CN103211743A - Preparation method of smoothing toner composition containing natural plant extract - Google Patents
Preparation method of smoothing toner composition containing natural plant extract Download PDFInfo
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- CN103211743A CN103211743A CN2013101574009A CN201310157400A CN103211743A CN 103211743 A CN103211743 A CN 103211743A CN 2013101574009 A CN2013101574009 A CN 2013101574009A CN 201310157400 A CN201310157400 A CN 201310157400A CN 103211743 A CN103211743 A CN 103211743A
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- 238000002360 preparation method Methods 0.000 title claims abstract description 7
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- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 claims abstract description 8
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- Cosmetics (AREA)
Abstract
The invention relates to a preparation method of a smoothing toner composition containing a natural plant extract. The method comprises the following steps of: 1) placing a phase 1 into a container, mixing and heating until completely dissolving, wherein the phase 1 comprises glycerol, butanediol and hydrogenated lecithin; 2) adding a phase 2 to phase 1, and uniformly stirring, wherein the phase 2 comprises polydimethylsiloxane, triethylhexanoin and squalane; 3) adding a phase 3 to the solution, and mixing, wherein the phase 3 is deionized water; 4) adding a phase 4 to the solution, and uniformly mixing, wherein the phase 4 comprises hydroxyethyl cellulose, sodium hyaluronate, Carbopol1342 and deionized water; and 5) adding a phase 5 at 50 DEG C, uniformly mixing, and discharging, wherein the phase 5 comprises triethanolamine, potassium hydroxide, a saussurea involucrate extract, a peony root extract, a lilium candidum extract and a preservative. The composition is capable of improving the skin color, adjusting the dark yellow state, and enabling skin to become moist and tender and white.
Description
Present patent application be application for a patent for invention (application number: 201110297683.8 applyings date: 11-09-27, invention and created name: a kind of the profit bright color toner/smoothing toner composition and method of making the same) divide an application.
Technical field
The invention belongs to a kind of toner/smoothing toner composition and method of making the same of Titanium Dioxide.
Background technology
Because modern people's rhythm of life is fast, and is subjected to various environmental effects, the frequent drying of skin, intensely dark pool.At this situation, we have prepared this toner/smoothing toner compositions that consumer is liked, and deep layer is nourished, the conditioning skin, improves the colour of skin, adjusts dark yellow state, make skin moist tender white.
Chinese invention patent application (application number: 200910010837.3 applyings date: 2009-03-24) disclose a kind of skincare humectant.It is made of according to the following number of weight ratio following component: the skin protection base material: natural dimethylamino proline acid: glycerol: Mel: shea butter: vitamin E=80-120: 5-12: 1-3: 10-20: 1-3: 2-4.This invention contains shea butter, glycerol, Mel isoreactivity and nourishes the composition of preserving moisture, and can help rapidly to moisten dry skin, makes the skin exquisiteness soft and smooth.
Chinese invention patent application (application number: 200710150410.4 applyings date: 2007-11-26) disclose a kind of cosmetic humectant that contains xylitol, it is made up of following materials based on weight: 2-10 part wetting agent, 0.1-2 part oils and fats, emulsifying agent 5-15 part, 60～80 parts in water.The cosmetic humectant of this invention can more deeply be diffused into the skin depths, combines with deep water, keeps skin moistened.
Summary of the invention
In order to solve the problem in the frequent drying of people's skin, intensely dark pool, an object of the present invention is to provide a kind of bright color toner/smoothing toner compositions of profit, said composition can deep layer nourish, nurse one's health skin, improves the colour of skin, adjusts dark yellow state, makes skin moist tender white.Another one purpose of the present invention provides a kind of above-mentioned bright color toner/smoothing toner preparation of compositions method of silk profit.
In order to realize above-mentioned first purpose, the present invention has adopted following technical scheme:
A kind of bright color toner/smoothing toner compositions of profit, described compositions comprises following component by mass percentage:
(a) 0.01% to 20% wetting agent;
(b) 0.01% to 20% skin moistening oils and fats;
(c) 0.01% to 10% surfactant;
(d) 0.01% to 10% thickening polymer;
(e) 0.01% to 10% skin conditioning agent; With
(f) 10% to 90% deionized water.
As preferably, described compositions comprises following component by mass percentage:
(a) 1% to 20% wetting agent;
(b) 0.01% to 15% skin moistening oils and fats;
(c) 0.01% to 8% surfactant;
(d) 0.01% to 8% thickening polymer;
(e) 0.01% to 8% skin conditioning agent; With
(f) 10% to 90% deionized water.
As preferred again, described compositions comprises following component by mass percentage:
(a) 2% to 20% wetting agent;
(b) 0.01% to 10% skin moistening oils and fats;
(c) 0.01% to 6% surfactant;
(d) 0.01% to 6% thickening polymer;
(e) 0.01% to 6% skin conditioning agent; With
(f) 10% to 90% deionized water.
As preferably, above-mentioned wetting agent is selected propylene glycol, sorbitol, butanediol, 1 for use, one or more in 2-hexanediol, caprylyl glycol, dipropylene glycol, glycerol, diglycerol, pentanediol, the Polyethylene Glycol, and what be preferred for this compositions is butanediol or glycerol; Described skin moistening oils and fats is selected one or more in polydimethylsiloxane, glycerol three (thylhexoic acid) ester and the squalane for use.
As preferably, above-mentioned surfactant is selected hydrolecithin for use.
As preferably, above-mentioned thickening polymer is selected one or more in carboxylic acid polyalcohol, cross-linked polyacrylate polymer, the synthetic high molecular polymer of cellulose ethers, the natural high molecular polymer for use; Preferably cellulose ethers and crosslinked acrylate polymer are more preferably by by CTFA called after hydroxyethyl-cellulose and acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer.
As preferably, above-mentioned skin conditioning agent is selected from one or more in hydrolyzed pearl, hyaluronate sodium, Herba Saussureae Involueratae extract, root of Paeonia suffruticosa Ardr. extract, the bermuda lily flower extract.
As preferably, above-mentioned said composition has also comprised one or more in pH regulator agent, food coloring, antiseptic, essence and the solvent.
The present composition also can comprise various other compositions.The function of the concrete composition of compositions of the present invention and effect will be described in more detail below.
Wetting agent
About by weight wetting agent of 0.01% to 20% among the present invention is a polyhydric alcohol, compositions described herein preferably comprises by the weight of described compositions about 1% to 20%, the wetting agent of 2%-20% more preferably, example comprises propylene glycol, sorbitol, butanediol, 1,2-hexanediol, caprylyl glycol, dipropylene glycol, glycerol, diglycerol, pentanediol, Polyethylene Glycol, and their mixture, what be preferred for this compositions is butanediol and glycerol.
The skin moistening oils and fats
Skin moistening oils and fats in the present composition can pin moisture, prevents excessive volatilization, makes skin keep the tender gloss of water.
Skin moistening oils and fats polydimethylsiloxane in the present composition, its weight by described compositions is about 0.01% to 20%, preferably is about 0.01% to 15%, and more preferably from about 0.01% to 10%.It is nontoxic, to skin and mucosa nonirritant, but eyes is had zest.It is generally accepted it is safe.Have excellent chemical stability, antistatic behaviour and breathability can freely be breathed skin.
Skin moistening oils and fats glycerol three (thylhexoic acid) ester in the present composition, its weight by described compositions is about 0.01% to 20%, preferably is about 0.01% to 15%, and more preferably from about 0.01% to 10%.It is a kind of triglycerin esters, derives from glycerol and fatty acid, is a kind of lightweight oils and fats, but antistatic is skin softening agent and conditioner.
Skin moistening oils and fats squalane in the present composition, its weight by described compositions is about 0.01% to 20%, preferably is about 0.01% to 15%, and more preferably from about 0.01% to 10%.It has the cosmetic properties of natural squalane, is a kind of colourless, tasteless, nontoxic high-purity liquid clothes hook linear paraffin, can give cosmetics fabulous and noble feel, moistens non-greasy, and it is lubricated to preserve moisture, and penetration is strong, and good stability.
Surfactant
Surfactant in the present composition is a hydrolecithin, is a kind of natural green emulsifying agent, and its main chemical compositions is lecithin, PHOSPHATIDYL ETHANOLAMINE and phosphatidylinositols.Total institute is known, and phospholipid is distributed in the animal and plant body widely, is one of important component part of biological cell.It is to metabolism, and membrane permeation plays important effect.
Phospholipid is by the lipophilic group of the fatty acid of two long-chains and glycerol be combined into and contains the material with interfacial activity that hydrophilic group constituted of phosphoric acid, amido simultaneously.Thereby it has good emulsifying dispersivity, wettability, stability and viscosity adjustment performance.Hydrolecithin among the present invention is to obtain by the hydrogenation to phospholipid of natural soybean, has overcome natural phospholipid not resistance to oxidation and thermal instability, has been widely used in each industrial circle of cosmetics and pharmaceuticals.Its feature also has persistent performance of keeping humidity, promotes the subcutaneous absorption of skin, reduces the zest of other surfactants to skin.
Thickening agent
In some embodiments, compositions of the present invention can also comprise one or more thickening agents, and described compositions comprises by the weight of described compositions about 0.01% to 10%, preferably is about 0.01% to 8%, more preferably from about 0.01% to 6% thickening agent.
The non-limiting kind of thickening agent comprises and is selected from following material: carboxylic acid polyalcohol (as Carbopol980), cross-linked polyacrylate polymer, synthetic high molecular polymer (as cellulose ethers), natural high molecular polymer (as natural gum), preferably cellulose ethers and crosslinked acrylate polymer are more preferably pressed CTFA called after hydroxyethyl-cellulose and acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer.
Skin conditioning agent
The various skin conditioner that the present composition added is Herba Saussureae Involueratae extract, root of Paeonia suffruticosa Ardr. extract, bermuda lily flower extract.
The content of the Herba Saussureae Involueratae extract that the present composition adds is preferably about 0.01% to 8% by the weight of described compositions, more preferably from about 0.01% to 6%, the active quantities of the Herba Saussureae Involueratae extract of the present composition is preferred about 0.001% to 8% by the weight of described compositions, and more preferably from about 0.001% to 6%.
The Herba Saussureae Involueratae extract that the present composition adds contains the fragrant glycoside of cloud, xuelianlactone, alkaloid, volatile oil, polysaccharide.Has antiinflammatory, antibiotic and analgesic activity.Promote the permeability of sebum, microcirculation improvement keeps skin elasticity.
The content of the root of Paeonia suffruticosa Ardr. extract that the present composition adds is preferably about 0.01% to 8% by the weight of described compositions, more preferably from about 0.01% to 6%, the active quantities of the Herba Saussureae Involueratae extract of the present composition is preferred about 0.001% to 8% by the weight of described compositions, and more preferably from about 0.001% to 6%.
The root of Paeonia suffruticosa Ardr. extract of the present composition, be rich in aminoacid, mineral, multivitamin and zinc, the selenium and other trace elements of needed by human body, have the powerful effect of releiving, can in the skin keratin cell, reduce the activity of melanin enzyme, thereby help to suppress to produce melanin; Has antibiotic, antiinflammation; The lymph circulation of chafe makes skin more glossy, improves skin matter, and after continuing to use, it is obscure and coarse to allow skin slowly say goodbye to, and skin is beautiful, the water profit.
The content of the bermuda lily flower extract that the present composition adds is preferably about 0.01% to 8% by the weight of described compositions, more preferably from about 0.01% to 6%, the active quantities of the Herba Saussureae Involueratae extract of the present composition is preferred about 0.001% to 8% by the weight of described compositions, and more preferably from about 0.001% to 6%.
The bermuda lily flower extract of the present composition, except that containing starch, protein, fat, carotene, vitamin, trace element, also contain some special nutritional labelings, as multiple alkaloids such as colchicine, have very strong moisture-retaining capacity, regulate skin moisture.
The hydrolyzed pearl of the present composition, its content is by the weight of the present composition about 0.01% to 10%, preferably be about 0.01% to 8%, be more preferably 0.01% to 6%, its active matter content is by the weight of the present composition about 0.001% to 10%, preferred about 0.001% to 8%, more preferably from about 0.001% to 6%.
The hydrolyzed pearl of the present composition is that the enzymolysis process by Margarita powder obtains, and contains a large amount of calcium ions and pearl protein, has the elimination oxygen-derived free radicals, anti-aging effects, and light speckle makes the beautiful gloss of skin.
The hyaluronate sodium of the present composition is the glutinous sugar of a kind of bionical thing, and molecular weight is greater than 1,000,000, and the hyaluronic acid sodium content of the present composition is about 0.01% to 10% by the invention composition weight meter, and is preferred about 0.01% to 5%, is more preferably 0.01% to 3%.
Contain 10% to 20% moisture in the normal human skin horny layer, it prevents skin aging, prevents that the various stimulations of external environment from all having significant role skin care.With advancing age or the variation of environment, moisture can drop to below 10%, and skin can be dry, produces wrinkle.The hyaluronate sodium of the present composition can be alleviated this problem, and its theoretical water retention value reaches 1000ml/g, is the key component of water conservation in the human body skin, and not only moistening effect is good, and do not have greasy feeling and stop up pore etc. shortcoming.Can also eliminate oxygen-derived free radicals, repair the skin that shines the back damage.
As preferred again, described compositions is made of following component by mass percentage:
It is not 0 that above-mentioned Herba Saussureae Involueratae extract, root of Paeonia suffruticosa Ardr. extract, bermuda lily flower extract and hydrolyzed pearl have a kind of composition at least.
In order to realize second above-mentioned purpose, the present invention has adopted following technical scheme:
A kind of bright color toner/smoothing toner preparation of compositions method of above-mentioned silk profit for preparing, this method comprises the steps:
1) butanediol, glycerol, hydrolecithin mix, and are heated to about 78 ℃, and dissolving forms phase 1 fully;
2) with polydimethylsiloxane, glycerol three (thylhexoic acid) ester, squalane, be heated to 78 ℃, stir, join in the phase 1 low speed homogenizing 5 minutes;
3), high speed homogenization 10-15 minute, add hydroxyethyl-cellulose, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, hyaluronate sodium again, high speed homogenization 10-15 minute with in the mixture more than the water suction;
4) be cooled to 50 ℃, add triethanolamine, Herba Saussureae Involueratae extract, root of Paeonia suffruticosa Ardr. extract, bermuda lily flower extract, hydrolyzed pearl, essence, pigment, solvent and antiseptic, middling speed homogenizing 8-10 minute, the back discharging stirs;
5) storage → inspection of semifinished product → fill → product inspection → warehouse-in.
The present invention is owing to adopted above-mentioned technical scheme, and product can keep the skin wet to skin after use, and the effective ingredient Titanium Dioxide in the plant extract promotes the glossy degree of skin.
The specific embodiment
Preparation process of the present invention is the state that each composition is mixed to the comparison homogeneous, and step is:
1. butanediol, glycerol, hydrolecithin mix, and are heated to about 78 ℃, and dissolving forms phase 1 fully;
2. with polydimethylsiloxane, glycerol three (thylhexoic acid) ester, squalane, be heated to 78 ℃, stir, join in the phase 1 low speed homogenizing 5 minutes;
3. with in the mixture more than the water suction, high speed homogenization 10-15 minute, add hydroxyethyl-cellulose, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, hyaluronate sodium again, high speed homogenization 10-15 minute;
4. be cooled to 50 ℃, add triethanolamine, Herba Saussureae Involueratae extract, root of Paeonia suffruticosa Ardr. extract, bermuda lily flower extract, hydrolyzed pearl, essence, pigment, solvent and antiseptic, middling speed homogenizing 8-10 minute, the back discharging stirs;
5. storage → the inspection of semifinished product → fill → product inspection → warehouse-in.
Specific embodiment:
* 1. acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer derives from Lubrizol
* 2. acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer derives from Lubrizol
Mutually 1 put into container and mix, be heated to 78 ℃, stirring and dissolving is complete; Phase 2 is added phase 1, stir, add phase 3, stirring, homogenizing are with its mixing.Add phase 4 then, stirring, homogenizing, mix homogeneously; To 50 ℃ of adding phases again 5, stirring, homogenizing, mix homogeneously, discharging.
Method of testing:
Of the present inventionly to preserve moisture and improve colour of skin effect in order to test, carried out investigation experiment on probation:
1, respondent: each department ordinary consumer 50 people, the trial state feedback form of Shou Huiing is 40 parts at last;
2, control time: on October 10th, 1 2008 on August 10th, 2008;
3, use product: No. 1 product is the product according to formulation of the present invention; No. 2 products are the rival factory similar products;
4, method of testing: after the tester face cleaning, about respectively No. 1 product and No. 2 products being coated on two cheek, observe and experience result of use;
5, the test form is as follows:
The use of table 11 product (60 days) feedback conclusive table
Table 22 product uses (60 days) feedback conclusive table
Table 31 product and No. 2 products improve the contrast statistical table of the colour of skin
The statistical table of table 4 tester recommended products model
| Proposed model | No. 1 | No. 2 |
| The recommendation number | 32 | 8 |
| Percentage ratio | 80% | 20% |
6, feedback conclusion:
The tester represents that all the moisture-retaining capacity of No. 1 product and nourishing effect all are better than product No. 2, and No. 1 product conditioning property is good, often uses back colour of skin improvement obviously, and is moist tender white; And there is not the people that allergic phenomena is arranged in the questionnaire that reclaims.
As shown in Table 5,80% people recommends to use product No. 1, has only 20% people to recommend to use product No. 2.
Claims (1)
1. toner/smoothing toner preparation of compositions method that contains natural plant extracts is characterized in that this method is as follows:
1) phase 1 is put into container and mix, be heated to 78 ℃, stirring and dissolving is complete, and described phase 1 is made of glycerol 10%, butanediol 4% and hydrolecithin 2% by weight percentage;
2) phase 2 is added phase 1, stir, described phase 2 is made of polydimethylsiloxane 5%, glycerol triethyl group alkyl caproate 3% and squalane 2% by weight percentage;
3) in above-mentioned solution, add phase 3, stirring, homogenizing, with its mixing, described phase 3 is deionized water 47.2% by weight percentage;
4) in above-mentioned solution, add phase 4 then, stirring, homogenizing, mix homogeneously, described phase 4 is made of hydroxyethyl-cellulose 0.5%, hyaluronate sodium 0.8%, Carbopol13420.3% and deionized water 20% by weight percentage;
5) be heated to 50 ℃ and add phase 5, stirring, homogenizing, mix homogeneously, discharging; Described phase 5 is made of triethanolamine 0.3%, 10% weight percent concentration potassium hydroxide 1%, Herba Saussureae Involueratae extract 0.5%, root of Paeonia suffruticosa Ardr. extract 1%, bermuda lily flower extract 2% and antiseptic 0.4% by weight percentage.
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| CN107519083A (en) * | 2017-08-28 | 2017-12-29 | 李冉冉 | Toner containing natural plant extracts |
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Denomination of invention: Preparation method of a skin softener composition containing natural plant extracts Granted publication date: 20141029 Pledgee: Agricultural Bank of China Limited Deqing County sub branch Pledgor: OSMUN BIOLOGICAL Co.,Ltd. Registration number: Y2024980023335 |