CN103222945B - Preparation method for skin softening water composition containing nature plant extract and hydrolyzed pearl - Google Patents
Preparation method for skin softening water composition containing nature plant extract and hydrolyzed pearl Download PDFInfo
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- CN103222945B CN103222945B CN201310157438.6A CN201310157438A CN103222945B CN 103222945 B CN103222945 B CN 103222945B CN 201310157438 A CN201310157438 A CN 201310157438A CN 103222945 B CN103222945 B CN 103222945B
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- hydrolyzed pearl
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Landscapes
- Cosmetics (AREA)
Abstract
The invention relates to a preparation method for a skin softening water composition containing a nature plant extract and hydrolyzed pearl. The preparation method comprises: 1) placing a phase 1 in a container to mix, heat and stir, wherein the phase 1 comprises glycerol, propylene glycol, butanediol and hydrolecithin; 2) adding a phase 2 to the phase 1, and stirring, wherein the phase 2 comprises polydimethylsiloxane and squalane; 3) adding a phase 3 to the prepared solution, and mixing, wherein the phase 3 comprises deionized water; 4) adding a phase 4, and uniformly mixing, wherein the phase 4 comprises hydroxyethyl cellulose, Carbopol1342, sodium hyaluronate and deionized water; and 5) adding a phase 5 when a temperature achieves 50 DEG C, uniformly mixing, and discharging the material, wherein the phase 5 comprises triethanolamine, essence, a snow lotus herb extract, a preservative, a madonna lily extract, a solvent and hydrolyzed pearl. With the composition, skin color can be improved, a dark yellow state can be regulated, and the skin can be moistened and whitened.
Description
Present patent application is dividing an application of application for a patent for invention (application number: 201110297683.8 applyings date: 11-09-27, invention and created name: a kind of moistens bright color toner/smoothing toner composition and method of making the same).
Technical field
The invention belongs to a kind of toner/smoothing toner composition and method of making the same of Titanium Dioxide.
Background technology
Because modern people's rhythm of life is fast, and be subject to various environmental effects, skin is dry, intensely dark pool often.For this situation, we have prepared this toner/smoothing toner compositions that consumer is liked, and deep layer is nourished, conditioning skin, improves the colour of skin, adjusts dark yellow state, make skin moist tender white.
Chinese invention patent application (application number: 200910010837.3 applyings date: 2009-03-24) disclose a kind of skincare humectant.It consists of according to the following number of weight ratio following component: skin protection base material: natural dimethylamino proline acid: glycerol: Mel: shea butter: vitamin E=80-120: 5-12: 1-3: 10-20: 1-3: 2-4.This invention is nourished moisturizing composition containing shea butter, glycerol, Mel isoreactivity, can help rapidly to moisten dry skin, makes skin exquisiteness soft and smooth.
Chinese invention patent application (application number: 200710150410.4 applyings date: 2007-11-26) disclose a kind of cosmetic humectant that contains xylitol, it is comprised of the raw material of following portions by weight: 2-10 part wetting agent, 0.1-2 part oils and fats, emulsifying agent 5-15 part, 60～80 parts, water.The cosmetic humectant of this invention can more deeply be diffused into skin depths, is combined with deep water, keeps the moist of skin.
Summary of the invention
In order to solve, people's skin is often dried, the problem in intensely dark pool, an object of the present invention is to provide a kind of bright color toner/smoothing toner compositions of profit, and said composition can deep layer nourish, nurse one's health skin, improves the colour of skin, adjusts dark yellow state, makes skin moist tender in vain.Another one object of the present invention is to provide a kind of preparation method of the above-mentioned bright color toner/smoothing toner compositions of silk profit.
In order to realize above-mentioned first object, the present invention has adopted following technical scheme:
Thread profit a bright color toner/smoothing toner compositions, described compositions comprises following component by mass percentage:
(a) 0.01% to 20% wetting agent;
(b) 0.01% to 20% skin moistening oils and fats;
(c) 0.01% to 10% surfactant;
(d) 0.01% to 10% thickening polymer;
(e) 0.01% to 10% skin conditioning agent; With
(f) 10% to 90% deionized water.
As preferably, described compositions comprises following component by mass percentage:
(a) 1% to 20% wetting agent;
(b) 0.01% to 15% skin moistening oils and fats;
(c) 0.01% to 8% surfactant;
(d) 0.01% to 8% thickening polymer;
(e) 0.01% to 8% skin conditioning agent; With
(f) 10% to 90% deionized water.
As preferred again, described compositions comprises following component by mass percentage:
(a) 2% to 20% wetting agent;
(b) 0.01% to 10% skin moistening oils and fats;
(c) 0.01% to 6% surfactant;
(d) 0.01% to 6% thickening polymer;
(e) 0.01% to 6% skin conditioning agent; With
(f) 10% to 90% deionized water.
As preferably, above-mentioned wetting agent is selected propylene glycol, sorbitol, butanediol, 1, one or more in 2-hexanediol, caprylyl glycol, dipropylene glycol, glycerol, diglycerol, pentanediol, Polyethylene Glycol, and what be preferred for this compositions is butanediol or glycerol; Described skin moistening oils and fats is selected one or more in polydimethylsiloxane, glycerol three (thylhexoic acid) ester and squalane.
As preferably, above-mentioned surfactant is selected hydrolecithin.
As preferably, above-mentioned thickening polymer is selected one or more in the synthetic high molecular polymer of carboxylic acid polyalcohol, cross-linked polyacrylate polymer, cellulose ethers, natural high molecular polymer; Preferably cellulose ethers and crosslinked acrylate polymer, be more preferably by by CTFA called after hydroxyethyl-cellulose and acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer.
As preferably, above-mentioned skin conditioning agent is selected from one or more in hydrolyzed pearl, hyaluronate sodium, Herba Saussureae Involueratae extract, root of Paeonia suffruticosa Ardr. extract, bermuda lily flower extract.
As preferably, above-mentioned said composition has also comprised one or more in pH adjusting agent, food coloring, antiseptic, essence and solvent.
The present composition also can comprise various other compositions.The function of the concrete composition of compositions of the present invention and effect will be described in more detail below.
Wetting agent
Approximately 0.01% to 20% wetting agent by weight in the present invention is polyhydric alcohol, compositions described herein preferably comprises by weight of the composition approximately 1% to 20%, the wetting agent of 2%-20% more preferably, example comprises propylene glycol, sorbitol, butanediol, 1,2-hexanediol, caprylyl glycol, dipropylene glycol, glycerol, diglycerol, pentanediol, Polyethylene Glycol, and their mixture, what be preferred for this compositions is butanediol and glycerol.
Skin moistening oils and fats
Skin moistening oils and fats in the present composition, can pin moisture, prevents excessive volatilization, makes skin keep the tender gloss of water.
Skin moistening oils and fats polydimethylsiloxane in the present composition, its by weight of the composition approximately 0.01% to 20%, be preferably about 0.01% to 15%, more preferably from about 0.01% to 10%.It is nontoxic, to skin and mucosa nonirritant, but irritant to eyes.It is generally accepted it is safe.Have good chemical stability, antistatic behaviour and breathability, can freely breathe skin.
Skin moistening oils and fats glycerol three (thylhexoic acid) ester in the present composition, its by weight of the composition approximately 0.01% to 20%, be preferably about 0.01% to 15%, more preferably from about 0.01% to 10%.It is a kind of triglycerin esters, derives from glycerol and fatty acid, is a kind of lightweight oils and fats, can antistatic, and be skin softening agent and conditioner.
Skin moistening oils and fats squalane in the present composition, its by weight of the composition approximately 0.01% to 20%, be preferably about 0.01% to 15%, more preferably from about 0.01% to 10%.It has the cosmetic properties of natural squalane, is a kind of colourless, tasteless, nontoxic high-purity liquid clothes hook linear paraffin, can give cosmetics fabulous and noble feel, moistens non-greasy, and moisturizing is lubricated, and penetration is strong, and good stability.
Surfactant
Surfactant in the present composition is hydrolecithin, is a kind of natural green emulsifying agent, and its main chemical compositions is lecithin, PHOSPHATIDYL ETHANOLAMINE and phosphatidylinositols.Total institute is known, and phospholipid is distributed in animal and plant body widely, is one of important component part of biological cell.It is to metabolism, and membrane permeation plays very important effect.
Phospholipid is the material with interfacial activity forming the lipophilic group being combined into by the fatty acid of two long-chains and glycerol and the hydrophilic group that simultaneously contains phosphoric acid, amido.Thereby it has good emulsifying dispersivity, wettability, stability and viscosity adjustment performance.Hydrolecithin in the present invention is to obtain by the hydrogenation to phospholipid of natural soybean, has overcome natural phospholipid not resistance to oxidation and thermal instability, has been widely used in each industrial circle of cosmetics and pharmaceuticals.Its feature also has lasting performance of keeping humidity, promotes the subcutaneous absorption of skin, reduces the zest of other surfactants to skin.
Thickening agent
In some embodiments, compositions of the present invention can also comprise one or more thickening agents, and described compositions comprises by weight of the composition approximately 0.01% to 10%, is preferably about 0.01% to 8%, more preferably from about 0.01% to 6% thickening agent.
The non-limiting kind of thickening agent comprises and is selected from following material: carboxylic acid polyalcohol (as Carbopol980), cross-linked polyacrylate polymer, synthetic high molecular polymer (as cellulose ethers), natural high molecular polymer (as natural gum), preferably cellulose ethers and crosslinked acrylate polymer, more preferably press CTFA called after hydroxyethyl-cellulose and acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer.
Skin conditioning agent
The various skin conditioner that the present composition adds is Herba Saussureae Involueratae extract, root of Paeonia suffruticosa Ardr. extract, bermuda lily flower extract.
The content of the Herba Saussureae Involueratae extract that the present composition adds is preferably approximately 0.01% to 8% by weight of the composition, more preferably from about 0.01% to 6%, the active quantities of the Herba Saussureae Involueratae extract of the present composition by weight of the composition preferably approximately 0.001% to 8%, more preferably from about 0.001% to 6%.
The Herba Saussureae Involueratae extract that the present composition adds, contains containing the fragrant glycoside of cloud, xuelianlactone, alkaloid, volatile oil, polysaccharide.There is antiinflammatory, antibacterial and analgesic activity.The permeability that promotes sebum, improves microcirculation, keeps skin elasticity.
The content of the root of Paeonia suffruticosa Ardr. extract that the present composition adds is preferably approximately 0.01% to 8% by weight of the composition, more preferably from about 0.01% to 6%, the active quantities of the Herba Saussureae Involueratae extract of the present composition by weight of the composition preferably approximately 0.001% to 8%, more preferably from about 0.001% to 6%.
The root of Paeonia suffruticosa Ardr. extract of the present composition, be rich in aminoacid, mineral, multivitamin and zinc, the selenium and other trace elements of needed by human body, there is the powerful effect of releiving, can in skin keratin cell, reduce the activity of melanin enzyme, thereby help to suppress to produce melanin; There is antibacterial, antiinflammation; The lymph circulation of chafe, makes skin more glossy, improves skin quality, after continuing to use, can allow skin slowly say goodbye to obscure and coarse, and skin is beautiful, water profit.
The content of the bermuda lily flower extract that the present composition adds is preferably approximately 0.01% to 8% by weight of the composition, more preferably from about 0.01% to 6%, the active quantities of the Herba Saussureae Involueratae extract of the present composition by weight of the composition preferably approximately 0.001% to 8%, more preferably from about 0.001% to 6%.
The bermuda lily flower extract of the present composition, except containing starch, protein, fat, carotene, vitamin, trace element, also contain some special nutritional labelings, as multiple alkaloids such as colchicine, there is very strong moisture-retaining capacity, regulate skin moisture.
The hydrolyzed pearl of the present composition, its content is pressed the weighing scale approximately 0.01% to 10% of the present composition, preferably be about 0.01% to 8%, be more preferably 0.01% to 6%, its active matter content is pressed the weighing scale approximately 0.001% to 10% of the present composition, preferably approximately 0.001% to 8%, more preferably from about 0.001% to 6%.
The hydrolyzed pearl of the present composition, is that the enzymolysis process by Margarita powder obtains, and contains a large amount of calcium ions and pearl protein, has elimination oxygen-derived free radicals, anti-aging effects, and light speckle, makes the beautiful gloss of skin.
The hyaluronate sodium of the present composition, is the glutinous sugar of a kind of bionical thing, and molecular weight is greater than 1,000,000, and the hyaluronic acid sodium content of the present composition is by invention composition weight meter approximately 0.01% to 10%, preferably approximately 0.01% to 5%, be more preferably 0.01% to 3%.
In normal human skin horny layer, contain 10% to 20% moisture, it prevents skin aging, prevents that the various stimulations of external environment from having significant role skin care.With advancing age or the variation of environment, moisture can drop to below 10%, and skin can be dried, and produces wrinkle.The hyaluronate sodium of the present composition can be alleviated this problem, and its theoretical water retention value reaches 1000ml/g, is the key component of water conservation in human body skin, and not only moistening effect is good, and without greasy feeling and stop up pore etc. shortcoming.Can also eliminate oxygen-derived free radicals, repair the skin of damage after shining.
As preferred again, described compositions consists of following component by mass percentage:
It is not 0 that above-mentioned Herba Saussureae Involueratae extract, root of Paeonia suffruticosa Ardr. extract, bermuda lily flower extract and hydrolyzed pearl have a kind of composition at least.
In order to realize second above-mentioned object, the present invention has adopted following technical scheme:
A preparation method of preparing the above-mentioned bright color toner/smoothing toner compositions of silk profit, the method comprises the following steps:
1) butanediol, glycerol, hydrolecithin mix, and are heated to 78 ℃ of left and right, dissolve completely, form phase 1;
2) by polydimethylsiloxane, glycerol three (thylhexoic acid) ester, squalane, be heated to 78 ℃, stir, join in phase 1 low speed homogenizing 5 minutes;
3) by mixture more than water suction, high speed homogenization 10-15 minute, then add hydroxyethyl-cellulose, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, hyaluronate sodium, high speed homogenization 10-15 minute;
4) be cooled to 50 ℃, add triethanolamine, Herba Saussureae Involueratae extract, root of Paeonia suffruticosa Ardr. extract, bermuda lily flower extract, hydrolyzed pearl, essence, pigment, solvent and antiseptic, middling speed homogenizing 8-10 minute, discharging after stirring;
5) storage → inspection of semifinished product → fill → product inspection → warehouse-in.
The present invention is owing to having adopted above-mentioned technical scheme, and product, after use, can keep the skin wet to skin, and the effective ingredient Titanium Dioxide in plant extract promotes the glossy degree of skin.
The specific embodiment
Preparation process of the present invention is the state of comparison homogeneous that each composition is mixed to, and step is:
1. butanediol, glycerol, hydrolecithin mix, and are heated to 78 ℃ of left and right, dissolve completely, form phase 1;
2. by polydimethylsiloxane, glycerol three (thylhexoic acid) ester, squalane, be heated to 78 ℃, stir, join in phase 1 low speed homogenizing 5 minutes;
3. by mixture more than water suction, high speed homogenization 10-15 minute, then add hydroxyethyl-cellulose, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, hyaluronate sodium, high speed homogenization 10-15 minute;
4. be cooled to 50 ℃, add triethanolamine, Herba Saussureae Involueratae extract, root of Paeonia suffruticosa Ardr. extract, bermuda lily flower extract, hydrolyzed pearl, essence, pigment, solvent and antiseptic, middling speed homogenizing 8-10 minute, discharging after stirring;
5. storage → the inspection of semifinished product → fill → product inspection → warehouse-in.
Specific embodiment:
* 1. acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, derives from Lubrizol
* 2. acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, derives from Lubrizol
Mutually 1 put into container and mix, be heated to 78 ℃, stirring and dissolving is complete; Phase 2 is added to phase 1, stir, add phase 3, stirring, homogenizing, by its mixing.Then add phase 4, stirring, homogenizing, mix homogeneously; Add again mutually 5 to 50 ℃, stir, homogenizing, mix homogeneously, discharging.
Method of testing:
In order to test moisturizing of the present invention and to improve colour of skin effect, carried out investigation experiment on probation:
1, respondent: each department ordinary consumer 50 people, 40 parts of the trial state feedback forms of finally regaining;
2, control time: on October 10th, 1 2008 on August 10th, 2008;
3, use product: No. 1 product is the product of preparing according to formula of the present invention; No. 2 products are rival factory similar products;
4, method of testing: after tester face is clean, respectively No. 1 product and No. 2 products are coated on two cheek in left and right, observe and experience result of use;
5, test form is as follows:
The use of No. 1 product of table 1 (60 days) feedback conclusive table
No. 2 products of table 2 are used (60 days) feedback conclusive table
No. 1 product of table 3 and No. 2 products improve the contrast statistical table of the colour of skin
The statistical table of table 4 tester recommended products model
| Proposed model | No. 1 | No. 2 |
| Recommendation number | 32 | 8 |
| Percentage ratio | 80% | 20% |
6, feedback conclusion:
Tester all represents, the moisture-retaining capacity of No. 1 product and nourish effect and be all better than product No. 2, and No. 1 product conditioning property is good, and after often using, the colour of skin is improved obviously, moist tender white; And there is not people to have allergic phenomena in the questionnaire reclaiming.
As shown in Table 5, No. 1 product of people's recommendation of 80%, only has No. 2 products of people's recommendation of 20%.
Claims (1)
1. contain a preparation method for the toner/smoothing toner compositions of natural plant extracts and hydrolyzed pearl, it is characterized in that this preparation method is as follows:
1) mutually 1 put into container and mix, be heated to 78 ℃, stirring and dissolving is complete, and described phase 1 is by weight percentage by glycerol 10%, propylene glycol 3%, and butanediol 8% and hydrolecithin 2.5% form;
2) phase 2 is added to phase 1, stir, described phase 2 consists of polydimethylsiloxane 5% and squalane 2% by weight percentage;
3) in above-mentioned steps 2) add mutually 3 in preparing solution, stir, homogenizing, to be mixed, described phase 3 consists of deionized water 42.5% by weight percentage;
4) then add phase 4, stirring, homogenizing, mix homogeneously, described phase 4 is by weight percentage by hydroxyethyl-cellulose 0.6%, and Carbopol1342 0.5%, and hyaluronate sodium 0.5% and deionized water 20% form;
5) add again mutually 5 to 50 ℃, stir, homogenizing, mix homogeneously, discharging; Described phase 5 is by weight percentage by triethanolamine 0.5%, essence 0.25%, and Herba Saussureae Involueratae extract 1%, antiseptic 0.4%, bermuda lily flower extract 2%, solvent 0.25% and hydrolyzed pearl 1% form.
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| US20050043398A1 (en) * | 2003-08-18 | 2005-02-24 | Christophe Carola | Use of chromen-4-one derivatives |
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Effective date of registration: 20230113 Address after: 313200 No. 99, Pearl Street, Moganshan high tech Industrial Development Zone, Deqing County, Huzhou City, Zhejiang Province Patentee after: OSMUN BIOLOGICAL Co.,Ltd. Address before: No. 518, Zhongxin North Road, Wukang Town, Deqing County, Huzhou City, Zhejiang Province, 313200 Patentee before: Shen Zhirong |
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Denomination of invention: Preparation method of a skin softener combination containing natural plant extracts and hydrolyzed pearls Granted publication date: 20141029 Pledgee: Agricultural Bank of China Limited Deqing County sub branch Pledgor: OSMUN BIOLOGICAL Co.,Ltd. Registration number: Y2024980023335 |