Background technology
In the past, ultraviolet radiation is the largest source injuring our skin, and present environmental pollution is the second largest factor of skin problem, and it can cause the drying of skin, stimulation, allergy, brings various skin situation.
Environmental pollution comprises 1, physical attack (dust, haze, sandstorm, PM2.5, computer radiate): PM2.5 diameter is less than pore and enters skin, and skin hydropenia, sensitivity, fat secretion are unbalance, aging, the problem that also can make blackhead, corse sweat pore.2, chemical attack (second hand smoking, vehicle exhaust, industrial pollution, waste gas etc.): except causing free radical increase, also can promote collagen disintegrate, reduce fine circulation, causes skin lax, dry, obscure.
In addition, urban life pressure, causes xerosis cutis to relax, to tarnish, colour of skin wan shape, thus accelerates skin aging, hinders skin vigorous and graceful; Simultaneously tired, stay up late, with advancing age, skin resistance declines, and is the most easily subject to external invasion and attack, causes allergy, dimness, lax dry skin.
Facial film is a kind of cosmetics that personage commonly uses of liking to be beautiful, and the form of facial film is also varied, and have powder face pack, cream pack, membranaceous facial film etc., facial film function is also varied, as moisturizing, whitening, defying age, Sage Extract etc.Moisture saver mask is a kind of conventional facial film, generally adds also moisturizing ingredient, as glycerol etc. in facial film.
Limax mucus have fall low-moisturely to scatter and disappear, the effect of wet skin, Chinese patent CN 102793655B discloses a kind of Regeneration and Repair facial mask liquid containing Limax pituitary extract.
Deep-sea salmon collagen protein is generally oral for people as health product, in cosmetics, particularly rarely has the interpolation of this material in facial film.
Pharmacology and clinical research show, Herb Gynostemmae Pentaphylli is almost non-toxic, have no side effect, and have anticancer, blood fat reducing, anti-aging effects, can strengthen body immune function, the side effect etc. of control glucocorticoid.Therefore Herb Gynostemmae Pentaphylli extract generally uses as medicine, health product.Chinese patent application CN 103191172A discloses the application of Herb Gynostemmae Pentaphylli extract in the cosmetics preparing skin anti-light aging.Chinese patent application CN 102871924A discloses the application of Herb Gynostemmae Pentaphylli extract as wetting agent.
Containing abundant mineral in grass green salicornia europaeal extract, there is effect of purification harmful substance.In addition, can help to dredge the passage transporting moisturizing materials in skin, make Water Cycle become more smooth and easy.Chinese patent application CN 103767972A and CN 104306318A discloses the application of grass green salicornia europaeal extract in moisture-keeping composition.
Natto fermentation elite is again polyglutamic acid sodium, and it has splendid moisturizing, storage capacity.Chinese patent application CN 103948532A discloses a kind of replenishing water and preserving moisture containing polyglutamic acid sodium and the cosmetics of skin of releiving.
A kind of natural water-retaining agent of avenabeta glucosan and isostearyl glyceryl pentaerythrityl ether, can assist the keratin in moisture content SCC, to reach moistening effect.Chinese patent application CN 102488628A discloses a kind of moisturizing, the anti-aging cosmetics formula that contain avenabeta glucosan.
Limax liquid, deep-sea salmon collagen protein, Herb Gynostemmae Pentaphylli extract, grass green salicornia europaeal extract, natto fermentation elite and avenabeta glucosan all have to be applied in moisture-keeping cosmetics, but there is not yet its compositions, and the application of said composition in facial mask liquid.
Meanwhile, the replenishing water and preserving moisture effect for moisture saver mask is in the market not fully up to expectations, and safety is unstable, fundamentally could not improve skin problem etc., therefore, is necessary to research and develop a kind of natural safety, the moisture saver mask liquid that moisturizing, lock water effect are good.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of moisture saver mask liquid, and it is natural safe, effective, can be absorbed fast by skin, and moistening effect is remarkable, effectively pins moisture simultaneously.
For solving the problems of the technologies described above, technical scheme of the present invention is:
A kind of moisture saver mask liquid, comprises following component: water, glycerol, propylene glycol, Natrulon H-10, ethoxy urea, Limax liquid, deep-sea salmon collagen protein, Herb Gynostemmae Pentaphylli extract, grass green salicornia europaeal extract, natto fermentation elite, avenabeta glucosan, carbomer, triethanolamine, hyaluronate sodium, methyl hydroxybenzoate, phenoxyethanol and essence.
Further, described moisture saver mask liquid comprises the component of following weight percent meter: water 75% ~ 90%, glycerol 2% ~ 5%, propylene glycol 2% ~ 5%, Natrulon H-10 2% ~ 5%, ethoxy urea 1% ~ 3%, Limax liquid 0.2% ~ 1%, deep-sea salmon collagen protein 0.2% ~ 1%, Herb Gynostemmae Pentaphylli extract 0.2% ~ 1%, grass green salicornia europaeal extract 0.2% ~ 1%, natto fermentation elite 0.2% ~ 1%, avenabeta glucosan 0.2% ~ 1%, carbomer 0.05% ~ 0.3%, triethanolamine 0.02% ~ 0.3%, hyaluronate sodium 0.01% ~ 0.05%, methyl hydroxybenzoate 0.05% ~ 0.3%, phenoxyethanol 0.3% ~ 0.8% and essence 0.03% ~ 0.08%.
As the preferred embodiment of the present invention, described moisture saver mask liquid is made up of the component of following weight percent meter: water 85.61%, glycerol 3%, propylene glycol 3%, Natrulon H-10 3%, ethoxy urea 1.5%, Limax liquid 0.5%, deep-sea salmon collagen protein 0.5%, Herb Gynostemmae Pentaphylli extract 0.5%, grass green salicornia europaeal extract 0.5%, natto fermentation elite 0.5%, avenabeta glucosan 0.5%, carbomer 0.1%, triethanolamine 0.1%, hyaluronate sodium 0.03%, methyl hydroxybenzoate 0.1%, phenoxyethanol 0.5% and essence 0.06%.
Limax liquid: Limax liquid is containing natural collagen protein, elastin, allantoin, Portugal (grape) alduronic acid, multivitamin etc.Skin deep layer is brought in nutrition contained by these compositions into, has and can repair skin, increases the nutrition of skin, the moisturizing of lock water, skin care whitening, print reparation of dispelling, anti-ageing multi-efficiency of waiting for a long time.
Deep-sea salmon collagen protein: the deep-sea salmon collagen protein being derived from Atlantic Oceanic Region, include the collagen protein of skin wilderness demand, itself and water have extraordinary affinity, very easily by percutaneous absorption, can keep skin moisture, allow skin shine reality brilliance.
Herb Gynostemmae Pentaphylli extract: the function improving the aquaporin in Skin Cell, promotes to produce aquaporin, imports moisture to cell interior, brings skin water profit from cell interior.Cell has been moistened, and skin also can become water profit thereupon.
Grass green salicornia europaeal extract: be rich in the mineral such as vitamin, aminoacid and calcium, ferrum, sodium, the barrier function that skin recovers good can be promoted, and fabulous moisturizing effect is provided; Grass green salicornia europaeal extract also improves the synthesis of T-5398-1, thus makes hornification coating more healthy and abundant, and then reaches good protection skin from environmental injury, prevents water loss.
Natto fermentation elite is again polyglutamic acid sodium, and being extracted by natto fermentation and form, is the plant moisturizing agent of pure natural.It has effect of degree of depth lock water, superpower moisturizing, reparation skin, can form natural containment, reduce trans epidermal water loss at skin surface; Go deep into skin bottom to keep the skin wet, there is perfect performance of keeping humidity.
Avenabeta glucosan: a kind of complex carbohydrate high with skin similarity, because it has unique compatibility and affinity for skin, avenabeta glucosan has the ability of to be tied up by moisture at skin, has to regulate moisturizing, maintain appropriateness, continue moisturizing, reduce the abilities such as stimulation.
Described Limax liquid, deep-sea salmon collagen protein, Herb Gynostemmae Pentaphylli extract, grass green salicornia europaeal extract, natto fermentation elite and avenabeta glucosan composite, again in conjunction with glycerol, propylene glycol, Natrulon H-10, ethoxy urea, carbomer, triethanolamine, hyaluronate sodium, the basic material such as methyl hydroxybenzoate and phenoxyethanol obtains moisture saver mask liquid of the present invention, each component is worked in coordination with, reaching moisture saver mask liquid of the present invention can fast by skin overall absorption, effective moisturizing, degree of depth lock water simultaneously, long-acting moisturizing, keep skin beauty water tender moist, improve skin withstand force, repair the objects such as skin lines.
Present invention also offers the preparation method of above-mentioned moisture saver mask liquid, have and comprise the following steps:
(1) water, glycerol, propylene glycol, Natrulon H-10, ethoxy urea, Limax liquid, deep-sea salmon collagen protein, Herb Gynostemmae Pentaphylli extract, grass green salicornia europaeal extract, natto fermentation elite, avenabeta glucosan, carbomer, hyaluronate sodium and methyl hydroxybenzoate are added in agitated kettle, open and stir and be heated to 78 ~ 82 DEG C, be stirred to said components and complete dissolving;
(2) continue to be stirred to temperature and reduce to 43 ~ 47 DEG C, then add phenoxyethanol and essence, be stirred to evenly;
(3) finally add triethanolamine, stir and obtain moisture saver mask liquid.
Further, the mixing speed of described stirring is 40 ~ 50 revs/min.
Therefore, relative with prior art, advantage of the present invention is:
(1) remarkable moisture-retaining capacity: moisture saver mask liquid of the present invention contains the abundant plant extraction composition such as Herb Gynostemmae Pentaphylli extract, grass green salicornia europaeal extract, go deep into skin bottom to keep the skin wet, moisture saver mask liquid can be absorbed rapidly by skin simultaneously, the nutrients such as Limax liquid, deep-sea salmon collagen protein fast and penetrate into skin bottom completely, repair skin lines, improve skin withstand force.
(2) moisturizing locks water simultaneously: moisture saver mask liquid of the present invention contains natto fermentation elite and avenabeta glucosan, the barrier function that skin recovers good can be promoted, effective minimizing trans epidermal water loss, pin moisture, keep 24 hours long-acting water profits, play perfect moisturizing lock aqueous energy, obviously improve the situations such as skin is lax, dry, obscure.
(3) each component of moisture saver mask liquid of the present invention is worked in coordination with, and moistening effect is good, and safe and non-stimulating, and the preparation method of moisture saver mask liquid of the present invention is simple simultaneously, can be applicable.
Detailed description of the invention
Further describe the present invention below by way of detailed description of the invention, but the present invention is not limited only to following examples.Within the scope of the invention or not departing from content of the present invention, spirit and scope, moisture saver mask liquid of the present invention is suitably improved, replaces the identical component of effect, will become apparent to those skilled in the art that they are all deemed to be included within scope of the present invention.
In the embodiment of the present invention 1 ~ 3 and comparative example 1 ~ 2 producer of constituent part and article No. as follows:
embodiment 1, moisture saver mask liquid of the present invention and preparation thereof
Formula: by weight percentage, water 85.61%, glycerol 3%, propylene glycol 3%, Natrulon H-10 3%, ethoxy urea 1.5%, Limax liquid 0.5%, deep-sea salmon collagen protein 0.5%, Herb Gynostemmae Pentaphylli extract 0.5%, grass green salicornia europaeal extract 0.5%, natto fermentation elite 0.5%, avenabeta glucosan 0.5%, carbomer 0.1%, triethanolamine 0.1%, hyaluronate sodium 0.03%, methyl hydroxybenzoate 0.1%, phenoxyethanol 0.5% and essence 0.06%.
Preparation: water, glycerol, propylene glycol, Natrulon H-10, ethoxy urea, Limax liquid, deep-sea salmon collagen protein, Herb Gynostemmae Pentaphylli extract, grass green salicornia europaeal extract, natto fermentation elite, avenabeta glucosan, carbomer, hyaluronate sodium and methyl hydroxybenzoate add in agitated kettle by (1), open and stir and be heated to 80 DEG C, be stirred to said components and complete dissolving;
(2) continue to be stirred to temperature and reduce to 45 DEG C, then add phenoxyethanol and essence, be stirred to evenly;
(3) finally add triethanolamine, stir and obtain moisture saver mask liquid.
The mixing speed of above-mentioned stirring is 45 revs/min.
embodiment 2, moisture saver mask liquid of the present invention and preparation thereof
Formula: by weight percentage, water 83.35%, glycerol 2%, propylene glycol 5%, Natrulon H-10 2%, ethoxy urea 3%, Limax liquid 0.2%, deep-sea salmon collagen protein 1%, Herb Gynostemmae Pentaphylli extract 0.2%, grass green salicornia europaeal extract 1%, natto fermentation elite 0.2%, avenabeta glucosan 1%, carbomer 0.3%, triethanolamine 0.02%, hyaluronate sodium 0.05%, methyl hydroxybenzoate 0.3%, phenoxyethanol 0.3% and essence 0.08%.
Preparation: water, glycerol, propylene glycol, Natrulon H-10, ethoxy urea, Limax liquid, deep-sea salmon collagen protein, Herb Gynostemmae Pentaphylli extract, grass green salicornia europaeal extract, natto fermentation elite, avenabeta glucosan, carbomer, hyaluronate sodium and methyl hydroxybenzoate add in agitated kettle by (1), open and stir and be heated to 78 DEG C, be stirred to said components and complete dissolving;
(2) continue to be stirred to temperature and reduce to 43 DEG C, then add phenoxyethanol and essence, be stirred to evenly;
(3) finally add triethanolamine, stir and obtain moisture saver mask liquid.
The mixing speed of above-mentioned stirring is 40 revs/min.
embodiment 3, moisture saver mask liquid of the present invention and preparation thereof
Formula: by weight percentage, water 82.16%, glycerol 5%, propylene glycol 2%, Natrulon H-10 5%, ethoxy urea 1%, Limax liquid 1%, deep-sea salmon collagen protein 0.2%, Herb Gynostemmae Pentaphylli extract 1%, grass green salicornia europaeal extract 0.2%, natto fermentation elite 1%, avenabeta glucosan 0.2%, carbomer 0.05%, triethanolamine 0.3%, hyaluronate sodium 0.01%, methyl hydroxybenzoate 0.05%, phenoxyethanol 0.8% and essence 0.03%.
Preparation: water, glycerol, propylene glycol, Natrulon H-10, ethoxy urea, Limax liquid, deep-sea salmon collagen protein, Herb Gynostemmae Pentaphylli extract, grass green salicornia europaeal extract, natto fermentation elite, avenabeta glucosan, carbomer, hyaluronate sodium and methyl hydroxybenzoate add in agitated kettle by (1), open and stir and be heated to 82 DEG C, be stirred to said components and complete dissolving;
(2) continue to be stirred to temperature and reduce to 47 DEG C, then add phenoxyethanol and essence, be stirred to evenly;
(3) finally add triethanolamine, stir and obtain moisture saver mask liquid.
The mixing speed of above-mentioned stirring is 50 revs/min.
Do testing performance index to the moisture saver mask liquid of embodiment 1 ~ 3, its test result is as follows:
1, outward appearance: semi-transparent flowing
2, pH value: 5.0 ~ 6.5
3, viscosity: 2,#12 1500 ~ 2500mpa
4, heat-resistant stability investigates (48 DEG C × 24h): qualified
5, cold-resistant study on the stability (-15 DEG C × 24h): qualified.
Soak non-woven fabrics mask when the present invention applies, every sheet leaching, containing moisture saver mask liquid 30g, obtains facial film finished product.First be equipped with the clean face of warm water with clean product during use, launched inwardly to be lightly spread in face by film cloth, flicking, to fitting completely, applies 10 ~ 15 minutes, uses weekly 2 ~ 3 times.
comparative example 1,
Formula: by weight percentage, water 85.61%, glycerol 3%, propylene glycol 3%, Natrulon H-10 3%, ethoxy urea 1.5%, Limax liquid 1%, deep-sea salmon collagen protein 1%, avenabeta glucosan 1%, carbomer 0.1%, triethanolamine 0.1%, hyaluronate sodium 0.03%, methyl hydroxybenzoate 0.1%, phenoxyethanol 0.5% and essence 0.06%.
Preparation method is with reference to embodiment 1.
comparative example 2,
Formula: by weight percentage, water 85.61%, glycerol 3%, propylene glycol 3%, Natrulon H-10 3%, ethoxy urea 1.5%, Herb Gynostemmae Pentaphylli extract 1%, grass green salicornia europaeal extract 1%, natto fermentation elite 1%, carbomer 0.1%, triethanolamine 0.1%, hyaluronate sodium 0.03%, methyl hydroxybenzoate 0.1%, phenoxyethanol 0.5% and essence 0.06%.
Preparation method is with reference to embodiment 1.
test example one, Product Safety evaluation (experiment of human body skin patch)
One, trial target: embodiment 1 ~ 3, moisture saver mask liquid prepared by comparative example 1 ~ 2
Tested crowd's number: 30 people
Age: between 20 ~ 50 years old
Sex: female 20 people, male 10 people
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
Two, patch method: select qualified speckle examination device, with closed patch experiment method, tested material being about 0.020ml ~ 0.025ml drips in speckle examination device, external special adhesive tape is covered on experimenter back, tested material is removed after 24 hours, within after removing respectively 0.5,6,12,24,48 hour, observe dermoreaction, according to its result of dermoreaction grade scale record in " cosmetics health specification ".
Three, experimental result: human skin patch result shows: 30 experimenters are by the patch test of the moisture saver mask liquid of embodiment 1 ~ 3, comparative example 1 ~ 2, dermoreaction is observed at 0.5,6,12,24,48 hour, wherein there is skin adverse reaction in 0 example, the moisture saver mask liquid use safety described in explanation.
test example two, product effect assessment
Part I:
One, trial target: the facial film that embodiment 1 ~ 3, comparative example 1 ~ 2 moisture saver mask liquid are made
Two, tested crowd
Sex number: female, 50 people
Age: between 20 ~ 40 years old
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
Grouping: be divided into 5 groups, often organize 10 people.
Three, method of testing: use Fes Kai Er SK-III skin moisture detector to test the moisture of forehead, left face, right face and chin skin respectively, and get arithmetic mean of instantaneous value, after experimenter cleans face, film cloth is launched to be lightly spread in face inwardly, flicking is to fitting completely, apply after 15 minutes, wash one's face with clear water, dry face, again by the skin moisture content of skin moisture tester test forehead, left face, right face and the same position of chin, and get arithmetic mean of instantaneous value, re-use skin moisture tester after 24 hours and test one time.Often organize 10 experimenters and tested result is got arithmetic mean of instantaneous value, test result is as following table 1:
Table 1 skin moisture content table with test results
From upper table 1, the moisturizing Be very effective of the embodiment of the present invention 1 ~ 3 moisture saver mask liquid, uses skin average moisture difference >6% before and after facial film, is also all better than comparative example 1 ~ 2, wherein with the moisturizing best results of embodiment 1, before and after using facial film, skin average moisture difference reaches 8.2%; The lock water effect of the embodiment of the present invention 1 ~ 3 moisture saver mask liquid is also fine simultaneously, and after using facial film, 24 hours skin average moisture reduction amplitudes are little, illustrate that moisture saver mask liquid moisturizing of the present invention effectively reduces skin water loss simultaneously.
Part II:
One, trial target: the facial film that embodiment 1 ~ 3, comparative example 1 ~ 2 moisture saver mask liquid are made
Two, tested crowd
Sex number: female, 100 people
Age: between 20 ~ 40 years old
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
Grouping: be divided into 5 groups, often organize 20 people, often organizes 28 ± 1 years old mean age.
Three, method of testing: after experimenter cleans face, launches to be lightly spread in face by film cloth inwardly, and flicking, to fitting completely, applies 15 minutes, uses 2 times weekly.
Testing evaluation result is as follows:
(two weeks) on probation feedback conclusive table of table 2 embodiment 1 moisture saver mask
(two weeks) on probation feedback conclusive table of table 3 embodiment 2 moisture saver mask
(two weeks) on probation feedback conclusive table of table 4 embodiment 3 moisture saver mask
(two weeks) on probation feedback conclusive table of table 5 comparative example 1 moisture saver mask
(two weeks) on probation feedback conclusive table of table 6 comparative example 2 moisture saver mask
From upper table 2 ~ 6, the moisture saver mask of tester to embodiment 1 is particularly approved, namely particularly approves the moisture saver mask liquid of embodiment 1.Tester all represents, the moisture saver mask of embodiment 1 is better than the moisture saver mask of embodiment 2 and embodiment 3 at moistening effect, and be all obviously better than comparative example 1 and comparative example 2, illustrate that the moistening effect of moisture saver mask liquid of the present invention is good, nutritious, easily by percutaneous absorption, allow abundant moisturizing at the bottom of flesh, repair skin lines, make skin beauty water tender moist glossy, effectively pin moisture simultaneously, after 24 hours, skin still keeps water tender moist, accomplish 24 hours long-acting water profits, life-time service obviously can improve the situations such as skin is lax, dry, obscure.People is not had to occur allergic phenomena in the questionnaire of simultaneously user.
Above-described embodiment is illustrative principle of the present invention and effect thereof only, but not for limiting the present invention.Any person skilled in the art scholar all without prejudice under spirit of the present invention and category, can modify above-described embodiment or changes.Therefore, such as have in art usually know the knowledgeable do not depart from complete under disclosed spirit and technological thought all equivalence modify or change, must be contained by claim of the present invention.