CN103222943B - Preparation method for instantaneous penetration skin regeneration water composition containing pansy flower extract, guava extract and hydrolyzed pearl - Google Patents
Preparation method for instantaneous penetration skin regeneration water composition containing pansy flower extract, guava extract and hydrolyzed pearl Download PDFInfo
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- CN103222943B CN103222943B CN201310156431.2A CN201310156431A CN103222943B CN 103222943 B CN103222943 B CN 103222943B CN 201310156431 A CN201310156431 A CN 201310156431A CN 103222943 B CN103222943 B CN 103222943B
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Abstract
The present invention relates to a preparation method for an instantaneous penetration skin regeneration water composition containing a pansy flower extract, a guava extract and hydrolyzed pearl. The preparation comprises: 1) carrying out sterilization on deionized water, cooling to a temperature of 70 DEG C, adding carbomer and sodium hyaluronate, and uniformly stirring; 2) when a temperature achieves about 45 DEG C, adding a phase 2, completely and uniformly stirring, and discharging the material, wherein the phase 2 comprises, by weight, 15% of glycerol, 8% of a witch hazel extract, 1% of 1,2-hexanediol/caprylyl glycol, 1% of dipotassium glycyrrhizinate, 1% of triethanolamine, 0.4% of a solubilizer, 0.2% of an essence, 0.4% of a preservative, 2% of a pansy flower extract, 2% of a guava extract, and 2% of hydrolyzed pearl; and 3) sequentially carrying out storage, half finished product inspection, filling, finished product inspection, and warehousing. With the composition, moisturizing can be performed on skin at night, deep penetration channels of skin can be opened, amino acids can be supplied, skin regeneration can be strengthened, and skin breathing is smooth.
Description
Present patent application is application for a patent for invention (application number: the 201110289426.X applying date: 11-09-27, innovation and creation
Title: a kind of wink saturating granulation promoting water composition and preparation method thereof) divisional application.
Technical field
The invention belongs to a kind of can the wink saturating granulation promoting water composition and preparation method thereof of moisturizing immediately.
Background technology
Because modern people's rhythm of life is fast, and by various environmental effect, skin is often in exsiccosis, dry, intensely dark pool.
Chinese invention patent application (application number: 200910010837.3 applyings date: 2009-03-24) discloses a kind of skincare humectant.It is made up of according to the following number of weight ratio following component: skin protection base material: natural dimethylamino proline acid: glycerol: Mel: shea butter: vitamin E=80-120: 5-12: 1-3: 10-20: 1-3: 2-4.This invention nourishes moisturizing composition containing shea butter, glycerol, Mel isoreactivity, can help rapidly moist dry skin, make skin exquisiteness soft and smooth.
Chinese invention patent application (application number: 200710150410.4 applyings date: 2007-11-26) discloses a kind of cosmetic humectant containing xylitol, it is made up of the raw material of following portions by weight: 2-10 part wetting agent, 0.1-2 part oils and fats, emulsifying agent 5-15 part, 60 ~ 80 parts, water.The cosmetic humectant of this invention can more deeply be diffused into skin depths, is combined with deep water, keeps the moist of skin.
Summary of the invention
Often be in exsiccosis to solve people's skin, the problem in dry, intensely dark pool, an object of the present invention is to provide saturating granulation promoting water composition of a kind of wink, said composition has instant moisturizing, makes skin full, is full of elasticity, tender feature glossy in vain.Another one object of the present invention is to provide the preparation method of saturating granulation promoting water composition of a kind of above-mentioned wink.
In order to realize above-mentioned first object, present invention employs following technical scheme:
A kind of wink saturating granulation promoting water composition, described granulation promoting water composition comprises following component by mass percentage:
The wetting agent of (a) 0.01% to 20%;
The thickening polymer of (b) 0.01% to 10%;
The antiinflammatory of (c) 0.01% to 10%;
(d) 0.01% to 10% skin conditioning agent;
The deionized water of (e) 10% to 90%.
As preferably, described granulation promoting water composition comprises following component by mass percentage:
The wetting agent of (a) 1% to 20%;
The thickening polymer of (b) 0.01% to 8%;
The antiinflammatory of (c) 0.01% to 10%;
(d) 0.01% to 10% skin conditioning agent;
The deionized water of (e) 10% to 90%.
As preferred again, described granulation promoting water composition comprises following component by mass percentage:
The wetting agent of (a) 2% to 20%;
The thickening polymer of (b) 0.01% to 6%;
The antiinflammatory of (c) 0.01% to 10%;
(d) 0.01% to 10% skin conditioning agent;
The deionized water of (e) 10% to 90%.
As preferably, above-mentioned wetting agent selects propylene glycol, sorbitol, butanediol, 1, one or more in 2-hexanediol, caprylyl glycol, dipropylene glycol, glycerol, diglycerol, pentanediol and Polyethylene Glycol, what be preferred for this compositions is glycerol or 1,2-hexanediol/caprylyl glycol.
As preferably, the high molecular polymer that above-mentioned thickening polymer selects carboxylic acid polyalcohol, cross-linked polyacrylate polymer, cellulose ethers to synthesize, one or more in natural high molecular polymer; Preferably acrylic crosslinking polymer, is more preferably the material by CTFA called after carbomer.
As preferably, above-mentioned antiinflammatory is glycyrrhizic acid dipotassium.
As preferably, above-mentioned skin conditioning agent be selected from hydrolyzed pearl, hyaluronate sodium, hamamelis extract, America elderberry, pansy extract and Fructus psidii guajavae immaturus extract one or more.
As preferably, above-mentioned compositions further comprises antiseptic and essence.
The present composition also can comprise other compositions various.Function and the effect of the concrete composition of compositions of the present invention will be described in more detail below.
Wetting agent
In the present invention by weight about 0.01% to 20% wetting agent be polyhydric alcohol, compositions described herein preferably comprises by weight of the composition about 1% to 20%, the more preferably wetting agent of 2%-20%, example comprises propylene glycol, sorbitol, butanediol, 1,2-hexanediol, caprylyl glycol, dipropylene glycol, glycerol, diglycerol, pentanediol, Polyethylene Glycol, and their mixture, what be preferred for this compositions is glycerol, 1,2-hexanediol/caprylyl glycol.
Thickening agent
In some embodiments, compositions of the present invention can also comprise one or more thickening agents, and described compositions comprises by weight of the composition about 0.01% to 10%, is preferably about 0.01% to 8%, more preferably from about the thickening agent of 0.01% to 6%.
The non-limiting kind of thickening agent comprises and is selected from following material: the high molecular polymer (as cellulose ethers) of carboxylic acid polyalcohol (as Carbopol980), cross-linked polyacrylate polymer, synthesis, natural high molecular polymer (as natural gum), preferably acrylic crosslinking polymer, more preferably presses the material of CTFA called after carbomer.
antiinflammatory
Present composition antiinflammatory is glycyrrhizic acid dipotassium, molecular formula: C
42h
60k
2o
16.Radix Glycyrrhizae just has removing toxic substances, antiinflammatory anti-allergic effects as medicine since ancient times.Its curative effect is widely known by the people.The further investigation of the effective ingredient of Radix Glycyrrhizae extract is shown: glycyrrhizic acid and potassium salt thereof have the effect of good anti-allergic effects, Detoxication and similar adrenal gland's sebum hormone, even if life-time service also has no side effect.Glycyrrhizic acid dipotassium is used for cosmetics and has the effects such as antiinflammatory, antiallergic, moisturizing.
Skin conditioning agent
The various skin conditioner that the present composition adds is hamamelis extract, America elderberry, pansy extract, Fructus psidii guajavae immaturus extract.
The content of the hamamelis extract that the present composition adds is preferably about 0.01% to 8% by weight of the composition, more preferably from about 0.01% to 6%, the active quantities of the hamamelis extract of the present composition by weight of the composition preferably about 0.001% to 8%, more preferably from about 0.001% to 6%.
The hamamelis extract that the present composition adds, main component includes tannin, gallic acid, catechin, procyanidin, Protoapigenone (kaempferol, Quercetin), quintessence oil (carvacrol, eugenol, hexenol), choline and Saponin etc., good astringent and antioxidant, also very effective when being used for treating comedo.
The content of the America elderberry that the present composition adds is preferably about 0.01% to 8% by weight of the composition, more preferably from about 0.01% to 6%, the active quantities of the America elderberry of the present composition by weight of the composition preferably about 0.001% to 8%, more preferably from about 0.001% to 6%.
The America elderberry that the present composition adds, containing Ramulus Sambuci Williamsii anthocyanin, anthocyanidin glycoside, morroniside etc.There is superpower moisturizing effect, and eye skin can be made to absorb nutritional labeling in time; Promote cutaneous circulation flow velocity simultaneously, reduce eye edema, very effective to dispelling eye black eye, allow two pupil look eagle-eyed.
The content of the pansy extract that the present composition adds is preferably about 0.01% to 8% by weight of the composition, more preferably from about 0.01% to 6%, the active quantities of the pansy extract of the present composition by weight of the composition preferably about 0.001% to 8%, more preferably from about 0.001% to 6%.
The pansy extract of the present composition, is rich in globulariacitrin, Saponin and vitamin C, tocopherol etc.Comprehensive conditioning skin, to the health status of water oil balance, has antibacterial action, the pox that significantly disappears effect.
The content of the Fructus psidii guajavae immaturus extract that the present composition adds is preferably about 0.01% to 8% by weight of the composition, more preferably from about 0.01% to 6%, the active quantities of the Fructus psidii guajavae immaturus extract of the present composition by weight of the composition preferably about 0.001% to 8%, more preferably from about 0.001% to 6%.
The Fructus psidii guajavae immaturus extract of the present composition, be rich in the trace element such as vitamin C, protein, fat, vitamin A, category-B vitamin, calcium, phosphorus, ferrum, can effectively in and free radical, enhance metabolism, skin is helped to discharge " toxin ", instant performance whitening skin and preserving moisture effect.
The hydrolyzed pearl of the present composition, its content is by the weighing scale about 0.01% to 10% of the present composition, preferably be about 0.01% to 8%, be more preferably 0.01% to 6%, its active matter content is by the weighing scale about 0.001% to 10% of the present composition, preferably about 0.001% to 8%, more preferably from about 0.001% to 6%.
The hydrolyzed pearl of the present composition, is obtained by the enzymolysis process of Margarita powder, containing a large amount of calcium ions and pearl protein, has elimination oxygen-derived free radicals, anti-aging effects, light speckle, make the beautiful gloss of skin.
The hyaluronate sodium of the present composition, be the glutinous sugar of a kind of bionical thing, molecular weight is greater than 1,000,000, the hyaluronic acid sodium content of the present composition by invention composition weight meter about 0.01% to 10%, preferably about 0.01% to 5%, be more preferably 0.01% to 3%.
Containing the moisture of 10% to 20% in normal human skin horny layer, it is to skin care, prevents skin aging, prevents the various stimulations of external environment from having significant role.With advancing age or the change of environment, moisture can drop to less than 10%, and skin can be dry, produces wrinkle.The hyaluronate sodium of the present composition can alleviate this problem, and its theoretical water retention value reaches 1000ml/g, and be the key component of water conservation in human body skin, not only moistening effect is good, and without greasy feeling and blocking pore etc. shortcoming.Can also oxygen-derived free radicals be eliminated, repair the skin of damage after shining.
As preferred again, described granulation promoting water composition is made up of following component by mass percentage:
| Deionized water | 50%～80% |
| Carbomer | 0.2%～１.５% |
| Hyaluronate sodium | 0.2%～1.5% |
| Glycerol | ８％～２0％ |
| Hamamelis extract | 2%～15% |
| 1,2-hexanediol/caprylyl glycol | 0.5%～1.5% |
| Glycyrrhizic acid dipotassium | 0.5%～3.0% |
| Triethanolamine | 0.2%～1.5% |
| Solubilizing agent | 0%～1.0% |
| Essence | 0%～0.8% |
| Antiseptic | 0%～1.0% |
| Hydrolyzed pearl | 0%～5.0% |
| America elderberry | 0%～5.0% |
| Pansy extract | 0%～5.0% |
| Guava extract | 0%～5.0% |
Above-mentioned hydrolyzed pearl, America elderberry, pansy extract and Fructus psidii guajavae immaturus extract have at least a kind of composition not to be 0.
In order to realize second above-mentioned object, present invention employs following technical scheme:
Prepare a preparation method for saturating granulation promoting water composition of above-mentioned wink, the method comprises the following steps:
1) deionized water, after sterilizing, adds thickening polymer and skin conditioning agent, stirs when being cooled to 65 ~ 75 DEG C;
2) to about 40 ~ 50 DEG C, add other components, stir, discharging;
3) storage → inspection of semifinished product → fill → product inspection → warehouse-in.
The present invention is owing to have employed above-mentioned technical scheme, and product after a procedure, can to the instant moisturizing of skin, the effective ingredient Titanium Dioxide in plant extract, promotes the glossy degree of skin.
Detailed description of the invention
Preparation process of the present invention is that each composition is mixed to more homogeneous state, and step is:
1. deionized water, after sterilizing, adds carbomer and hyaluronate sodium, stirs when being cooled to 70 DEG C.
2., about to 45 DEG C, add other components, stir, discharging.
3. storage → the inspection of semifinished product → fill → product inspection → warehouse-in.
Specific embodiment:
Phase 1 is put into container and is mixed, and stirring and dissolving is complete; Phase 2 is added phase 1, stirs, discharging.
Method of testing:
In order to test wink of the present invention thoroughly, cosmetic result, carried out investigation on probation and tested:
1, respondent: each department ordinary consumer 50 people, the trial state feedback form finally regained 45 parts;
2, control time :-2009 years on the 10th February 10 of December in 2008;
3, product is used: No. 1 product is the product prepared according to formula of the present invention; No. 2 products are rival factory similar products;
4, method of testing: after tester face is clean, is coated in No. 1 product and No. 2 products on two cheek in left and right respectively, observes and experience result of use;
5, form is tested as follows:
Use (60 days) the feedback conclusive table of table 1 No. 1 product
Table 2 No. 2 products use (60 days) feedback conclusive table
The wink saturating Contrast on effect statistical table of table 3 No. 1 product and No. 2 products
The cosmetic result contrast statistical table of table 4 No. 1 product and No. 2 products
The statistical table of table 5 tester recommended products model
| Proposed model | No. 1 | No. 2 |
| Recommendation number | ３９ | ６ |
| Percentage ratio | 86.67% | 13.33% |
6, conclusion is fed back:
Tester all represents, the wink saturating moisturizing effect of No. 1 product is quite outstanding, and skin is softening level and smooth instantaneously; Slightly sticky sense, but moisture retention is fabulous, and also after often using, face makes use good than No. 2 products, and the colour of skin is more moistened, brighter.And do not have people to have allergic phenomena in the questionnaire reclaimed.
As shown in Table 5, people's recommendation No. 1 product of 86.67%, only has people's recommendation No. 2 products of 13.33%.
Claims (1)
1. one kind containing pansy extract, guava extract and hydrolyzed pearl wink saturating granulation promoting water composition preparation method, it is characterized in that the method is made up of following step: 1) with composition weight percentages, remove ionized water 65.5 % by weight, after sterilizing, add carbomer 1 % by weight and hyaluronate sodium 0.5 % by weight when being cooled to 70 DEG C, stir; 2) to 45 DEG C, add phase 2, stir, discharging; Described phase 2 presses composition weight percentages by glycerol 15 % by weight, hamamelis extract 8 % by weight, 1,2-hexanediol/caprylyl glycol 1 % by weight, glycyrrhizic acid dipotassium 1 % by weight, triethanolamine 1 % by weight, solubilizing agent 0.4 % by weight, essence 0.2 % by weight, antiseptic 0.4 % by weight, pansy extract 2 % by weight, guava extract 2 % by weight and hydrolyzed pearl 2 % by weight are formed; 3) storage → inspection of semifinished product → fill → product inspection → warehouse-in.
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| CN201110289426.XA Division CN102370606B (en) | 2011-09-27 | 2011-09-27 | skin penetration and tissue regeneration lotion composition and preparation method thereof |
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| CN103222943B true CN103222943B (en) | 2015-03-25 |
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Effective date of registration: 20151119 Address after: 313200 Zhejiang province Deqing County Wukang Center Road No. 518 Patentee after: Zhejiang OSM Group Co.,Ltd. Address before: 313200 Zhejiang city of Huzhou province Deqing County Wukang Town Center Road No. 518 Patentee before: Shen Zhirong |
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Effective date of registration: 20230106 Address after: 313200 No. 99, Pearl Street, Moganshan high tech Industrial Development Zone, Deqing County, Huzhou City, Zhejiang Province Patentee after: OSMUN BIOLOGICAL Co.,Ltd. Address before: No. 518, Zhongxin North Road, Wukang Town, Deqing County, Zhejiang Province, 313200 Patentee before: Zhejiang OSM Group Co.,Ltd. |