CN102935055B - Hydrolat moisturizing facial mask - Google Patents
Hydrolat moisturizing facial mask Download PDFInfo
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- CN102935055B CN102935055B CN201210516696.4A CN201210516696A CN102935055B CN 102935055 B CN102935055 B CN 102935055B CN 201210516696 A CN201210516696 A CN 201210516696A CN 102935055 B CN102935055 B CN 102935055B
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- hydrolat
- hydrosol
- skin
- moisture
- moisturizing
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Abstract
The invention discloses a hydrolat moisturizing facial mask. The method comprises the following steps: putting a hydrolat with moisturizing efficacy into a container, then adding hyaluronic acid, fish collagen, water soluble vitamin and lauric acid modified superoxide dismutase into the container, and stirring the solution until the solution is completely dissolved; then adding aloe extracting solution and supguard GM-BP preservative into the solution, and uniformly stirring, uniformly dripping the obtained liquid onto a non-woven fabric facial mask, then conducting sealed packaging to obtain a product, namely the hydrolat moisturizing facial mask. The hydrolat with moisturizing efficacy includes rose hydrolat, witch hazel hydrolat, jasmine hydrolat, marigold hydrolat, sandalwood hydrolat and the like, and any one of the hydrolat or combination of any two or more of the hydrolat can be adopted. The hydrolat moisturizing facial mask prepared by adopting the method disclosed by the invention has the advantages that the moisturizing effect is prominent, and the mask is safe and can not irritate a human body, and the like.
Description
Technical field:
The present invention relates to cosmetic field, particularly a kind of hydrosol moisture saver mask.
Background technology:
Hydrosol has another name called Hua Shui, crystal's oil, and it is the water staying in distillation extraction quintessence oil process, is the by-product of producing quintessence oil.Hydrosol, except containing a small amount of derived essential oil, also contains the water-soluble substances in whole plants, and its contained mineral nutrient (as tannin and flavonoid) is that quintessence oil lacks.The characteristic of its low concentration is easily absorbed by skin, and completely without essence and alcoholic content, fragrance is light pleasant, non-stimulated to skin gentleness, is a kind of ideal cosmetic material.
Facial film is a kind of cosmetics that personage commonly uses of liking to be beautiful, and the form of facial film is also varied, has powder face pack, cream pack, membranaceous facial film etc., and facial film function is also varied, as moisturizing, whitening, moisten, speckle dispelling etc.Moisture saver mask is a kind of conventional facial film, generally adds also moisturizing composition in facial film, and as glycerol etc., the existing pure natural raw material of these moisturizing compositions, also has industrial chemicals.If facial film producer adopts low-grade raw material, or working condition and processing technique poor, the facial film of production not only can not be improved looks, and easily brings on the contrary ill symptomses such as sufferings, inflammation, redness, indivedual severe patients are even disfeatured.
Hydrosol is also little as the application of cosmetic material or product, the hydrosol product major part of selling in the market is just simply distributed into bottle hydrosol and sells, the cosmetics that it are developed to various functions are not a lot, and the facial film take hydrosol as primary raw material on market is also fewer.
One " collagen wet-retaining face mask and preparation method thereof " by name authorized by State Intellectual Property Office, number of patent application is 200610020676.2 patent of invention, it is with porcine collagen, cellulose derivative, starch, wetting agent and cross-linking agent are a kind of facial film prepared by raw material, collagen protein is a kind of well cosmetic material, it has skin care, slow down aging, beauty treatment, the effects such as wrinkle-chasing, but the degree that collagen protein is absorbed by the body is very important index, the collagen protein (General Requirements≤1000D) of micromolecule amount is easily absorbed by people, the prepared porcine collagen of patent of the disclosure does not describe its molecular weight.In addition, patent of the present disclosure does not explain with regard to effect of product, also has the weak points such as processing step is many, complicated operation with this disclosed method converted products.
State Intellectual Property Office discloses one " a kind of moisture saver mask " by name, number of patent application is 201110103296.6 patent of invention, it is with deionized water, Sorbitol, hydrolytic collagen, vitamin E, potassium alginate, hyaluronic acid, two imidazolidinyl urea and Radix Mori extract are a kind of facial film prepared by raw material, there are some shortcomings and deficiencies parts in the patent of the disclosure: two imidazolidinyl urea are a kind of antiseptic that are mainly used in cosmetics, it is to reach antiseptical object by slow release formaldehyde, generally its addition should not exceed 0.3%, and the addition of this open formula is 1-2%, therefore prepared product is to have potential harm to human body, the molecular weight of hydrolytic collagen used does not explain, product efficacy prepared by disclosed method does not explain etc.
For the shortcomings and deficiencies part of prior art, on market, on some present situations lack of standardization of moisture saver mask and market, hydrosol is applied in to the less situation in facial film aspect, there is plurality of advantages in conjunction with hydrosol again, therefore, exploitation is a kind of take hydrosol as main raw material(s), and the facial film with moisture-keeping efficacy is just significant.
Summary of the invention:
The technical problem to be solved in the present invention is the hydrosol facial film take hydrosol as main raw material(s) is mixed with moisture-keeping efficacy.Prepared hydrosol facial film except have moistening effect obviously, also have human body without advantages such as any stimulations.
The technical scheme that the present invention solves the problems of the technologies described above is: have the stock solution of moisture-keeping efficacy take hydrosol as main raw material(s) is mixed with, then stock solution is dripped equably on non-woven fabrics facial film, then pack.
The stock solution that the present invention has a moisture-keeping efficacy be by following formulation by weight than formulated:
Hyaluronic acid 0.1～0.5%,
Fish collagen 0.2～1%,
Watermiscible vitamin E 0.5～2%,
La-SOD 0.001～0.005%,
Aloe extraction solution 2～5%,
Germall BP antiseptic 0.05～0.1%,
The hydrosol with moisture-keeping efficacy adds to 100%.
In stock solution of the present invention, described fish collagen is to adopt the skin of pure natural tilapia to produce through enzymolysis, its molecular weight≤1000D.
In stock solution of the present invention, described La-SOD activity unit number is 4,000,000 U/ gram.
In stock solution of the present invention, described Aloe extraction solution is to be added in appropriate deionized water with fresh aloe, and water decocts, until the solid matter content of aqueous solution is to 5.0～5.1%, then cooling, filters, and decolouring forms.
In stock solution of the present invention, the described hydrosol with moisture-keeping efficacy is wherein any one or wherein arbitrarily two or more the combination in MEIGUI CHUNLU, Radix Hamamelidis Mollis hydrosol, jasmine hydrosol, Flos Inulae hydrosol and Lignum Santali Albi hydrosol.
Non-woven membrane of the present invention, material is viscose rayon or terylene or both materials that arbitrary proportion mixes in proportion, grammes per square metre is 30～150 grams/m
2, be shaped as face shape, have the hole of suitable size at eye, nostril and face place, so that eyes, nostril and face can expose.
Preparation method of the present invention comprises the steps:
Take in proportion hydrosol and put into a container, then hyaluronic acid, fish collagen, watermiscible vitamin E and Modified Superoxide Dismutase are added to container, stir, until dissolve completely;
Take in proportion Aloe extraction solution and germall BP antiseptic adds in solution, and stir, gained liquid is the stock solution with moisture-keeping efficacy;
Stock solution is evenly dripped on ground non-woven fabrics facial film, and the weight of every non-woven fabrics facial film dropping stock solution is 8～15 grams, then packs, and the product of gained is product of the present invention.
Using method of the present invention is: after clean face, take the packing of product of the present invention apart, the facial film of the inside is taken out and applied equably at face, after 15～30 minutes, take facial film.
The selected composition of the present invention has following effect and effect:
Hyaluronic acid: it can improve skin-nourishing metabolism, makes that skin is tender, smooth, wrinkle removing, increase elasticity, prevents aging, is again good Percutaneous absorption enhancer in moisturizing.
Fish collagen: it can supplement each layer of required nutrition of skin, makes collagen increased activity in skin, has skin care, the effects such as slow down aging, beauty treatment, wrinkle-chasing.
Watermiscible vitamin E: the effect such as elasticity that it has the aging of preventing, regulates female incretion and keep skin.
Lauric acid is superoxide dismutase modified: it is higher with respect to there is no superoxide dismutase modified activity, half-life is longer, heat stability higher (storing 3.2 years non-inactivations at 25 ℃), and it has removing interior free yl, defying age, the effects such as the formation of inhibition melanocyte.
Aloe extraction solution: the effects such as it has anti-inflammation, moistens moisturizing, defying age, hypo-allergenic, it contains water conservation lignin, has strong permeability, helps nutrient substance Transdermal absorption.
MEIGUI CHUNLU: it have keep the skin wet, the effect such as moisturizing, fast antiinflammatory, antiallergic, antipruritic and slow down aging.
Radix Hamamelidis Mollis hydrosol: it can significantly improve skin lock water moisture-retaining capacity, energy rapid permeability skin, allows cell possess sufficient moisture, and it also has good moisturizing effects to the skin after shining, it also has the aging skin of reparation cell in addition, improves the effects such as dull-looking skin.
Jasmine hydrosol: the skin of its dry hydropenia is very effective, and it has superior moistening effect, can make skin softness, flexible, can improve little microgroove, makes skin delicate bright.
Flos Inulae hydrosol: it has and well moisten moistening effect dry skin, in addition, it also has bactericidal antiphlogistic, improves responsive skin quality, desalinates effects such as repairing cicatrix.
Lignum Santali Albi hydrosol: it has and well moisten moistening effect the skin of aging, dry and hydropenia, increases the water content of skin, in addition it also there is prevention wrinkle, the effect such as neural of relaxing.
Facial film of the present invention contains the multiple composition with moist moisturizing, and it is skin care well, keeps the moisture of skin, and it can also the dry skin of gentrify simultaneously, and delay skin aging, prevents or slow down the appearance of wrinkle of skin.The product raw material overwhelming majority used is pure natural raw material, and safety is without any zest.
The specific embodiment
Embodiment 1
Take 96.349 parts of MEIGUI CHUNLU and put in a container, then 0.001 part of 0.1 part of hyaluronic acid, 1 part of fish collagen, 0.5 part of watermiscible vitamin E and La-SOD is added in container, stir, until dissolve completely; Take 0.05 part of 2 parts of Aloe extraction solution and germall BP antiseptic again and add in solution, and stir, the uniform liquid of gained is dripped on ground non-woven fabrics facial film, then pack, the product of gained is MEIGUI CHUNLU moisture saver mask, i.e. the present embodiment 1.
Embodiment 2
Take 95.138 parts of Radix Hamamelidis Mollis hydrosols and put in a container, then 0.002 part of 0.2 part of hyaluronic acid, 0.8 part of fish collagen, 0.8 part of watermiscible vitamin E and La-SOD is added in container, stir, until dissolve completely; Take 0.06 part of 3 parts of Aloe extraction solution and germall BP antiseptic again and add in solution, and stir, the uniform liquid of gained is dripped on ground non-woven fabrics facial film, then pack, the product of gained is Radix Hamamelidis Mollis hydrosol moisture saver mask, i.e. the present embodiment 2.
Embodiment 3
Take 94.277 parts of jasmine hydrosols and put in a container, then 0.003 part of 0.3 part of hyaluronic acid, 0.6 part of fish collagen, 1 part of watermiscible vitamin E and La-SOD is added in container, stir, until dissolve completely; Take 0.07 part of 4 parts of Aloe extraction solution and germall BP antiseptic again and add in solution, and stir, the uniform liquid of gained is dripped on ground non-woven fabrics facial film, then pack, the product of gained is jasmine hydrosol moisture saver mask, i.e. the present embodiment 3.
Embodiment 4
Take 93.116 parts of Flos Inulae hydrosols and put in a container, then 0.004 part of 0.4 part of hyaluronic acid, 0.4 part of fish collagen, 1.5 parts of watermiscible vitamin Es and La-SOD is added in container, stir, until dissolve completely; Take 0.08 part of 4.5 parts of Aloe extraction solution and germall BP antiseptic again and add in solution, and stir, the uniform liquid of gained is dripped on ground non-woven fabrics facial film, then pack, the product of gained is Flos Inulae hydrosol moisture saver mask, i.e. the present embodiment 4.
Embodiment 5
Take 92.195 parts of Lignum Santali Albi hydrosols and put in a container, then 0.005 part of 0.5 part of hyaluronic acid, 0.2 part of fish collagen, 2 parts of watermiscible vitamin Es and La-SOD is added in container, stir, until dissolve completely; Take 0.1 part of 5 parts of Aloe extraction solution and germall BP antiseptic again and add in solution, and stir, the uniform liquid of gained is dripped on ground non-woven fabrics facial film, then pack, the product of gained is Lignum Santali Albi hydrosol moisture saver mask, i.e. the present embodiment 5.
Non-woven fabrics facial film material described in embodiment 1～5 is the material that viscose rayon and terylene mix, and wherein viscose rayon percentage by weight is 90%, fiber weight percentage is 10%, and the grammes per square metre of non-woven fabrics facial film is 60 grams/m
2, be shaped as face shape, size and the size of face, non-woven fabrics facial film has the hole of suitable size at eye, nostril and face place, can expose with person who happens to be on hand for an errand's eyes, nostril and face.
The weight that stock solution described in embodiment 1～5 drops on non-woven fabrics facial film is 12 ± 0.2 grams.
In order to verify the safety of product of the present invention, the prepared sample of embodiment 1～5 is all sent to third party and detects detection of skin zest, the skin irritation test of continuous 14 days all does by 3 regular grade New Zealand white rabbit to each sample in testing agency, in 14 days all there is not red and swollen and edema phenomenon in the skin of 3 white rabbits, third party testing agency is the repeatedly intact skin irritant test skin irritation strength grading standard in (GB15979-2002) according to " disposable use hygienic article sanitary standard ", the sample conclusion prepared to embodiment 1～5 is nonirritant material.
In order to verify whether product of the present invention meets corresponding hygienic practice, the prepared sample of embodiment 1～5 is all sent to third party testing agency testing product and whether meets corresponding hygienic practice, third party testing agency passes through outward appearance, fragrance, pH value, methanol content, arsenic content, lead content, mercury content, total plate count, yeast and mold number, excrement colibacillus group number, the indexs such as bacillus pyocyaneus (Pseudomonas aeruginosa) number and staphylococcus aureus number detect, the testing result requirement that all conforms with the regulations, finally judge that the prepared sample of embodiment 1～5 all meets " facial film " restriction requirement (QB/T2872-2007).
In order further to understand the present invention, the inventor organizes 50 volunteers to test, and 50 volunteers are divided into into 5 groups, every group of 10 people.Test point is carried out for two days, the method of first day test is that (non-woven fabrics facial film is identical with the present invention's non-woven fabrics facial film used using pure water facial film for every volunteer, but the liquid adding is pure water) frontly first test respectively forehead with Fes Kai Er SK-III type hand-held digital display skin moisture tester, left face, the moisture of right face and chin skin, and get arithmetic mean of instantaneous value, then after cleaning face, apply facial film of the present invention, after 20 minutes, take off facial film, wash one's face with clear water, dry face, after 1 hour, test forehead with skin moisture tester again, left face, the skin moisture content of right face and the same position of chin, and get arithmetic mean of instantaneous value, the method of test in second day is identical with first day method of testing, but facial film used is facial film of the present invention, the first group tests this experimental example 1 product, the second group tests this experimental example 2 products, the 3rd group tests this experimental example 3 products, the 4th group tests this experimental example 4 products, and the 5th group tests this experimental example 5 products.Tested result is got arithmetic mean of instantaneous value by every group of 10 volunteers, and test result is as following table:
After five groups of volunteers use respectively pure water facial film and the prepared product of embodiment 1～5 to contrast, the prepared product of embodiment 1～5 all can obviously improve facial skin moisture.
In order further to understand the present invention, the inventor continues to provide the embodiment product of each group of test to above-mentioned 5 groups of volunteers, and to 50 volunteers using product of the present invention to follow up a case by regular visits to after 3 days, 7 days, 15 days and 30 days, by following up a case by regular visits to each four times of 50 volunteers, all there is not the ill symptomses such as facial sufferings, redness, edema, inflammation, verified again the safety of product of the present invention.
In order further to understand the present invention, the inventor 1 volunteer of each extraction from above-mentioned 5 groups of volunteers describes:
Case 1: Tang × ×, female, 29 years old, using the front facial skin moisture meansigma methods of the present invention was 19.8%, and forehead has fine wrinkle, after using this experimental example 1 product 1 month, facial skin moisture meansigma methods is 27.4%, has increased by 7.6% before, and the fine wrinkle at forehead place obviously alleviates simultaneously, facial skin is also more flexible, in whole use procedure without any ill symptoms.
Case 2: Xue ×, female, 32 years old, using the front facial skin moisture meansigma methods of the present invention was 22.8%, and forehead has fine wrinkle, after using this experimental example 2 product 1 month, facial skin moisture meansigma methods is 29.5%, has increased by 6.7% before, the fine wrinkle at forehead place obviously alleviates simultaneously, facial skin also more originally had to a certain degree and bleached, and skin is also more flexible, in whole use procedure without any ill symptoms.
Case 3: Lee × ×, female, 43 years old, for drying property skin, skin is often peeled, especially at dry weather, decortication phenomenon is more obvious, and using facial skin moisture meansigma methods before the present invention is only 13.6%, after using this experimental example 3 product 1 month, facial skin moisture meansigma methods is 22.3%,, increased by 8.7%, dry skin has obtained quite significantly improving, even if at dry weather, also seldom there is the situation of skin peeling, in whole use procedure without any ill symptoms.
Case 4: Ouyang ×, female, 26 years old, using the front facial skin moisture meansigma methods of the present invention was 24.3%, and face has slight speckle to print, after using this experimental example 4 product 1 month, facial skin moisture meansigma methods is 30.5%, has increased by 6.2% before, and facial skin is also more flexible simultaneously, speckle on the face prints also more also to be had and alleviated, in whole use procedure without any ill symptoms.
Case 5: white horse with a black mane × ×, female, 35 years old, using the front facial skin moisture meansigma methods of the present invention was 17.4%, and forehead has obvious wrinkle, after using this experimental example 5 product 1 month, facial skin moisture meansigma methods is 24.2%, has increased by 6.8% before, and the fine wrinkle at forehead place obviously alleviates simultaneously, facial skin is also more flexible, in whole use procedure without any ill symptoms.
Claims (2)
1. a hydrosol moisture saver mask, it is the stock solution take hydrosol as main raw material(s) is mixed with moisture-keeping efficacy, then stock solution is dripped on non-woven fabrics facial film equably by the amount of 8～15 grams/piece, then packs and form, it is characterized in that, described stock solution is to adopt following percentage by weight formula:
Described fish collagen is to adopt the skin of pure natural tilapia to produce through enzymolysis, its molecular weight≤1000D;
The activity unit number of described La-SOD is 4,000,000 U/ gram;
Described Aloe extraction solution is to be added in appropriate deionized water with fresh aloe, and water decocts, until the solid matter content of aqueous solution is to 5.0～5.1%, then cooling, filters, and decolouring forms.
2. a kind of hydrosol moisture saver mask according to claim 1, it is characterized in that, the hydrosol with moisture-keeping efficacy in described former formula of liquid is wherein any one or wherein arbitrarily two or more the combination in MEIGUI CHUNLU, Radix Hamamelidis Mollis hydrosol, jasmine hydrosol, Flos Inulae hydrosol and Lignum Santali Albi hydrosol.
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| CN201210516696.4A CN102935055B (en) | 2012-12-04 | 2012-12-04 | Hydrolat moisturizing facial mask |
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| CN201210516696.4A CN102935055B (en) | 2012-12-04 | 2012-12-04 | Hydrolat moisturizing facial mask |
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| CN102935055B true CN102935055B (en) | 2014-05-21 |
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Cited By (1)
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| CN106902072A (en) * | 2017-01-17 | 2017-06-30 | 长沙协浩吉生物工程有限公司 | A kind of compound method of ferment moisture retention night cream |
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| CN104905985B (en) * | 2014-05-30 | 2017-12-29 | 中国石油化工股份有限公司青岛安全工程研究院 | Application of the laurate modification SOD in cosmetics |
| CN104887609B (en) * | 2015-06-19 | 2017-09-12 | 广州科玛生物科技股份有限公司 | A kind of moisture saver mask liquid and preparation method thereof |
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