CN101199472B - Pearl vitamin E whitening moisturizing face masque and process for preparing same - Google Patents
Pearl vitamin E whitening moisturizing face masque and process for preparing same Download PDFInfo
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- CN101199472B CN101199472B CN200710302100XA CN200710302100A CN101199472B CN 101199472 B CN101199472 B CN 101199472B CN 200710302100X A CN200710302100X A CN 200710302100XA CN 200710302100 A CN200710302100 A CN 200710302100A CN 101199472 B CN101199472 B CN 101199472B
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Abstract
The invention discloses a whitening and moistening pearl and vitamin E facial mask and its preparation method. The facial mask contains the following materials(based on weight proportion): hexadecanol2-10%, pearl powder 1-12%, olive oil 2-5%, green tea extract 0.1-2%, Alfa arbutin 0.3-2%, vitamin E 0.5-4%, tween80 1-8%, methylparaben 0.2%, fatty acid polyoxyethylene ether 1-8%, a proper amount ofessence, humectant 1-5% and water. The product of the invention overcomes the inconvenience of DIY facial masks made with pearl powder for external use and the invention provides a whitening and moistening pearl vitamin E facial mask which can moisten and whiten skin, refresh dull and coarse skin caused by aging, and provides moisture and nutrition for skin. The invention is simple in making process and low in cost and is convenient to use.
Description
One, invention field
The present invention relates to a kind of skin care item and preparation method thereof, more particularly relate to a kind of pearl vitamin E whitening moisturizing face masque and preparation method thereof with health and beauty function
Two, background technology
Facial film is a kind of special cosmetics, be coated on and form thin film on the skin of face, skin is isolated from the outside out, effective ingredient in the facial film can infiltrate skin, play skin care, have additional nutrients, promote skin technical ability and metabolism, skin of face is pure white, soft, refreshing to relax thereby make, and retains youthful vitality.At present, facial film goods on the market are divided into paste, liquid, glue and powdery by its state, wherein occupy the majority with gluey facial film.From constituent, the Chinese herbal medicine facial film is in the majority.Margarita is exactly rare Chinese medicine since ancient times, and " Kaibao Bencao " said: " be coated with face, make us moist good color; Be coated with brothers, peeling skin hangnail." traditional Chinese medical science thinks, Margarita GUIXIN, Liver Channel, gorgeous appearance skin Caring, skin moistening granulation promoting, speckle removing subtract wrinkle, slow down aging.Vitamin E is " the most direct captor of free radical ", has powerful oxidation resistance, and it can contain that melanin generates, and prevents pigmentation, skin whitening, slow down aging.
The general self-made face pack DIY of Margarita powder external consumer, but complicated operation, it is very inconvenient to use, and has limited the external of Margarita powder to a certain extent.With Margarita powder and dimension E reasonable compatibility, the cream pack market of making yet there are no sale but at present.Marketing research shows first three function of skin care item market capacity rank: preserve moisture, whiten, crease-resistant.Therefore, the pearl vitamin E facial film of inventing a kind of Pear Power moisture-keeping efficacy is well positioned to meet client's demand, has extensive market prospects.
Three, goal of the invention
One of purpose of the present invention provides a kind of pearl vitamin E whitening moisturizing face masque.
Two of purpose of the present invention provides a kind of preparation method of pearl vitamin E whitening moisturizing face masque.
These and other objects of the present invention will further embody and set forth by following detailed description and explanation.
Pearl vitamin E whitening moisturizing face masque of the present invention is characterized in that forming (percentage by weight) by following raw materials according:
Hexadecanol 2-10% modified nanometer Margarita powder 1-12%
Green tea extract 0.1-2% alpha-arbutin 0.3-2%
Olive oil 2-5% vitamin E 0.5-4%
Tween 80 1-8% methyl parahydroxybenzoate 0.2%
Aliphatic acid polyethenoxy ether 1-8% essence is an amount of
Wetting agent 1-5% pure water adds to 100%.
Further, pearl vitamin E whitening moisturizing face masque of the present invention, form (percentage by weight) by following raw materials according:
Hexadecanol 3-8% modified nanometer Margarita powder 1-12%
Green tea extract 0.5-2% alpha-arbutin 0.6-2%
Olive oil 2-5% vitamin E 0.8-3%
Tween 80 1-7% methyl parahydroxybenzoate 0.2%
Aliphatic acid polyethenoxy ether 2-6% essence is an amount of
Wetting agent 1-5% pure water adds to 100%.
What can select is, pearl vitamin E whitening moisturizing face masque of the present invention is formed (percentage by weight) by following raw materials according:
Hexadecanol 4-6% modified nanometer Margarita powder 2-10%
Green tea extract 0.5-1.8% alpha-arbutin 0.6-1.8%
Olive oil 2-4% vitamin E 1.0-3%
Tween 80 2-5% methyl parahydroxybenzoate 0.2%
Aliphatic acid polyethenoxy ether 2-5% essence is an amount of
Wetting agent 2-4% pure water adds to 100%.
Be preferably, pearl vitamin E whitening moisturizing face masque of the present invention, form (percentage by weight) by following raw materials according:
Hexadecanol 4-6% modified nanometer Margarita powder 5-10%
Green tea extract 0.5-1.8% alpha-arbutin 0.6-1.8%
Olive oil 2-4% vitamin E 1.5-3%
Tween 80 2-5% methyl parahydroxybenzoate 0.2%
Aliphatic acid polyethenoxy ether 2-5% essence is an amount of
Wetting agent 3-4% pure water adds to 100%.
In pearl vitamin E whitening moisturizing face masque of the present invention, described wetting agent can be hyaluronic acid, glycerol, sorbitol or pyrrolidone sodium carboxylate, can be used alone, and also can use mixture.Described Margarita powder is a nanoscale, and particle size range is the 1-100 nanometer.
In pearl vitamin E whitening moisturizing face masque of the present invention, described Margarita powder carries out modification earlier to be handled, modified technique is: take by weighing nanometer Margarita powder earlier, adding deionized water and stirring makes it form suspension, the mass fraction that makes nanometer Margarita powder is 10%-30%, suspension is joined in the reactor, heated at constant temperature, activation temperature is 80-90 ℃, what adding configured is the surfactant of basic 1.8%-2.0% with dried Margarita powder, priming reaction under stirring condition, and the time is 40-50min, filter then, freeze-day with constant temperature, comminution by gas stream obtains the modified nanometer Margarita powder product.Described surfactant is by sodium stearate 40-70 weight %, and enuatrol 10-30 weight % and sodium palmitate 10-30 weight % form, and activator is coated on the nanometer Margarita powder surface.
What can select is, in pearl vitamin E whitening moisturizing face masque of the present invention, described Margarita powder carries out modification earlier to be handled, modified technique is: take by weighing nanometer Margarita powder earlier, adding deionized water and stirring makes it form suspension, the mass fraction that makes nanometer Margarita powder is 15%-25 weight %, suspension is joined in the reactor, heated at constant temperature to activation temperature is 80-90 ℃, what adding configured is the surfactant of basic 1.8%-2.0% with dried Margarita powder, priming reaction under stirring condition, and the time is 45-50min, filter then, freeze-day with constant temperature, comminution by gas stream obtains the modified nanometer Margarita powder product.Described surfactant is by sodium stearate 50-65 weight %, and enuatrol 15-25 weight % and sodium palmitate 15-25 weight % form, and activator is coated on the nanometer Margarita powder surface.
Pearl vitamin E whitening moisturizing face masque of the present invention can prepare by following preparation method, hexadecanol, olive oil, aliphatic acid polyethenoxy ether and Tween 80 are mixed and be heated to 60-80 ℃, then other components of the residue except that essence and methyl parahydroxybenzoate are heated to same temperature, the latter is added the former stirring and emulsifying, stir adding essence and methyl parahydroxybenzoate when being chilled to 45 ℃ of left and right sides, continue to stir evenly to room temperature.
What can select is, pearl vitamin E whitening moisturizing face masque of the present invention can prepare by following preparation method, hexadecanol, olive oil, aliphatic acid polyethenoxy ether and Tween 80 are mixed and be heated to 65-75 ℃, then other components of the residue except that essence and methyl parahydroxybenzoate are heated to same temperature, the latter is added the former stirring and emulsifying, stir adding essence and methyl parahydroxybenzoate when being chilled to 45 ℃ of left and right sides, continue to stir evenly to room temperature.
Product of the present invention has overcome the inconvenience of existing Margarita powder external self-made face pack DIY, providing a kind of can deep layer nourish skin whitening, improve skin because of aging cause coarse, dark and gloomy unglazed, for skin provides the whitening skin and preserving moisture pearl vitamin E facial film of moisture and nutrition, its processing technology is simple, cost is low, easy to use.
During use, facial film is spread upon face (avoiding eye and lip skin) uniformly, wash after 10-15 minute, use 2-3 time weekly.
In the present invention, the specific surface area of nanometer Margarita powder is big, easily adsorbed gas, medium or with its effect, thereby lose original surface nature, cause adhesion and reunion, or high and contact interface is bigger because of its surface energy, make speeding up of grain growth.Nanometer Margarita powder is hydrophilic oleophobic in addition, is strong polarity, and there is the stronger hydroxyl of hydrophilic on its surface, be strong basicity, make the affinity variation of itself and organic solvent, easily form aggregation, cause in organic media and to disperse inhomogeneously, cause two storeroom boundary defects, directly effect is bad.The present invention is by carrying out surface modification treatment to nanometer Margarita powder, solve that the nanometer Margarita powder bad dispersibility brings system in emulsion process, emulsifying agent being destroyed of causing of a difficult problem pockety and surface free energy height and cause the drawback of product stability difference.
By to the pre-treatment of nanometer Margarita powder surface modification, activator is coated on the nanometer Margarita powder surface, and its lipophile is strengthened, and dispersive property is improved in apolar medium.
In product of the present invention, if necessary, can also add other additives, (this product is the commercially available prod as green tea extract, also can be with reference to CN-200610128914, the manufacture method that name is called green tea extract prepares), in the white-skinned face function compositions such as alpha-arbutin, Radix Glycyrrhizae extract one or more.Arbutin can and by self and the combining of tryrosinase, quicken melanic decomposition and drainage, deposit dispelling stain and freckle thereby reduce skin pigment.It does not but produce side effect such as toxic, zest, sensitization to melanocyte, also has skin moistening, more effects such as wound, sterilization and collaborative antiinflammatory simultaneously, is skin-whitening and speckle eliminating activating agent safely and effectively at present.Green tea extract has very strong removing free radical and antioxidative ability, and whitening of skin had tangible effect.Nanometer Margarita powder, vitamin E, arbutin, green tea extract are rationally composite, synergism, and whitening effect is better.
The all raw material of Shi Yonging etc. all is conventional uses in the present invention, can buy from market.In the present invention, refer in particular to as non-, all amount, percentage ratios are unit of weight.
Below in conjunction with embodiment the present invention is carried out concrete description, as known by the technical knowledge, the present invention can realize by other the embodiment that does not break away from its spirit or essential feature.Therefore, following embodiment with regard to each side, all just illustrates, and is not only.All within the scope of the present invention or the change that is equal in the scope of the present invention all be included in the invention.
Four, the specific embodiment
Embodiment 1
By the following method Margarita powder being carried out modification handles:
Take by weighing nanometer Margarita powder earlier, adding deionized water and stirring makes it form suspension, the mass fraction that makes nanometer Margarita powder is 10 weight %, suspension is joined in the reactor heated at constant temperature, activation temperature is about 85 ℃, what adding configured is the surfactant of basic 1.8 weight % with dried Margarita powder, priming reaction under stirring condition, and the time is 40min, filtration then, freeze-day with constant temperature, comminution by gas stream obtain the modified nanometer Margarita powder product.Described surfactant is by sodium stearate 60 weight %, and enuatrol 20 weight % and sodium palmitate 20 weight % form, and activator is coated on the nanometer Margarita powder surface.
Embodiment 2
By the following method Margarita powder being carried out modification handles:
Take by weighing nanometer Margarita powder earlier, adding deionized water and stirring makes it form suspension, the mass fraction that makes nanometer Margarita powder is 30 weight %, suspension is joined in the reactor heated at constant temperature, activation temperature is about 85 ℃, what adding configured is the surfactant of basic 2.0 weight % with dried Margarita powder, priming reaction under stirring condition, and the time is 50min, filtration then, freeze-day with constant temperature, comminution by gas stream obtain the modified nanometer Margarita powder product.Described surfactant is by sodium stearate 50 weight %, and enuatrol 25 weight % and sodium palmitate 25 weight % form, and activator is coated on the nanometer Margarita powder surface.
Embodiment 3
By the following method Margarita powder being carried out modification handles:
Take by weighing nanometer Margarita powder earlier, adding deionized water and stirring makes it form suspension, the mass fraction that makes nanometer Margarita powder is 20 weight %, suspension is joined in the reactor heated at constant temperature, activation temperature is about 83 ℃, what adding configured is the surfactant of basic 1.9 weight % with dried Margarita powder, priming reaction under stirring condition, and the time is 45min, filtration then, freeze-day with constant temperature, comminution by gas stream obtain the modified nanometer Margarita powder product.Described surfactant is by sodium stearate 55 weight %, and enuatrol 22 weight % and sodium palmitate 23 weight % form, and activator is coated on the nanometer Margarita powder surface.
Embodiment 4
Take by weighing raw material in following ratio:
2 kilograms in 10 kilograms of olive oil of 3 kilograms of modified nanometer Margarita powder of hexadecanol
0.2 kilogram of green tea extract, 0.5 kilogram of alpha-arbutin
0.2 kilogram of 3 kilograms of methyl parahydroxybenzoate of 4 kilograms of Tween 80s of vitamin E
3 kilograms of essence of aliphatic acid polyethenoxy ether are an amount of
2 kilograms of pure water of wetting agent add to 100 kilograms.
Prepare by the following method:
Hexadecanol, olive oil, aliphatic acid polyethenoxy ether and Tween 80 are mixed and be heated to 60 ℃, then other components of the residue except that essence and methyl parahydroxybenzoate are heated to same temperature, the latter is added the former stirring and emulsifying, mixing time is 20 minutes, mixing speed is 1500 rev/mins, continue to stir adding essence and methyl parahydroxybenzoate when being chilled to 45 ℃ of left and right sides, continue to stir evenly to room temperature.
Embodiment 5
Take by weighing raw material in following ratio:
2 kilograms in 12 kilograms of olive oil of 8 kilograms of modified nanometer Margarita powder of hexadecanol
1.2 kilograms of green tea extracts, 1.8 kilograms of alpha-arbutins
0.2 kilogram of 5 kilograms of methyl parahydroxybenzoate of 2 kilograms of Tween 80s of vitamin E
2 kilograms of essence of aliphatic acid polyethenoxy ether are an amount of
2 kilograms of pure water of wetting agent add to 100 kilograms.
Prepare by the following method:
Hexadecanol, olive oil, aliphatic acid polyethenoxy ether and Tween 80 are mixed and be heated to 60 ℃, then other components of the residue except that essence and methyl parahydroxybenzoate are heated to same temperature, the latter is added the former stirring and emulsifying, mixing time is 15 minutes, mixing speed is 1500 rev/mins, continue to stir adding essence and methyl parahydroxybenzoate when being chilled to 45 ℃ of left and right sides, continue to stir evenly to room temperature.
Embodiment 6
Take by weighing raw material in following ratio:
2.5 kilograms in 8 kilograms of olive oil of 5 kilograms of modified nanometer Margarita powder of hexadecanol
1.5 kilograms of green tea extracts, 1.3 kilograms of alpha-arbutins
0.2 kilogram of 4 kilograms of methyl parahydroxybenzoate of 3 kilograms of Tween 80s of vitamin E
3 kilograms of essence of aliphatic acid polyethenoxy ether are an amount of
3 kilograms of pure water of wetting agent add to 100 kilograms.
Prepare by the following method:
Hexadecanol, olive oil, aliphatic acid polyethenoxy ether and Tween 80 are mixed and be heated to 80 ℃, then other components of the residue except that essence and methyl parahydroxybenzoate are heated to same temperature, the latter is added the former stirring and emulsifying, mixing time is 10 minutes, mixing speed is 1500 rev/mins, continue to stir adding essence and methyl parahydroxybenzoate when being chilled to 45 ℃ of left and right sides, continue to stir evenly to room temperature.
Embodiment 7
Take by weighing raw material in following ratio:
3.5 kilograms in 5 kilograms of olive oil of 4 kilograms of modified nanometer Margarita powder of hexadecanol
0.4 kilogram of green tea extract, 0.8 kilogram of alpha-arbutin
0.2 kilogram of 3 kilograms of methyl parahydroxybenzoate of 2.5 kilograms of Tween 80s of vitamin E
3.5 kilograms of essence of aliphatic acid polyethenoxy ether are an amount of
2.5 kilograms of pure water of wetting agent add to 100 kilograms.
Prepare by the following method:
Hexadecanol, olive oil, aliphatic acid polyethenoxy ether and Tween 80 are mixed and be heated to 70 ℃, then other components of the residue except that essence and methyl parahydroxybenzoate are heated to same temperature, the latter is added the former stirring and emulsifying, mixing time is 30 minutes, mixing speed is 1500 rev/mins, continue to stir adding essence and methyl parahydroxybenzoate when being chilled to 45 ℃ of left and right sides, continue to stir evenly to room temperature.
Claims (8)
1. a pearl vitamin E whitening moisturizing face masque is characterized in that being made up of following raw materials according, by weight percentage:
Hexadecanol 2-10% modified nanometer Margarita powder 1-12%
Green tea extract 0.1-2% alpha-arbutin 0.3-2%
Olive oil 2-5% vitamin E 0.5-4%
Tween 80 1-8% methyl parahydroxybenzoate 0.2%
Aliphatic acid polyethenoxy ether 1-8% essence is an amount of
Wetting agent 1-5% pure water adds to 100%;
Above-mentioned modified nanometer Margarita powder is to add deionized water and stir with nanometer Margarita powder to make it form suspension, the mass fraction that makes nanometer Margarita powder is 10%-30%, suspension is joined in the reactor, heated at constant temperature, activation temperature are 80-90 ℃, and what adding configured is the surfactant of basic 1.8%-2.0% with dried Margarita powder, priming reaction under stirring condition, time is 40-50min, and filtration then, freeze-day with constant temperature, comminution by gas stream obtain the modified nanometer Margarita powder product;
Above-mentioned surfactant is by sodium stearate 40-70 weight %, and enuatrol 10-30 weight % and sodium palmitate 10-30 weight % form.
2. pearl vitamin E whitening moisturizing face masque according to claim 1 is characterized in that being made up of following raw materials according, by weight percentage:
Hexadecanol 3-8% modified nanometer Margarita powder 1-12%
Green tea extract 0.5-2% alpha-arbutin 0.6-2%
Olive oil 2-5% vitamin E 0.8-3%
Tween 80 1-7% methyl parahydroxybenzoate 0.2%
Aliphatic acid polyethenoxy ether 2-6% essence is an amount of
Wetting agent 1-5% pure water adds to 100%;
Above-mentioned modified nanometer Margarita powder is to add deionized water and stir with nanometer Margarita powder to make it form suspension, the mass fraction that makes nanometer Margarita powder is 10%-30%, suspension is joined in the reactor, heated at constant temperature, activation temperature are 80-90 ℃, and what adding configured is the surfactant of basic 1.8%-2.0% with dried Margarita powder, priming reaction under stirring condition, time is 40-50min, and filtration then, freeze-day with constant temperature, comminution by gas stream obtain the modified nanometer Margarita powder product;
Above-mentioned surfactant is by sodium stearate 40-70 weight %, and enuatrol 10-30 weight % and sodium palmitate 10-30 weight % form.
3. pearl vitamin E whitening moisturizing face masque according to claim 1 is characterized in that being made up of following raw materials according, by weight percentage:
Hexadecanol 4-6% modified nanometer Margarita powder 2-10%
Green tea extract 0.5-1.8% alpha-arbutin 0.6-1.8%
Olive oil 2-4% vitamin E 1.0-3%
Tween 80 2-5% methyl parahydroxybenzoate 0.2%
Aliphatic acid polyethenoxy ether 2-5% essence is an amount of
Wetting agent 2-4% pure water adds to 100%;
Above-mentioned modified nanometer Margarita powder is to add deionized water and stir with nanometer Margarita powder to make it form suspension, the mass fraction that makes nanometer Margarita powder is 10%-30%, suspension is joined in the reactor, heated at constant temperature, activation temperature are 80-90 ℃, and what adding configured is the surfactant of basic 1.8%-2.0% with dried Margarita powder, priming reaction under stirring condition, time is 40-50min, and filtration then, freeze-day with constant temperature, comminution by gas stream obtain the modified nanometer Margarita powder product;
Above-mentioned surfactant is by sodium stearate 40-70 weight %, and enuatrol 10-30 weight % and sodium palmitate 10-30 weight % form.
4. pearl vitamin E whitening moisturizing face masque according to claim 1 is characterized in that being made up of following raw materials according, by weight percentage:
Hexadecanol 4-6% modified nanometer Margarita powder 5-10%
Green tea extract 0.5-1.8% alpha-arbutin 0.6-1.8%
Olive oil 2-4% vitamin E 1.5-3%
Tween 80 2-5% methyl parahydroxybenzoate 0.2%
Aliphatic acid polyethenoxy ether 2-5% essence is an amount of
Wetting agent 3-4% pure water adds to 100%;
Above-mentioned modified nanometer Margarita powder is to add deionized water and stir with nanometer Margarita powder to make it form suspension, the mass fraction that makes nanometer Margarita powder is 10%-30%, suspension is joined in the reactor, heated at constant temperature, activation temperature are 80-90 ℃, and what adding configured is the surfactant of basic 1.8%-2.0% with dried Margarita powder, priming reaction under stirring condition, time is 40-50min, and filtration then, freeze-day with constant temperature, comminution by gas stream obtain the modified nanometer Margarita powder product;
Above-mentioned surfactant is by sodium stearate 40-70 weight %, and enuatrol 10-30 weight % and sodium palmitate 10-30 weight % form.
5. according to the described pearl vitamin E whitening moisturizing face masque of one of claim 1-4, it is characterized in that described wetting agent is a kind of or wherein several mixture in hyaluronic acid, glycerol, sorbitol or the pyrrolidone sodium carboxylate.
6. according to the described pearl vitamin E whitening moisturizing face masque of one of claim 1-4, it is characterized in that described Margarita powder is a nanoscale, particle size range is the 1-100 nanometer.
7. according to the described pearl vitamin E whitening moisturizing face masque of one of claim 1-4, it is characterized in that activator is coated on the nanometer Margarita powder surface.
8. according to the preparation method of one of claim 1-7 described pearl vitamin E whitening moisturizing face masque, it is characterized in that hexadecanol, olive oil, aliphatic acid polyethenoxy ether and Tween 80 being mixed and being heated to 60-80 ℃, then other components of the residue except that essence and methyl parahydroxybenzoate are heated to same temperature, the latter is added the former stirring and emulsifying, stir adding essence and methyl parahydroxybenzoate when being chilled to 45 ℃ of left and right sides, continue to stir evenly to room temperature.
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Address after: 311800 Zhejiang Province, Zhuji city Jiyang street street, Sha Sha Road No. 48 Patentee after: Zhejiang changshengniao health Polytron Technologies Inc Address before: The beauty of Zhejiang province Zhuji city street 311800 No. 80 5 floor Patentee before: Zhejiang Changshengniao Pearl Biotechnology Co., Ltd. |
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