CN102697696B - Pearl powder sun cream - Google Patents

Pearl powder sun cream Download PDF

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Publication number
CN102697696B
CN102697696B CN 201210192227 CN201210192227A CN102697696B CN 102697696 B CN102697696 B CN 102697696B CN 201210192227 CN201210192227 CN 201210192227 CN 201210192227 A CN201210192227 A CN 201210192227A CN 102697696 B CN102697696 B CN 102697696B
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CN
China
Prior art keywords
margarita powder
phase component
pearl powder
oil
lipophile
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Expired - Fee Related
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CN 201210192227
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Chinese (zh)
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CN102697696A (en
Inventor
戴钧钧
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WUXI SIYUAN COSMETICS Co CO Ltd
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WUXI SIYUAN COSMETICS Co CO Ltd
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Priority to CN 201210192227 priority Critical patent/CN102697696B/en
Publication of CN102697696A publication Critical patent/CN102697696A/en
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Publication of CN102697696B publication Critical patent/CN102697696B/en
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Abstract

The invention discloses pearl powder sun cream which comprises water in oil emulsifier, mineral oil, isooctyl palmitate, heterogenous cetane, octyl methoxycinnamate, benzophenone-3, modified lipophilic pearl powder, titanium dioxide, glycerol, magnesium sulphate heptahydrate, water, essence and preservative agents, and all the components are mixed according to a proportion and are processed through the processing steps of heating, uniformly stirring, homogenizing, cooling and the like. According to the invention, modified pearl powder serves as a component playing the role of beauty, the surface of a pearl powder particle that is modified is lipophilic instead of hydrophilic, the surface of the pearl powder particle is smoother and is good in lubricity, the compatibility of pearl powder and organic medium is improved, and the modified pearl powder in the sun cream has excellent dispersivity and stability, so that the pearl powder can give full play to moistening and whitening.

Description

The Margarita powder sunscreen cream
Technical field
The present invention relates to sunscreen cream, relate in particular to the sunscreen cream that adds Margarita powder.
Background technology
Ultraviolet in the sunlight is to cause skin blackening and aging main cause, resists ultraviolet by the mode of smearing sunscreen cream to skin usually.The action principle of sunscreen cream is that skin and ultraviolet are kept apart, thereby prevents the skin sunburn.
Margarita is exactly classical beauty treatment medical material since ancient times, successive dynasties medical science monumental works such as Compendium of Material Medica, " Mingyi Bielu ", " opening precious vegetation " all point out Margarita have calm the nerves, detoxify, preserve youthful looks, effect such as correcting and skin moisturizing and rejuvenating, make skin gloss pure white, its beauty treatment mechanism is aminoacid and the trace element that contains various needed by human body in the Margarita, its nutritional labeling and the required nutrient of human skin approach, be easy to be absorbed by the body, have good aesthetic health care and function in delaying senility.The Margarita powder that Margarita processes from strand is the most general a kind of mode of using pearl cosmetic.Margarita powder can solve face oil and dead bark problem, specifically, can play skin whitening, antidotal effect by the activity of enhancement of SOD, and therefore, Margarita powder can be used as a kind of additive of sunscreen cream, plays and moistens the auxiliaring effect of whitening.
At present, prior art is directly to add to after the crushing pearl in the sunscreen cream, and the Margarita powder specific grain surface of preparation is long-pending big, easily be agglomerated into knot, and mostly be hydrophilic oleophobic property, not only be difficult for absorbing, even stop up pore easily and cause folliculitis, influence the performance of Margarita powder effect.
Summary of the invention
The objective of the invention is the above-mentioned defective at the Margarita sunscreen cream existence of prior art for preparing, a kind of Margarita powder sunscreen cream is provided, Margarita powder wherein has fabulous dispersibility in described sunscreen cream, moistens the effect of whitening thereby Margarita powder is given full play to.
The technical solution used in the present invention is as follows:
A kind of Margarita powder sunscreen cream is prepared from by the component of following weight percentage ratio:
The A phase component:
Water-in-oil emulsifier 2~5%
White oil 2~8%
Iso-octyl palmitate 1~6%
Isomery hexadecane 2~7%
Octyl methoxycinnamate 2~5%
Benzophenone-3 2~3%
Modification lipophile Margarita powder 1~8%
Titanium dioxide 2~6%
The B phase component:
Glycerol 5~15%
Magnesium sulfate heptahydrate 0.2~1%
The C phase component
Essence 0.1~0.3%
Antiseptic 0.01~0.5%
Surplus is water
Preparation process is:
Described modification lipophile Margarita powder and titanium dioxide are evenly dispersed in the oil phase system of being made up of described water-in-oil emulsifier, white oil, iso-octyl palmitate, isomery hexadecane, octyl methoxycinnamate and benzophenone-3, obtain the A phase component; Again described glycerol, Magnesium sulfate heptahydrate are mixed with described water, obtain the B phase component; A phase component and B phase component are heated to 85~90 ℃ respectively, then the B phase component are delayed in the adding A phase component slowly, stir fast simultaneously, use homogenizers to carry out homogenizing after all adding finishes and handle, 3~5 minutes time, be cooled to 40~45 ℃ afterwards; Add the C phase component at last, continue to be stirred to cooling fully, discharging obtains finished product;
Wherein, modification lipophile Margarita powder is prepared by following step:
(1) by following component with the percetage by weight compositing formula:
Margarita powder 80~95%
Double stearic acid aluminium 2~15%
Poly-methyl silsesquioxane 1~5%
Dimethicone 0.5~4%
(2) Margarita powder being broken into fineness is 1000~20000 purpose Margarita powder, be that the poly-methyl silsesquioxane of 0.5~15 μ m is mixed stirring by described percentage by weight with double stearic acid aluminium, grain diameter, and after three-roller grinds evenly, the viscosity that adds described percentage by weight is the dimethicone of 5~100cs, mix and stir, continuation is ground 2~3 times at three-roller, obtains Powdered finished product.
Its further technical scheme is as follows:
Described water-in-oil emulsifier is a kind of in the two stearates of polyglycereol (3), polyglycereol (2) isostearate.
Described antiseptic is isothiazolone, a kind of in the 2-phenyl phenol.
The grain diameter of described poly-methyl silsesquioxane is preferably 2~6 μ m.
Described dimethyl-silicon oil viscosity is preferably 5~30cs.
Useful technique effect of the present invention is:
Adopt the modification Margarita powder as the component that plays cosmetology function among the present invention, the Margarita powder particle surface of handling through modification becomes lipophile by hydrophilic, the Margarita powder particle surface is more smooth, lubricity is good, improved the affinity of Margarita powder and organic media, make the modification Margarita powder in described sunscreen cream, have fabulous dispersibility and stability, moisten the effect of whitening thereby Margarita powder is given full play to.
The specific embodiment
Below in conjunction with embodiment, the specific embodiment of the present invention is described.
Embodiment 1
A kind of sunscreen cream that adds the modification Margarita powder is by being prepared from by following components in weight percentage:
The A phase component:
The two stearates 2% of polyglycereol (3)
White oil 8%
Iso-octyl palmitate 1%
Isomery hexadecane 7%
Octyl methoxycinnamate 2%
Benzophenone-3 3%
Modification lipophile Margarita powder 1%
Titanium dioxide 6%
The B phase component:
Glycerol 5%
Magnesium sulfate heptahydrate 1%
The C phase component:
Essence 0.1%
Isothiazolone 0.5%
Surplus is water
Preparation process is:
Described modification lipophile Margarita powder and titanium dioxide are evenly dispersed in the oil phase system of being made up of the two stearates of described polyglycereol (3), white oil, iso-octyl palmitate, isomery hexadecane, octyl methoxycinnamate and benzophenone-3, obtain the A phase component; Again described glycerol, Magnesium sulfate heptahydrate are mixed with described water, obtain the B phase component; A phase component and B phase component are heated to 85 ℃ respectively, then the B phase component are delayed in the adding A phase component slowly, stir fast simultaneously, use homogenizers to carry out homogenizing after all adding finishes and handle, 3 minutes time, be cooled to 40 ℃ afterwards; Add the C phase component at last, continue to be stirred to cooling fully, discharging obtains finished product;
Wherein, modification lipophile Margarita powder is prepared by following step:
(1) by following component with the percetage by weight compositing formula:
Margarita powder 81%
Double stearic acid aluminium 14%
Poly-methyl silsesquioxane 1%
Dimethicone 4%
(2) preparation method is specific as follows: with grinder Margarita being ground to form fineness is 1000 purpose Margarita powder, be that the poly-methyl silsesquioxane of 0.5 μ m is mixed stirring by described percentage by weight with aluminium stearate, granular size, and after three-roller grinds evenly, the viscosity that adds described percentage by weight is the dimethicone of 100cs, mix and stir, continuation is ground 3 times at three-roller, obtains Powdered finished product.
Oleophylic service check: the Powdered modification lipophile of gained Margarita powder finished product is put into deionized water, and stir with Glass rod, water is still transparent fully, more above-mentioned Powdered finished product is put into white oil, no granule swims in the surface, proves that gained modification lipophile Margarita powder has good lipophile.
Embodiment 2
A kind of sunscreen cream that adds the modification Margarita powder is by being prepared from by following components in weight percentage:
The A phase component:
Polyglycereol (2) isostearate 5%
White oil 2%
Iso-octyl palmitate 6%
Isomery hexadecane 2%
Octyl methoxycinnamate 5%
Benzophenone-3 2%
Modification lipophile Margarita powder 8%
Titanium dioxide 2%
The B phase component:
Glycerol 15%
Magnesium sulfate heptahydrate 0.2%
The C phase component:
Essence 0.3%
2-phenyl phenol 0.01%
Surplus is water
Preparation process is:
Described modification lipophile Margarita powder and titanium dioxide are evenly dispersed in the oil phase system of being made up of described polyglycereol (2) isostearate, white oil, iso-octyl palmitate, isomery hexadecane, octyl methoxycinnamate and benzophenone-3, obtain the A phase component; Again described glycerol, Magnesium sulfate heptahydrate are mixed with described water, obtain the B phase component; A phase component and B phase component are heated to 90 ℃ respectively, then the B phase component are delayed in the adding A phase component slowly, stir fast simultaneously, use homogenizers to carry out homogenizing after all adding finishes and handle, 5 minutes time, be cooled to 45 ℃ afterwards; Add the C phase component at last, continue to be stirred to cooling fully, discharging obtains finished product;
Wherein, modification lipophile Margarita powder is prepared by following step:
(1) by following component with the percetage by weight compositing formula:
Margarita powder 93%
Double stearic acid aluminium 2%
Poly-methyl silsesquioxane 4.5%
Dimethicone 0.5%
(2) preparation method is specific as follows: with grinder Margarita being ground to form fineness is 20000 purpose Margarita powder, be that the poly-methyl silsesquioxane of 15 μ m is mixed stirring by described percentage by weight with aluminium stearate, granular size, and after three-roller grinds evenly, the viscosity that adds described percentage by weight is the dimethicone of 5cs, mix and stir, continuation is ground 2 times at three-roller, obtains Powdered finished product.
Oleophylic service check: the Powdered modification lipophile of gained Margarita powder finished product is put into deionized water, and stir with Glass rod, water is still transparent fully, more above-mentioned Powdered finished product is put into white oil, no granule swims in the surface, proves that gained modification lipophile Margarita powder has good lipophile.
Above-described embodiment 1~2 described each raw material is the commercially available universal product.
The measure of merit of embodiment 1~2 prepared sunscreen cream:
Select 20 trial volunteers for use, be divided into two groups at random, every group of 10 people smear for respectively two groups of experimenters with the prepared Margarita powder sunscreen cream of embodiment 1~2, once a day, are applied in facial after clean of morning and health exposes the position, smear continuously 30 days.
Test result: after 30 days, observe and experimenter's reaction according to operating position, by
Range estimation and sense learning through practice, skin are all glossy than moistening before using, and no dry sensation, and tool whitening effect do not have irritated reaction.
Above-described only is preferred implementation of the present invention; the present invention is not limited to above embodiment; other improvement and variation that those skilled in the art directly derive under the prerequisite that does not break away from spirit of the present invention and design or associate all should be thought to be included in protection scope of the present invention.

Claims (4)

1. Margarita powder sunscreen cream is characterized in that being prepared from by the component of following weight percentage ratio:
The A phase component:
Water-in-oil emulsifier 2~5%
White oil 2~8%
Iso-octyl palmitate 1~6%
Isomery hexadecane 2~7%
Octyl methoxycinnamate 2~5%
Benzophenone-3 2~3%
Modification lipophile Margarita powder 1~8%
Titanium dioxide 2~6%
The B phase component:
Glycerol 5~15%
Magnesium sulfate heptahydrate 0.2~1%
The C phase component
Essence 0.1~0.3%
Antiseptic 0.01~0.5%
Surplus is water
Preparation process is:
Described modification lipophile Margarita powder and titanium dioxide are evenly dispersed in the oil phase system of being made up of described water-in-oil emulsifier, white oil, iso-octyl palmitate, isomery hexadecane, octyl methoxycinnamate and benzophenone-3, obtain the A phase component; Again described glycerol, Magnesium sulfate heptahydrate are mixed with described water, obtain the B phase component; A phase component and B phase component are heated to 85~90 ℃ respectively, then the B phase component are delayed in the adding A phase component slowly, stir fast simultaneously, use homogenizers to carry out homogenizing after all adding finishes and handle, 3~5 minutes time, be cooled to 40~45 ℃ afterwards; Add the C phase component at last, continue to be stirred to cooling fully, discharging obtains finished product;
Wherein, modification lipophile Margarita powder is prepared by following step:
(1) by following component with the percetage by weight compositing formula:
Margarita powder 80~95%
Double stearic acid aluminium 2~15%
Poly-methyl silsesquioxane 1~5%
Dimethicone 0.5~4%
(2) Margarita powder being broken into fineness is 1000~20000 purpose Margarita powder, be that the poly-methyl silsesquioxane of 0.5~15 μ m is mixed stirring by described percentage by weight with double stearic acid aluminium, grain diameter, and after three-roller grinds evenly, the viscosity that adds described percentage by weight is the dimethicone of 5~100cs, mix and stir, continuation is ground 2~3 times at three-roller, obtains Powdered finished product.
2. according to the described Margarita powder sunscreen cream of claim 1, it is characterized in that described water-in-oil emulsifier is a kind of in the two stearates of polyglycereol (3), polyglycereol (2) isostearate.
3. according to the described Margarita powder sunscreen cream of claim 1, the grain diameter that it is characterized in that described poly-methyl silsesquioxane is 2~6 μ m.
4. according to the described Margarita powder sunscreen cream of claim 1, it is characterized in that described dimethyl-silicon oil viscosity is 5~30cs.
CN 201210192227 2012-06-12 2012-06-12 Pearl powder sun cream Expired - Fee Related CN102697696B (en)

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Application Number Priority Date Filing Date Title
CN 201210192227 CN102697696B (en) 2012-06-12 2012-06-12 Pearl powder sun cream

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Application Number Priority Date Filing Date Title
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CN102697696B true CN102697696B (en) 2013-08-07

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Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110200874A (en) * 2019-07-08 2019-09-06 卢琛 A kind of whitening and spot eliminating cream and preparation method thereof
CN112121001B (en) * 2020-10-19 2021-08-10 广东创美抗衰老研究有限公司 Non-irritant essence with whitening and moisturizing functions and preparation method thereof
CN112472655A (en) * 2020-10-26 2021-03-12 刘赛 Preparation method of pearl powder sun cream
CN114053202B (en) * 2021-12-30 2024-01-26 欧诗漫生物股份有限公司 Sun-screening composition and sun-screening agent

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101199472B (en) * 2007-12-24 2010-06-02 浙江长生鸟珍珠生物科技有限公司 Pearl vitamin E whitening moisturizing face masque and process for preparing same
CN101199471A (en) * 2007-12-28 2008-06-18 浙江长生鸟珍珠生物科技有限公司 Pearl whitening moisturizing astringent and process for preparing same
CN101288638A (en) * 2008-05-23 2008-10-22 海南京润珍珠生物技术股份有限公司 Cream pearl powder skin care products
CN101773463A (en) * 2009-01-09 2010-07-14 苏州知微堂生物科技有限公司 Selenium-enriched nano pearl powder formula and production method thereof
CN101982164B (en) * 2010-10-26 2013-02-27 浙江长生鸟珍珠生物科技有限公司 Modified pearl cherry vitamin C sleeping mask and preparation method thereof
CN102327196A (en) * 2011-08-19 2012-01-25 广州市白云联佳精细化工厂 Sun-proof BB (Blemish Balm) cream and preparation method thereof
CN102397222A (en) * 2011-11-18 2012-04-04 大连得达科技发展有限公司 Safety sunscreen lotion

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