle for a long time for the direct moistening effect of moisturizing cosmetic
The long-time services such as the metamorphosis of influence and skin surface that the seasonal variety of matter layer is given test.Before facial mask sticks, measurement
The cuticula moisture content at tested position.Trial target is sticked with latex finger cot；Tested position before bedtime within first day weekly
Stick facial mask.Application time is 6 weeks.Before measurement cosmetics stick respectively, stick latter 1 week, 2 weeks, 3 weeks, 4 weeks, 5 weeks and 6 weeks
Cuticula moisture content；The cuticula moisture content for respectively being tested position takes 3 measurements, takes its average value；Measurement result is shown in Table 2.
The skin hydration degree of 2 different time of table
| Group | Before sticking | 1w | 2w | 3w | 4w | 5w | 6w |
| Embodiment 5 | 27.4 | 35.2 | 36.7 | 37.3 | 38.2 | 39.5 | 40.2 |
| Control group | 27.8 | 29.0 | 29.5 | 28.5 | 27.9 | 30.2 | 29.3 |
As can be seen from Table 2, facial mask of the present invention is significantly improved to the hydrauture of skin, final raising skin
Up to 46.7%, and within the testing time, (6 weeks) skin hydration degree is constantly in the increase stage to hydrauture, illustrates that the facial mask has
There is apparent moistening effect, the raising degree of skin hydration degree is up to 181%.And the commercially available moisture saver mask of control group,
It is found in long-term experiment, moistening effect is not obvious.
Human skin patch is carried out according to the above method using the obtained moisture saver mask liquid of embodiment 1-4 and moisturizing is imitated
Fruit test, obtains the test result similar with above-mentioned test result.
Those skilled in the art is not under conditions of departing from the spirit and scope of the present invention that claims determine, also
Various modifications can be carried out to the above content.Therefore the scope of the present invention is not limited in above explanation, but by
The range of claims determines.
Claims (10)
1. a kind of moisture saver mask liquid, which is characterized in that be prepared from the following materials: casein antibacterial peptide, ceramide, pyrroles
Alkanone carboxylic acid, lactic acid, konjaku glucomannan, antioxidant, diethanol amine, EDETATE SODIUM, carbomer, plants essential oil, Chinese medicine moisturizing
Extract and deionized water.
2. a kind of moisture saver mask liquid according to claim 1, which is characterized in that by following raw material according to parts by weight prepare and
At: 10-15 parts of casein antibacterial peptide, 50-70 parts of ceramide, 10-20 parts of 2-pyrrolidone-5-carboxylic acid, 10-20 parts of lactic acid, konjaku Portugal
Sweet glycan 30-50 parts, 1-5 parts of antioxidant, 1-3 parts of diethanol amine, 0.1-1 parts of EDETATE SODIUM, 1-2 parts of carbomer, plants essential oil
1-5 parts, 10-15 parts of Chinese medicine moisturizing extract and 70-100 parts of deionized water.
3. a kind of moisture saver mask liquid according to claim 2, which is characterized in that by following raw material according to parts by weight prepare and
At: 12-14 parts of casein antibacterial peptide, 55-65 parts of ceramide, 12-17 parts of 2-pyrrolidone-5-carboxylic acid, 14-17 parts of lactic acid, konjaku Portugal
Sweet glycan 35-47 parts, 2-4 parts of antioxidant, 2-3 parts of diethanol amine, 0.2-0.6 parts of EDETATE SODIUM, 1.2-1.8 parts of carbomer, plant
2-4 parts of object essential oil, 12-14 parts of Chinese medicine moisturizing extract and 80-90 parts of deionized water.
4. a kind of moisture saver mask liquid according to claim 3, which is characterized in that by following raw material according to parts by weight prepare and
At: 13 parts of casein antibacterial peptide, 2 parts of Cer AP, 16 parts of 2-pyrrolidone-5-carboxylic acid, 15 parts of lactic acid, 42 parts of konjaku glucomannan,
3 parts of antioxidant, 2.5 parts of diethanol amine, 0.4 part of EDETATE SODIUM, 1.5 parts of carbomer, 3 parts of plants essential oil, Chinese medicine moisturizing extract
13 parts and 87 parts of deionized water.
5. a kind of moisture saver mask liquid according to claim 1, which is characterized in that the Chinese medicine moisturizing extract is according to lower section
Method is prepared:
(1) 25 parts of gynostemma pentaphylla, 25 parts of Poria cocos, 20 parts of Radix Angelicae Sinensis, 20 parts of Siraitia grosvenorii, 15 parts of lily, root of kirilow rhodiola are weighed according to parts by weight
10 parts, 5 parts of honey and 5 parts of the bletilla striata, will other Chinese medicines are dry in addition to honey, beat powder, obtain traditional Chinese medicine powder；
(2) extractor is added in traditional Chinese medicine powder, deionized water is added by solid-to-liquid ratio 1:(20-40), be heated to 100 DEG C of boilings, reflux
After 5h is extracted in stirring, filtering, filter residue discards after extracting 1 time repeatedly, combined extract, and being concentrated into density is 1-1.5g/cm3, adds
Enter honey, stir evenly, obtains Chinese medicine moisturizing extract.
6. a kind of moisture saver mask liquid according to claim 5, which is characterized in that the speed of agitator is 300-500r/min.
7. a kind of moisture saver mask liquid according to claim 1, which is characterized in that the antioxidant is selected from 2,6- three-level butyl-
4- methylphenol, bis- (3,5- three-level butyl -4- hydroxy phenyl) thioethers, four (β-(3,5- three-level butyl -4- hydroxy phenyl) third
Acid) pentaerythritol ester, three monooctyl esters, three last of the ten Heavenly stems esters, three (Lauryl Alcohol) esters, three (16 carbon alcohol) esters, potassium sorbate, sorbic acid, cream
One or more of sour sodium and tea polyphenols.
8. a kind of moisture saver mask liquid according to claim 1, which is characterized in that the plants essential oil is selected from lavender oil, lemon
One or more of lemon oil, bergamot oil, caryophyllus oil, peppermint oil, cinnamon oil, attar of rose, rosemary oil and thyme linaloe oil.
9. a kind of preparation method of moisture saver mask liquid described in -8 any claims according to claim 1, which is characterized in that according to
Following methods preparation:
(1) reactor is added in ceramide, 2-pyrrolidone-5-carboxylic acid, lactic acid, konjaku glucomannan and Chinese medicine moisturizing extract, in
Speed stirring obtains viscous fluid A to being uniformly mixed；
(2) antioxidant, diethanol amine, EDETATE SODIUM and carbomer are uniformly mixed, are added in viscous fluid A, in former speed stirring
1/5 deionized water is added, is warming up to 60 DEG C, continues to stir, 1/5 deionized water is added after 30min, to deionized water
It after adding, after high-speed stirred 20min, is cooled to room temperature, mixing speed is reduced to middling speed, plants essential oil is added and casein is anti-
Bacterium peptide obtains moisture saver mask liquid after mixing evenly.
10. preparation method according to claim 9, which is characterized in that the moderate-speed mixer revolving speed is 300-500r/min, institute
Stating high-speed stirred revolving speed is 500-700r/min.
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