CN109481382A - A kind of moisture-regulating agent of the water containing bermuda lily and preparation method thereof and facial mask application - Google Patents
A kind of moisture-regulating agent of the water containing bermuda lily and preparation method thereof and facial mask application Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
The invention discloses moisture-regulating agent of a kind of water containing bermuda lily and preparation method thereof and facial mask application.The moisture-regulating agent includes following parts by weight of component: 80 ~ 120 parts of bermuda lily water, 0.4 ~ 0.65 part of Semen Persicae extract, 0.08 ~ 0.15 part of aloe barbadensis Miller leaf juice powder, print plus 0.08 ~ 0.15 part of fruit seed oil, 0.08 ~ 0.15 part of camellia seed oil, 0.08 ~ 0.15 part of peony seed oil；The moisture-regulating agent uses pure lily water replenishing water and preserving moisture, Chinese prescription is formed with aloe, Semen Persicae extract compatibility, using the natural skin cares grease such as rational proportion collocation print plus fruit seed oil, camellia seed oil and peony seed oil, moisten effect can be played to skin, the problem of being applied to replenishing water and preserving moisture facial mask, can effectively solve skin missing moisture.
Description
Technical field
The present invention relates to cosmetic technical fields, more particularly, to a kind of moisture-regulating agent of water containing bermuda lily
And preparation method thereof and facial mask application.
Background technique
In recent years, with the raising of people 's material life level, the mankind increasingly focus on maintain oneself, various health care products,
Skin care item emerge one after another.As skin care item common in a kind of daily life, the purpose is to make up makeup removing and wash one's face still facial mask
Insufficient cleaning cooperates other essential ingredients to realize other maintenance functions, such as replenishing water and preserving moisture, beauty on this basis
White, anti-aging, Sage Extract etc..And some replenishing water and preserving moisture products in the market, the effect is unsatisfactory for moisturizing, hold time compared with
It is short；Certain products are even added to the substances such as lead, mercury in formula or promote cortex cracking-off agent, have damaged the normal physiology of skin
Metabolism, cannot not only achieve the purpose that replenishing water and preserving moisture, be also easy to cause serious skin problem.Therefore it provides one kind can solve
Skin lacks moisture problem, and the facial mask of replenishing water and preserving moisture is of great significance.
Bermuda lily is rich in protein, sugar, phosphorus, iron and various trace elements, medical value and food with higher
With value, bermuda lily sweet and slightly bitter taste, cold nature is flat, effect Yin nourishing and lung moistening, and external application moisten skin, current fresh rare by lily
Flower is applied to the relevant report of preparation replenishing water and preserving moisture facial mask.
Summary of the invention
Exist for the application technology of the technical deficiency of replenishing water and preserving moisture facial mask and lily in the prior art in terms of facial mask
Deficiency, the present invention provides a kind of moisture-regulating agent of water containing bermuda lily, and the moisture-regulating agent is made using lily water
For the important component of replenishing water and preserving moisture, compatibility can play skin with a variety of natural moisture preserving ingredients such as aloe, Semen Persicae extract
The problem of moisten effect is applied to preparation replenishing water and preserving moisture product, can effectively solve skin missing moisture.
Another technical problem to be solved by the present invention is that providing the preparation of the moisture-regulating agent of the water containing bermuda lily
Method.
A present invention also technical problems to be solved are to provide the application of the moisture-regulating agent of the water containing bermuda lily.
The purpose of the present invention is achieved through the following technical solutions:
A kind of moisture-regulating agent of water containing bermuda lily, each component including following parts by weight: bermuda lily are provided
80~120 parts of water, 0.4~0.65 part of Semen Persicae extract, 0.08~0.15 part of aloe barbadensis Miller leaf juice powder, print plus fruit seed oil
0.08~0.15 part, 0.08~0.15 part of camellia seed oil, 0.08~0.15 part of peony seed oil.
Preferably, the moisture-regulating agent of the water containing bermuda lily includes each component of following parts by weight: bermuda lily
85~100 parts of water of flower, 0.45~0.55 part of Semen Persicae extract, 0.09~0.12 part of aloe barbadensis Miller leaf juice powder, print plus fruit seed
Oily 0.09~0.12 part, 0.09~0.12 part of camellia seed oil, 0.09~0.12 part of peony seed oil.
It is further preferred that the moisture-regulating agent includes each component of following parts by weight: bermuda lily water 90~95
Part, 0.48~0.52 part of Semen Persicae extract, 0.09~0.1 part of aloe barbadensis Miller leaf juice powder, print plus fruit seed oil 0.09~0.1
Part, 0.09~0.1 part of camellia seed oil, 0.09~0.1 part of peony seed oil.
The technological gap of existing skin care moisturizing is filled up in the moisture-regulating agent of the water containing bermuda lily, using Chinese medicine " monarch
Minister assistant makes " thought guidance progress prescription compatibility, using lily as monarch drug in a prescription, Semen Persicae is ministerial drug, and aloe is adjutant, wherein hundred
Flower sweet and slightly bitter taste is closed, cold nature is flat, effect Yin nourishing and lung moistening, and external application is moistened skin；Fat oil contained by Semen Persicae can make skin angle
The softening of matter layer, moisturizes skin care；Aloe barbadensis Miller leaf juice powder is rich in aloe polysaccharide, protein, organic acid, amino acid and microelement
Etc. multiple efficacies ingredient, have strengthen immunity, moisturizing, anti-oxidant and other effects.The present invention passes through long term test, according to reasonable
The components compatibility is formed the raw material of the moisture-regulating agent of the water containing bermuda lily by dosage, and is applied to replenishing water and preserving moisture face
Film not only can effectively solve the problem of skin lacks moisture, moreover it is possible to so that skin is kept long-acting and moisten.
For the moisturizing effect for further playing collaboration, the moisture-regulating agent also includes print plus fruit seed oil, tea seed
The natural skin cares grease such as oil and peony seed oil can make skin keep moistening for a long time with " monarch " Chinese prescription compatibility, and
And skin will not be damaged, wherein camellia seed oil contains vitamin E and antioxidant content, it can protect skin, and skin is made to have light
Pool, and peony seed oil unsaturated fatty acid rich in, external application can eliminate pigment deposition with beautifying face and moistering lotion, reduce wrinkle, make
Skin exquisiteness is bright and clean, high resilience, contains alpha-linolenic acid and linoleic acid in print plus fruit seed oil, on the one hand, alpha-linolenic acid can lead to
Inhibition inflammation and skin care are crossed, enables skin moisten strong, may additionally facilitate the life of skin corium collagen and elastin fiber
It is long, it enables skin soft fine and smooth, on the other hand, there is excellent affinity and penetration to skin, be easy to be absorbed by the skin, to mend
Lipid nutrient needed for filling skin, repairs dry skin and the skin fat sour water damaged due to contact surface activating agent is flat,
Maintain and enhance the normal configuration and function of Skin Cell film and interstitial；Simultaneously ventilative water conservation can also be formed in skin surface
Film weakens the moisture loss of deep skin, moistens skin holding smooth flexible.
The moisture-regulating agent of the water containing bermuda lily can be under the essential idea of compatibility of the present invention, using this field
Existing achievable technological means is prepared.
It is that will print to add fruit present invention simultaneously provides the preferred preparation method of the moisture-regulating agent of the water containing bermuda lily
Seed oil, camellia seed oil, peony seed oil mixing, are added Semen Persicae extract, aloe barbadensis Miller leaf juice powder and bermuda lily water,
Be thoroughly mixed uniformly to get.
Wherein, the bermuda lily water in the present invention can be made by conventional method in that art, and the present invention provides one kind can
The method of choosing is made: after bermuda lily and solvent are mixed, extracting by conventional method in that art.The solvent can be
The Extraction solvent of this field routine, preferably one of water, ethyl alcohol and 1,3-BDO or a variety of.The method of the extraction can
For infusion process, percolation, decocting method, reflux extraction or ultrasonic extraction etc..Preferably, the bermuda lily water is by white flower
After lily bermuda lily and ethyl alcohol mixing, obtained using ultrasonic extraction.
Present invention simultaneously provides application of the moisture-regulating agent of the water containing bermuda lily in facial mask.
It is further preferred that the facial mask includes mask substrate and facial mask essence, the mask substrate is seaweed mask
Cloth contains the moisture-regulating agent in the facial mask essence.Further, the Essence is made of A phase and B phase raw material,
Wherein contain the moisture-regulating agent in B phase.
Essence of the present invention can be carried on other mask substrates, it is preferable that, mask substrate selection sea
Algae facial mask cloth.Seaweed mask cloth is made of alginate fibre, due to alginate fibre be rich in polysaccharide, high unsaturated fatty acid, taurine,
Carotenoid, steroid be pure and a variety of life active compounds such as laminine, as mask substrate, soft, stealthy, patch skin,
The water-retaining property that skin can be increased increases the moistening effect of skin, increases the austerity and elasticity of skin, makes loose skin
Reply younger state.The present invention is arranged in pairs or groups using seaweed mask cloth and Essence of the present invention, and being adapted property is very good, Essence load
In seaweed mask cloth, load effect is good, and moisture-regulating effect complements each other.
Further, the facial mask essence is prepared by following parts by weight of component:
The A phase includes: 0.88~1.65 part of butanediol, 0.64~1.2 part of methyl gluceth -20, hyaluronic acid
0.24~0.45 part of sodium, 0.72~1.35 part of trehalose, 0.24~0.45 part of dipotassium glycyrrhizinate, 0.72~1.35 part of glycerol, urine
0.24~0.45 part of Bursin, 0.4~0.65 part of Scleroglucan, 0.16~0.3 part of parahydroxyacet-ophenone, acrylic acid (ester) class/
0.08~0.15 part of 0.08~0.15 part of C10-30 alkylol acrylamide acid esters cross-linked polymer and laruyl alcohol phosphate potassium；
The B phase include: 80~125 parts of moisture-regulating agent, 0.08~0.15 part of arginine, decoyl hydroximic acid 0.024~
0.045 part, 0.04~0.075 part of glycerol caprylate, 0.32~0.6 part of 1,2- pentanediol.
Further, the facial mask essence is prepared by following parts by weight of component:
The A phase includes: 0.99~1.32 part of butanediol, 0.72~0.96 part of methyl gluceth -20, hyalomitome
0.27~0.36 part of sour sodium, 0.81~1.08 part of trehalose, 0.27~0.36 part of dipotassium glycyrrhizinate, 0.72~0.96 part of glycerol,
0.27~0.36 part of allantoin, 0.45~0.6 part of Scleroglucan, 0.18~0.24 part of parahydroxyacet-ophenone, acrylic acid (ester) class/
0.09~0.12 part of 0.09~0.12 part of C10-30 alkylol acrylamide acid esters cross-linked polymer and laruyl alcohol phosphate potassium；
The B phase include: 90~100 parts of moisture-regulating agent, 0.09~0.12 part of arginine, decoyl hydroximic acid 0.027~
0.036 part, 0.045~0.06 part of glycerol caprylate, 0.36~0.48 part of 1,2- pentanediol.
Minimum 2000 molecular weight hyaluronic acids of molecular weight, high-effective penetrating provide skin long Kubo on the market for present invention selection
Wet power, rapid maintenance skin is dry and astringent, uncomfortable, can more promote the synthesis of skin self collagen fiber and hyaluronic acid.With other battalion
It supports components matching to use, the more preferable effect for promoting nutrient absorption can be played.Facial mask of the invention utilizes the guarantor of Chinese prescription
Wet conditioner acts synergistically with nutritional ingredients such as Sodium Hyaluronates, blending the east and the west, there is prevention to make with maintenance problem skin
With can form water conservation film in skin surface, enable skin keep bright water profit state, alleviate skin sensation of dryness.
The present invention provides a kind of preparation method of preferred facial mask essence, and the preparation method of the facial mask essence includes
Following steps:
S1. above-mentioned A phase raw material is sequentially added in water phase pot, stirring is warming up to 80~90 DEG C, stirs, and keeps the temperature
It is spare；
S2. after mixing evenly, homogeneous 1~10 minute, vacuumizes, and constant temperature 10~20 minutes；
When being S3. cooled to 40~45 DEG C, above-mentioned B phase raw material is sequentially added, stirs, every a raw material of addition,
A raw material under stirring adds again to after dissolving；
When being S4. cooled to 32~38 DEG C, discharging is stood to get the facial mask essence.
Further, in step S1, the temperature is 80~85 DEG C；Preferably, the temperature is 85 DEG C.
Further, in step S2, the homogenizing time is 2~5 minutes；Preferably, the homogenizing time is 3 minutes.
Further, in step S3, when being cooled to 45 DEG C, above-mentioned B phase raw material is added, stirs.
Further, in step S4, when being cooled to 38 DEG C, discharging is stood to get the facial mask essence.
Compared with prior art, the beneficial effects of the present invention are:
The present invention provides a kind of moisture-regulating agent of water containing bermuda lily, are guidance with Chinese medicine " monarch " thought
Prescription is carried out, using lily as monarch drug in a prescription, Semen Persicae is ministerial drug, and aloe is adjutant, wherein lily sweet and slightly bitter taste, cold nature is flat, function
Yin nourishing and lung moistening is imitated, external application is moistened skin；Fat oil contained by Semen Persicae can be such that keratoderma softens, and moisturize skin care；Curacao
Aloe leaf juice powder has enhancing rich in multiple efficacies ingredients such as aloe polysaccharide, protein, organic acid, amino acid and microelements
Immunity, moisturizing, anti-oxidant and other effects.The present invention passes through long term test, forms the components compatibility according to reasonable dosage
The raw material of the moisture-regulating agent of the water containing bermuda lily, and it is applied to replenishing water and preserving moisture facial mask, it not only can effectively solve skin
The problem of lacking moisture, moreover it is possible to make skin keep long-acting and moisten.
Also containing the natural skin cares oil such as print plus fruit seed oil, camellia seed oil and peony seed oil in moisture-regulating agent of the invention
Rouge can make skin keep moistening for a long time using rational proportion and " monarch " Chinese prescription compatibility, and will not damage skin
Skin.
From the point of view of overall composition, the present invention provides a kind of full-featured green face pack, by key component ratio
It holds, containing a variety of beneficial skin ingredients such as vitamin, protein, allantoin in product, and Chinese prescription and Sodium Hyaluronate is assisted
Same-action, it is blending the east and the west, there is prevention and maintenance effect to problem skin, water conservation film can be formed in skin surface, enable flesh
Skin keeps bright water to moisten state, alleviates skin sensation of dryness.
Replenishing water and preserving moisture facial mask of the invention uses pure white colored lily water moisturizing, does not add a drop secondary water, without essence, nothing
Preservative, under the collocation of pure plant ingredient, not only remained bermuda lily water moisten skin the effect of, but also be added to more
The pure natural beauty plant component of kind, makes it complement each other, skin is allowed to fully absorb nutrition.
The present invention uses the facial mask cloth of alginate fibre preparation, and soft, stealthy, patch skin, collocation is rich in nourishing and moisturizing ingredient
Facial mask essence can increase the water-retaining property of skin, increase the moistening effect of skin, increase the austerity and elasticity of skin,
Loose skin is set to restore younger state.
Specific embodiment
To facilitate the understanding of the present invention, present invention work more comprehensively, is meticulously described below in conjunction with embodiment, but this hair
Bright protection scope is not limited to embodiment in detail below.
Unless otherwise defined, all technical terms used hereinafter and the normally understood meaning of those skilled in the art
It is identical.Technical term used herein is intended merely to the purpose of description specific embodiment, it is no intended to limit of the invention
Protection scope.
For convenience of description, it is exemplified below heretofore described primary raw material as follows, unless stated otherwise its preparation side
Method is commercially available.Specifically:
Bermuda lily water, LILIUM CANDIDUM FLOWER WATER, in the present invention, the bermuda lily water
It is preferred that bermuda lily grinding and sieving (30 mesh) is used, according to the solid-liquid ratio (g:mL) of 1:18, with the second of volume fraction 90%
Alcohol ultrasonic extraction 85min is obtained, wherein the frequency of ultrasonic extraction is 30kHz, power 600W.
Semen Persicae extract, PRUNUS PERSICA (PEACH) KERNEL EXTRACT, regular market purchase.
Aloe barbadensis Miller leaf juice powder, ALOE BARBADENSIS LEAF JUICE POWDER, regular market purchase.
Print plus fruit seed oil, PLUKENETIA VOLUBILIS SEED OIL are purchased from bright Ji Ya.
Camellia seed oil, CAMELLIA OLEIFERA SEED OIL are purchased from Guangzhou Ming Hui Fine Chemical Co., Ltd.
Peony seed oil, LINUM USITATISSIMUM (LINSEED) SEED OIL are purchased from bright Ji Ya.
Scleroglucan (hydrolysis Scleroglucan), Hydrolyzed Sclerotium Gum (HSG), regular market purchase hydrolyzes small
The chemical component of pyrenomycetes glue is scleroglucan, is the hydrolysis natural small molecule amount β-Portugal decomposited by the white beautiful bacterium of a fungi plant
Glycan can prevent the invasion of extraneous bacterial virus, stop intradermal nutrients with splendid water lock ability and skin care bioactivity
The loss of matter, mechanicalness, it is physical, also there is chemically and in terms of the protection of biological skin injury remarkable efficacy, in addition,
Hydrolyzing Scleroglucan is also a kind of skin care item skin sense " modifying agent ", can assign the tender sense of cunning of facial mask essence velvet.
Dipotassium glycyrrhizinate, regular market purchase, No. CAS: 68797-35-3, structural formula is as follows:
Dipotassium glycyrrhizinate is the effect of Radix Glycyrrhizae proposes neutralization acquisition through water ingredient, is extensively answered in medicine food and daily chemicals field
With in the present invention, being cooperateed with Sodium Hyaluronate and play antibacterial removing toxic substances, anti-inflammatory antiallergic and other effects, and corticosteroid can be activated
The effect of closing object, preventing cosmetic allergic contact dermatitis from reacting, promotes the absorption of skin care item.
Allantoin, regular market purchase, CAS 97-59-6, structural formula are as follows:
Allantoin is a kind of hydantoin derivatives as made from glyoxalic acid, urea synthesizing, and allantoin can promote cell raw
Long, quickening wound healing, cutin-softening albumen simultaneously alleviate xerodermia, and in the present invention, it is just right that allantoin can play
Sterilization and anticorrosion, nourish moisturizing, it is anti-oxidant convergence etc. multi-efficiencies.
Decoyl hydroximic acid, regular market purchase, No. CAS: 7377-03-9.
Glycerol caprylate, regular market purchase, No. CAS: 26402-26-6.
1,2- pentanediol, regular market purchase, No. CAS: 5343-92-0.
Parahydroxyacet-ophenone, regular market purchase, No. CAS: 99-93-4.
Butanediol, regular market purchase, No. CAS: 107-88-0.
Methyl gluceth -20, regular market purchase, No. CAS: 68239-42-9.
Sodium Hyaluronate, regular market purchase, No. CAS: 9067-32-7.
Trehalose, regular market purchase, No. CAS: 99-20-7.
Arginine, regular market purchase, No. CAS: 74-79-3.
Glycerol, regular market purchase, No. CAS: 56-81-5.
Laruyl alcohol phosphate potassium, regular market purchase, structural formula are as follows:
Laruyl alcohol phosphate potassium have class phosphatide characteristic, it is natural, highly-safe, it is nontoxic it is non-stimulated have excellent emulsification,
The performances such as dispersion, softness are not only able to play certain emulsification in the present invention, moreover it is possible to assist with Sodium Hyaluronate, allantoin
With moisture-keeping function is played, keep skin is long-acting to moisten.
Acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer, regular market purchase is by multiple at being grouped as
Copolymer has excellent emulsification, dispersion, thickening power, is cooperateed with Scleroglucan as skin care item skin sense " modifying agent ", can be assigned
It gives facial mask essence and comfortably slides tender sense.
Embodiment 1
The present embodiment provides a kind of replenishing water and preserving moisture facial mask, facial mask includes mask substrate and facial mask essence, and mask substrate is
Seaweed mask cloth, facial mask essence are made of A phase and B phase raw material, are specifically prepared by following parts by weight of component:
A phase includes: 0.88 part of butanediol, 1.2 parts of methyl gluceth -20,0.24 part of Sodium Hyaluronate, trehalose
0.72 part, 0.45 part of dipotassium glycyrrhizinate, 0.72 part of glycerol, 0.24 part of allantoin, 0.65 part of Scleroglucan, parahydroxyacet-ophenone
0.15 part of 0.16 part, acrylic acid (ester) class/0.08 part of C10-30 alkylol acrylamide acid esters cross-linked polymer and laruyl alcohol phosphate potassium；
B phase includes: 81 parts of moisture-regulating agent, 0.15 part of arginine, 0.024 part of decoyl hydroximic acid, glycerol caprylate 0.04
Part, 0.6 part of 1,2- pentanediol.
Moisture-regulating agent in the present embodiment B phase raw material uses the moisture-regulating agent of the water containing bermuda lily, including following
The each component of parts by weight: 80 parts of bermuda lily water, 0.4 part of Semen Persicae extract, 0.08 part of aloe barbadensis Miller leaf juice powder, print add
Fruit seed oil 0.15 part, 0.15 part of camellia seed oil, 0.08 part of peony seed oil；
The preparation method of the moisture-regulating agent of the above-mentioned water containing bermuda lily, includes the following steps: to print plus fruit seed is oily, oily
Tea-seed oil, peony seed oil mixing, are added Semen Persicae extract, aloe barbadensis Miller leaf juice powder and bermuda lily water, sufficiently stir
Mix be uniformly mixed to get.
The present embodiment facial mask essence described according to the preparation of following processing step:
S1. above-mentioned A phase raw material is sequentially added in water phase pot, stirring is warming up to 85 DEG C, stirs, and keeps the temperature standby
With；
S2. after mixing evenly, homogeneous 3 minutes, vacuumize, and constant temperature 15 minutes；
When being S3. cooled to 45 DEG C, above-mentioned B phase raw material is added, stirs, every a raw material of addition is stirred to molten
Xie Houzai a raw material under adding；
When being S4. cooled to 38 DEG C, discharging is stood to get the facial mask essence.
Embodiment 2
The present embodiment provides a kind of replenishing water and preserving moisture facial mask, facial mask includes mask substrate and facial mask essence, and mask substrate is
Seaweed mask cloth；Facial mask essence is made of A phase and B phase raw material, is specifically prepared by following parts by weight of component:
A phase includes: 1.65 parts of butanediol, 0.64 part of methyl gluceth -20,0.45 part of Sodium Hyaluronate, trehalose
1.35 parts, 0.24 part of dipotassium glycyrrhizinate, 1.35 parts of glycerol, 0.45 part of allantoin, 0.4 part of Scleroglucan, parahydroxyacet-ophenone 0.3
0.08 part of part, acrylic acid (ester) class/0.15 part of C10-30 alkylol acrylamide acid esters cross-linked polymer and laruyl alcohol phosphate potassium；
B phase includes: 121 parts of moisture-regulating agent, 0.08 part of arginine, 0.045 part of decoyl hydroximic acid, glycerol caprylate
0.075 part, 0.32 part of 1,2- pentanediol.
The processing step of facial mask essence is prepared with embodiment 1.
Moisture-regulating agent in the present embodiment B phase raw material includes each component of following parts by weight: bermuda lily water 120
Part, 0.65 part of Semen Persicae extract, 0.15 part of aloe barbadensis Miller leaf juice powder, print plus fruit seed oil 0.08 part, 0.08 part of camellia seed oil,
0.15 part of peony seed oil；The preparation method of the moisture-regulating agent of the above-mentioned water containing bermuda lily is walked referring to the operation of embodiment 1
Suddenly.
Embodiment 3
The present embodiment provides a kind of replenishing water and preserving moisture facial mask, facial mask includes mask substrate and facial mask essence, and mask substrate is
Seaweed mask cloth；Facial mask essence is made of A phase and B phase raw material, is specifically prepared by following parts by weight of component:
A phase includes: 1.32 parts of butanediol, 0.72 part of methyl gluceth -20,0.36 part of Sodium Hyaluronate, trehalose
1.08 parts, 0.27 part of dipotassium glycyrrhizinate, 0.96 part of glycerol, 0.27 part of allantoin, 0.45 part of Scleroglucan, parahydroxyacet-ophenone
0.12 part of 0.18 part, acrylic acid (ester) class/0.09 part of C10-30 alkylol acrylamide acid esters cross-linked polymer and laruyl alcohol phosphate potassium；
B phase includes: 90 parts of moisture-regulating agent, 0.12 part of arginine, 0.027 part of decoyl hydroximic acid, glycerol caprylate 0.045
Part, 0.36 part of 1,2- pentanediol.
The processing step of facial mask essence is prepared with embodiment 1.
Moisture-regulating agent in the present embodiment B phase raw material includes each component of following parts by weight: 85 parts of bermuda lily water,
0.6 part of Semen Persicae extract, 0.14 part of aloe barbadensis Miller leaf juice powder, print plus fruit seed oily 0.09 part, 0.11 part of camellia seed oil, tree peony
0.13 part of seed oil；The preparation method of the moisture-regulating agent of the above-mentioned water containing bermuda lily, referring to the operating procedure of embodiment 1.
Embodiment 4
The present embodiment provides a kind of replenishing water and preserving moisture facial mask, facial mask includes mask substrate and facial mask essence, and mask substrate is
Seaweed mask cloth；Facial mask essence is made of A phase and B phase raw material, is specifically prepared by following parts by weight of component:
A phase includes: 1.4 parts of butanediol, 1 part of methyl gluceth -20,0.4 part of Sodium Hyaluronate, trehalose 1.2
Part, 0.36 part of dipotassium glycyrrhizinate, 1.2 parts of glycerol, 0.42 part of allantoin, 0.6 part of Scleroglucan, 0.28 part of parahydroxyacet-ophenone,
0.1 part of acrylic acid (ester) class/0.12 part of C10-30 alkylol acrylamide acid esters cross-linked polymer and laruyl alcohol phosphate potassium；
B phase includes: 100 parts of moisture-regulating agent, 0.13 part of arginine, 0.04 part of decoyl hydroximic acid, glycerol caprylate 0.07
Part, 0.5 part of 1,2- pentanediol.
The processing step of facial mask essence is prepared with embodiment 1.
Moisture-regulating agent in the present embodiment B phase raw material includes each component of following parts by weight: 98 parts of bermuda lily water,
It is 0.12 part of 0.55 part of Semen Persicae extract, 0.09 part of aloe barbadensis Miller leaf juice powder, print plus fruit seed oil, 0.09 part of camellia seed oil, male
Red 0.12 part of seed oil；The preparation method of the moisture-regulating agent of the above-mentioned water containing bermuda lily, referring to the operating procedure of embodiment 1.
Embodiment 5
The present embodiment provides a kind of replenishing water and preserving moisture facial mask, facial mask includes mask substrate and facial mask essence, and mask substrate is
Seaweed mask cloth；Facial mask essence is made of A phase and B phase raw material, is specifically prepared by following parts by weight of component:
A phase includes: 0.99 part of butanediol, 0.96 part of methyl gluceth -20,0.27 part of Sodium Hyaluronate, trehalose
0.81 part, 0.27 part of dipotassium glycyrrhizinate, 0.81 part of glycerol, 0.32 part of allantoin, 0.5 part of Scleroglucan, parahydroxyacet-ophenone
0.09 part of 0.24 part, acrylic acid (ester) class/0.1 part of C10-30 alkylol acrylamide acid esters cross-linked polymer and laruyl alcohol phosphate potassium；
B phase includes: 91 parts of moisture-regulating agent, 0.09 part of arginine, 0.036 part of decoyl hydroximic acid, glycerol caprylate 0.06
Part, 0.48 part of 1,2- pentanediol.
The processing step of facial mask essence is prepared with embodiment 1.
Moisture-regulating agent in the present embodiment B phase raw material includes each component of following parts by weight: 90 parts of bermuda lily water,
It is 0.11 part of 0.48 part of Semen Persicae extract, 0.12 part of aloe barbadensis Miller leaf juice powder, print plus fruit seed oil, 0.12 part of camellia seed oil, male
Red 0.1 part of seed oil；The preparation method of the moisture-regulating agent of the above-mentioned water containing bermuda lily, referring to the operating procedure of embodiment 1.
Embodiment 6
The present embodiment provides a kind of replenishing water and preserving moisture facial mask, facial mask includes mask substrate and facial mask essence, and mask substrate is
Seaweed mask cloth；Facial mask essence is made of A phase and B phase raw material, is specifically prepared by following parts by weight of component:
A phase includes: 1.2 parts of butanediol, 0.8 part of methyl gluceth -20,0.3 part of Sodium Hyaluronate, trehalose 1
Part, 0.32 part of dipotassium glycyrrhizinate, 0.9 part of glycerol, 0.3 part of allantoin, 0.48 part of Scleroglucan, 0.2 part of parahydroxyacet-ophenone, third
0.1 part of olefin(e) acid (ester) class/0.09 part of C10-30 alkylol acrylamide acid esters cross-linked polymer and laruyl alcohol phosphate potassium；
B phase includes: 96 parts of moisture-regulating agent, 0.11 part of arginine, 0.03 part of decoyl hydroximic acid, glycerol caprylate 0.05
Part, 0.4 part of 1,2- pentanediol.
The processing step of facial mask essence is prepared with embodiment 1.
Moisture-regulating agent in the present embodiment B phase raw material includes each component of following parts by weight: 95 parts of bermuda lily water,
0.5 part of Semen Persicae extract, 0.1 part of aloe barbadensis Miller leaf juice powder, print plus fruit seed oily 0.1 part, 0.1 part of camellia seed oil, peony seeds
0.09 part of oil；The preparation method of the moisture-regulating agent of the above-mentioned water containing bermuda lily, referring to the operating procedure of embodiment 1.
Embodiment 7
Indices detection, detection are carried out to the facial mask that Examples 1 to 6 is prepared according to standard QB/T 2872-2017
As a result as follows:
(1) organoleptic indicator
Appearance: translucent liquid shape；
Fragrance: without essence addition, the natural fragrance of raw material bermuda lily meet regulation fragrance.
(2) physical and chemical index
PH value (25 DEG C): 6.25
Viscosity (2#, 6rpm): 1920mpas
Heat-resistant stability: kept at 40 ± 1 DEG C for 24 hours, restore to after room temperature with test before no significant difference；
Cold-resistant stability: keeping for 24 hours at -8 ± 2 DEG C, after restoring to room temperature with test before no significant difference；
Photostability: it is kept under ultraviolet light for 24 hours, with no significant difference before test.
(3) hygienic chemistry index
Mask product prepared by the present invention is detected by the method for " cosmetics health specification " 2015, testing result is shown in Table 1.
Table 1
| Sanitary index | Standard requirements | Testing result | Single item evaluation |
| Total plate count, CFU/g | ≤1000 | ≤420 | It is qualified |
| Yeast and mold sum, CFU/g | ≤100 | ≤35 | It is qualified |
| Heat-resisting coliform, g | It must not detect | It is not detected | It is qualified |
| Staphylococcus aureus, g | It must not detect | It is not detected | It is qualified |
| Pseudomonas aeruginosa, g | It must not detect | It is not detected | It is qualified |
| Mercury, mg/kg | ≤1 | ≤1 | It is qualified |
| Lead, mg/kg | ≤10 | ≤4 | It is qualified |
| Arsenic, mg/kg | ≤2 | ≤2 | It is qualified |
| Cadmium, mg/kg | ≤5 | ≤4 | It is qualified |
| Methanol, mg/kg | ≤2000 | ≤500 | It is qualified |
| Dioxanes, mg/kg | ≤30 | ≤21 | It is qualified |
| Asbestos, mg/kg | It must not detect | It is not detected | It is qualified |
(4) application method
After face cleaning, facial mask of the invention is lain on the face, smooths facial mask with hand.
(5) specified risk material safety evaluation
Each raw material for preparing facial mask to the present invention carries out specified risk material security evaluation, and specific assessment result is shown in Table 2.
Table 2
8 skin irritation test of embodiment
By taking replenishing water and preserving moisture facial mask prepared by the method for Examples 1 to 6 as an example, stimulation of the replenishing water and preserving moisture facial mask to skin is observed
Property and allergic reaction, provide reference to evaluate its safety.
(1) skin irritation test is carried out using rabbit, divides intact skin group and damage skin group, for 24 hours by rabbit before test
Back backbone diamond wool shaves off, and the replenishing water and preserving moisture facial mask and rabbit skin and mucosa prepared respectively with the embodiment of the present invention 1~6 is kept
After contacting 1d, continuous 7d, whether there is or not the stimulate the reactions such as erythema, oedema for observation skin.
(2) skin allergy experiment is carried out using cavy, the replenishing water and preserving moisture facial mask prepared with the embodiment of the present invention 1~6 weekly
It is kept in contact 2 times with guinea pig skin mucous membrane, contacts 4h or more every time, continuous 3 weeks, whether there is or not the allergy such as erythema, oedema for observation skin
Reaction.
Experimental result:
The intact skin and damaged skin of rabbit, remove after being intended for single use or be used for multiple times for 24 hours, respectively at 1,24,48,
72h observation, is showed no erythema and oedema, and stimulate the reaction mean scores are < 0.5, nonirritant.
In guinea pig skin allergic experiment, does not occur the cutaneous anaphylaxises such as the obvious erythema of skin, oedema and other are systemic
Allergic reaction.
Therefore, replenishing water and preserving moisture facial mask of the invention will not cause irritative response to rabbit intact skin and damage skin,
To guinea pig skin without allergic reaction, there is good cutaneous safety.
Comparative example 1
The process conditions of this comparative example reference embodiment 6, the main distinction are: substituting bermuda lily using deionized water
Water.
Comparative example 2
The process conditions of this comparative example reference embodiment 6, the main distinction are: moisture-regulating agent is extracted without Semen Persicae
Object.
Comparative example 3
The process conditions of this comparative example reference embodiment 6, the main distinction are: moisture-regulating agent is free of Aloe Barbadensis Miller
Juice powder.
Comparative example 4
Referring to the process conditions of embodiment 6, the main distinction is this comparative example: moisture-regulating agent without print plus fruit seed oil,
Camellia seed oil and peony seed oil.
Comparative example 5~8
Referring to the process conditions of embodiment 6, the main distinction is for comparative example 5~8, the moisture-regulating of the water containing bermuda lily
Agent respectively includes following parts by weight of component:
Replenishing water and preserving moisture effect experiment
1. test material: replenishing water and preserving moisture facial mask prepared by Examples 1 to 6 and comparative example 1~8.
2. subjects: volunteer between 20~45 years old.
3. test method:
In the environment of 25 DEG C of room temperature, relative humidity 50%, the back of the hand first is cleaned with clean water, then respectively by difference wait try
It is rectangular that sample uniformly divides into 3 × 3cm.Embodiment and comparative example apply the facial mask of correlation method preparation in specified skin part,
After 30min and 60min, remove each determinand, 0 after removing facial mask, 60,120, digital skin moisture content is used after 240min
Tester is measured the skin of subject's application facial mask, obtains skin moisture content.
4. test result: test result is shown in Table 3.
Influence of 3 facial mask of table to skin moisture content
As shown in Table 3:
(1) facial mask of Examples 1 to 6 preparation 0min after removing facial mask can make skin moisture content reach 45% or more,
And it can keep skin moisture 40% or more in the 240min after removing, there is significant replenishing water and preserving moisture effect；When application
Between 60min, remove 0min skin moisture content after facial mask and be compared to application time 30min and be not significantly reduced, illustrate this
Inventing the application in 60min of long-acting replenishing water and preserving moisture facial mask and not will cause moisture content is led to the nutrition being dissolved in water by facial mask back suction
The phenomenon that substance is lost with the back suction of moisture content；Wherein, the replenishing water and preserving moisture effect of embodiment 6 is best.
(3) the moisture-regulating agent ingredient that facial mask prepared by comparative example 1~4 uses is different from the present invention, the facial mask application time
60min is compared with 30min, and 0min skin moisture content has dropped 17% or so after removing facial mask, and skin moisturizing effect is poor.
(4) the moisture-regulating agent component ratio and difference of the invention that facial mask prepared by comparative example 5~8 uses, moisturizing are protected
Wet significant effect reduces.
Use feeling scoring
The replenishing water and preserving moisture facial mask that above-described embodiment 1~6 and comparative example 1~8 are prepared carries out effect performance test, with
Totally 200 people are tested sample to each 100 people of men and women, and tested sample did not used other drugs or cosmetics during test, with 2 weeks
Experience scores mean value to investigate the performance for evaluating replenishing water and preserving moisture facial mask of the present invention, and evaluation criterion is as shown in table 4.
4 standards of grading of table
| Scoring | Description |
| 80~100 | Effect is obvious/without allergic phenomena |
| 60~80 | Effect is general/without allergic phenomena |
| 40~60 | Having a degree of improves/has a little allergic phenomena |
| < 40 points | No effect/allergy serious |
After test carries out 4 weeks (2 times/d), acquisition experimental result is as shown in table 5:
Table 5
Experimental result is shown: replenishing water and preserving moisture facial mask disclosed by the invention uses pure white colored lily water moisturizing, does not add one
Secondary water is dripped, without essence, preservative free increase the moistening effect of skin under the collocation of pure plant ingredient, increase flesh
The austerity and elasticity of skin make loose skin restore younger state.
Obviously, above-described embodiment is only intended to clearly illustrate technical solution of the present invention example, and is not
Restriction to embodiments of the present invention.For those of ordinary skill in the art, on the basis of the above description also
It can make other variations or changes in different ways.There is no necessity and possibility to exhaust all the enbodiments.It is all
Made any modifications, equivalent replacements, and improvements etc. within the spirit and principles in the present invention should be included in right of the present invention and want
Within the protection scope asked.
Claims (10)
1. a kind of moisture-regulating agent of water containing bermuda lily, which is characterized in that each component including following parts by weight: white flower hundred
Close 80 ~ 120 parts of water of flower, 0.4 ~ 0.65 part of Semen Persicae extract, 0.08 ~ 0.15 part of aloe barbadensis Miller leaf juice powder, print plus fruit seed oil
0.08 ~ 0.15 part, 0.08 ~ 0.15 part of camellia seed oil, 0.08 ~ 0.15 part of peony seed oil.
2. moisture-regulating agent according to claim 1, which is characterized in that each component including following parts by weight: bermuda lily
85 ~ 100 parts of water of flower, 0.45 ~ 0.55 part of Semen Persicae extract, 0.09 ~ 0.12 part of aloe barbadensis Miller leaf juice powder, print plus fruit seed oil
0.09 ~ 0.12 part, 0.09 ~ 0.12 part of camellia seed oil, 0.09 ~ 0.12 part of peony seed oil.
3. moisture-regulating agent according to claim 1 or claim 2, which is characterized in that each component including following parts by weight: white flower hundred
Close 90 ~ 95 parts of water of flower, 0.48 ~ 0.52 part of Semen Persicae extract, 0.09 ~ 0.1 part of aloe barbadensis Miller leaf juice powder, print plus fruit seed oil
0.09 ~ 0.1 part, 0.09 ~ 0.1 part of camellia seed oil, 0.09 ~ 0.1 part of peony seed oil.
4. the preparation method of any one of claims 1 to 3 moisture-regulating agent, which is characterized in that be that will print to add fruit seed oil, oil
Tea-seed oil, peony seed oil mixing, are added Semen Persicae extract, aloe barbadensis Miller leaf juice powder and bermuda lily water, sufficiently stir
Mix be uniformly mixed to get.
5. application of any one of the claim 1 ~ 4 moisture-regulating agent in facial mask.
6. application according to claim 5, which is characterized in that the facial mask includes mask substrate and facial mask essence, institute
Stating mask substrate is seaweed mask cloth, contains the described in any item moisture-regulating agent of claim 1 ~ 4 in the facial mask essence.
7. application according to claim 6, which is characterized in that the facial mask essence is made of A phase and B phase raw material, institute
Stating B phase includes the described in any item moisture-regulating agent of claim 1 ~ 4；
The A phase includes: 0.88 ~ 1.65 part of butanediol, 0.64 ~ 1.2 part of methyl gluceth -20, Sodium Hyaluronate 0.24
~ 0.45 part, 0.72 ~ 1.35 part of trehalose, 0.24 ~ 0.45 part of dipotassium glycyrrhizinate, 0.72 ~ 1.35 part of glycerol, allantoin 0.24 ~
0.45 part, 0.4 ~ 0.65 part of Scleroglucan, 0.16 ~ 0.3 part of parahydroxyacet-ophenone, acrylic acid (ester) class/C10-30 alkylol acrylamide
0.08 ~ 0.15 part of 0.08 ~ 0.15 part of acid esters cross-linked polymer and laruyl alcohol phosphate potassium；
The B phase include: 80 ~ 125 parts of moisture-regulating agent, 0.08 ~ 0.15 part of arginine, 0.024 ~ 0.045 part of decoyl hydroximic acid,
0.04 ~ 0.075 part of glycerol caprylate, 0.32 ~ 0.6 part of 1,2- pentanediol.
8. application according to claim 7, which is characterized in that the A phase includes: 0.99 ~ 1.32 part of butanediol, methyl Portugal
- 20 0.72 ~ 0.96 parts of sugar alcohol polyethers, 0.27 ~ 0.36 part of Sodium Hyaluronate, 0.81 ~ 1.08 part of trehalose, dipotassium glycyrrhizinate
0.27 ~ 0.36 part, 0.81 ~ 0.96 part of glycerol, 0.27 ~ 0.36 part of allantoin, 0.45 ~ 0.6 part of Scleroglucan, parahydroxyacet-ophenone
0.18 ~ 0.24 part, acrylic acid (ester) class/0.09 ~ 0.12 part of C10-30 alkylol acrylamide acid esters cross-linked polymer and laruyl alcohol phosphoric acid
0.09 ~ 0.12 part of ester potassium；
The B phase include: 90 ~ 100 parts of moisture-regulating agent, 0.09 ~ 0.12 part of arginine, 0.027 ~ 0.036 part of decoyl hydroximic acid,
0.045 ~ 0.06 part of glycerol caprylate, 0.36 ~ 0.48 part of 1,2- pentanediol.
9. according to the described in any item applications of claim 5 ~ 8, which is characterized in that the preparation method of the facial mask essence includes
Following steps:
S1. above-mentioned A phase raw material is sequentially added in water phase pot, stirring is warming up to 80 ~ 90 DEG C, stirs, and keeps the temperature spare；
S2. after mixing evenly, homogeneous 1 ~ 10 minute, vacuumizes, and constant temperature 10 ~ 20 minutes；
When being S3. cooled to 40 ~ 45 DEG C, above-mentioned B phase raw material is sequentially added, stirs, every a raw material of addition, stirring is extremely
A raw material under adding again after dissolution；
When being S4. cooled to 32 ~ 38 DEG C, discharging is stood to get the facial mask essence.
10. application according to claim 9, which is characterized in that in step S2, the homogenizing time is 2 ~ 5 minutes；It is preferred that
Ground, the homogenizing time are 3 minutes.
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