CN110507562B - Light sensation concealer CC cream and preparation method thereof - Google Patents

Light sensation concealer CC cream and preparation method thereof Download PDF

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Publication number
CN110507562B
CN110507562B CN201910800863.XA CN201910800863A CN110507562B CN 110507562 B CN110507562 B CN 110507562B CN 201910800863 A CN201910800863 A CN 201910800863A CN 110507562 B CN110507562 B CN 110507562B
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cream
stirring
concealer
polydimethylsiloxane
light sensation
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CN110507562A (en
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杨菊
曹波
苏秀妹
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Guangdong Bailichen Biotechnology Co ltd
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Guangdong Bailichen Biotechnology Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/29Titanium; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/12Face or body powders for grooming, adorning or absorbing
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/04Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/004Aftersun preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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Abstract

The invention provides light sensation concealer CC cream and a preparation method thereof, belonging to the technical field of cosmetics, and the light sensation concealer CC cream comprises the following components in percentage by weight: 1-20% of inorganic powder, 5-10% of emulsifier, 0.5-3.0% of thickener, 1-3% of stabilizer, 8-17% of humectant, 15-45% of grease, 0.4-0.8% of preservative, 1-10% of skin conditioner and 25-40% of water.

Description

Light sensation concealer CC cream and preparation method thereof
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to light sensation concealer CC cream and a preparation method thereof.
Background
With the improvement of the living standard of consumers and the increasing severity of environmental pollution, more and more people begin to pay attention to the skin care of the consumers. Meanwhile, with the continuous development of cosmetics and the increasing demand of women for beauty, various multifunctional cosmetics come into force, but various problems also exist.
Chinese patent CN105902446B discloses an anti-allergy skin cream and a preparation method thereof, wherein the product is prepared from the following components in percentage by weight, based on 100% of the total weight: 3.5-6.5% of emulsifier, 0.5-2% of co-emulsifier, 5-12% of grease, 2-5% of functional grease, 0.5-2% of antioxidant, 0.05-0.1% of metal ion chelating agent, 6-12% of polyalcohol, 2-8% of humectant, 0.2-0.7% of water phase thickener, 0.1-0.6% of thickening stabilizer, 6-20% of skin conditioner, 0.5-1.5% of plant preservative and the balance of water. However, the skin care cream is relatively weak in ultraviolet resistance, has no advantage in natural color matching, and can cause unnatural makeup under sunlight irradiation.
Chinese patent CN107468572A discloses a color-moistening barrier emulsion and a preparation method thereof, wherein the color-moistening barrier emulsion comprises the following components: 6-7 wt% of titanium dioxide; mica, 2-2.5 wt%; 1-1.5 wt% of yellow iron oxide; red iron oxide, 0.1-0.2 wt%; black iron oxide, 0.05-0.08 wt%; 0.5-1 wt% of zinc oxide; humectant 8.8-14.4 wt%; glycoprotein, 0.5-1.5 wt%; 0.3-1 wt% of tea extract; 0.15-0.25 wt% of maltodextrin; 8-12 wt% of cyclopentadimethylsiloxane; 2.7-5.2 wt% of softening agent; 2.1-3.2 wt% of emulsifier; 1-2 wt% of a polydimethylsiloxane/vinyl polydimethylsiloxane crosspolymer; 1-2 wt% of Opuntia ficus-indica extract; 0.32-0.5 wt% of a skin conditioner; PPG-5-cetyl polyether-10 phosphate, 0.05-0.15 wt%; 0.0148-0.0195 wt% of preservative; 0.005-0.01 wt% of aromatic; the balance of water. The color-moistening barrier emulsion can effectively isolate dirty air, cover blemishes and prevent sunburn, and has the characteristics of refreshing, no greasiness, smooth pores, no burden, difficult makeup removal, skin modification and protection and the like. However, the main effect of the isolation emulsion is sun-screening, and the isolation emulsion has no advantages in aspects of adjusting skin color and keeping natural makeup effect, and is not suitable for people with sensitive skin.
Besides the skin care cream and the isolation cream, products such as the concealer CC cream are popular with women because the CC cream has multiple effects of foundation make-up, sun protection, isolation and skin care, is convenient to use and can help women loving beauty to quickly create perfect images. However, in daily makeup, the ordinary concealer CC cream appears to be not natural in makeup, not ruddy in complexion and heavy in color, and also appears to be not enough in dryness and moistening of the skin and easy to generate floating powder under outdoor sunlight irradiation.
Aiming at the problems of unnatural makeup and poor ultraviolet resistance of cosmetics such as skin care cream and isolation cream, and the problems of heavy weight, no moisture, easy floating powder and the like of CC cream, a defect covering CC cream is sought, so that the defect covering CC cream can naturally moisten skin color, can effectively cover and repair the defect and realize natural color matching.
Disclosure of Invention
The invention provides a light sensation concealer CC cream and a preparation method thereof, aiming at the problems in the prior art, the concealer CC cream can naturally moisten skin color after being used, and can effectively conceal and repair the skin color and realize natural color matching.
In order to achieve the purpose, the technical scheme adopted by the invention is as follows:
a light sensation concealer CC cream comprises the following components in percentage by weight: 1-20% of inorganic powder, 5-10% of emulsifier, 0.5-3.0% of thickener, 1-3% of stabilizer, 8-17% of humectant, 15-45% of grease, 0.4-0.8% of preservative, 1-10% of skin conditioner and 25-40% of water; the skin conditioner comprises one or more of rose oil, aloe vera extract and cactus extract.
Preferably, the skin conditioner is rose oil, aloe vera extract and cactus extract in a weight ratio of 0.5-3:0.2-10: 1. Further preferably, the skin conditioner is rose oil, aloe vera extract and cactus extract in a weight ratio of 2:5: 1.
Preferably, the light sensation concealer CC cream comprises the following components in percentage by weight: 10-18% of inorganic powder, 5-8% of emulsifier, 1.0-2.5% of thickener, 1-2% of stabilizer, 9-17% of humectant, 18-30% of grease, 0.5-0.7% of preservative, 2.5-5% of skin conditioner and 30-38% of water.
Further preferably, the light sensation concealer CC cream comprises the following components in percentage by weight: 15% of inorganic powder, 6% of emulsifier, 2% of thickener, 1.8% of stabilizer, 15% of humectant, 20% of grease, 0.6% of preservative, 3.2% of skin conditioner and 36.4% of water.
Further, the inorganic powder comprises one or more of titanium dioxide, zinc oxide, talcum powder, iron oxide, boron nitride and bismuth oxychloride; preferably, the inorganic powder comprises 36-70% of titanium dioxide, 1.0-5.0% of iron oxide red, 3-10% of iron oxide yellow, 0.5-4.0% of iron oxide black, 12-35% of boron nitride and 3-11% of bismuth oxychloride. The titanium dioxide is a pigment treated by silicon, shows more excellent oil phase dispersibility and hydrophobic property, and can improve the stability, skin-sticking property and covering power of the product; the average particle size of the powder is 0.2-0.5 μm, and the particle size is close to the theoretical excellent particle size of titanium dioxide, so that the titanium dioxide powder has high tinting strength, high glossiness and high covering power; the bismuth oxychloride is treated by stearate, the surface of the bismuth oxychloride powder has water resistance and lipophilicity, and the bismuth oxychloride powder has good dispersion and stability, so that the agglomeration phenomenon among particles is not easy to occur, and the formability of the product can be improved.
Further, the emulsifier comprises one or more of polyglycerol-2 oleate, glycerol isostearate, cetyl PEG/PPG-10/1 polydimethylsiloxane, lauryl PEG/PPG-18/18 polydimethylsiloxane, isosteareth-20, sorbitan sesquioleate, PEG-10 polydimethylsiloxane and cetyl polyethylene glycol; preferably, the emulsifier comprises a mixture of sorbitan sesquioleate, cetyl PEG/PPG-10/1 dimethicone and lauryl PEG/PPG-18/18 dimethicone; further preferably, the emulsifier comprises sorbitan sesquioleate 40-75%, cetyl PEG/PPG-10/1 polydimethylsiloxane 6-30%, lauryl PEG/PPG-18/18 polydimethylsiloxane 6-40%.
Further, the thickener comprises one or more of acrylic acid (ester)/ethylhexyl acrylate/polydimethylsiloxane methacrylate copolymer, acrylic acid (ester)/stearyl alcohol acrylate/polydimethylsiloxane methacrylate copolymer, disteardimonium hectorite, polyquaternium, stearyl polydimethylsiloxane and magnesium aluminum silicate; preferably, the thickener comprises a mixture of (ester) acrylates/ethylhexyl acrylate/dimethicone methacrylate copolymer, disteardimonium hectorite, stearyl dimethicone; further preferably, the thickener comprises 0.5-15% of acrylic acid (ester)/ethylhexyl acrylate/polydimethylsiloxane methacrylate copolymer, 24-67% of disteardimonium hectorite and 20-75% of stearyl polydimethylsiloxane.
Further, the stabilizer comprises one or more of sodium chloride, magnesium sulfate, sodium sulfate and magnesium stearate; preferably, the stabilizer comprises a mixture of sodium chloride and magnesium sulfate; preferably, the stabilizer comprises 30-67% of sodium chloride and 30-67% of magnesium sulfate; still more preferably, the stabilizer is sodium chloride and magnesium sulfate in a weight ratio of 1: 1.
Further, the humectant comprises one or more of glycerin, propylene glycol and butylene glycol.
Further, the grease comprises one or more of white oil, trimethylolpropane triisostearate, polydimethylsiloxane, ethylhexyl palmitate, isopropyl palmitate, jojoba oil and isomeric hexadecane; preferably, the oil comprises a mixture of white oil, hydrogenated sweet almond oil, trimethylolpropane triisostearate, polydimethylsiloxane and ethylhexyl palmitate; more preferably, the grease comprises 50-55% of white oil, 20-32% of trimethylolpropane triisostearyl fatty acid ester, 10-24% of polydimethylsiloxane and 3-16% of ethylhexyl palmitate. Wherein the white oil is 26# white oil.
Further, the preservative comprises one or two of methylparaben and phenoxyethanol.
The invention also provides a preparation method of the light sensation concealer CC cream, which comprises the following steps:
(1) mixing and grinding inorganic powder and 67% of grease by weight to obtain a material A1;
(2) mixing the thickener accounting for 43 percent of the total weight with the residual grease, fully stirring, and heating to be transparent to obtain a material A2;
(3) stirring the rest of the thickening agent and the emulsifier, heating to dissolve, adding the material A1 and the material A2, and homogenizing to obtain a material A;
(4) heating and stirring water, humectant, stabilizer and preservative, then preserving heat, sterilizing, cooling, adding skin conditioner, stirring and mixing to obtain a material B;
(5) adjusting the stirring speed of the material A, vacuumizing, slowly adding the material B, reducing the stirring speed, homogenizing, and maintaining vacuum stirring for defoaming to obtain the light sensation concealer CC cream.
Further, grinding in the step (1) is carried out for 2-3 times by adopting a three-roller machine; the thickener accounting for 43 percent of the total weight accounts for 43 percent of the total weight of the thickener, and the grease is similar to the thickener.
Further, the heating in the step (2) is carried out at a temperature of 75-80 ℃.
Further, in the step (3), the heating is carried out at the temperature of 75-80 ℃, the stirring and the homogenization are carried out in an emulsifying pot, and the homogenization time is 4-6 min.
Further, in the step (4), the heating is carried out at the temperature of 80-85 ℃, the heat preservation and the sterilization are carried out for 25-30min, and the temperature is reduced to 40 ℃.
Further, in the step (5), the stirring speed of the material A is adjusted to be 350-; stirring and defoaming for 15-25 min.
The technical effects obtained by the invention are as follows:
1. the nanometer titanium dioxide is photochromic powder, can resist the damage of ultraviolet rays in the UVB wave band to the skin, not only can absorb the ultraviolet rays, but also can reflect and scatter the ultraviolet rays; adding stearate-treated bismuth oxychloride, which can form a light-sensitive film on the skin; therefore, the skin color tone can be darkened under the irradiation of ultraviolet rays, and the skin color can jump back to the original color tone when the skin is not irradiated, so that the skin can be naturally and freely made up at any time and any place.
2. The cactus extract which is rich in active ingredients such as amino acid, superoxide dismutase (SOD), polysaccharide and the like and has the functions of nourishing and moisturizing the skin is added; the aloe extract is also added, and the aloe contains various amino acids, vitamins, polysaccharides, anthraquinone compounds, minerals, various enzymes and other effective components, and the components have the effects of moisturizing the skin and preventing ultraviolet rays from burning and dermatitis of the skin; and rose oil is added to lighten spots, effectively brighten skin color and keep skin moist and not dry. Therefore, the cactus extract, the aloe extract and the rose oil have the effects of cooperatively moisturizing, moistening and sticking skin, brightening skin, having good make-up property and the like; the light sensation concealer CC cream prepared by the invention has the advantages of natural luster, skin friendliness, difficult removal of makeup and good effect of lasting makeup.
Detailed Description
It should be noted that, in the present invention, each raw material is a general commercially available product, and therefore, the source thereof is not particularly limited. Wherein, the titanium dioxide is purchased from Shanghai sheath chemical Co., Ltd, and has a Kingsun 0205# trade name; bismuth oxychloride was purchased from baihabo ltd, guang, under the trade name timiron liquid Silver and contained bismuth oxychloride and ethylhexyl hydroxystearate in a ratio of 7: 3. The aloe extract is obtained from Aloe Fine chemical Co., Ltd, Guangzhou city, and contains aloe extract, coconut oil and white oil at a ratio of 2:1: 1; the Cactus Extract is obtained from vast Sen Biotech, Guangzhou under the trade name of Cactus Extract, and comprises water, Cactus Extract and glycerol at a ratio of 5:3: 2.
The specific components and their specific formulations for examples 1-5 are shown in Table 1:
TABLE 1
Figure BDA0002182269780000051
Figure BDA0002182269780000061
Example 1
A preparation method of light sensation concealer CC cream comprises the following steps:
(1) mixing inorganic powder and 67 percent of grease by total weight by using a three-roller machine, and grinding for 2 times to obtain a material A1;
(2) mixing the thickener accounting for 43 percent of the total weight with the residual grease, fully stirring, and heating to be transparent to obtain a material A2, wherein the heating temperature is 75 ℃;
(3) stirring the rest of the thickening agent and the emulsifier, heating for dissolving, adding the material A1 and the material A2, and homogenizing to obtain a material A, wherein the heating temperature is 75 ℃; stirring and homogenizing in an emulsifying pot for 6 min;
(4) heating water, humectant, stabilizer and antiseptic to 80 deg.C, stirring, sterilizing at constant temperature for 30min, cooling to 40 deg.C, adding skin conditioner, stirring, and mixing to obtain material B;
(5) adjusting the stirring speed of the material A to 350r/min, vacuumizing, slowly adding the material B, reducing the stirring speed to 150r/min, homogenizing for 12min at 1500r/min, and keeping the vacuum stirring for defoaming for 15min to obtain the light sensation concealer CC cream.
Example 2
A preparation method of light sensation concealer CC cream comprises the following steps:
(1) mixing inorganic powder and 67% of grease by total weight by using a three-roller machine, and grinding for 3 times to obtain a material A1;
(2) mixing the thickener accounting for 43 percent of the total weight with the residual grease, fully stirring, and heating to be transparent to obtain a material A2, wherein the heating temperature is 80 ℃;
(3) stirring the rest of the thickening agent and the emulsifier, heating for dissolving, adding the material A1 and the material A2, and homogenizing to obtain a material A, wherein the heating temperature is 80 ℃; stirring and homogenizing in an emulsifying pot for 4 min;
(4) heating water, humectant, stabilizer and antiseptic to 85 deg.C, stirring, sterilizing for 25min, cooling to 40 deg.C, adding skin conditioner, stirring, and mixing to obtain material B;
(5) adjusting the stirring speed of the material A to 450r/min, vacuumizing, slowly adding the material B, reducing the stirring speed to 250r/min, homogenizing for 8min at 1400r/min, and keeping the vacuum stirring for defoaming for 25min to obtain the light sensation concealing CC cream.
Example 3
A preparation method of light sensation concealer CC cream comprises the following steps:
(1) mixing inorganic powder and 67% of grease by total weight by using a three-roller machine, and grinding for 2 times to obtain a material A1;
(2) mixing the thickener accounting for 43 percent of the total weight with the residual grease, fully stirring, and heating to be transparent to obtain a material A2, wherein the heating temperature is 78 ℃;
(3) stirring the rest of the thickening agent and the emulsifier, heating for dissolving, adding the material A1 and the material A2, and homogenizing to obtain a material A, wherein the heating temperature is 78 ℃; stirring and homogenizing in an emulsifying pot for 5 min;
(4) heating and stirring water, humectant, stabilizer and antiseptic, sterilizing at a constant temperature for 28min, cooling to 40 deg.C, adding skin conditioner, stirring, and mixing to obtain material B;
(5) adjusting the stirring speed of the material A to 400r/min, vacuumizing, slowly adding the material B, reducing the stirring speed to 200r/min, homogenizing for 10min at 1450r/min, and keeping the vacuum stirring for defoaming for 20min to obtain the light sensation concealer CC cream.
Example 4
A preparation method of light sensation concealer CC cream comprises the following steps:
(1) mixing inorganic powder and 67 percent of grease by total weight by using a three-roller machine, and grinding for 2 times to obtain a material A1;
(2) mixing the thickener accounting for 43 percent of the total weight with the residual grease, fully stirring, and heating to be transparent to obtain a material A2, wherein the heating temperature is 75 ℃;
(3) stirring the rest of the thickening agent and the emulsifier, heating for dissolving, adding the material A1 and the material A2, and homogenizing to obtain a material A, wherein the heating temperature is 75 ℃; stirring and homogenizing in an emulsifying pot for 4 min;
(4) heating and stirring water, humectant, stabilizer and preservative, keeping the temperature and sterilizing for 25min, cooling to 40 ℃, adding skin conditioner, stirring and mixing to obtain a material B;
(5) adjusting the stirring speed of the material A to 350r/min, vacuumizing, slowly adding the material B, reducing the stirring speed to 150r/min, homogenizing for 12min at 1500r/min, and keeping the vacuum stirring for defoaming for 15min to obtain the light sensation concealer CC cream.
Example 5
(1) Mixing inorganic powder and 67% of grease by total weight by using a three-roller machine, and grinding for 3 times to obtain a material A1;
(2) mixing the thickener accounting for 43 percent of the total weight with the residual grease, fully stirring, and heating to be transparent to obtain a material A2, wherein the heating temperature is 80 ℃;
(3) stirring the rest of the thickening agent and the emulsifier, heating for dissolving, adding the material A1 and the material A2, and homogenizing to obtain a material A, wherein the heating temperature is 80 ℃; stirring and homogenizing in an emulsifying pot for 4 min;
(4) heating water, humectant, stabilizer and antiseptic to 85 deg.C, stirring, sterilizing for 25min, cooling to 40 deg.C, adding skin conditioner, stirring, and mixing to obtain material B;
(5) adjusting the stirring speed of the material A to 450r/min, vacuumizing, slowly adding the material B, reducing the stirring speed to 250r/min, homogenizing for 8min at 1400r/min, and keeping the vacuum stirring for defoaming for 25min to obtain the light sensation concealer CC cream.
Comparative example 1
A preparation method of light sensation concealer CC cream comprises the following steps:
the difference from example 3 is only that the polish rod concealer CC cream comprises the following components in percentage by weight: 0.8% of inorganic powder, 11% of emulsifier, 0.3% of thickener, 3.2% of stabilizer, 7% of humectant, 48% of grease, 0.3% of preservative, 12% of skin conditioner and 17.4% of water. The ingredients of the inorganic powder, the emulsifier, the thickener, the stabilizer, the humectant, the grease, the preservative and the skin conditioner are the same as those in example 3, and the weight percentage of the ingredients is also the same as that in example 3.
Comparative example 2
The difference from example 3 is only that the polish rod concealer CC cream comprises the following components in percentage by weight: 25% of inorganic powder, 3% of emulsifier, 4% of thickener, 0.8% of stabilizer, 17.4% of humectant, 12.3% of grease, 1% of preservative, 13% of skin conditioner and 23.5% of water. The ingredients of the inorganic powder, the emulsifier, the thickener, the stabilizer, the humectant, the grease, the preservative and the skin conditioner are the same as those in example 3, and the weight percentage of the ingredients is also the same as that in example 3.
Comparative example 3
The only difference from example 3 is that the skin conditioning agent is centella asiatica extract, in an amount of 3.2 g.
Comparative example 4
The only difference from example 3 is that the weight ratio of rose oil, aloe vera extract and cactus extract was 0.3:11:0.8 (the total weight of rose oil, aloe vera extract and cactus extract was identical to example 3).
Comparative example 5
The only difference from example 3 is that the weight ratio of rose oil, aloe vera extract and cactus extract was 4:0.1:2 (the total weight of rose oil, aloe vera extract and cactus extract was identical to example 3).
Comparative example 6
The only difference from example 3 is that in the preparation process step (1) no fat was added, only the whole fat was added in step (2), and at the same time, no thickener was added in step (2) and only the whole thickener was added in step (3).
First, product safety assessment
The evaluation method comprises the following steps:
1) the test substance: products obtained in examples 1 to 5 and comparative examples 1 to 6
2) Negative control: blank control
3) Subject: 110 healthy volunteers of 20-40 years old are selected, half of the volunteers are male and female, and the volunteers do not use anti-inflammatory drugs or cosmetics in the last two months.
4) The test method comprises the following steps: 110 volunteers were selected and randomly divided into 11 groups of 10 persons each, and the product tests of examples 1 to 5 and comparative examples 1 to 6 were performed. The light sensation concealer CC creams of examples 1 to 5 and comparative examples 1 to 6 of the present invention were put into a spot tester (non-irritating tape was used for the spot tester) in an amount of 0.03 g. The non-irritating adhesive tape containing the light sensation concealing CC cream is applied to the inner side of the forearm of a subject, one side is a control area (not applied), the other side is a test area, and the control area and the test area are lightly pressed by hands to be uniformly applied to the skin for 24 hours. After the adhesive tape is removed, skin reactions are observed for 0.5h, 12h, 24h and 48h respectively, and the results are recorded according to the skin reaction grading standard in technical Specification for cosmetic safety (2015 edition).
And (3) test results: the results of the human skin patch test show that all the subjects pass the patch test and observe skin reactions at 0.5h, 12h, 24h and 48h, wherein no adverse reactions such as skin erythema, pimple, blister and the like appear in examples 1-5 and comparative examples 1-6, which indicates that the product of the invention is safe and non-irritant.
Second, sensory analysis and evaluation
The evaluation method comprises the following steps:
1) the test substance: the products obtained in examples 1 to 5 and comparative examples 1 to 6.
2) Subject: 110 healthy female volunteers of 20-40 years old were selected and divided into 11 groups at random.
3) The evaluation method comprises the following steps: the subjects applied the samples of examples 1-5 and comparative examples 1-6 to the face. The coating amount is 0.02mg/cm2After the use, the texture, the ductility, the durability, the light sensation, the make-up feeling and the concealer feeling of the product are evaluated. The results were scored (0-10 points, higher points represent texture, extensibility, durability, light feel, make-up feel, and better concealer feel) and then recorded as average points. The results are shown in Table 2 below.
TABLE 2
Figure BDA0002182269780000111
As can be seen from Table 1, examples 1-5 showed better overall results than the products of comparative examples 1-3. The products of examples 4-5 performed better than those of examples 1-2, and the product of example 3 performed the best. The raw material proportions of the comparative examples 1-2 are out of the range, the used light sensation effect, the naked makeup effect and the like are not as good as those of the examples, the product of the comparative example 3 uses the centella extract to replace the three conditioners, and the effect is not as good as that of the example 3; the products of comparative examples 4-5 used skin conditioner ingredients outside the scope of the present invention and were less effective than example 3. The texture of the product in comparative example 6 was inferior to that of example 3, indicating that the modification of the preparation method also affected the properties of the product.
Third, moisture retention test
Selecting 110 healthy female volunteers of 20-40 years old, randomly dividing into 11 groups of 10 persons, and standing for 10min at room temperature of 22-26 deg.C and humidity of 40-60% before testing. The products prepared in examples 1 to 5 and comparative examples 1 to 6 were then tried on the face (use amount 0.02 mg/cm)2Paint), for 0.5h, then the Corneometer moisture test probe of MPA10 multifunctional skin tester from CK, germany was used to test the skin moisture content values at 0.5h, 1h, 2h and 4h after use of the product, recorded as shown in table 3 below:
TABLE 3
Figure BDA0002182269780000112
Figure BDA0002182269780000121
As can be seen from Table 3, the products of examples 1-5 all retained moisture well, wherein the skin moisture content values at different time points for the product of example 3 were the highest among the examples, indicating that the product of example 3 retained moisture optimally, for example 4-5 times, and for example 1-2 again. The moisture content values of the products of comparative examples 1-6 were all lower than those of example 3, indicating that the proportions of the raw materials of the products, as well as the preparation method, more or less affected the properties of the products.
Finally, it should be noted that the above-mentioned contents are only used for illustrating the technical solutions of the present invention, and not for limiting the protection scope of the present invention, and that the simple modifications or equivalent substitutions of the technical solutions of the present invention by those of ordinary skill in the art can be made without departing from the spirit and scope of the technical solutions of the present invention.

Claims (3)

1. A light sensation concealer CC cream is characterized in that: comprises the following components in percentage by weight: 10-18% of inorganic powder, 5-8% of emulsifier, 1.0-2.5% of thickener, 1-2% of stabilizer, 9-17% of humectant, 18-30% of grease, 0.5-0.7% of preservative, 2.5-5% of skin conditioner and 30-38% of water; the skin conditioner is rose oil, aloe extract and cactus extract in a weight ratio of 2:5:1, 2.5:10:1 or 3:6: 1;
the inorganic powder comprises one or more of titanium dioxide, zinc oxide, talcum powder, iron oxide, boron nitride and bismuth oxychloride;
the emulsifier comprises one or more of polyglycerol-2 oleate, glycerol isostearate, cetyl PEG/PPG-10/1 polydimethylsiloxane, lauryl PEG/PPG-18/18 polydimethylsiloxane, isosteareth-20, sorbitan sesquioleate, PEG-10 polydimethylsiloxane and cetyl polyethylene glycol;
the thickening agent comprises one or more of acrylic acid (ester)/ethylhexyl acrylate/polydimethylsiloxane methacrylate copolymer, acrylic acid (ester)/stearyl alcohol acrylate/polydimethylsiloxane methacrylate copolymer, disteardimonium hectorite, polyquaternium, stearyl polydimethylsiloxane and aluminum magnesium silicate;
the stabilizing agent comprises one or more of sodium chloride, magnesium sulfate, sodium sulfate and magnesium stearate;
the humectant comprises one or more of glycerol, propylene glycol and butanediol;
the grease comprises one or more of white oil, trimethylolpropane triisostearate, polydimethylsiloxane, ethylhexyl palmitate, isopropyl palmitate, jojoba oil and isomeric hexadecane.
2. The light sensation concealer CC cream as claimed in claim 1, wherein: the preservative comprises methylparaben and phenoxyethanol, and the content of the methylparaben accounts for 0.3-0.4% of the total weight of the light sensation concealer CC cream.
3. The method for preparing light concealer CC cream as claimed in claim 1 or 2, wherein the method comprises the following steps: the method comprises the following steps:
(1) mixing and grinding inorganic powder and 67% of grease by total weight to obtain a material A1;
(2) mixing the thickener accounting for 43 percent of the total weight with the residual grease, fully stirring, and heating to be transparent to obtain a material A2;
(3) stirring the rest of the thickening agent and the emulsifier, heating to dissolve, adding the material A1 and the material A2, and homogenizing to obtain a material A;
(4) heating and stirring water, humectant, stabilizer and preservative, then preserving heat, sterilizing, cooling, adding skin conditioner, stirring and mixing to obtain a material B;
(5) adjusting the stirring speed of the material A, vacuumizing, slowly adding the material B, reducing the stirring speed, homogenizing, and maintaining vacuum stirring for defoaming to obtain the light sensation concealer CC cream.
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