CN103169643B - Washing-free sleeping mask composition containing natural plant extractives - Google Patents

Abstract

The invention relates to a washing-free sleeping mask composition containing natural plant extractives. The mask composition is formed by the following components: a phase 1: cyclomethicone, evening primrose seed oil, caprylic/capric triglyceride and essences; a phase 2: de-ionized water, methyl hydroxybenzoate, glycerol, allantoin, hydroxyethyl acrylate/acrylyl dimethyl sodium taurate copolymer, xanthan gum, EDTA (Ethylene Diamine Tetraacetic Acid) disodium and hydroxyethyl cellulose; and a phase 3: sodium hyaluronate, herb trinity flower extractives, de-ionized water, glycine betaine, dipotassium glycyrrhizinate, guava extractives, American elderberry extractives, and DMDM hydantoin/iodopropynyl butylcarbamate. A preparation method comprises the following steps of: putting the phase 1 into a container to be mixed; putting the phase 2 into another container to be heated to 80 DEG C; adding the phase 2 when the temperature is 60 DEG C; emulsifying, homogenizing and agitating uniformly; reducing the temperature to 50 DEG C and adding the phase 3; and agitating uniformly and discharging. The mask composition disclosed by the invention has the characteristics of moisturizing skins at night, supplementing amino acid and strengthening a skin refreshing capability.

Description

A kind of Disposable sleep facial mask composition containing natural plant extracts

Present patent application is application for a patent for invention (application number: 2011103056185 applyings date: 2011-10-11, invention and created name: dividing an application a kind of Disposable sleep facial mask composition and preparation method thereof).

Technical field

The invention belongs to Disposable sleep facial mask composition of a kind of moisturizing in night and preparation method thereof.

Background technology

In order to allow skin also can absorb sufficient moisture at night, keep the tender state of water.Chinese invention patent application (application number: 201010519548.9 applyings date: 2010-10-26) disclose a kind of modified pearl cherry vitamin C sleeping mask and preparation method thereof, this patent is by reacting with surfactant after nanometer Margarita powder heat-activated, make modified nanometer Margarita powder, again by turbine stirring at water disperse modified Margarita powder, by hyaluronate sodium, glycerin polyether, butanediol is soluble in water, fully stir and heat, afterwards by polysorbas20, isononyl isononanoate, the formula components such as cetearyl alcohol add oil cauldron, after stirring homogenizing, be chilled to 45 ℃ of left and right, successively add additive and essence, antiseptic etc., make modified pearl cherry vitamin C sleeping mask.This patent can fully be infiltrated skin at sleep period chien shih moisture and nutritional labeling, concentrates and improves skin state.

Summary of the invention

In order to allow skin also can absorb sufficient moisture at night, keep the tender state of water.An object of the present invention is to provide a kind of Disposable sleep facial mask composition, this mask composition can allow skin in abundant moisturizing at night, for skin is opened percdation passage, supplements aminoacid, strengthening skin updating ability, breathe smooth and easy.Another object of the present invention is to provide a kind of preparation method of above-mentioned disposable sleep facial film combination.

In order to realize above-mentioned first object, the present invention has adopted following technical scheme:

A Disposable sleep facial mask composition, described mask composition comprises following component by weight percentage:

(a) 0.01% to 30% skin moistening oils and fats;

(b) 0.01% to 20% wetting agent;

(c) 0.01% to 10% thickening polymer;

(d) 0.01% to 10% skin conditioning agent;

(e) 10% to 90% deionized water.

As preferably, described mask composition comprises following component by weight percentage:

(a) 1% to 20% skin moistening oils and fats;

(b) 1% to 20% wetting agent;

(c) 0.01% to 8% thickening polymer;

(d) 0.01% to 8% skin conditioning agent;

(e) 10% to 90% deionized water.

As preferred again, described mask composition comprises following component by weight percentage:

(a) 5% to 15% skin moistening oils and fats;

(b) 5% to 20% wetting agent;

(c) 0.01% to 6% thickening polymer;

(d) 0.01% to 6% skin conditioning agent;

(e) 10% to 90% deionized water.

As preferably, described skin moistening oils and fats is selected one or more in Cyclomethicone, caprylic/capric triglyceride, Radix Oenotherae erythrosepalae oil.

As preferably, described wetting agent is selected betanin, propylene glycol, sorbitol, butanediol, 1, in 2-hexanediol, caprylyl glycol, dipropylene glycol, glycerol, diglycerol, pentanediol and Polyethylene Glycol one or more; What be preferred for this compositions is betanin, glycerol or propylene glycol again.

As preferably, described thickening polymer is selected in polysaccharide, acrylic copolymer and cellulosic polymer one or more; Be preferred for again this compositions be in CTFA called after 2-(Acryloyloxy)ethanol/sodium acryloyldimethyl taurate copolymers, xanthan gum and hydroxyethyl-cellulose one or more.

As preferably, described skin conditioning agent is selected in allantoin, Margarita powder, pansy flowers extract, America Ramulus Sambuci Williamsii extract, Fructus psidii guajavae immaturus extract and hyaluronate sodium one or more.

As preferably, said composition also comprises antiinflammatory, and described antiinflammatory is selected glycyrrhizic acid dipotassium.

As preferably, described said composition also comprises one or more in chelating agen, antiseptic and essence.

The present composition also can comprise various other compositions.The function of the concrete composition of compositions of the present invention and effect will be described in more detail below.

Skin moistening oils and fats

Skin moistening oils and fats in the present composition, can pin moisture, prevents excessive volatilization, makes skin keep the tender gloss of water.

Soothing oil alicyclic ring polydimethylsiloxane in the present composition, its by weight of the composition approximately 0.01% to 20%, be preferably about 0.01% to 15%, more preferably from about 0.01% to 10%.It is nontoxic, to skin and mucosa nonirritant, It is generally accepted it is safe.Have good chemical stability, antistatic behaviour and breathability, can freely breathe skin, and the skinfeel that silk is sliding, reduces sticky sense.

Skin moistening oils and fats caprylic/capric triglyceride in the present composition, its by weight of the composition approximately 0.01% to 20%, be preferably about 0.01% to 15%, more preferably from about 0.01% to 10%.It is low viscosity oils and fats, and fabulous skin isostearyl glyceryl pentaerythrityl ether, is easily absorbed, and gives skin silk sliding gloss.

Skin moistening oils and fats Radix Oenotherae erythrosepalae oil in the present composition, its by weight of the composition approximately 0.01% to 20%, be preferably about 0.01% to 15%, more preferably from about 0.01% to 10%.Extracted form natural plant, containing multiple fatty acid, mainly comprise linoleic acid (linoleicacid), gamma-Linolenic acid (γ-linolenic acid), oleic acid (oleic acid), Palmic acid (palmitic acid), stearic acid (stearic acid), cis-6,9,12-, 28 carbon-trienic acid (cis-6,9,12-octadecatrienoic acid), cis-9,12,15-28 carbon-trienic acid (cis-9,12,15-octadecatrienoic acid).Contained gamma-Linolenic acid is the essential fatty acid that human body can not be synthetic, can improve xerosis cutis, itch or even the effect of inflammation.Radix Oenotherae erythrosepalae oil also has antioxidation, moistens and softening skin, and be good emollient.

Wetting agent

Approximately 0.01% to 20% wetting agent by weight in the present invention is polyhydric alcohol, compositions described herein preferably comprises by weight of the composition approximately 1% to 20%, the wetting agent of 2%-20% more preferably, example comprises propylene glycol, sorbitol, butanediol, 1,2-hexanediol, caprylyl glycol, dipropylene glycol, glycerol, diglycerol, pentanediol, Polyethylene Glycol, and their mixture, what be preferred for this compositions is glycerol, propylene glycol.

Another kind of wetting agent betanin in the present invention, formal name used at school Betaine, is natural Moisture factor, absorbs fast, active high new moisturizer, can improve rapidly the moisture holding capacity of skin, activated cell vigor, keeps skin moist, smooth.

Thickening agent

In some embodiments, compositions of the present invention can also comprise one or more thickening agents, and described compositions comprises by weight of the composition approximately 0.01% to 10%, is preferably about 0.01% to 8%, more preferably from about 0.01% to 6% thickening agent.

The non-limiting kind of thickening agent comprises and is selected from following material: carboxylic acid polyalcohol (as Carbopol980), cross-linked polyacrylate polymer, synthetic high molecular polymer (as cellulose ethers), natural high molecular polymer (as natural gum).

Acrylate copolymer in the present composition, by the material of CTFA called after 2-(Acryloyloxy)ethanol/sodium acryloyldimethyl taurate copolymers, it has remarkable emulsifying thickening capabilities, gives the quality of product softness.

Xanthan gum in the present composition, claims again Xanthan gum, HANSHENGJIAO, and Xanthan Gum is a kind of monospore polysaccharide being produced by false xanthomonas fermentation, and natural carbohydrate, is fabulous thickening agent and stabilizing agent.

Hydroxyethyl-cellulose in the present composition; the water-soluble cellulose ether of nonionic; be a kind of white or faint yellow, tasteless, nontoxic pulverulent solids, has good thickening, suspension, dispersion, emulsifying, bonding, film forming, protection moisture and the characteristics such as protecting colloid is provided.

Antiinflammatory

The glycyrrhizic acid dipotassium of the present composition, makes antiinflammatory, molecular formula: C ₄₂h ₆₀k ₂o ₁₆.Radix Glycyrrhizae just has removing toxic substances, antiinflammatory anti-allergic effects as medicine since ancient times.Its curative effect is widely known by the people.Effective ingredient further investigation to Radix Glycyrrhizae extract shows: glycyrrhizic acid and potassium salt thereof have the effect of good anti-allergic effects, Detoxication and similar adrenal gland's sebum hormone, even if life-time service also has no side effect.Glycyrrhizic acid dipotassium has the effects such as antiinflammatory, antiallergic, moisturizing for cosmetics.

Skin conditioning agent

The various skin conditioner that the present composition adds is allantoin, Margarita powder, pansy flowers extract, America Ramulus Sambuci Williamsii extract, Fructus psidii guajavae immaturus extract and hyaluronate sodium.

The allantoin of the present composition is a kind of amphoteric compound, can form double salt in conjunction with many kinds of substance.The content of the allantoin that the present composition adds is preferably approximately 0.01% to 20% by weight of the composition, and more preferably from about 0.01% to 10%.

Above-mentioned allantoin has shading, sterilization and anticorrosion, pain relieving, antioxidation, can make skin keep moisture content, moist and soft, is the additive of the cosmetics such as cosmetology.The cosmetics that add allantoin have protective tissue, hydrophilic, absorb water and the effect such as prevent that moisture from distributing; Make skin softness and high resilience, and have beautiful gloss.Allantoin can also promote tissue growth, cell metabolism, soften cuticle albumen.Because traditional handicraft extracts from natural animal-plant that the content of natural allantoin is very low, complex process, cost be too high, cannot use on a large scale, therefore the existing main chemical synthesis that adopts is extracted synthetic allantoin, as carbamide glyoxalic acid direct condensing method, acetic acid acid calcium salt acid-soluble method, carbamide dichloroacetic acid heating, oxalic acid electrolysis oxidation of glyoxal, Chloral synthetic method etc.

The Margarita powder of the present composition, its content is pressed the weighing scale approximately 0.01% to 10% of the present composition, is preferably about 0.01% to 8%, is more preferably 0.01% to 6%.

The Margarita powder of the present composition, for nano level Margarita powder, pure physical pulverization makes, contain and be rich in the various trace elements such as 18 seed amino acids, large number of biological activated calcium, abundant vitamin B complex and zinc-iron selenium, can regulate human endocrine, effectively suppress pigmentation, strengthen skin metabolism ability, promote reepithelialization, whitening effect skin.

The content of the pansy flowers extract that the present composition adds is preferably approximately 0.01% to 8% by weight of the composition, more preferably from about 0.01% to 6%, the active quantities of the pansy flowers extract of the present composition by weight of the composition preferably approximately 0.001% to 8%, more preferably from about 0.001% to 6%.

The pansy flowers extract of the present composition, is rich in globulariacitrin, Saponin and vitamin C, tocopherol etc.Conditioning skin, to the health status of water oil balance, has antibacterial action, the pox that significantly disappears effect comprehensively.

The content of the America Ramulus Sambuci Williamsii extract that the present composition adds is preferably approximately 0.01% to 8% by weight of the composition, more preferably from about 0.01% to 6%, the active quantities of the America Ramulus Sambuci Williamsii extract of the present composition by weight of the composition preferably approximately 0.001% to 8%, more preferably from about 0.001% to 6%.

The America Ramulus Sambuci Williamsii extract that the present composition adds, contains Ramulus Sambuci Williamsii anthocyanin, anthocyanidin glycoside, morroniside etc.There is superpower moisturizing effect, and can make eye skin absorb in time nutritional labeling; Promote cutaneous circulation flow velocity simultaneously, reduce eye edema, very effective to dispelling eye black eye, allow two pupils look eagle-eyed.

The content of the Fructus psidii guajavae immaturus extract that the present composition adds is preferably approximately 0.01% to 8% by weight of the composition, more preferably from about 0.01% to 6%, the active quantities of the Fructus psidii guajavae immaturus extract of the present composition by weight of the composition preferably approximately 0.001% to 8%, more preferably from about 0.001% to 6%.

The Fructus psidii guajavae immaturus extract of the present composition, be rich in the trace element such as vitamin C, protein, fat, vitamin A, category-B vitamin, calcium, phosphorus, ferrum, can be effectively in and free radical, enhance metabolism, help skin to discharge " toxin ", immediately bring into play whitening skin and preserving moisture effect.

The hyaluronate sodium of the present composition, be the glutinous sugar of a kind of bionical thing, molecular weight is greater than 1,000,000, and the hyaluronic acid sodium content of the present composition is by invention composition weight meter approximately 0.01% to 10%, preferably approximately 0.01% to 5%, be more preferably 0.01% to 3%.

In normal human skin horny layer, contain 10% to 20% moisture, it prevents skin aging, prevents that the various stimulations of external environment from having significant role skin care.With advancing age or the variation of environment, moisture can drop to below 10%, and skin can be dried, and produces wrinkle.The hyaluronate sodium of the present composition can be alleviated this problem, and its theoretical water retention value reaches 1000ml/g, is the key component of water conservation in human body skin, and not only moistening effect is good, and without greasy feeling and stop up pore etc. shortcoming.Can also eliminate oxygen-derived free radicals, repair the skin of damage after shining.

As preferred again, said composition consists of following component by mass percentage:

It is not 0 that above-mentioned pansy flowers extract, guava extract, America Ramulus Sambuci Williamsii extract, Margarita powder have at least a kind of.

In order to realize second above-mentioned object, the present invention has adopted following technical scheme:

A method for above-mentioned Disposable sleep facial mask composition, is characterized in that the method comprises the following steps:

1) by oil phase substance mix homogeneously;

2) water and aqueous substance are mixed, be heated to 70 ℃～90 ℃, to dissolving;

3) heat to 55 ℃～65 ℃, oil phase adds water, and homogenizing stirs; To 50 ℃, add other components, stir discharging.

The present invention is owing to having adopted above-mentioned technical scheme, and after use, this sleep surface film composition is that skin is opened infiltration lane, deep layer moisturizing, osmotrophy material.Can allow skin in abundant moisturizing at night, for skin is opened percdation passage, supplement aminoacid, strengthening skin updating ability, breathe smooth and easy.

The specific embodiment

Preparation process of the present invention is the state of comparison homogeneous that each composition is mixed to, and step is:

1. oil phase mix homogeneously.

2. water, glycerol, 2-(Acryloyloxy)ethanol/sodium acryloyldimethyl taurate copolymers, methyl hydroxybenzoate, allantoin, xanthan gum, hydroxyethyl-cellulose, EDETATE SODIUM mix, and are heated to 80 ℃ and are uniformly dispersed.

3. heat to 60 ℃, oil phase adds water, and homogenizing stirs.

4. during to 50 ℃, add all the other components, stir, discharging.

5. storage → the inspection of semifinished product → fill → product inspection → warehouse-in.

Specific embodiment:

Phase 1 is put into container and is mixed; 2 put into another vessel in heating to 80 ℃ mutually; Add mutually 2 to 60 ℃ of phases 1, emulsifying, homogenizing, stirs, and is cooled to 50 ℃, adds mutually 3, after stirring, discharging.

Method of testing:

In order to test moisturizing of the present invention, conditioning effect, carried out investigation experiment on probation:

1, respondent: each department ordinary consumer 50 people, 46 parts of the trial state feedback forms of finally regaining;

2, control time: December in 2008 on February 10th, 1 2009 on the 10th;

3, use product: No. 1 product is the product of preparing according to formula of the present invention; No. 2 products are rival factory similar products;

4, method of testing: after tester face is clean, respectively No. 1 product and No. 2 products are coated on two cheek in left and right, observe and experience result of use;

5, test form is as follows:

The use of No. 1 product of table 1 (60 days) feedback conclusive table

No. 2 products of table 2 are used (60 days) feedback conclusive table

The conditioning effect contrast statistical table of No. 1 product of table 3 and No. 2 products

Model

Product conditioning effect is evaluated (meter per capita)

?	Fine	Better	Generally	Poor	Very poor	Do not know
							No. 1 product	38	5	3	0	0	0
No. 2 products	25	12	8	1	0	0

The statistical table of table 4 tester recommended products model

Proposed model	No. 1	No. 2
			Recommendation number	39	7
Percentage ratio	84.78％	15.22％

6, feedback conclusion:

Tester all represents, No. 1 product, again can be too not thick and heavy in moisturizing, allows skin experience water profit and can freely breathe again, and after often using, the colour of skin is obviously ruddy glossy, and wrinkle obviously reduces, delicate penetrating, and does not have people to have allergic phenomena in the questionnaire reclaiming.

As shown in Table 5, No. 1 product of people's recommendation of 84.78%, only has No. 2 products of people's recommendation of 15.22%.

Claims (1)

1. containing a Disposable sleep facial mask composition for natural plant extracts, it is characterized in that described mask composition consists of following component by mass percentage:

Phase 1:

Cyclomethicone 5% Radix Oenotherae erythrosepalae oil 2%

Caprylic/capric triglyceride 3% essence 0.2%;

Phase 2:

Deionized water 48.3% methyl hydroxybenzoate 0.2%

Glycerol 15% allantoin 1%

2-(Acryloyloxy)ethanol/sodium acryloyldimethyl taurate copolymers 3% xanthan gum 0.3%

EDTA disodium 0.1% hydroxyethyl-cellulose 0.1%;

Phase 3:

Hyaluronate sodium 1% pansy flowers extract 2%

Deionized water 10% betanin 45%

Glycyrrhizic acid dipotassium 0.5% guava extract 2%

America Ramulus Sambuci Williamsii extract 2% DMDM Hydantoin/iodine propilolic alcohol butyl mephenesin Carbamate 0.3%;

The preparation method of above-mentioned mask composition is as follows:

Phase 1 is put into container and is mixed; 2 put into another vessel in heating to 80 ℃ mutually; Add mutually 2 to 60 ℃ of phases 1, emulsifying, homogenizing, stirs, and is cooled to 50 ℃, adds mutually 3, after stirring, discharging.