CN101982164B - Modified pearl cherry vitamin C sleeping mask and preparation method thereof - Google Patents
Modified pearl cherry vitamin C sleeping mask and preparation method thereof Download PDFInfo
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Abstract
The invention relates to a modified pearl cherry vitamin C sleeping mask. The preparation method of the sleeping mask comprises the following steps: heating nanometer pearl powder to activate, reacting with surfactant to prepare modified nanometer pearl powder, dispersing the modified pearl powder in aqueous phase through turbine stirring, dissolving sodium hyaluronate, glyceryl polyether and butanediol in water, fully stirring, heating, then adding the components of the formula such as Tween-20, isononyl isononanoate and cetearyl alcohol in a pan, stirring to homogenize, cooling to about 45 DEG C, and adding additives, essence, preservative and the like in turn to prepare the modified pearl cherry vitamin C sleeping mask. In the sleeping mask of the invention, the surfactant reacts with the surface hydroxyl groups of the nanometer pearl powder so that the affinity of pearl powder to organic medium is increased and the detects of the nanometer pearl powder that the specific area is large and the nanometer pearl powder is easy to agglomerate and is hydrophilic and oleophobic can be overcome; and cherry vitamin C and nutrient components with permeability and moisture retention capacity are also used, thus the moisture and nutrient components in the mask of the invention can completely permeate the skin during sleep and the state of the skin can be improved intensively.
Description
Technical field
The present invention relates to a kind of facial film with nutrition beauty functions and preparation method thereof, particularly a kind of sleep facial film that contains modified pearl powder and Fructus Pruni pseudocerasi Vc nutrition and preparation method thereof.
Background technology
Margarita is exactly classical beauty treatment medical material since ancient times, and the successive dynasties medical science monumental works such as Compendium of Material Medica, " Mingyi Bielu ", " opening precious vegetation " point out all that Margarita has and calm the nerves, detoxify, preserve youthful looks, and makes us that gloss is pure white, the effect of correcting and skin moisturizing and rejuvenating.Vitamin C has powerful oxidation resistance, can generate by check melanin, prevents pigmentation, and it is rich in the fruit such as Fructus Pruni pseudocerasi, Fructus Fragariae Ananssae.
At present, the major function of the nourishing pack on the market has antioxidation, toxin expelling, fragrant atmosphere, crease-resistant etc., also contain nanometer Margarita powder and vitamin Cs in its nutrition more, even but in cleawhite pack, added vitamin C, also make facial film oxidized variable color in circulation because of ascorbic unstability, even rotten, thereby limited the application of vitamin C in facial film, large because of the nanometer Margarita powder specific surface area equally, easily reunite, and be hydrophilic oleophobic, can't get a desired effect therefore directly apply in the facial film.
The kind of facial film has cream pack, fruit jelly shape facial film, the non-woven fabrics facial film that is soaked with nutrition and facial film made of paper in the prior art, but common facial film generally can only be applied ointment or plaster 15 to 30 minutes, nutrition can't be fully absorbed within the so short time, applying ointment or plaster for a long time then, facial film can become dry, can absorb simultaneously the moisture in the skin, can bring injury to skin on the contrary.
Summary of the invention
The defective that exists in order to overcome prior art, the present invention adopts modified pearl powder and Fructus Pruni pseudocerasi vitamin C compatibility to be prepared into paste sleep facial film.Surfactant activation Margarita powder has increased Margarita powder surface repulsion makes its surface change hydrophobicity into by hydrophilic; the use problems such as nanometer Margarita powder is easily reunited, hydrophilic oleophobic have been solved; add Fructus Pruni pseudocerasi vitamin C extracting solution and effectively protected vitamin C, it is difficult for destroyed.
One of the object of the invention provides a kind of prescription with modified pearl cherry vitamin C sleeping mask of nourishing healthy beauty functions.
Two of the object of the invention provides the preparation method of modified pearl powder.
Three of the object of the invention provides a kind of preparation method with pearl cherry vitamin C sleeping mask of nourishing healthy beauty functions.
Four of the object of the invention provides a kind of using method of the facial film of sleeping.
Prescription following (by weight percentage) with modified pearl cherry vitamin C sleeping mask of nourishing healthy beauty functions of the present invention:
Glycerin polyether-26 5-15% modified pearl powder 0.1-1%
Butanediol 5-10% ascorbic acid glucoside 0.1-1%
Isononyl isononanoate 1-5% antiseptic 0.1-1%
Cetearyl alcohol 1-5% polyquaternary ammonium salt-51 0.1-1%
Polysorbas20 0.5-5% Radix Hamamelidis Mollis distillate 1-5%
An amount of co-emulsifier 1-5% of hyaluronate sodium
Phytosterol/caprylic/capric triglyceride 0.5-5%
Polydimethyl siloxanes/polydimethy siloxanes alcohol 0.5-5%
Malpighia coccigera berry extract 0.1-1% pigment is an amount of
An amount of hydrolecithin 0.1-1% of essence
Deionized water adds to 100%
Modified pearl cherry vitamin C sleeping mask of the present invention is filled a prescription preferably and is:
Glycerin polyether-26 8-12% modified pearl powder 0.1-0.5%
Butanediol 5-8% ascorbic acid glucoside 0.1-0.5%
Isononyl isononanoate 2-4% antiseptic 0.5-1%
Cetearyl alcohol 2-4% polyquaternary ammonium salt-51 0.5-1%
Polysorbas20 0.8-2% Radix Hamamelidis Mollis distillate 1-3%
An amount of co-emulsifier 0.5-2% of hyaluronate sodium
Phytosterol/caprylic/capric triglyceride 0.8-1.5%
Polydimethyl siloxanes/polydimethy siloxanes alcohol 0.8-1.5%
Malpighia coccigera berry extract 0.4-0.8% pigment is an amount of
An amount of hydrolecithin 0.1-1% of essence
Deionized water adds to 100%
Wherein said Malpighia coccigera berry extract is western India Walnut extract (extracting method can with reference to CN01142223 Fructus Pruni pseudocerasi extract and extracting method thereof), and its Vitamin C content is very high.Antiseptic can be selected a kind of of diazolidinyl urea, methyl hydroxybenzoate, propyl hydroxybenzoate or their complex.Described co-emulsifier is polyacrylamide/C13-14 isoparaffin/laureth-7, is commercially available cosmetic material.
The method that the present invention preparation has a modified pearl cherry vitamin C sleeping mask of nourishing healthy beauty functions be first with complexed surfactant to the Margarita powder modification, again by turbine stirring at water disperse modified Margarita powder, and pour synthermal oil phase into thereupon, after stirring homogenizing, be chilled to and add one by one rest additive and essence, antiseptic etc. about 45 ℃, fill finished product under the room temperature.
The used Margarita powder raw material average particle size range of the present invention is the 40-200 nanometer, and the modified technique of Margarita powder is:
(1) mass fraction that will prepare in advance is that 15-30% nanometer Margarita powder suspended emulsion adds in the reactor, and heated at constant temperature activates, and activation temperature is 75-85 ℃;
(2) add the surfactant that accounts for Margarita powder dry weight 1.5-3%, stir 20-40min, Margarita powder is coated by activating agent, and described surfactant is comprised of (w%) 40-60% sorbester p17,20-40% PEG400 and 10-30% butyl acetate,
(3) then with the 3000-3500 rev/min of centrifugal 10-20min of rotating speed and collect the modified pearl layer, oven dry, pulverize and namely get modified nanometer Margarita powder.
In above-mentioned technique of Margarita powder being carried out modified technique, be chosen as preferably: the Margarita powder particle size range is the 40-100 nanometer, mass fraction is 20-25%, surfactant accounts for the 1.5-2% of Margarita powder dry weight, activation temperature is 80-85 ℃, and soak time is 15-20min, and with 3500 rev/mins of centrifugal 10-15min, used surfactant preferred (w%) 45-55% sorbester p17,25-30% PEG400 and 15-20% butyl acetate.
The inventive method is by surfactant and the reaction of nanometer Margarita powder surface hydroxyl, having increased Margarita powder surface repulsion makes its surface change hydrophobicity into by hydrophilic, Margarita powder is strengthened the organic media affinity, solve the inhomogeneous difficult problem of system and the poor drawback of product stability that the nanometer Margarita powder bad dispersibility is brought.
Pearl cherry vitamin C sleeping mask of the present invention prepares by the following method:
(1) with hyaluronate sodium, glycerin polyether-26, butanediol in they gross weight 3-5 deionized water doubly, fully stir and heat, in the time of 70-75 ℃, add successively polysorbas20, the modified pearl powder forms colloidal suspension;
(2) isononyl isononanoate, cetearyl alcohol, phytosterol/caprylic/capric triglyceride, cetearyl alcohol are added oil cauldron and be stirred and heated to 80-85 ℃ of dissolving, then to wherein adding polydimethyl siloxanes/polydimethy siloxanes alcohol;
(3) the emulsifying pot is evacuated to 0.03-0.06MPa, sucks water, be heated with stirring to 80-85 ℃ and with 800-1200r/min speed homogenizing 3-10min, again oil phase is sucked in accordance with the law, be evacuated to 0.1MPa, continue homogenizing 5-10min;
(4) add co-emulsifier under the normal pressure, add one by one pigment, ascorbic acid glucoside, polyquaternary ammonium salt-51, Radix Hamamelidis Mollis distillate and Malpighia coccigera berry extract when being cooled to 55-65 ℃;
(5) add antiseptic and essence and stirring at 40-50 ℃ at last;
(6) the finely dispersed mastic of fill under room temperature.
The sleep using method of facial film of the present invention is: before the sleep facial film is spread upon face (avoiding eye and lip skin) equably, the second day rear cleaning of waking up is used 2-3 time weekly.The product nonirritant, no dependence, without any side effects, not red, pneumonedema, have Fructus Pruni pseudocerasi fragrance concurrently, be easy to be accepted by consumer, in the situation that 600 all ages and classes section people of random searching try out, satisfaction rate maintains more than 87%, illustrates that the product effect is fine, sees table 1 for details.
The below is typical contrast effect:
(1) Lee * *, woman, 29 years old, writer often stays up late, and skin is usually dry, wrinkling, matt, once selected common cream pack, adhered to using two months, skin is still dry matt, and tries out this product 20 days, per two days once, skin of face recovers gloss, pale, high resilience substantially, and the microgroove disappearance, and Lee describes that with " just like newborn " this sleep facial film brings her impression.
(2) Wu *, the woman, 37 years old, outside work, large because of long-term pressure, motion is few, causes the skin layer oils and fats too much.Once used common cream pack two months, skin of face is still very greasy and nonelastic, and after 20 days, whitening skin, high resilience, salubrious are in person to using the result very satisfied with this product.
Table 1 pearl cherry vitamin C sleeping mask trial effect
The sleep facial film of the inventive method preparation contains a large amount of permeability moisturizing compositions such as butanediol, cetearyl alcohol, hyaluronate sodium etc., can form sealed thin film and prevent water loss, lastingly moisturizing, because the present invention has carried out modification with nanometer Margarita powder, make it overcome the nanometer Margarita powder specific surface area large, easily reunite, and the defective that is hydrophilic oleophobic, join again the nutritional labeling that the beauty treatment anti-oxidation efficacy is arranged with Fructus Pruni pseudocerasi vitamin C etc., so that facial film of the present invention can fully infiltrate skin at sleep period chien shih moisture and nutritional labeling, concentrate and improve the skin state, Rapid-Repair stay up late continuously or pressure excessive to face bring tired out and very thirsty, the special cycle care product that belongs to " importing type " or " reinforced ", compare with common facial film, it is rich in infiltration moisturizing composition, permeability is good, but also has whitening, control oil, the effect of Exfoliating Scrub.Facial film of the present invention can rest on face for a long time, can not siphon away the skin internal moisture, is fit to all kinds skin and uses, thereby have extensive market prospect in facial film market.
The specific embodiment
The present invention will be helped to understand by following embodiment, but content of the present invention can not be limited.
Embodiment 1
Step 1, by the following method Margarita powder is carried out modification:
Be that 20% Margarita powder (mean diameter 50 nanometers) suspended emulsion adds in the reactor with mass fraction, being heated to activation temperature is 85 ℃, add the surfactant that accounts for Margarita powder dry weight 2%, constantly stir 20min, then with 3500 rev/mins of rotating speeds from 10min and collect the modified pearl powder, oven dry is pulverized, and makes the modified pearl powder.Wherein used surfactant is comprised of (w%) 45% sorbester p17,25% PEG400 and 30% butyl acetate, and Margarita powder is coated by activating agent.
Step 2, take by weighing raw material in following ratio:
Glycerin polyether-26 10kg modified pearl powder 0.1kg
Butanediol 5kg ascorbic acid glucoside 0.1kg
Isononyl isononanoate 3kg antiseptic 1kg
Cetearyl alcohol 2kg polyquaternary ammonium salt-51 0.5kg
Polysorbas20 1kg Radix Hamamelidis Mollis distillate 1kg
Hyaluronate sodium 0.05kg co-emulsifier 2kg
Phytosterol/caprylic/capric triglyceride 1kg
Polydimethyl siloxanes/polydimethy siloxanes alcohol 4kg
Malpighia coccigera berry extract 0.2kg pigment is an amount of
An amount of hydrolecithin 0.2kg of essence
Deionized water adds to
100kg
Step 3, by following method preparation sleep facial film:
Get first the hyaluronate sodium, glycerin polyether-26, butanediol of formula ratio in the 70kg deionized water, fully stir and heat, about 70 ℃, add successively polysorbas20, the modified pearl powder forms colloidal suspension; Again isononyl isononanoate, cetearyl alcohol, phytosterol/caprylic/capric triglyceride, cetearyl alcohol are added oil cauldron and be stirred and heated to 85 ℃ of dissolvings, then to wherein adding polydimethyl siloxanes/polydimethy siloxanes alcohol; Then the emulsifying pot is evacuated to 0.03-0.06MPa, sucks water, and be heated with stirring to 80 ℃, with 1000r/min speed homogenizing 5min, oil phase is sucked again the emulsifying pot in accordance with the law, continue homogenizing 5min, be evacuated to vacuum to 0.1MPa; Then under normal pressure, add co-emulsifier, be cooled to add one by one below 55 ℃ pigment, ascorbic acid glucoside, polyquaternary ammonium salt-51, Radix Hamamelidis Mollis distillate and Malpighia coccigera berry extract; Add antiseptic and essence and stir the finely dispersed mastic of fill under room temperature at 40 ℃ at last.
Embodiment 2
Step 1: by the following method Margarita powder is carried out modification:
Be that 15% Margarita powder (mean diameter is in 100 nanometers) suspended emulsion adds in the reactor with the mass fraction of in advance preparation, heated at constant temperature, activation temperature is 75 ℃, add the surfactant that accounts for Margarita powder dry weight 1.5% for preparing, constantly stir 40min, then with 3000 rev/mins of centrifugal 20min of rotating speed, freeze-day with constant temperature, comminution by gas stream, make modified nanometer Margarita powder.Wherein used surfactant is comprised of (w%) 60% sorbester p17,20% PEG400 and 20% butyl acetate, and Margarita powder is coated by activating agent.
Step 2: take by weighing raw material in following ratio:
Glycerin polyether-26 6kg modified pearl powder 0.8kg
Butanediol 8kg ascorbic acid glucoside 0.5kg
Isononyl isononanoate 2kg antiseptic 0.5kg
Cetearyl alcohol 1kg polyquaternary ammonium salt-51 0.2kg
Polysorbas20 3kg Radix Hamamelidis Mollis distillate 3kg
Hyaluronate sodium 0.02kg co-emulsifier 3kg
Phytosterol/caprylic/capric triglyceride 4kg
Polydimethyl siloxanes/polydimethy siloxanes alcohol 2kg
Malpighia coccigera berry extract 0.8kg pigment is an amount of
An amount of hydrolecithin 0.6kg of essence
Deionized water adds to
100kg
Step 3: prepare the sleep facial film by following method:
First with hyaluronate sodium, glycerin polyether-26, butanediol in the heavy deionized water of 75kg, fully stir and heat, about 75 ℃, add successively polysorbas20, the modified pearl powder forms colloidal suspension; Again isononyl isononanoate, cetearyl alcohol, phytosterol/caprylic/capric triglyceride, cetearyl alcohol are added oil cauldron and be stirred and heated to 80 ℃ of dissolvings, then to wherein adding polydimethyl siloxanes/polydimethy siloxanes alcohol; Then with water suction emulsifying pot, and be heated with stirring to 80 ℃, simultaneously with behind the 1200r/min speed homogenizing 6min with the oil phase suction, continue homogenizing 8min, evacuation; Then add co-emulsifier, be cooled to add one by one below 55 ℃ pigment, ascorbic acid glucoside, polyquaternary ammonium salt-51, Radix Hamamelidis Mollis distillate and Malpighia coccigera berry extract; Add antiseptic and essence and stir the finely dispersed mastic of fill under room temperature at 45 ℃ at last.
Embodiment 3
Step 1: by the following method Margarita powder is carried out modification:
Be that 30% Margarita powder (mean diameter is 150 nanometers) suspended emulsion adds in the reactor with the mass fraction of in advance preparation, heated at constant temperature, activation temperature is 80 ℃, add the surfactant that accounts for Margarita powder dry weight 2.5% for preparing, constantly stir 30min, then with 3000 rev/mins of centrifugal 15min of rotating speed, freeze-day with constant temperature, comminution by gas stream, make modified nanometer Margarita powder.Wherein used surfactant is comprised of (w%) 50% sorbester p17,30% PEG400 and 20% butyl acetate, and Margarita powder is coated by activating agent.
Step 2: take by weighing raw material in following ratio:
Glycerin polyether-26 8kg modified pearl powder 0.8kg
Butanediol 8kg ascorbic acid glucoside 0.5kg
Isononyl isononanoate 1kg antiseptic 0.8kg
Cetearyl alcohol 1.5kg polyquaternary ammonium salt-51 0.4kg
Polysorbas20 2kg Radix Hamamelidis Mollis distillate 2kg
Hyaluronate sodium 0.04kg co-emulsifier 1kg
Phytosterol/caprylic/capric triglyceride 2.5kg
Polydimethyl siloxanes/polydimethy siloxanes alcohol 3kg
Malpighia coccigera berry extract 0.5kg pigment is an amount of
An amount of hydrolecithin 0.4kg of essence
Deionized water adds to
100kg
Step 3: prepare the sleep facial film by following method:
First with hyaluronate sodium, glycerin polyether-26, butanediol in the deionized water of 72kg, fully stir and heat, about 75 ℃, add successively polysorbas20, the modified pearl powder forms colloidal suspension; Again isononyl isononanoate, cetearyl alcohol, phytosterol/caprylic/capric triglyceride, cetearyl alcohol are added oil cauldron and be stirred and heated to 82 ℃ of dissolvings, then to wherein adding polydimethyl siloxanes/polydimethy siloxanes alcohol; Then with water suction emulsifying pot, and be heated with stirring to 82 ℃, simultaneously with behind the 800r/min speed homogenizing 5min with the oil phase suction, continue homogenizing 10min, evacuation; Then add co-emulsifier, be cooled to add one by one below 60 ℃ pigment, ascorbic acid glucoside, polyquaternary ammonium salt-51, Radix Hamamelidis Mollis distillate and Malpighia coccigera berry extract; Add antiseptic and essence and stir the finely dispersed mastic of fill under room temperature at 45 ℃ at last.
Claims (6)
1. modified pearl cherry vitamin C sleeping mask, its prescription by weight percentage is:
The average particle size range of modified pearl powder is the 40-200 nanometer, and its preparation method is:
(1) mass fraction that will prepare in advance is that 15-30% nanometer Margarita powder suspended emulsion adds in the reactor, and heated at constant temperature activates, and activation temperature is 75-85 ℃;
(2) add the surfactant that accounts for Margarita powder dry weight 1.5-3%, stir 20-40min, wherein surfactant is comprised of 40-60% sorbester p17,20-40% PEG400 and 10-30% butyl acetate by weight percentage;
(3) then with the 3000-3500 rev/min of centrifugal 10-20min of rotating speed and collect the modified pearl layer, oven dry, pulverize.
2. modified pearl cherry vitamin C sleeping mask as claimed in claim 1 is characterized in that described antiseptic is a kind of in diazolidinyl urea, methyl hydroxybenzoate, the propyl hydroxybenzoate or their complex.
3. modified pearl cherry vitamin C sleeping mask as claimed in claim 1 is characterized in that described co-emulsifier is polyacrylamide/C13-14 isoparaffin/laureth-7.
4. modified pearl cherry vitamin C sleeping mask as claimed in claim 1, the average particle size range that it is characterized in that described modified pearl powder is the 50-100 nanometer, nanometer Margarita powder suspended emulsion mass fraction is 20-25%, surfactant accounts for the 1.5-2% of Margarita powder dry weight, activation temperature is 80-85 ℃, soak time is 25-30mi n, and with 3500 rev/mins of centrifugal 10-15min.
5. modified pearl cherry vitamin C sleeping mask as claimed in claim 1 is characterized in that described surfactant is the 45-55% sorbester p17 by weight percentage, 25-30% PEG400 and 15-20% butyl acetate, and each composition sum is 100%.
6. the using method of modified pearl cherry vitamin C sleeping mask as claimed in claim 1 is characterized in that before the sleep facial film being spread upon face equably, avoids eye and lip skin, and the second day rear cleaning of waking up is used 2-3 time weekly.
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| CN102670476A (en) * | 2012-06-12 | 2012-09-19 | 无锡丝源化妆品有限公司 | Modified pearl powder serving as cosmetic and skincare product additive |
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| WO2018003850A1 (en) * | 2016-06-28 | 2018-01-04 | ロート製薬株式会社 | Topical composition containing ascorbic acid and/or salts thereof |
| CN106265433A (en) * | 2016-08-24 | 2017-01-04 | 刘艺鹏 | Margarita Fructus Pruni pseudocerasi sleep mask |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101199472B (en) * | 2007-12-24 | 2010-06-02 | 浙江长生鸟珍珠生物科技有限公司 | Pearl vitamin E whitening moisturizing face masque and process for preparing same |
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| CN104856916A (en) * | 2015-04-29 | 2015-08-26 | 桐城市牯牛背农业开发有限公司 | Water fennel sleeping mask and processing technology thereof |
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