CN102935055A - Hydrolat moisturizing facial mask - Google Patents

Hydrolat moisturizing facial mask Download PDF

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Publication number
CN102935055A
CN102935055A CN2012105166964A CN201210516696A CN102935055A CN 102935055 A CN102935055 A CN 102935055A CN 2012105166964 A CN2012105166964 A CN 2012105166964A CN 201210516696 A CN201210516696 A CN 201210516696A CN 102935055 A CN102935055 A CN 102935055A
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hydrosol
hydrolat
moisture
skin
moisturizing
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CN2012105166964A
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CN102935055B (en
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蔡剑波
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Shenzhen Yanqian Science & Technology Co ltd
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Shenzhen Yanqian Science & Technology Co ltd
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Abstract

The invention discloses a hydrolat moisturizing facial mask. The method comprises the following steps: putting a hydrolat with moisturizing efficacy into a container, then adding hyaluronic acid, fish collagen, water soluble vitamin and lauric acid modified superoxide dismutase into the container, and stirring the solution until the solution is completely dissolved; then adding aloe extracting solution and supguard GM-BP preservative into the solution, and uniformly stirring, uniformly dripping the obtained liquid onto a non-woven fabric facial mask, then conducting sealed packaging to obtain a product, namely the hydrolat moisturizing facial mask. The hydrolat with moisturizing efficacy includes rose hydrolat, witch hazel hydrolat, jasmine hydrolat, marigold hydrolat, sandalwood hydrolat and the like, and any one of the hydrolat or combination of any two or more of the hydrolat can be adopted. The hydrolat moisturizing facial mask prepared by adopting the method disclosed by the invention has the advantages that the moisturizing effect is prominent, and the mask is safe and can not irritate a human body, and the like.

Description

A kind of hydrosol moisture saver mask
Technical field:
The present invention relates to cosmetic field, particularly a kind of hydrosol moisture saver mask.
Background technology:
Hydrosol has another name called Hua Shui, crystal's oil, and it is the water that stays in distillation extraction quintessence oil process, is the by-product of producing quintessence oil.Hydrosol also contains the water-soluble substances in whole plants except containing a small amount of derived essential oil, its contained mineral nutrient (such as tannin and flavonoid) is that quintessence oil lacks.The characteristic of its low concentration is absorbed by skin easily, and fully without essence and alcoholic content, fragrance is light pleasant, and is non-stimulated to the skin gentleness, is a kind of ideal cosmetic material.
Facial film is a kind of cosmetics that the personage commonly uses of liking to be beautiful, and the form of facial film is also varied, and powder face pack, cream pack, membranaceous facial film etc. are arranged, and the facial film function also is varied, such as moisturizing, whitening, moisten, speckle dispelling etc.Moisture saver mask is a kind of facial film commonly used, generally adds also moisturizing composition in the facial film, and such as glycerol etc., the existing pure natural raw material of these moisturizing compositions also has industrial chemicals.If facial film producer adopts low-grade raw material, perhaps working condition and processing technique are relatively poor, and the facial film of production not only can not be improved looks, and bring easily on the contrary ill symptomses such as sufferings, inflammation, redness, indivedual severe patients even disfeatured.
Hydrosol as the application of cosmetic material or product also seldom, the hydrosol product of selling in the market is most of just simply to be distributed into the bottle sale to hydrosol, the cosmetics that it are developed to various functions are not a lot, and the facial film take hydrosol as primary raw material on the market is also fewer.
One " collagen wet-retaining face mask and preparation method thereof " by name authorized by State Intellectual Property Office, number of patent application is 200610020676.2 patent of invention, it is with porcine collagen, cellulose derivative, starch, wetting agent and cross-linking agent are a kind of facial film of raw material preparation, collagen protein is a kind of good cosmetic material, it has skin care, slow down aging, beauty treatment, the effects such as wrinkle-chasing, but the degree that collagen protein is absorbed by the body is very important index, (General Requirements≤1000D) absorbed by the people easily, the prepared porcine collagen of the patent of the disclosure does not describe its molecular weight the collagen protein of small-molecular weight.In addition, patent of the present disclosure does not explain with regard to the effect of product, also has the weak points such as processing step is many, complicated operation with this disclosed method converted products.
State Intellectual Property Office discloses one " a kind of moisture saver mask " by name, number of patent application is 201110103296.6 patent of invention, it is with deionized water, Sorbitol, hydrolytic collagen, vitamin E, potassium alginate, hyaluronic acid, two imidazolidinyl urea and Radix Mori extract are a kind of facial film of raw material preparation, there are some shortcomings and deficiencies parts in the patent of the disclosure: two imidazolidinyl urea are a kind of antiseptic that are mainly used in the cosmetics, it is to reach the antiseptical purpose by slow release formaldehyde, generally its addition should not surpass 0.3%, and the addition of this open prescription is 1-2%, and therefore prepared product is to have potential harm to human body; The molecular weight of used hydrolytic collagen does not explain; The product efficacy of disclosed method preparation does not explain etc.
Shortcomings and deficiencies part for prior art, on some present situations lack of standardization of moisture saver mask and the market hydrosol is applied in the less situation in facial film aspect on the market, in conjunction with hydrosol plurality of advantages is arranged again, therefore, develop a kind ofly take hydrosol as main raw material(s), the facial film with moisture-keeping efficacy is just significant.
Summary of the invention:
The technical problem to be solved in the present invention is the hydrosol facial film that has moisture-keeping efficacy take hydrosol as main raw material(s) is mixed with.Prepared hydrosol facial film except have moistening effect obviously, also have human body without advantages such as any stimulations.
The technical scheme that the present invention solves the problems of the technologies described above is: have the stock solution of moisture-keeping efficacy as main raw material(s) is mixed with take hydrosol, then stock solution is dripped equably on the non-woven fabrics facial film, pack and get final product.
The stock solution that the present invention has moisture-keeping efficacy is to form than preparation by following formulation by weight:
Hyaluronic acid 0.1~0.5%,
Fish collagen 0.2~1%,
Watermiscible vitamin E 0.5~2%,
Modified Superoxide Dismutase 0.001~0.005%
Aloe extraction solution 2~5%,
Germall BP antiseptic 0.05~0.1%,
Hydrosol with moisture-keeping efficacy adds to 100%.
In the stock solution of the present invention, described fish collagen is to adopt the skin of pure natural tilapia to produce its molecular weight≤1000D through enzymolysis.
In the stock solution of the present invention, described Modified Superoxide Dismutase is La-SOD, and its activity unit number is 4,000,000 U/ grams.
In the stock solution of the present invention, described Aloe extraction solution is to be added in an amount of deionized water with fresh aloe, and water decocts, until the solid matter content of aqueous solution is to 5.0~5.1%, then cooling is filtered, and decolouring forms.
In the stock solution of the present invention, described hydrosol with moisture-keeping efficacy is wherein any one or wherein arbitrarily two or more the combination in MEIGUI CHUNLU, Radix Hamamelidis Mollis hydrosol, jasmine hydrosol, Flos Inulae hydrosol and the Lignum Santali Albi hydrosol.
Non-woven membrane of the present invention, material are the in proportion arbitrary proportion material of mixing of viscose rayon or terylene or both, and grammes per square metre is 30~150 gram/m 2, be shaped as face shape, have the hole of suitable size at eye, nostril and face place, so that eyes, nostril and face can expose.
Preparation method of the present invention comprises the steps:
Take by weighing in proportion hydrosol and put into a container, again hyaluronic acid, fish collagen, watermiscible vitamin E and Modified Superoxide Dismutase are added container, stir, until fully dissolving;
Take by weighing in proportion Aloe extraction solution and germall BP antiseptic and add in the solution, and stir, gained liquid is the stock solution with moisture-keeping efficacy;
Stock solution is evenly dripped on the ground non-woven fabrics facial film, and the weight of every non-woven fabrics facial film dropping stock solution is 8~15 grams, then packs, and the product of gained is product of the present invention.
Using method of the present invention is: behind the cleaning face, take the packing of product of the present invention apart, the facial film taking-up of the inside is also applied equably at face, take facial film after 15~30 minutes and get final product.
The selected composition of the present invention has following effect and effect:
Hyaluronic acid: it can improve the skin-nourishing metabolism, and make that skin is tender, smooth, wrinkle removing, increase elasticity, prevent aging, be again good Percutaneous absorption enhancer in moisturizing.
Fish collagen: it can replenish the required nutrition of each layer of skin, makes collagen increased activity in the skin, skin care is arranged, the effects such as slow down aging, beauty treatment, wrinkle-chasing.
Watermiscible vitamin E: the effects such as elasticity that it has the aging of preventing, regulates female incretion and keep skin.
Lauric acid is superoxide dismutase modified: it is higher with respect to there not being superoxide dismutase modified activity, half-life is longer, heat stability higher (3.2 years non-inactivations of 25 ℃ of lower storages), and it has the removing interior free yl, defying age, the effects such as formation of inhibition melanocyte.
Aloe extraction solution: it has anti-inflammation, moistens moisturizing, defying age, the effect such as hypo-allergenic, and it contains the water conservation lignin, has strong permeability, helps the nutrient substance Transdermal absorption.
MEIGUI CHUNLU: it have keep the skin wet, the effects such as moisturizing, fast antiinflammatory, antiallergic, antipruritic and slow down aging.
The Radix Hamamelidis Mollis hydrosol: it can significantly improve skin lock water moisture-retaining capacity, and energy rapid permeability skin allows cell possess sufficient moisture, and it also has good moisturizing effects to the skin after shining, and it also has the aging skin of reparation cell in addition, improves the effects such as dull-looking skin.
The jasmine hydrosol: the skin of its dry hydropenia is very effective, and it has superior moistening effect, can make skin soft, flexible, can improve little microgroove, makes skin delicate bright.
The Flos Inulae hydrosol: it has well moist moistening effect to the skin of drying, and in addition, it also has bactericidal antiphlogistic, improves responsive skin quality, desalinates effects such as repairing cicatrix.
The Lignum Santali Albi hydrosol: it has the skin of aging, drying and hydropenia well moistens moistening effect, increases the water content of skin, in addition it also have the prevention wrinkle, the effect such as neural of relaxing.
Facial film of the present invention contains multiple composition with moist moisturizing, and it is skin care well, keeps the moisture of skin, the skin that it can also the gentrify drying simultaneously, delay skin aging, the appearance that prevents or slow down wrinkle of skin.The used raw material overwhelming majority of product is the pure natural raw material, and safety is without any zest.
The specific embodiment
Embodiment 1
Take by weighing 96.349 parts of MEIGUI CHUNLU and put in the container, again with in 0.1 part of hyaluronic acid, 1 part of fish collagen, 0.5 part of watermiscible vitamin E and 0.001 part of adding container of La-SOD, stir, until fully dissolving; Take by weighing 0.05 part of 2 parts of Aloe extraction solution and germall BP antiseptic again and add in the solution, and stir, on the uniform liquid dropping ground non-woven fabrics facial film with gained, then pack, the product of gained is the MEIGUI CHUNLU moisture saver mask, and namely present embodiment 1.
Embodiment 2
Take by weighing 95.138 parts of Radix Hamamelidis Mollis hydrosols and put in the container, again with in 0.2 part of hyaluronic acid, 0.8 part of fish collagen, 0.8 part of watermiscible vitamin E and 0.002 part of adding container of La-SOD, stir, until fully dissolving; Take by weighing 0.06 part of 3 parts of Aloe extraction solution and germall BP antiseptic again and add in the solution, and stir, on the uniform liquid dropping ground non-woven fabrics facial film with gained, then pack, the product of gained is Radix Hamamelidis Mollis hydrosol moisture saver mask, and namely present embodiment 2.
Embodiment 3
Take by weighing 94.277 parts of jasmine hydrosols and put in the container, again with in 0.3 part of hyaluronic acid, 0.6 part of fish collagen, 1 part of watermiscible vitamin E and 0.003 part of adding container of La-SOD, stir, until fully dissolving; Take by weighing 0.07 part of 4 parts of Aloe extraction solution and germall BP antiseptic again and add in the solution, and stir, on the uniform liquid dropping ground non-woven fabrics facial film with gained, then pack, the product of gained is jasmine hydrosol moisture saver mask, and namely present embodiment 3.
Embodiment 4
Take by weighing 93.116 parts of Flos Inulae hydrosols and put in the container, again with in 0.4 part of hyaluronic acid, 0.4 part of fish collagen, 1.5 parts of watermiscible vitamin Es and 0.004 part of adding container of La-SOD, stir, until fully dissolving; Take by weighing 0.08 part of 4.5 parts of Aloe extraction solution and germall BP antiseptic again and add in the solution, and stir, on the uniform liquid dropping ground non-woven fabrics facial film with gained, then pack, the product of gained is Flos Inulae hydrosol moisture saver mask, and namely present embodiment 4.
Embodiment 5
Take by weighing 92.195 parts of Lignum Santali Albi hydrosols and put in the container, again with in 0.5 part of hyaluronic acid, 0.2 part of fish collagen, 2 parts of watermiscible vitamin Es and 0.005 part of adding container of La-SOD, stir, until fully dissolving; Take by weighing 0.1 part of 5 parts of Aloe extraction solution and germall BP antiseptic again and add in the solution, and stir, on the uniform liquid dropping ground non-woven fabrics facial film with gained, then pack, the product of gained is Lignum Santali Albi hydrosol moisture saver mask, and namely present embodiment 5.
Embodiment 1~5 described non-woven fabrics facial film material is the material that viscose rayon and terylene mix, and wherein the viscose rayon percentage by weight is 90%, fiber weight percentage is 10%, and the grammes per square metre of non-woven fabrics facial film is 60 gram/m 2, be shaped as face shape, size and the size of people's face, the non-woven fabrics facial film has the hole of suitable size at eye, nostril and face place, can expose with person who happens to be on hand for an errand's eyes, nostril and face.
The weight that embodiment 1~5 described stock solution drops on the non-woven fabrics facial film is 12 ± 0.2 grams.
In order to verify the safety of product of the present invention, embodiment 1~5 prepared sample all is sent to the third party and detects the detection of skin zest, continuous 14 days skin irritation test is all done with 3 regular grade New Zealand white rabbit to each sample by testing agency, red and swollen and edema phenomenon all appear in the skin of 3 white rabbits in 14 days, third party testing agency is the nonirritant material according to " disposable use hygienic article sanitary standard " the repeatedly intact skin irritant test skin irritation strength grading standard in (GB15979-2002) to embodiment 1~5 prepared sample conclusion.
In order to verify whether product of the present invention meets corresponding hygienic practice, embodiment 1~5 prepared sample all is sent to third party testing agency testing product and whether meets corresponding hygienic practice, third party testing agency passes through outward appearance, fragrance, pH value, methanol content, arsenic content, lead content, mercury content, total plate count, the yeast and mold number, the excrement colibacillus group number, the indexs such as bacillus pyocyaneus (Pseudomonas aeruginosa) number and staphylococcus aureus number detect, testing result is requirement up to specification all, judges that at last embodiment 1~5 prepared sample all meets " facial film " requirement for restriction (QB/T2872-2007).
In order further to understand the present invention, the inventor organizes 50 volunteers to test, and 50 volunteers are divided into into 5 groups, every group of 10 people.Test divides to be carried out in two days, the method of first day test is that (the used non-woven fabrics facial film of non-woven fabrics facial film and the present invention is identical using the pure water facial film for every volunteer, but the liquid that adds is pure water) frontly test respectively forehead with Fes Kai Er SK-III type hand-held digital display skin moisture tester first, left face, the moisture of right face and chin skin, and get arithmetic mean of instantaneous value, then apply facial film of the present invention after cleaning face, take off facial film after 20 minutes, wash one's face with clear water, dry face, test forehead with the skin moisture tester again after 1 hour, left face, the skin moisture content of right face and the same position of chin, and get arithmetic mean of instantaneous value; The method of second day test is identical with the first day method of testing, but used facial film is facial film of the present invention, the first group tests this experimental example 1 product, the second group tests this experimental example 2 products, the 3rd group tests this experimental example 3 products, the 4th group tests this experimental example 4 products, and the 5th group tests this experimental example 5 products.Every group of 10 volunteers get arithmetic mean of instantaneous value with the result who tests, test result such as following table:
Figure BSA00000817993900041
After five groups of volunteers used respectively pure water facial film and embodiment 1~5 prepared product to compare, embodiment 1~5 prepared product all can obviously improve the facial skin moisture.
In order further to understand the present invention, the inventor continues to provide the embodiment product of each group test to above-mentioned 5 groups of volunteers, and using product of the present invention to follow up a case by regular visits to after 3 days, 7 days, 15 days and 30 days to 50 volunteers, by to each four times follows up a case by regular visits to of 50 volunteers, the ill symptomses such as facial sufferings, redness, edema, inflammation all do not occur, verified again the safety of product of the present invention.
In order further to understand the present invention, the inventor respectively extracts 1 volunteer and describes from above-mentioned 5 groups of volunteers:
Case 1: Tang * *, the woman, 29 years old, using the front facial skin moisture meansigma methods of the present invention was 19.8%, and forehead has fine wrinkle, use after this experimental example 1 product 1 month, facial skin moisture meansigma methods is 27.4%, has increased by 7.6% before, and the fine wrinkle at forehead place obviously alleviates simultaneously, facial skin is also more flexible, in whole use procedure without any ill symptoms.
Case 2: Xue *, the woman, 32 years old, using the front facial skin moisture meansigma methods of the present invention was 22.8%, and forehead has fine wrinkle, use after this experimental example 2 products 1 month, facial skin moisture meansigma methods is 29.5%, has increased by 6.7% before, the fine wrinkle at forehead place obviously alleviates simultaneously, facial skin also more originally had to a certain degree and bleached, and skin is also more flexible, in whole use procedure without any ill symptoms.
Case 3: Lee * *, woman, 43 years old, be drying property skin, skin is often peeled, especially at dry weather, the decortication phenomenon is more obvious, uses that facial skin moisture meansigma methods is 13.6% only before the present invention, uses after this experimental example 3 products 1 month, facial skin moisture meansigma methods is 22.3%, increased by 8.7%, dry skin has obtained quite significantly improving, even if at dry weather, the situation that skin peeling also seldom occurs, in whole use procedure without any ill symptoms.
Case 4: Ouyang *, the woman, 26 years old, using the front facial skin moisture meansigma methods of the present invention was 24.3%, and there is slight speckle seal in face, use after this experimental example 4 products 1 month, facial skin moisture meansigma methods is 30.5%, has increased by 6.2% before, and facial skin is also more flexible simultaneously, on the face speckle seal also more also had and alleviated, in whole use procedure without any ill symptoms.
Case 5: white horse with a black mane * *, the woman, 35 years old, using the front facial skin moisture meansigma methods of the present invention was 17.4%, and forehead has obvious wrinkle, use after this experimental example 5 products 1 month, facial skin moisture meansigma methods is 24.2%, has increased by 6.8% before, and the fine wrinkle at forehead place obviously alleviates simultaneously, facial skin is also more flexible, in whole use procedure without any ill symptoms.

Claims (7)

1. hydrosol moisture saver mask, it is the stock solution that has moisture-keeping efficacy take hydrosol as main raw material(s) is mixed with, and then stock solution is dripped equably on the non-woven fabrics facial film, packs to form again, it is characterized in that described stock solution is to adopt following percentage by weight prescription:
Hyaluronic acid 0.1~0.5%,
Fish collagen 0.2~1%,
Watermiscible vitamin E 0.5~2%,
Modified Superoxide Dismutase 0.001~0.005%
Aloe extraction solution 2~5%,
Germall BP antiseptic 0.05~0.1%,
Hydrosol with moisture-keeping efficacy adds to 100%.
2. a kind of hydrosol moisture saver mask according to claim 1 is characterized in that, described fish collagen is to adopt the skin of pure natural tilapia to produce its molecular weight≤1000D through enzymolysis.
3. a kind of hydrosol moisture saver mask according to claim 1 is characterized in that, described Modified Superoxide Dismutase is La-SOD, and its activity unit number is 4,000,000 U/ grams.
4. a kind of hydrosol moisture saver mask according to claim 1 is characterized in that, described Aloe extraction solution is to be added in an amount of deionized water with fresh aloe, water decocts, until the solid matter content of aqueous solution is to 5.0~5.1%, and then cooling, filter, decolouring forms.
5. a kind of hydrosol moisture saver mask according to claim 1, it is characterized in that described hydrosol with moisture-keeping efficacy is wherein any one or wherein arbitrarily two or more the combination in MEIGUI CHUNLU, Radix Hamamelidis Mollis hydrosol, jasmine hydrosol, Flos Inulae hydrosol and the Lignum Santali Albi hydrosol.
6. a kind of hydrosol moisture saver mask according to claim 1 is characterized in that, described non-woven membrane material is the in proportion arbitrary proportion material of mixing of viscose rayon or terylene or both, and the non-woven membrane grammes per square metre is 30~150 gram/m 2, non-woven membrane is shaped as face shape, has the hole of suitable size at eye, nostril and face place, can expose with person who happens to be on hand for an errand's eyes, nostril and face.
7. a kind of hydrosol moisture saver mask according to claim 1 is characterized in that, the weight of every non-woven fabrics facial film dropping stock solution is 8~15 grams.
CN201210516696.4A 2012-12-04 2012-12-04 Hydrolat moisturizing facial mask Expired - Fee Related CN102935055B (en)

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CN103285174A (en) * 2013-06-29 2013-09-11 王玉欣 Nursing ointment for repairing scars
CN104887609A (en) * 2015-06-19 2015-09-09 广州科玛生物科技有限公司 Moisturizing mask liquid and preparation method thereof
CN104905985A (en) * 2014-05-30 2015-09-16 中国石油化工股份有限公司 Application of lauric acid modified SOD in cosmetics
CN106389171A (en) * 2015-08-03 2017-02-15 孙伟治 Purely-botanic natural-component-compounded hydrolat-series toner and making method thereof
CN106667811A (en) * 2017-03-17 2017-05-17 蒋旭峰 Additive-free skincare cosmetic containing deep purifying factors CPEs
CN106726683A (en) * 2016-12-28 2017-05-31 安徽檀鑫科技有限公司 A kind of Multifunctional mask liquid and its preparation technology
CN106860214A (en) * 2017-01-17 2017-06-20 长沙协浩吉生物工程有限公司 A kind of compound method of ferment moisture saver mask
CN106860072A (en) * 2017-01-17 2017-06-20 长沙协浩吉生物工程有限公司 A kind of compound method of ferment moisturizing day cream
CN107875069A (en) * 2017-12-22 2018-04-06 广州环亚化妆品科技有限公司 A kind of mineral clay mask and preparation method thereof
CN109528526A (en) * 2018-12-29 2019-03-29 株洲千金药业股份有限公司 Plant essence skin conditioning agent and preparation method thereof and oil control and acne removal application

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Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103285174A (en) * 2013-06-29 2013-09-11 王玉欣 Nursing ointment for repairing scars
CN104905985A (en) * 2014-05-30 2015-09-16 中国石油化工股份有限公司 Application of lauric acid modified SOD in cosmetics
CN104905985B (en) * 2014-05-30 2017-12-29 中国石油化工股份有限公司青岛安全工程研究院 Application of the laurate modification SOD in cosmetics
CN104887609A (en) * 2015-06-19 2015-09-09 广州科玛生物科技有限公司 Moisturizing mask liquid and preparation method thereof
CN104887609B (en) * 2015-06-19 2017-09-12 广州科玛生物科技股份有限公司 A kind of moisture saver mask liquid and preparation method thereof
CN106389171A (en) * 2015-08-03 2017-02-15 孙伟治 Purely-botanic natural-component-compounded hydrolat-series toner and making method thereof
CN106726683A (en) * 2016-12-28 2017-05-31 安徽檀鑫科技有限公司 A kind of Multifunctional mask liquid and its preparation technology
CN106860214A (en) * 2017-01-17 2017-06-20 长沙协浩吉生物工程有限公司 A kind of compound method of ferment moisture saver mask
CN106860072A (en) * 2017-01-17 2017-06-20 长沙协浩吉生物工程有限公司 A kind of compound method of ferment moisturizing day cream
CN106667811A (en) * 2017-03-17 2017-05-17 蒋旭峰 Additive-free skincare cosmetic containing deep purifying factors CPEs
CN107875069A (en) * 2017-12-22 2018-04-06 广州环亚化妆品科技有限公司 A kind of mineral clay mask and preparation method thereof
CN109528526A (en) * 2018-12-29 2019-03-29 株洲千金药业股份有限公司 Plant essence skin conditioning agent and preparation method thereof and oil control and acne removal application

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