CN104800121B - A kind of daily necessities composition containing nephrite and its preparation method and application - Google Patents
A kind of daily necessities composition containing nephrite and its preparation method and application Download PDFInfo
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Abstract
The invention discloses a kind of daily necessities compositions containing nephrite and its preparation method and application, and the daily necessities composition is made of the raw material for including following weight percent：Nephrite 10~40%, gold 0.005~0.01%, silver 0.001~0.01%, Moringa extract 0.1~5%, natural antiseptic agent 0.25%~0.3%；The grain size of the nephrite is 5~20nm；The grain size of the gold is 30~80nm；The grain size of the silver is 25~50nm；The natural antiseptic agent be containing Baical Skullcap root P.E 5 40%, Flos Hibisci Mutabilis extract 5 40%, Olive leaf P.E 20 60% Chinese medical extract.The daily necessities composition containing nephrite of the present invention has lower coefficient of friction, excellent use feeling, and also has effects that whitening, nourishing, reparation.
Description
Technical field
The invention belongs to skin care item and cosmetic technical field, more particularly it relates to a kind of day containing nephrite
Articles for use composition and its preparation method and application.
Background technology
In general, jade is roughly divided into jadeite and nephrite, and jadeite is the lead pyroxenite group mineral for belonging to pyroxenite race, is by silicon
The monoclinic system substance that acid, aluminium oxide, sodium carbonate are formed, is hardness compact block as crystal, gloss is black, dark green, green
Color is transparent or translucent.Say common " jade ", that is primarily referred to as jadeite.
Nephrite is the monoclinic system pyribole minerals of inosilicate, is divided into tremolite jade and snake in magnesia marble
Petrochemical industry hyperalkaline nephrite, their quality is with its fine structures shape, i.e., with the tremolite-actinolite crystalline substance by beam group and fiber
The fineness of formation determines, it is known that fiber is more superfine, and quality is more excellent.
On such jade, according to the report in German medical field document, jadeite and nephrite are two kinds of different ores, it
As most jewel, containing silicon and oxygen, but opposite jadeite is with granular pattern Crystallization, nephrite the difference is that
Be as cellulosic, countless crystal and particle aggregate as hair formed, particularly different from the sodium and aluminium in jadeite
Constituent, nephrite are with the three kind mineral beneficial to human body, i.e., calcium, magnesium, iron are as principal component.Nephrite is recently published to height
Blood pressure, diabetes, causing circulatory obstacle, the treatment zone of heart disease and the disease caused by nephropathy are come strong influence.Separately
Outside, taken greatly according to new agriculture book on Chinese herbal medicine, Tang materia medica, Compendium of Materia Medica etc. it is known that jade is ground into sesame seed, can moisten the five internal organs
Six internal organs not only have the effect for being completely exhausted out the waste accumulated for a long time in vivo, but also due to the heat in removal stomach and to digestion
System is effective, pants to bronchus and the anemia felt bad of body heat rise heart is effective；During the broiling summer, jade carving teacher
Fu is accidentally injured at work by cutter, will not inflammation, and the time healed than normal fast, therefore, in face or body
When having scar, a few days is wiped at scar position with nephrite, scar can disappear.The principal component of nephrite is almost without side-effects, and human body is sent out
Wave remarkable efficiency.
But while known nephrite has human body the medicine efficiency of brilliance as described above, but due to its rareness, only make
For the part such as necklace, ring, bracelet, decoration is used with jewel ornament at one's side.Actual conditions are, particularly nephrite plus
Needed in work many time and effort and need degree of fineness note that so if be not the practician that has protracted experience,
Nephrite cannot be carried out to fine processing.Because being high price product, so while economic burden, also almost without soft to utilizing
Jade is developed as general daily necessities.Therefore, people's an urgent demand in order to more valuably utilize nephrite various lives
The research and development of articles for use or medical supplies and body cosmetic products etc..
As the influence to skin, ultraviolet light is not only, near infrared ray is also increasingly considered problem.It is therefore desirable to one
The basic ingredient that kind can cover near infrared ray is used in cosmetics or daily necessities.In addition, cosmetics or daily necessities are also paid much attention to
Sense of touch.It is known to cosmetics or daily necessities zinc oxide to be coordinated to assign the purpose of UV absorbing properties.But Zinc oxide particles
In the case of ultra micron for below 100nm, there is lead to the problem of abrasive feel, sense of touch variation.In existing literature, also have and match somebody with somebody
Conjunction has cosmetics of 0.5 μm~20 μm of the zinc oxide as infrared shield substance.But the average friction of the Zinc oxide particles
Coefficient is big, thus in the case of a large amount of cooperations, there is lead to the problem of abrasive feel, use feeling difference etc.Also, the oxidation
The total visible light transmittance of zinc particle is low, there are problems that the transparency is poor, occurs whitening etc.
The effect of how using known to nephrite, with the use of other additives, preparing one kind will not be such that sense of touch deteriorates, simultaneously
And the daily necessities composition that transparency etc. is had excellent performance is very important.
The content of the invention
Based on this, the defects of in order to overcome the above-mentioned prior art, the present invention provides a kind of daily necessities groups containing nephrite
Object is closed, which will not deteriorate sense of touch, and transparency etc. is had excellent performance.
In order to realize foregoing invention purpose, this invention takes following technical schemes：
A kind of daily necessities composition containing nephrite, the daily necessities composition is by including the raw material of following weight percent
Composition：
The grain size of the nephrite is 5~20nm；The grain size of the gold is 30~80nm；The grain size of the silver for 25~
50nm；The natural antiseptic agent is 5-40% containing Baical Skullcap root P.E, Flos Hibisci Mutabilis extract 5-40%, Olive leaf P.E 20-
60% Chinese medical extract.
In wherein some embodiments, the grain size of the nephrite is 5~10nm, and the grain size of the gold is 30~50nm, institute
The grain size for stating silver is 25~35nm.
In wherein some embodiments, the nephrite is one or both of serpentine, the tremolite.
In wherein some embodiments, the microstructure of the nephrite is hair felty texture, micro- blade blastic texture, shows
Microfibre blastic texture, micro- fiber-cryptocrystalline blastic texture, micro- blade-cryptocrystalline blastic texture, radial structure,
Or broom shape structure.
In wherein some embodiments, the microstructure of the nephrite is radial structure.
In wherein some embodiments, the Moringa extract by the tree root of the Moringa by that will dry and grind, seed,
Or blade is added in into the solvent of ethanol/water=9/1, is countercurrently extracted and is obtained at 80 DEG C.
In wherein some embodiments, the natural antiseptic agent is prepared by following methods：After Chinese medicine is crushed, mistake
Sieve, after impregnating 1-2h together with Extraction solvent, is extracted, extracting solution is centrifuged with high pressure homogenization method machine at normal temperatures
Afterwards, with macroporous resin adsorption, repeatedly eluted with the ethyl alcohol of 10-95%, collect eluent, be concentrated under reduced pressure into medicinal extract shape to get；Institute
Extraction solvent is stated as water, ethyl alcohol or ethanol water.
In wherein some embodiments, the daily necessities composition further includes group conventional in daily necessities or cosmetic field
Point.
The present invention also provides the preparation methods of the above-mentioned daily necessities composition containing nephrite, comprise the following steps：
By nephrite, gold and silver mixing, it is ground together；Moringa extract and daily necessities or cosmetics are added after grinding
Conventional component in field, 60~70 DEG C are stirred mixing, then make to reach uniform using mixer for well-distribution, de-bubbled,
After filtering, natural antiseptic agent is added, is cooled down using heat exchanger etc. and reaches product.
The present invention also provides the application of the above-mentioned daily necessities composition containing nephrite, the application is led including cosmetics
Late frost, the face frost that compacts, visage block cream, ultra light sun block lotion, conditioning vanishing cream, reparation eye cream, facial mask, face mask cream, hand are such as nourished in domain
Film, foot film, hand lotion, spats frost, moisturizing liquid, lipstick, the application further include daily necessities field, such as perfumed soap, toothpaste, gargle
Water, shampoo, shower cream etc..
The daily necessities composition containing nephrite of the present invention will not deteriorate sense of touch, and transparency etc. is had excellent performance, and
The daily necessities compound has whitening, nourishing, reparation, anti-inflammatory and other effects.
The above-mentioned of the application and other features, aspect and advantage is more readily understood with reference to following detailed description.
Specific embodiment
Participate in the election of the detailed description of the invention below that method is preferably implemented and including embodiment this public affairs can be more easily understood
Open content.A large amount of terms can be referred in description below and claims, these terms are defined as following meanings.
Singulative includes plural number and object is discussed, unless the context clearly dictates otherwise.
" optional " or " optionally " refer to that the item described thereafter or event may or may not occur, and this is retouched
State the situation that the situation including event generation and event do not occur.
Approximate term in specification and claims is used for modifying quantity, represents specific the present invention is not limited to this
Quantity further includes the modified part of the acceptable change without cause related basic function close to the quantity.Phase
It answers, modifies a numerical value with " about ", " about " etc., mean that the invention is not restricted to the exact numericals.It is approximate in some examples
Term likely corresponds to the precision of the instrument of measured value.In present specification and claims, scope limits can be with
It combines and/or exchanges, these scopes include all subranges contained therebetween if not stated otherwise.
The first aspect of the present invention provides a kind of daily necessities composition containing nephrite, and the daily necessities composition is by wrapping
Include the raw material composition of following weight percent：
The grain size of the nephrite is 5~20nm；The grain size of the gold is 30~80nm；The grain size of the silver for 25~
50nm；The natural antiseptic agent is 1-40% containing Baical Skullcap root P.E, Flos Hibisci Mutabilis extract 1-40%, Olive leaf P.E 1-80%
Chinese medical extract.
In the present invention, the term " nephrite " is the monoclinic system pyribole minerals of inosilicate, is made in the present invention
It is the Qilian jade in nephrite, they have fine structure, and fiber is superfine, best in quality.The grain of nephrite in the present invention
Footpath is at 5~20 nanometers.The particle that grain size is 5~20 nanometers more can be mutual with alkalescent anion water under the heat temperature close to body temperature
Effect generates micro remote red place's microwave, and is more easy to be less readily available for absorption by the skin.Preferably, the grain size of the nephrite is 5~10nm.As
Some of preferred embodiments of the present invention, the nephrite are one or both of serpentine, the tremolite.
In the present invention, the processing mode of nephrite is：Moisture removal-utilization is gone in filtration of demineralized water (preliminary impurity screening)-drying
Solvent reconciliation-operating pressure obtains requiring nephrite-sterilization treatment of grain size-utilize solvent for 0.5~2 atmospheric pressure microfiltration (MF)
It reconciles.
As some of preferred embodiments of the present invention, the microstructure of the nephrite is hair felty texture, micro-
Blade blastic texture, micro- nematoblastic texture, micro- fiber-cryptocrystalline blastic texture, micro- blade-cryptocrystalline metacrystal knot
Structure, radial structure or broom shape structure.Different microstructural nephrites have the performance of daily necessities composition certain shadow
It rings.It is highly preferred that the microstructure of the nephrite is radial structure.When nephrite is radial structure, structure is easier to
It is coated by nanogold and nano silver, so as to which beneficial effects of the present invention be better achieved.
In the present invention, the term " gold " is the molecule of 30~80nm of grain size, is nanogold, has high electricity
Sub- density, dielectric property and catalytic action can be combined with a variety of large biological molecules, and not influence its bioactivity.Preferably, institute
The grain size for stating gold is 30~50nm.
In the present invention, the term " silver " is the molecule of 25~50nm of grain size, is nano silver, to large intestine bar
The tens of kinds of pathogenic microorganisms such as bacterium, gonococcus, chlamydia trachomatis have strong inhibition and killing effect, and will not generate resistance to
Pharmacological property.Preferably, the grain size of the silver is 25~35nm.
In the present invention, the term " Moringa extract " is the extract for extracting from Moringa oleifera.Moringa is India's sheet
The little tree on ground, but cultivate all over the world and transplanted in many environment popularized very much.
In the present invention, the Moringa extract is prepared by following methods, the described method includes：By two at 80 DEG C
Secondary adverse current extraction, in 17.5L ethyl alcohol 90, i.e. ratio=9/1 of ethanol/water, extraction 2.5kg dryings and the Moringa of grinding
It is one or more of in tree root, blade, whole seed；In environment after 50 DEG C of coolings, recycled by solid/liquid separation extracted
Solution；Drying sample, so as to obtain 243g extracts, the wherein extract is characterized in that the oil and 0.02% of 36% content
The total polyphenols of content represent that the oil includes the triglycerides and fat of (i) 10% with the g of the pyrogallol of 100g dry extracts
The polar lipid of acid and (ii) 10%, wherein the whole seed is the seed that crust is not removed.
In the present invention, the term " natural antiseptic agent " is nonirritant, avirulent non-chemical synthetic preservative,
It is 5-40% containing Baical Skullcap root P.E, Flos Hibisci Mutabilis extract 5-40%, the Chinese medical extract of Olive leaf P.E 20~60%.It is described
Natural antiseptic agent is prepared by following methods：After Chinese medicine is crushed, sieving, after impregnating 1-2h together with Extraction solvent,
It is extracted under room temperature with high pressure homogenization method machine, after extracting solution is centrifuged, with macroporous resin adsorption, with 10-95%'s
Ethyl alcohol repeatedly elutes, collect eluent, be concentrated under reduced pressure into medicinal extract shape to get；The Extraction solvent is water, ethyl alcohol or ethyl alcohol are water-soluble
Liquid.The natural antiseptic agent of the present invention can inhibit gram-positive bacteria, and Gram-negative bacteria, saccharomycete and mould have wider
Antimicrobial spectrum.The natural antiseptic agent is free of the substance of chemical synthesis, has no toxic side effect, and skin irritation is small, and property is stablized, and safely may be used
It leans on.In addition, Baical Skullcap root P.E in addition to antibacterial effect, also has effects that anti-inflammatory, Green Tea Extract；Flos Hibisci Mutabilis extract except
Outside with antibacterial effect, also with white-skinned face function；Olive leaf P.E in addition to antibacterial effect, also have it is very strong it is anti-from
By base effect.So natural antiseptic agent composition of the invention is in addition to antimicrobial preservative efficacy, at the same have Green Tea Extract and
Whitening and skin-protecting effect, this is that chemical synthesis preservative institute is incomparable.
Daily necessities composition of the present invention further includes component conventional in daily necessities or cosmetic field.It such as can be
Arbitrary coloring pigment, extender pigment, water composition, the oil components used in fields.Cosmetics neck can also be added
The other components in domain, such as small molecule sodium hyaluronate, Co-Q10, Panthenol, allantoin, silk decoding peptide, blue copper life peptide, salmon
Nasal cartilages extract (non-synthetic EGF) etc..
It is not particularly limited as above-mentioned coloring pigment, it can be cited for example that：Inorganic white pigment (such as titanium dioxide
Deng)；Inorganic red series pigments (such as iron oxide (iron oxide red), iron titanate etc.)；Inorganic brown series pigments (such as gamma oxidation
Iron etc.)；Inorganic yellow series pigments (such as iron oxide yellow, loess etc.)；Inorganic black series pigments (such as Black Rouge, suboxides
Titanium etc.)；Inorganic purple series pigments (such as manganese violet, cobalt violet etc.)；Inorganic green series pigments (such as chromium oxide, chromium hydroxide, metatitanic acid
Cobalt etc.)；Inorganic blueness series pigments (such as ultramarine, Prussian blue etc.)；Pearl pigment (such as coated by titanium dioxide mica, dioxy
Change titanium cladding bismuth oxychloride, coated by titanium dioxide talcum, coloring coated by titanium dioxide mica, bismuth oxychloride, guanin etc.)；Gold
Belong to powder pigments (such as aluminium powder, copper powders etc.)；The organic pigments such as zirconium, barium or aluminum lake (such as No. 201 red, red 202
Number, it is No. 204 red, No. 205 red, No. 220 red, No. 226 red, No. 228 red, No. 405 red, No. 203 orange, orange
No. 204, yellow 205, yellow 401 and the blue organic pigments such as No. 404；No. 3 red, No. 104 red, No. 106 red,
Red No. 227, No. 230 red, No. 401 red, No. 505 red, No. 205 orange, yellow 4, Sunset Yellow FCF, yellow 202,
Yellow 203, green 3 and blueness No. 1 etc.)；Natural pigment (such as chlorophyll, beta carotene etc.) etc..
It is not particularly limited as above-mentioned extender pigment, it can be cited for example that mica, synthetic mica, sericite, talcum, height
Ridge soil, calcium carbonate, magnesium carbonate, barium sulfate, aluminium oxide etc..
Be not particularly limited as above-mentioned water composition and oil components, for example, can contain oil component, surfactant,
Moisturizer, higher alcohol, metal ion block agent, natural and synthesis macromolecule, water solubility and oil-soluble macromolecule, ultraviolet radiation absorption
Agent, various extracting solutions, inorganic and organic pigment, inorganic and organic clay, through metallic soap handle or silicone-treated it is inorganic
With the colorants such as organic pigment, organic dyestuff, preservative, antioxidant, pigment, thickener, pH adjusting agent, fragrance, cooling agent,
The ingredients such as antiperspirant, fungicide, activating skin agent.Specifically, 1 in following cited gradation compositions can arbitrarily be coordinated
Kind or two or more, by conventional method come manufacture the present invention daily necessities composition.Do not have for the use level of these gradation compositions
It is particularly limited to, as long as not damage the scope of effect of the present invention.
It is not particularly limited as above-mentioned oil components, it can be cited for example that：Avocado oil, camellia oil, turtle oil, Australia are hard
Fruit oil, corn oil, ermine oil, olive oil, rapeseed oil, egg yolk oil, sesame oil, persic oil, wheat-germ oil, camellia caul-fat, castor-oil plant
Oil, Linseed oil, safflower oil, cottonseed oil, perilla oil, soybean oil, peanut oil, tea-seed oil, Chinese torreyanut oil, rice bran oil, Paulownia
Oil, Japanese tung oil, SIMMONDSIA CHINENSIS SEED OIL (jojoba oil), embryo oil, triglycerin, tricaprylin, three different tripalmitins,
Cocoa butter, coconut oil, house oil, hydrogenated coconut oil, palm oil, tallow, suet, hydrogenated tallow, palm kernel oil, lard, neatsfoot stock,
Rhus succedanea kernel oil, hydrogenated oil and fat, hoof oil, haze tallow, rilanit special, beeswax, candelila wax, cotton wax, Brazil wax, red bayberry
Wax, insect wax, spermaceti, lignite wax, chaff wax, lanolin, kapok wax, acetic acid lanolin, liquid lanolin, sugarcane wax, lanoceric acid
Isopropyl ester, lauric acid hexyl ester, reduction lanolin, jojoba waxes, hard lanolin, shellac wax, POE lanolin alcohol ether, POE wools
Lipidol acetic acid esters, POE cholesterol ethers, lanoceric acid polyethylene glycol, POE hydrogenated lanolins alcohol ether, atoleine, ceresine, Cetorhinus maximus
Alkane, alkane, pure white ceresine, squalene, vaseline, microwax etc..
It is not particularly limited as lipophile nonionic surfactant, it can be cited for example that：Sorbitan list oleic acid
Ester, sorbitan list isostearate, Span-20, sorbitan monopalmitate, D-sorbite
Acid anhydride monostearate, Span-83, sorbitan trioleate, five -2 ethyl hexanoic acid diglycerol sorb
The sorbitan aliphatic esters classes such as sugar alcohol acid anhydride, four -2 ethyl hexanoic acid diglycerol sorbitan；Single oleic acid glyceride, list
Erucic acid glyceride, sesquialter olein, glycerin monostearate, α, α '-oleic acid pyroglutamic acid glyceride (α, α '-
Glyceryl oleate pyroglutamate), the glycerine polyglycerol fatty acid class such as glycerol monostearate malic acid；It is single stearic
The methyl glycol fatty acid esters class such as acid propylene glycol ester；Rilanit special derivative, alkyl glycerylether etc..
It is not particularly limited as hydrophilic non-ionic surfactant, it can be cited for example that：POE sorbitans list oil
Acid esters, POE- sorbitan monostearates, POE- sorbitan monooleates, four oleate of POE- sorbitans etc.
POE sorbitan aliphatic ester classes；POE- D-sorbites monolaurate, POE- sorbitol monooleates, POE- sorboses
The POE sorbitan fatty acid esters such as five oleate of alcohol, POE- sorbitan monostearates；POE- glyceryl monostearates,
The POE glycerine fatty acid esters such as POE- glycerol monoisostearates, POE- glyceryl triisostearates；Polysorbate 80, POE
The POE fatty acid esters such as the mono- dioleate of distearate, POE, diglycol stearate；POE lauryl ethers, POE oil alkene
The POE alkyl ethers such as base ether, POE stearyl ethers, POE docosyls ether, POE2- octyldodecyls ether, POE cholestane alcohol ethers
Class；The POE alkyl phenyl ethers such as POE octyl phenyl ethers, POE nonylplenyl ethers, POE dinonyl phenyl ethers；Polypropylene glycol and ring
The general stream Buddhist nun gram type class such as the addition polymers of oxidative ethane；POEPOP cetyl ethers, POEPOP2- decyls myristyl ether,
The POEPOP alkyl ethers such as POEPOP monobutyl ethers, POEPOP hydrogenated lanolins, POEPOP glycerin ethers；POE castor oil,
POE rilanit specials, POE rilanit special lists isostearate, three isostearate of POE rilanit specials, POE hydrogenated castors
The POE castor oil rilanit special derivatives such as oily list pyroglutamic acid list isostearic acid diester, POE rilanit special maleates；
The POE beeswax lanolin derivatives such as POE D-sorbite beeswaxs；Cocoanut fatty acid diethanolamide, lauric acid monoethanol acyl
The alkanolamides such as amine, aliphatic acid isopropanol amide；POE methyl glycol fatty acid esters, POE alkylamines, POE fatty acid amides, Sucrose Fatty Acid Ester
Fat acid esters, POE nonyl phenyl formaldehyde condensation products, alkyl ethoxy dimethyl amine, three oleyl alcohol phosphates etc..
As other surfactants, range fit example that can be to have no problem in terms of stability and skin irritation
Such as fatty acid soaps, high alkyl sulfate salt, POE triethanolamine lauryl sulfates, alkyl ether sulphate salts anionic surface
Activating agent；Alkyl trimethyl ammonium salt, Fixanol, alkyl quaternary ammonium salts, alkyl dimethyl benzyl ammonium salt, POE alkylamines, alkane
The cationic surfactants such as base amine salt, polyamine derivative of fatty acid；And imidazoline system amphoteric surfactant, glycine betaine
It is the amphoteric surfactantes such as surfactant.
As other surfactants, range fit example that can be to have no problem in terms of stability and skin irritation
Such as fatty acid soaps, high alkyl sulfate salt, POE triethanolamine lauryl sulfates, alkyl ether sulphate salts anionic surface
Activating agent；Alkyl trimethyl ammonium salt, Fixanol, alkyl quaternary ammonium salts, alkyl dimethyl benzyl ammonium salt, POE alkylamines, alkane
The cationic surfactants such as base amine salt, polyamine derivative of fatty acid；And imidazoline system amphoteric surfactant, glycine betaine
It is the amphoteric surfactantes such as surfactant.
It is not particularly limited as above-mentioned moisturizer, it can be cited for example that xylitol, D-sorbite, maltitol, sulfuric acid
Chondroitin, hyaluronic acid, mucoitin sulfate, trichosanic acid, Atelocollagen, cholesteryl -12- hydroxy stearic acid esters, sodium lactate,
Bile salt, short chain soluble collagen, diglycerol (EO) PO addition products, filature flower extract, Yarrow extract, grass
Sweet-scented osmanthus extract etc..
It is not particularly limited as above-mentioned higher alcohol, it can be cited for example that：Laruyl alcohol, cetyl alcohol, stearyl alcohol, behenyl
The straight chain alcohols such as alcohol, myristyl alcohol, oily enol, cetostearyl alcohol；Single stearyl glycerin ether (batyl alcohol), 2- decyl tetradecyl alcohols, sheep
The branched-chain alcohos such as hair lipidol, cholesterol, phytosterol, hexyl dodecanol, isooctadecanol, octyldodecanol；Etc..
It is not particularly limited as metal ion block agent, it can be cited for example that 1- hydroxyl ethanes -1,1- diphosphonic acid, 1- hydroxyls
It is base ethane -1,1- diphosphonic acid acid tetrasodium salt, sodium citrate, sodium polyphosphate, sodium metaphosphate, gluconic acid, phosphoric acid, citric acid, anti-
Bad hematic acid, succinic acid, EDTA acid etc..
It is not particularly limited as above-mentioned water-soluble macromolecule, it can be cited for example that：Arabic gum, bassora gum, half
Newborn glycan, guar gum, carob, karaya gum, carragheen, pectin, Qiong Zhi, Wen Quinces seed (marmelo , Wen Quinces), brown alga
Department of botanys' macromolecules such as glue (brown alga extract), starch (rice, corn, potato, wheat), glycyrrhizic acid；Xanthans, Portugal gather
The department of microbiology macromolecule such as sugar, succinic acid glucan, amylopectin；The animals such as collagen, casein, albumin, gelatin system
Macromolecule.
It is not particularly limited as semi-synthetic water soluble polymer, it can be cited for example that：Carboxymethyl starch, methylhydroxy third
The starch-series macromolecule such as base starch；Methylcellulose, nitrocellulose, ethyl cellulose, methylhydroxypropylcellulose, hydroxyl
Ethyl cellulose, cellulose sodium sulfate, hydroxy propyl cellulose, sodium carboxymethylcellulose (CMC), avicel cellulose, cellulose
The cellulose polymers such as powder；The alginic acid such as mosanom, propylene glycol alginate system macromolecule；Etc..
It is not particularly limited as synthesizing water-solubility macromolecule, it can be cited for example that：Polyvinyl alcohol, polyvinylmethyl ethers,
The vinyl polymers such as polyvinylpyrrolidone；The polyoxyethylene system such as polyethylene glycol 20,000,40,000,60,000 high score
Son；Poloxalkol copolymerization is macromolecule；Sodium Polyacrylate, polyethyl acrylate, polyacrylamide etc. third
Olefin(e) acid system macromolecule；Polyethylene imine, cationic polymer etc..
Be not particularly limited as Inorganic water-soluble macromolecule, it can be cited for example that bentonite, aluminum magnesium silicate (VEEGUM),
Synthetic soapstone, hectorite, silicic acid anhydride etc..
The second aspect of the present invention provides the preparation method of the above-mentioned daily necessities composition containing nephrite, including following step
Suddenly：
By nephrite, gold and silver mixing, it is ground together；Moringa extract and daily necessities or cosmetics are added after grinding
Conventional component in field, 60~70 DEG C are stirred mixing, then make to reach uniform using mixer for well-distribution, de-bubbled,
After filtering, natural antiseptic agent is added, is cooled down using heat exchanger etc. and reaches product.
The preparation method of the daily necessities composition of the present invention is by first will again be put into after nephrite, gold and silver-colored mixed grinding
Nanogold and nano silver due to the good ductility of Jin Heyin, by grinding, can be coated on nephrite by unclassified stores,
So as to which the good technique effect of sense of touch of the present invention be better achieved.
The third aspect of the present invention provides the application of the above-mentioned daily necessities composition containing nephrite, and the application includes changing
Late frost, the face frost that compacts, visage block cream, ultra light sun block lotion, conditioning vanishing cream, reparation eye cream, facial mask, face are such as nourished in cosmetic field
Film cream, hand film, foot film, hand lotion, spats frost, moisturizing liquid, lipstick, the application further includes daily necessities field, such as perfumed soap, tooth
Cream, mouthwash, shampoo, shower cream etc..
The grain size of nephrite particle in the daily necessities composition of the present invention belongs to nanoscale in 5~20nm, and grain size is small, tool
There are preferable permeability and far infrared Microwave emission, it is easier to be absorbed by the skin of human body, skin surface is absorbed into subcutaneously
After tissue, the nano-scale particle of nephrite generates far infrared microwave with the interaction of anion and body temperature, faint so as to generate
Thermo-magnetic effect slightly heats up fever, the metabolism to promote blood circulation with cell, enhances cell viability and cell tissue absorbs
Power is beneficial to regeneration, effective delaying skin failure, and has certain bactericidal bacteriostasis, and passes through addition nanometer
Gold and nano silver, can play synergistic effect together with nephrite, so as to realize the good technique effect of sense of touch of the present invention, and
With whitening, nourishing, reparation, anti-inflammatory and other effects.
Hereinafter, the present invention is explained in more detail by embodiment, it should be appreciated that these embodiments are only
It is exemplary and not restrictive.It is if raw materials used to be all commercially available without other explanations.
The present invention is described in detail referring to several examples.
The formula of Examples 1 to 7 and comparative example 1~4 is as shown in table 1.Used in comparative example 1 nephrite, Jin Heyin (A,
B, C) grain size be respectively 3um, 10um and 20um, nephrite, gold and the silver in comparative example 2 are joined together with other components
It is prepared.Nephrite is contained only in comparative example 3, Jin Heyin is not contained, contains only nephrite and gold in comparative example 4, do not contain silver.
The average grain diameter of the raw material of following embodiment is measured using laser diffraction and scattering formula particle size distribution device.
Measurement device is using BeckmanCoulter LS13320 types, using its intermediate value (D50 values) as average grain diameter.
Wherein component raw material is as follows：
A1：Serpentine nephrite, grain size 5nm, hair felty texture
A2：Serpentine nephrite, grain size 10nm, radial structure
A3：Tremolite nephrite, grain size 20nm, micro- nematoblastic texture
A4：Serpentine nephrite, grain size 10nm, micro- fiber-cryptocrystalline blastic texture
A5：Serpentine nephrite, grain size 10nm, broom shape structure
A6：Serpentine nephrite, grain size 10nm, micro- blade blastic texture
A7：Serpentine nephrite, grain size 10nm, micro- blade-cryptocrystalline blastic texture
B1：Nanogold, grain size 30nm
B2：Nanogold, grain size 50nm
B3：Nanogold, grain size 80nm
C1：Nano silver, grain size 25nm
C2：Nano silver, grain size 35nm
C3：Nano silver, grain size 50nm
D：Moringa extract
E：Natural antiseptic agent, containing Baical Skullcap root P.E 30%, Flos Hibisci Mutabilis extract 20%, Olive leaf P.E 50% Chinese medicine
Extract.
The formula of the daily necessities composition of 1 Examples 1 to 7 of table and comparative example 1~4
The performance measurement result of the daily necessities composition of Examples 1 to 7 and comparative example 1~4 is shown in Table 2.
1st, the measure of average friction coefficient
The double faced adhesive tape of 25mm wide is pasted on glass slide, puts daily necessities composition, is opened using powder puff expansion,
Average friction coefficient during loading 25g loads is measured using KatoTech friction fremitus testers (KES-SE types).
2nd, the measure of total visible light transmittance
Daily necessities composition is added in bottle, is vibrated 90 minutes, obtained using paint mixing unit (PaintConditioner)
Dispersion liquid.Obtained dispersion liquid is applied to glass slide using scraping strip coating machine #6, uses spectrophotometer (Japan's light splitting system
V-570 types) measure wavelength 400nm and 550nm when total light transmittance.
3rd, the measure of near infrared ray reflective rate
Daily necessities composition is added in the aluminium lid of diameter 35mm, deep about 10mm, using forcing press under 15tf loads
Suppress within 20 seconds, obtain test film, using spectrophotometer (Japan is divided V-570 types processed) in wavelength 1000nm and 2000nm
Under for obtained test film carry out spectral reflectance measure.
The performance test results of the daily necessities composition of 2 Examples 1 to 7 of table and comparative example 1~4
It was found from data above, it is used cooperatively compared with nephrite and gold, silver one of both or nephrite, nanometer is only used only
When the nephrite of rank, gold, silver three are used cooperatively, there is lower coefficient of friction, excellent use feeling illustrates nephrite, Jin He
Silver-colored three has significant synergistic effect.In addition, when nephrite microstructure for it is radial when, compared with other microstructures,
With more excellent performance.When nephrite is coated by gold, silver, when being mixed with compared with three and other compositions, it may have
More excellent performance.In addition, the daily necessities composition containing nephrite of the present invention also has effects that whitening, nourishing, reparation.
Foregoing example is merely illustrative, some features of feature for explaining the present invention.Appended claim
The scope as wide as possible that requirement is contemplated that is intended to, and embodiments as presented herein is only according to all possible embodiment
Combination selection embodiment explanation.Therefore, the purpose of applicant is that appended claim is not illustrated the present invention
Feature exemplary selectional restriction.And the progress in science and technology will not formed due to the inaccuracy of language performance and not
The possible equivalent or son being presently considered are replaced, and these variations also should in the conceived case be interpreted by appended
Claim covers.
Claims (4)
1. a kind of daily necessities composition containing nephrite, which is characterized in that the daily necessities composition is by including following weight hundred
Divide the raw material composition of ratio：
Nephrite 10-40%
Golden 0.005-0.01%
Silver-colored 0.001-0.01%
Moringa extract 0.1-5%
Natural antiseptic agent 0.25-0.3%；
The microstructure of the nephrite is radial structure；The natural antiseptic agent is 5-40% containing Baical Skullcap root P.E, Flos Hibisci Mutabilis
The Chinese medical extract of extract 5-40%, Olive leaf P.E 20-60%；The grain size of the nephrite is 5~10nm, the gold
Grain size is 30~50nm, and the grain size of the silver is 25~35nm.
2. the daily necessities composition according to claim 1 containing nephrite, which is characterized in that the Moringa extract is by leading to
It crosses and adds in tree root, seed or the blade of Moringa that is dry and grinding into the solvent of ethanol/water=9/1, countercurrently carried at 80 DEG C
It takes and obtains；The natural antiseptic agent is prepared by following methods：After Chinese medicine is crushed, sieving is soaked together with Extraction solvent
After steeping 1-2h, extracted at normal temperatures with high pressure homogenization method machine, after extracting solution is centrifuged, with macroporous resin adsorption,
Repeatedly eluted with the ethyl alcohol of 10-95%, collect eluent, be concentrated under reduced pressure into medicinal extract shape to get；The Extraction solvent is water, second
Alcohol or ethanol water.
3. contain the daily necessities composition of nephrite according to claim 1-2 any one of them, which is characterized in that the daily necessities
Composition further includes component conventional in cosmetic field.
4. application of the daily necessities composition in cosmetic field containing nephrite described in claim 3, which is characterized in that institute
Cosmetics are stated to nourish late frost, the face frost that compacts, visage block cream, ultra light sun block lotion, conditioning vanishing cream, reparation eye cream, facial mask, hand
Film, foot film, hand lotion, spats frost, moisturizing liquid or lipstick.
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| CN105832635A (en) * | 2016-04-29 | 2016-08-10 | 安徽恋尚你食品有限公司 | Moringa oleifera hand cream and preparing method thereof |
| CN105853250A (en) * | 2016-05-13 | 2016-08-17 | 诺斯贝尔化妆品股份有限公司 | Cosmetic composition containing gold collagen |
| CN107661228A (en) * | 2017-10-20 | 2018-02-06 | 广州市西瑶玉池科技有限公司 | A kind of multiple-effect toothpaste of the mineral element containing the tremolite |
| CN107875049A (en) * | 2017-10-20 | 2018-04-06 | 广州市西瑶玉池科技有限公司 | A kind of mothproof sound of baby talk cream of the mineral element containing the tremolite |
| CN107661233A (en) * | 2017-10-23 | 2018-02-06 | 广州市西瑶玉池科技有限公司 | A kind of anhydrous toothpaste of the mineral element containing the tremolite and preparation method thereof |
| CN107822920A (en) * | 2017-10-23 | 2018-03-23 | 广州市西瑶玉池科技有限公司 | A kind of inflammation-diminishing toothpaste of the mineral element containing the tremolite |
| CN107837217A (en) * | 2017-10-23 | 2018-03-27 | 广州市西瑶玉池科技有限公司 | A kind of anti-apolexis composition of mineral element containing the tremolite and its application |
| CN107951731A (en) * | 2018-01-16 | 2018-04-24 | 广州市美姿贺化妆品有限公司 | Application of the nanometer gold in late frost and the late frost that is made from it and preparation method thereof |
| CN112826837A (en) * | 2021-03-15 | 2021-05-25 | 福建广生健康科技有限公司 | Traditional Chinese medicine composition for treating hair/scalp diseases and application thereof |
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| CN103432047B (en) * | 2013-09-12 | 2015-07-22 | 广东轻工职业技术学院 | Natural preservative composition and application thereof in cosmetics |
| CN104140133A (en) * | 2014-07-27 | 2014-11-12 | 惠州市银嘉环保科技有限公司 | Antibacterial oil absorption compound kieselguhr and application thereof |
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