CN104027271B - Emulsion and preparation method thereof - Google Patents

Emulsion and preparation method thereof Download PDF

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Publication number
CN104027271B
CN104027271B CN201410272335.9A CN201410272335A CN104027271B CN 104027271 B CN104027271 B CN 104027271B CN 201410272335 A CN201410272335 A CN 201410272335A CN 104027271 B CN104027271 B CN 104027271B
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skin
extract
emulsion
wrinkle
water
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CN201410272335.9A
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Chinese (zh)
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CN104027271A (en
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楼彪
施金金
卢正君
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娇时日化(杭州)股份有限公司
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Abstract

nullThe invention discloses a kind of emulsion and preparation method,Not enough for existing emulsion,Utilize a kind of its technology of emulsion resisting skin wrinkle energy delaying skin aging of effective ingredient research and development of plant extract,The present invention program is mainly by Folium Camelliae sinensis extract,Cortex Mori extract,Algae extract,Radix Et Caulis Acanthopanacis Senticosi extract,Papaya extract,Flos Rosae Rugosae extract,Water,Ethylhexyl palmitate,Glycerol,Isononyl isononanoate,Caprylic/capric triglyceride,Butyrospermum parkii fruit fat,Polydimethylsiloxane,Cetearyl alcohol,1,2 pentanediols,Methyl sesquistearate,PEG 20 methyl sesquistearate,Glyceryl stearate,Carbomer,Arginine,Xanthan gum,1,2 hexanediol,Ethohexadiol and hyaluronate sodium composition,Effective ingredient is deep into bottom cell,Increase the synthesis of collagen protein,Increase water humidity and degree of compacting,Significantly reduce wrinkle of skin rapidly,Skin is made to recover young elastic,Shine young honorable,The problem that skin ageing occurs in prevention.

Description

Emulsion and preparation method thereof

Technical field

The present invention relates to a kind of skin care item, more specifically, it relates to a kind of emulsion.

Background technology

Emulsion is a kind of liquid frost class cosmetics, and emulsion has good skin moistening effect, also has moistening effect, the suitableeest Closing the spring being dried, season in autumn two uses, if skin is neutral, it is also possible to use in winter.When spring and autumn uses, except skin moistening is protected Outside wet effect, it is also possible to the weather that the isolation external world is dried, prevent skin water loss too fast, it is to avoid skin is dry and cracked, peeling, be dry When dry season goes out must skin care item.

With advancing age, the Skin Cell 26S Proteasome Structure and Function of people has a very large change, as thinning in epidermis, corium Fiber tearing, lipoatrophy, sweat gland, smegma reduce, and then shine into cutis laxa, follow the string, and add existing Exposing to the weather and overworked etc. former in radiation that environmental pollution in generation life, all day are brought in the face of computer, work Because being all further exacerbated by the aging degree of skin.

From the biological mechanism analysis of slow down aging: if to reach to resist the old and feeble purpose of skin, it is necessary to prevent Collagen protein broken with run off, the synthesis of stimulation collagen is to be formed anti-wrinkle and degree of compacting and elastic reduction; Prevent the loss of mucopolysaccharide;Prevent the loss of lipid;Prevent the minimizing of moisture;Suppression melanosome transfer, promotes melanocyte Degraded, improves bioavailability, but the anti-wrinkle product trophism occurred on market today is not enough, and with the addition of substantial amounts of mineral The artificial chemical agent such as oil, preservative, essence, pigment, using effect is inconspicuous, and safety cannot guarantee that.

Summary of the invention

The deficiency existed for prior art, it is an object of the invention to provide a kind of opposing skin wrinkle and can delay flesh Emulsion that skin is old and feeble and preparation method thereof.

For achieving the above object, the technical scheme is that a kind of emulsion, it is mixed by following raw material, presses Mass percent calculates, and is respectively as follows:

Percentage composition

Water 50-70

Ethylhexyl palmitate 2-10

Glycerol 2-5

Isononyl isononanoate 1-8

Caprylic/capric triglyceride 1-5

Butyrospermum parkii fruit fat 1-5

Polydimethylsiloxane 1-5

Cetearyl alcohol 1-5

1,2-pentanediol 1-5

Folium Camelliae sinensis extract 0.5-1.5

Radix Et Caulis Acanthopanacis Senticosi extract 0.5-1.5

Algae extract 0.5-1.5

Glyceryl stearate 1-3

Flos Rosae Rugosae extract 1-5

Carbomer 0.2-0.8

Arginine 0.1-0.5

Xanthan gum 0.1-0.6

1,2-hexanediol 0.1-0.7

Ethohexadiol 0.1-0.4

Hyaluronate sodium 0.01-0.05.

As preferably, the emulsion described in this programme also includes papaya water, and its mass percent is 0.5-1.5.

As preferably, the emulsion described in this programme also includes methyl sesquistearate, and its mass percent is 1- 2。

As preferably, the emulsion described in this programme also includes PEG-20 methyl sesquistearate, its percent mass Ratio is 1-2.

By using technique scheme, the conventional formulation of emulsion is simultaneously introduced Folium Camelliae sinensis extract, Radix Acanthopanacis Senticosi root Extract, algae extract, Flos Rosae Rugosae extract and papaya water, be also added into other compositions accordingly, each chemical composition Concrete function and effect described below:

Folium Camelliae sinensis extract has another name called tea tannin, tea polyphenols;It it is polyhydroxyl phenolic compound general name contained in Folium Camelliae sinensis.Existing Scientific investigations showed that: tea polyphenols has the strongest antioxidation, its oxidation resistance is synthetic antioxidant BHT , 4~6 times of BHA, be 6~7 times of ME, 5~1 0 times of VC, and consumption is few: 0.01~0.03% can act as With, and without the potential toxic and side effects of synthetic.Tea polyphenols and protein are with hydrophobic bond and nitrogen key mode generation compound reaction, in day Make people's skin produce convergence with in chemistry because of it, therefore commonly referred to as it has convergence.This character makes the cosmetics containing polyphenol exist Under waterproof condition, skin is had good adhesive ability, and thick pore can be made to shrink, make the skin contraction relaxed, compact And reduce wrinkle, so that skin shows the outward appearance of exquisiteness.Collagenase and elastoser there are is inhibitory action simultaneously, can hinder Only the content of elastin laminin declines or degeneration, maintains skin elasticity and wrinkle resistant effect.Tea polyphenols is i.e. that one has moisture-keeping function Natural product, because of in its molecule containing polyol structure, can the moisture absorption in atmosphere.The moisturizing of tea polyphenols also reside in have transparent The inhibitory activity of matter acid enzyme. thus reach real physiological deep moisturizing effect in skin care item.

Radix Et Caulis Acanthopanacis Senticosi extract extraction people from Siberia Radix Ginseng, rich in polysaccharide and the composite parts of various glycoprotein, these Composition forms one layer of film compacted at skin surface, tightens up at once and skin care.This film forming phenomenon is to have polysaccharide polymerization knot Structure on skin the dried physical change formed and occur, just can substantially observe that subtracting of wrinkle is light and lax in the short time Compacting of skin.Contain multiple nutritional components such as Syringa oblata Lindl. element, isoflavone, SOD, mcg vitamin and mineral etc., institute simultaneously With life-time service energy nourishes rough skin, improve skin quality, desalinate wrinkle.

Algae extract is a kind of excellent emollient, and the active matter mass-energy being not only because in Sargassum is combined with skin protein Form the gel of moisture retention, and it can also form protecting film by hydration on the surface of skin, prevents moisture from evaporating. Algae extract contains multiple antioxidation composition, can reduce melanin and generate, alleviate melanin pigmentation, increase skin corium collagen protein, Thus play speckle dispelling, wrinkle resistant, defying age, and protection cell exempts the effect of light radiation damage.And can help, improve skin Immunity and protective effect.The function remembered by cell shape, for skin replenishing collagen, repairs the most impaired or depression Skin, recovers the normal condition of skin;Being effectively improved expansion property acne scars, Intradermal or subcutaneous tissue injury, epithelium contracts, the degree of depth Wrinkle or the defect of other soft tissues.

Flos Rosae Rugosae extract has strong fragrance, gentleness is releived, and whitening disappears fat and blood dissipating blood stasis skin care skin moistening, wrinkle resistant despeckle Effect.

Papaya water main composition is VA, VC, tannin, organic acid etc., has good antioxidation, can in case Stop the skin aging that the environmental pollutions such as UV radiation cause, can effectively suppress the activity of Collagenase, alleviate the spy of skin aging Property.Also there is whitening effect simultaneously.

Flos Rosae Rugosae extract is i.e. natural attached pastil, can remove again the black speck on skin simultaneously, make the tender white nature of skin, Anti-wrinkle is the most helpful.

Radix Et Caulis Acanthopanacis Senticosi extract can adjust internal organs QI and blood function, improves blood circulation, enhances metabolism, and makes skin obtain To enough QI-blood circulation and normal nutrition, thus reach the purpose of moistening five ZANG-organs, improving healthy complexion, inhibit skin and decline Always.

Ethylhexyl palmitate is a kind of yellowish oily liquids, the most oxidizable, invariant color, good stability, has good Skin moistening, extension and permeability, moisten and soften skin, again without greasy feeling, be good emollient.

Isononyl isononanoate has many methyl branches structure of uniqueness, and dry and comfortable and soft feel, is splendid emollient, Good to silicone oil intermiscibility, it is possible to resolve the problem that silicone oil low temperature separates out, it is stabilizer and the coupling agent of silicone oil, colorant is had very well Dispersibility, viscosity is low, and skinfeel is salubrious, without greasy feeling.

Polydimethylsiloxane, also known as silicone oil, owing to having good lubricity, does not hinder the normal function of skin, and And be a kind of comparatively ideal hydrophobic base, often share make protective ointment with greasing base, be used for preventing water solublity thing Matter and the stimulation of acid, alkali liquor etc. or corrosion.

Caprylic/capric triglyceride is easy to be absorbed by the skin, and the uniform and smooth of cosmetics is played well effect, makes Skin lubrication is glossy, can be as the base material of Moisture factor, for the stabilizer as cosmetics, antifreezing agent, homogeneous agent.

Butyrospermum parkii fruit fat is abundant moisturizing agent, easily absorbs, rich in unsaturated fatty acid, can strengthen the moisturizing energy of skin Power, can be moistened the skin that dryness and cutin are impaired, Ka Lite tree extract, relative to other plant oil, containing the highest Ratio fat accompaniment, particularly grows triterpene alcohol and vitamin E, vitamin A, allantoin etc., the nutrition of the nutrient of necessity Abundant, it is possible to prevent skin water loss, help healing of wound, increase skin defence capability and compliance, be rare skin protection Natural component.

Glucate SS, has excellent emulsifying, dispersion, solubilising power, and the compatibility with skin is also The best.

Arginine is a kind of common alpha amino acid, can be as a kind of nutritional supplement in emulsion so that this emulsion has Good trophism, has good opsonic action for skin.

The present invention is prevented the broken of collagen protein by algae extract and is run off, and the synthesis of stimulation collagen is with to crease-resistant Stricture of vagina is formed and degree of compacting and elastic reduction;Prevent the stream of mucopolysaccharide;Prevent the loss of lipid;Radix Et Caulis Acanthopanacis Senticosi extract can be Skin surface is formed and compacts film, increases degree of compacting, assist simultaneously with Folium Camelliae sinensis extract, Butyrospermum parkii fruit fat, papaya water with And Flos Rosae Rugosae extract, prevent skin oxidative, reach effect of whitening, slow down aging, increase the opposing of skin environment to external world Property, and whole formula adds arginine, hyaluronate sodium etc. and supplements the nutrients as skin conditioning agent, help skin, no Containing any additive and pigment, fundamentally solving skin problem, effect is obvious, safety and also have no side effect.

Detailed description of the invention

Embodiment one:

A kind of emulsion, it is as follows that its internal each composition carries out proportioning by its percent mass: the water of 50%, the Palmic acid second of 10% The own ester of base, the glycerol of 2.35%, the isononyl isononanoate of 8%, the caprylic/capric triglyceride of 1%, the Butyrospermum parkii fruit fat of 5%, 1% Polydimethylsiloxane, the cetearyl alcohol of 5%, the 1 of 1%, 2-pentanediol, the methyl sesquistearate of 2%, 2% PEG-20 methyl sesquistearate, the Folium Camelliae sinensis extract of 0.5%, the Radix Et Caulis Acanthopanacis Senticosi extract of 0.5%, the algae of 0.5% carries Take thing, the papaya water of 0.5%, the glyceryl stearate of 3%, the Flos Rosae Rugosae extract of 5%, the carbomer of 0.8%, the essence of 0.1% Propylhomoserin, the xanthan gum of 0.6%, the 1 of 0.7%, 2-hexanediol, the ethohexadiol of 0.4%, the hyaluronate sodium of 0.05%.

Embodiment two:

A kind of emulsion, it is as follows that its internal each composition carries out proportioning by its percent mass: the water of 60.07%, the Palmic acid of 6% Octyl Nitrite, the glycerol of 5%, the isononyl isononanoate of 4%, the caprylic/capric triglyceride of 3%, the Butyrospermum parkii fruit fat of 2%, 2% Polydimethylsiloxane, the cetearyl alcohol of 2%, the 1 of 5%, 2-pentanediol, the methyl sesquistearate of 1.2%, The PEG-20 methyl sesquistearate of 1.2%, the Folium Camelliae sinensis extract of 1%, the Radix Et Caulis Acanthopanacis Senticosi extract of 1%, the algae of 1% carries Take thing, the papaya water of 1%, the glyceryl stearate of 2%, the Flos Rosae Rugosae extract of 1%, the carbomer of 0.4%, the smart ammonia of 0.5% Acid, the xanthan gum of 0.2%, the 1 of 0.2%, 2-hexanediol, the ethohexadiol of 0.2%, the hyaluronate sodium of 0.03%.

Embodiment three:

A kind of emulsion, it is as follows that its internal each composition carries out proportioning by its percent mass: the water of 70%, the Palmic acid second of 2% The own ester of base, the glycerol of 2%, the isononyl isononanoate of 1%, the caprylic/capric triglyceride of 5%, the Butyrospermum parkii fruit fat of 1%, 5% Polydimethylsiloxane, the cetearyl alcohol of 1%, the 1 of 2%, 2-pentanediol, the methyl sesquistearate of 1%, 1% PEG-20 methyl sesquistearate, the Folium Camelliae sinensis extract of 1.5%, the Radix Et Caulis Acanthopanacis Senticosi extract of 1.5%, the algae of 1.5% carries Take thing, the papaya water of 1.5%, the glyceryl stearate of 1%, the Flos Rosae Rugosae extract of 1.19%, the carbomer of 0.2%, 0.3% Arginine, the xanthan gum of 0.1%, the 1 of 0.1%, 2-hexanediol, the ethohexadiol of 0.1%, the hyaluronate sodium of 0.01%.

A kind of method preparing this emulsion, including the most several steps:

S1: by ethylhexyl palmitate, isononyl isononanoate, caprylic/capric triglyceride, Butyrospermum parkii fruit fat, poly-two Methylsiloxane, methyl sesquistearate, PEG-20 methyl sesquistearate, glyceryl stearate heat To 70-100 DEG C (preferably optimum temperature is 80 DEG C), stirring and dissolving forms oil phase material;

S2: by water, glycerol, cetearyl alcohol, 1,2-pentanediol, xanthan gum, 1,2-hexanediol, ethohexadiol, arginine, thoroughly Bright matter acid sodium is heated to 70-100 DEG C (preferably optimum temperature is 80 DEG C), and stirring and dissolving is mixed to form aqueous phase material;

S3: by oil phase material slowly suction aqueous phase while stirring, vacuum emulsifying (most preferably continues 8 points in 5-10 minute Clock);

S4: open cooling water under low rate mixing and cool down, aqueous phase material and the oil phase material of mixing are cooled to 40-50 DEG C (optimum temperature 45 DEG C), adds carbomer, stirs;

S5: add Folium Camelliae sinensis extract, Radix Et Caulis Acanthopanacis Senticosi extract, algae extract, papaya water, Flos Rosae Rugosae extract, fill Divide and stir;

S6: be slowly stirred, is cooled to 30-40 DEG C of (optimum temperature is 35 DEG C) discharging afterwards, sampling, enters fill operation, enters Row fill, packaging.

Embodiment four:

Use product prepared by above-described embodiment, select 40 45-60 year the healthy population that do not limits of men and women use, with The using effect of commercially available anti-wrinkle product contrasts, the most following each table of service condition.

Using method: require the protective skin cream that the most early, middle and late use is once described, using method is for taking appropriate painting It is put on the desired area such as face, cervical region, is the most softly massaged into absorption.

In temperature 20-30 DEG C, relative humidity is 60-90%, is divided at random by the healthy population that 80 45-60 year men and women do not limit Become four A, B, C, D tetra-groups: A group use embodiment 1 product, B group use embodiment 2 product, C group use embodiment 3 product, D group Use group uses 5 kinds of commercially available anti-wrinkle product respectively, uses skinanalysis apparatus surveying record result, effect before and after 1 month Relatively.To recovering, skin elasticity value is the biggest, and lifting effect of compacting is the best;Skin friction power is the least, and surface is the most smooth, desalinates microgroove Effect is the best;Skin water content is the highest, and skin is the most moist.Lifting improved values of compacting need to be effective more than or equal to 5, and desalination microgroove changes Kind value need to be reduced more than being effective equal to 10, and moistening moisturizing improved values need to be effective more than or equal to 5.The volunteer's number that will improve Percentage ratio is registered, and the results are shown in Table 1:

Table 1:

Embodiment 1 product Embodiment 2 product Embodiment 3 product Commercially available prod Compact lifting 90% 80% 85% 60% Desalination microgroove 95% 95% 90% 55% Moisten moisturizing 95% 90% 85% 65%

In sum, anti-wrinkle emulsion effective percentage of the present invention is significantly stronger than commercially available anti-wrinkle product, having in terms of lifting of compacting Efficiency reaches 85%, and the effective percentage in terms of desalination microgroove reaches 93.3%, and the effective percentage in terms of moist moisturizing reaches 90%, is using this After invention, at lifting of compacting, desalination microgroove, all along with the use time increases, effect is the most obvious to moisten three aspects of moisturizing.

The present invention has the following advantages:

1. opposing skin aging, makes skin more smooth;

2. suppression melanin generates, and accelerates skin-whitening;

3. increase skin oxidation resistance, play the problem alleviating skin infection;

4. antiallergic is sun-proof, moisturizing control oily, strengthen skin immunization power;

5. whitening disappears fat and blood dissipating blood stasis.

Claims (3)

1. an emulsion, is characterized in that: it is mixed by following raw material, calculates by mass percentage, is respectively as follows:
2. an emulsion, is characterized in that: it is mixed by following raw material, calculates by mass percentage, is respectively as follows:
3. an emulsion, is characterized in that: it is mixed by following raw material, calculates by mass percentage, is respectively as follows:
CN201410272335.9A 2014-06-17 2014-06-17 Emulsion and preparation method thereof CN104027271B (en)

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Publication number Priority date Publication date Assignee Title
CN106176331A (en) * 2015-05-04 2016-12-07 广州十长生化妆品有限公司 A kind of have antioxidation, defying age, the prescription of whitening effect, cosmetics and preparation method thereof
CN105919886A (en) * 2016-06-13 2016-09-07 广东万海细胞生物科技有限公司 Quick-acting wrinkle repairing emulsion and preparation method thereof
CN106109284B (en) * 2016-06-24 2019-04-02 杭州兰茜化妆品有限公司 A kind of facial mask and preparation method thereof
WO2018049608A1 (en) * 2016-09-14 2018-03-22 冯宝欣 Quantum light wave erugation and skincare cream and preparation method therefor
CN107174547A (en) * 2017-05-25 2017-09-19 杭州千岛湖蓝色天使实业有限公司 A kind of anti-fog haze emulsion
CN107028845A (en) * 2017-06-23 2017-08-11 湖北立天生物工程有限公司 A kind of papaya cold cream and preparation method containing a variety of pure natural plant extracts

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103393568A (en) * 2013-07-28 2013-11-20 娇时化妆品(杭州)有限公司 Whitening and freckle-removing cream

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103393568A (en) * 2013-07-28 2013-11-20 娇时化妆品(杭州)有限公司 Whitening and freckle-removing cream

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