KR101584511B1 - The method to manufacturing the cosmetic powder production improved in stability of dual-functional materials - Google Patents

Abstract

The present invention relates to a method for manufacturing powder cosmetics having improved stability of a dual functional material, and a method for manufacturing a powder cosmetic using dual functional materials such as ethylhexyl methoxycinnamate and niacinamide, The present invention relates to a method of manufacturing powder cosmetics in which the stability of a dual functional material is improved through a dispersion process.
The present invention relates to a method for preparing a water-soluble polymer, which comprises mixing (S1) an extender pigment, (S2) mixing a water-soluble melt to the mixture prepared in the step (S1) (S4) of adding a dye to the mixture prepared in the step (S3) and coloring the mixture, and a step (S5) of putting the mixture prepared in the step (S4) into a pulverizer and pulverizing Thereby providing a powder cosmetic preparation method with improved stability of the material. Further, it is preferable that the present invention uses niacinamide as a water soluble melt. In addition, the present invention preferably uses ethylhexyl methoxycinnamate as a fat-soluble melt.

Description

BACKGROUND OF THE INVENTION 1. Field of the Invention [0001] The present invention relates to a method for manufacturing powder cosmetics,

The present invention relates to a method for manufacturing powder cosmetics having improved stability of a dual functional material, and a method for manufacturing a powder cosmetic using dual functional materials such as ethylhexyl methoxycinnamate and niacinamide, The present invention relates to a method of manufacturing powder cosmetics in which the stability of a dual functional material is improved through a dispersion process.

Cosmetics refers to products that are used in the human body to maintain or improve the health of the skin and hair, to make the appearance of the body clean, beautify, charm, change the appearance brightly, and have a slight effect on the human body.

In recent years, with the development of medicine and science, the life expectancy of human beings has increased to the age of 100, and it is rapidly entering the age of aging. Therefore, the desire to show younger and healthier people is increasing. As the interest in cosmetics has increased, the age group using cosmetics has widened and the cosmetics market, which is considered to be women's exclusive products, has been expanded by the use of men, and the use of cosmetics Is increasing.

In such a change, the consumer desires a product having a substantial effect, such as reduction of fine lines and visible skin whitening effect, rather than a product having temporary skin improvement effect.

In general, cosmetics are manufactured through dispersion, emulsification, solubilization, mixing, filling, packaging and molding processes, and can be classified into emulsified products, solubilized products, and dispersed products depending on the product shape. Among them, a dispersed product is a product in which a water-soluble polymer substance is dispersed in base (purified water, etc.), and cosmetics are manufactured by dispersing inorganic, organic, pearl and pigment used in make-up cosmetics into various base materials. The cosmetics thus manufactured have an aesthetic role in enhancing the covering and coloring properties to produce natural color skin and protect the skin from the external environment.

For example, makeup cosmetics, which is one of the dispersed products, is mixed with an extender pigment, a white pigment, and a color pigment in a mixer, and then the binder is sprayed, mixed and pulverized. However, such a mixing method has a limitation in uniform mixing This results in a decrease in the stability and quality of the formulation.

Korean Patent Laid-Open No. 10-2007-0072434 discloses a prior art dispersed product which is known in the art and which relates to a solid ultraviolet ray blocking cosmetic composition which comprises an organic ultraviolet blocking agent, an inorganic ultraviolet blocking agent, a wax component, Activators, oil components, silicone polymers and pigments.

However, there is a disadvantage in that the dispersion of the binder is more difficult and the problem of powder aggregation is further exacerbated by mixing the water-soluble material first and then the water-soluble material while using the wax as a binder.

Korean Patent Laid-Open No. 10-2012-0122282 discloses a cosmetic material prepared by using a mixed solvent of ethanol, water, and glycerin, and more specifically, The present invention relates to a makeup cosmetic composition which does not cause cracks on the surface of a product even after solvent is volatilized by using a mixed solvent of ethanol, water and glycerin, maintains the quality of the product for a long time, and gives improved moisturizing power and soft feeling.

However, the conventional art has a disadvantage in that the skin moisturizing effect can not be sustained for a long time due to a high content of ethanol, and also there is a problem in that an efficient dispersion process can not proceed because the oil-soluble material and the water-soluble material are mixed at the same time.

SUMMARY OF THE INVENTION Accordingly, the present invention has been made keeping in mind the above problems occurring in the prior art, and it is an object of the present invention to provide a method for manufacturing a powder cosmetic which improves the stability of a dual functional material simultaneously achieving whitening and wrinkle functioning.

Another object of the present invention is to provide a powder cosmetic manufacturing method in which the stability of a dual functional material is improved through a dispersion process using a water-soluble and oil-soluble raw material.

The present invention relates to a method for preparing a water-soluble polymer, which comprises mixing (S1) an extender pigment, (S2) mixing a water-soluble melt to the mixture prepared in the step (S1) (S4) of adding a dye to the mixture prepared in the step (S3) and coloring the mixture, and a step (S5) of putting the mixture prepared in the step (S4) into a pulverizer and pulverizing Thereby providing a powder cosmetic preparation method with improved stability of the material.

Further, it is preferable that the present invention uses niacinamide as a water soluble melt.

In addition, the present invention preferably uses ethylhexyl methoxycinnamate as a fat-soluble melt.

As described above, the powder cosmetic manufacturing method improved in stability of the dual functional material according to the present invention has the effect of simultaneously realizing the whitening function and the wrinkle function.

In addition, the present invention can provide a powder cosmetic manufacturing method in which the stability of a dual functional material is improved through a dispersion process using a water-soluble and oil-soluble raw material.

BRIEF DESCRIPTION OF THE DRAWINGS Figure 1 is a flow chart showing a method of making a powder cosmetic with improved stability of a dual functional material.

In order to attain the above object, the present invention provides a method for producing a mixture, comprising the steps of (S1) mixing an extender pigment, (S2) mixing a water soluble melt with the mixture prepared in the step (S1) (S4) of adding a dye to the mixture prepared in the step (S3) and coloring the mixture, and a step of pulverizing the mixture prepared in the step (S4) into a pulverizer S5) in order to improve the stability of the dual functional material.

Further, it is preferable that the present invention uses niacinamide as a water soluble melt.

In addition, the present invention preferably uses ethylhexyl methoxycinnamate as a fat-soluble melt.

Hereinafter, the present invention will be described in detail.

The present invention provides a method of manufacturing a powder cosmetic with improved stability of a dual functional material. The production method preferably includes but is not limited to the following steps.

In the method for manufacturing powder cosmetics with improved stability of the dual functional material according to the present invention, step (S1) of mixing the extender pigment is carried out. The extender pigment is composed of TALC FM SSA, TR-2 AS (Snow crystal powder), Softitan 60, Z-COTE HP1 and SILICA BEAD SS to complement the defects of the skin and improve the physical properties of the cosmetic. 300, Micro TiO2 (Sericite) SS, FP-OMC, EA-209, GANZPEARL GMX-0610A and KSP-300.

The TALC FM SSA is composed of 98% of talc and 2% of dimethicone. It improves the spreadability of the powder to improve spreadability and lumpiness, and improves the affinity with the skin, adhesion and persistence, and the texture of use.

The TR-2 AS (Snow Crystal Powder) is a synthetic fluorphlogopite triethoxycaprylylsilane (Synthetic Fluphlogopite triethoxycycllylsilane), which has the effect of maintaining a lavish facial state without changing color after oil absorption.

Softitan 60 is composed of 55% of titanium dioxide, 40% of silica, and 5% of triethoxy caprylylsilane. The particle size of titanium dioxide is more than 100 nm. Softitan 60 can block both ultraviolet rays A and B at the same time because it has high SPF (Sun Protection Factor) and PFA (Protection Factor for UVA) when applying cosmetic composition. When applied to a cosmetic composition, the effect of multi- It improves the feeling of toughness inherent in titanium dioxide and gives a feeling of soft feeling.

The Z-COTE HP1 is composed of 96% zinc oxide and 4% triethoxycaprylylsilane, and is used as a skin protection agent with antibacterial and non-toxic materials. The Z-COTE HP1 absorbs light and has broad spectral UV attenuation properties due to its reflective properties, and thus is used in sun care products. It has a hydrophobic property, good dispersibility and good compatibility with oil-soluble components (oil).

The SILICA BEAD SS is a natural or synthetic organic spherical powder that spreads smoothly, has a high transparency, allows natural makeup, and gives skin-correcting effect.

The above-mentioned FTL-300 is a needle-shaped titanium dioxide having a rutile structure and is used to enhance the mechanical properties of cosmetic materials and is known as a good dispersing raw material.

Said micro TiO ₂ (Sericite) SS is a white inorganic pigment which is chemically stable and has a high defect complementing ability to the skin. The TiO ₂ prevents ultraviolet rays from penetrating the skin and is excellent in the effect of shielding ultraviolet rays by scattering ultraviolet rays .

The FP-OMC is composed of 60% of methyl methacrylate crosspolymer and 40% of ethyl hexyl methoxycinnamate. It is an odorless white fine powder with an average particle size of 8 μm. The FP-OMC is widely used in cosmetics to protect ultraviolet rays.

EA-209 is an acrylic acid-ethylene copolymer and is an odorless fine white powder. When the EA-209 is present on the skin, light is scattered while the shape of the fine lines of the skin is scattered while the skin is exposed to light, and the skin can be protected from light.

GANZPEARL GMX-0610A is polymethyl methacrylate, which is obtained by suspension polymerization or emulsion polymerization of methacrylic acid methyl monomer and drying. The polymethylmethacrylic acid is a polymer which is excellent in weather resistance, heat resistance, chemical resistance, transparency, hardness, etc. and has a high safety. It has no irritation to the skin and is excellent in absorbency such as lubrication, touch, swelling, perspiration, Good sex.

The KSP-300 is diphenyl dimethicone as an INCI name, and has an average particle size of 5 μm and a white powder. It is used for skin care, make-up and sun cream products without absorbing silicon.

The extender pigment is preferably 80.0 to 89.5% by weight, more preferably 82.5 to 87.2% by weight, based on the total weight of the powder cosmetic composition. If the extender pigment is less than 80.0% by weight based on the total weight of the powder cosmetic composition, there is a problem that the ultraviolet ray shielding effect and the skin correcting effect are poor. When the extender pigment exceeds 89.5% by weight, the extraneous pigment particles are agglomerated to cause whitening .

Table 1 shows the content ratios when only five components are used according to one embodiment of the present invention, and Table 2 shows the content ratios of raw materials constituting the extender pigments according to another embodiment of the present invention. It represents the content ratio when branch components are used.

Raw material Content ratio (% by weight) TALC FM SSA 20.0 to 28.0 TR-2 AS (Snow crystal powder) 34.0 to 62.0 Z-COTE HP1 12.0 to 18.0 Softitan 60 1.0 to 5.0 SILICA BEAD SS 5.0 to 15.0

Raw material Content ratio (% by weight) TALC FM SSA 15.0 to 22.0 FTL-300 3.0 to 7.0 TR-2 AS (Snow crystal powder) 19.0 to 59.5 Micro TiO ₂ (Sericite) SS 3.0 to 7.0 Softitan 60 1.5 to 3.0 Z-COTE HP1 7.0 to 13.0 FP-OMC 1.5 to 5.0 SILICA BEAD SS 5.0 to 10.0 EA-209 1.5 to 5.0 GANZPEARL GMX-0610A 2.5 to 7.0 KSP-300 0.5 to 2.0

In the mixing step (S1) of the extender pigment of the present invention, TALC FM SSA, TR-2 AS (Snow crystal powder), Z-COTE HP1 and Softitan 60 among the components shown in Table 1 were put into a mixer and heated at a speed of 200 to 300 rpm It is preferable to mix for 5 to 20 seconds, more preferably for 8 to 15 seconds at a speed of 220 to 280 rpm. Then, it is preferable to mix SILICA BEAD SS at a speed of 580 to 680 rpm for 100 to 250 seconds, more preferably at a speed of 600 to 650 rpm for 150 to 200 seconds.

In another example, TALC FM SSA, FTL-300, TR-2 AS, Micro TiO ₂ (Sericite) SS, Softitan 60 and Z-COTE HP1 among the components shown in Table 2 were placed in a mixer, It is preferable to mix for 5 to 20 seconds at the rpm rate, more preferably for 8 to 15 seconds at the rate of 220 to 280 rpm. Then, it is preferable to add FP-OMC, SILICA BEAD SS, EA-209, GANZPEARL GMX-0610A and KSP-300 and then mix at a speed of 580 to 680 rpm for 100 to 250 seconds, Mix at 650 rpm for 150-200 seconds.

(S2) of mixing a water-soluble melt with the mixture prepared in the step (S1) of mixing the extender pigment. The water-soluble lysate is used to realize a dual function whitening function and a dispersing process of cosmetics, and is composed of niacinamide and water.

Niacinamide, which has the molecular formula C ₆ H ₆ N ₂ O, is also called nicotinamide and has been used primarily in the cosmetic field to obtain a whitening effect. On the other hand, since niacinamide has a hydrotropic property, it can be used as a cosolubilizing agent to help dissolve poorly soluble materials. Hydrotropy refers to the phenomenon of increasing the solubility of water-insoluble or sparingly soluble substances in water by adding a relatively large amount of a third substance. A solubilizing agent is a third substance that makes two kinds of liquids that are not mixed with each other into a stable emulsion (emulsion), and is also referred to as an emulsifier.

The water is used to prepare an aqueous solution of niacinamide.

The water-soluble dissolution product is preferably 3.0 to 7.0% by weight, more preferably 4.0 to 6.0% by weight based on the total weight of the powder cosmetic composition. If the content of the water soluble dissolving agent is less than 3.0% by weight based on the total weight of the powder cosmetic composition, there is a problem that the effect on skin whitening is deteriorated. If the water soluble dissolving agent is more than 7.0% by weight, skin irritation may occur or the feeling on use may deteriorate.

The content ratios of the raw materials constituting the water soluble lysate are shown in the following table, and Table 3 shows the content ratio of niacinamide and water.

Raw material Content ratio (% by weight) Niacinamide 38.0 to 52.0 water 48.0 to 62.0

In the step (S2) of mixing the water-soluble melt of the present invention, niacinamide and water, which are components of Table 3, are dispersed at 70 to 90 ° C, more preferably 75 to 80 ° C, , And the mixture is preferably mixed at a speed of 450 to 600 rpm for 5 to 20 seconds, more preferably at a speed of 500 to 550 rpm for 8 to 15 seconds. Further, the mixture is further mixed at a speed of 900 to 1,500 rpm for 100 to 200 seconds, more preferably at a speed of 1,000 to 1,300 rpm for 130 to 180 seconds.

The external dispersion refers to a process in which raw materials are mixed to be mixed or dispersed, and the dispersion is firstly dispersed in a specific solvent to increase the dispersibility.

(S3) of mixing the fat-soluble melt with the mixture prepared in the step (S2) of mixing the water-soluble melt. The above-mentioned fat soluble solubles are used for realizing the double functional middle wrinkle improving function and dispersing process of cosmetics. Ethylhexyl methoxycinnamate and COSMOL 222 (S), DUB SSOD, Dermosoft GMCY and Sensiva SC 50 , And can further comprise an aqueous solution of white ginseng polysaccharide, Baekhwaseol NS, an essential oil base, a consonant tone, and a consonantal defense step.

The ethylhexyl methoxycinnamate is the molecular formula C ₁₈ H ₂₆ O ₃ and is also referred to as octyl methoxycinnamate. In the field of cosmetics, it was mainly used as an ultraviolet absorber to absorb ultraviolet UV-B from the sun. UV-B, which corresponds to a wavelength of 280 to 320 nm in the ultraviolet wavelength, is associated with photoaging of the skin, and photoaging is a phenomenon in which the skin is aged due to exposure to the sun. As the photoaging progresses, more and thicker fan wrinkles of the exposed face, neck, arms, and hands and pigmentation such as speckled black spots and spots are typical phenomena. Unlike biological aging, which simply becomes thinner and less structured, photoaged skin becomes uncomfortable due to the presence of abnormal, elastic fiber-like substances in the upper dermis, which can not support the skin, which is the original function of the dermis. Ultraviolet rays cause damage to skin cells directly, causing skin aging, skin cancer, and inflammation of skin, resulting in secondary damage of active oxygen species and aging caused by oxidation. As a result, it inhibits the production of collagen and elastic fibers that make up the dermis, and promotes the action of the enzymes that break down the collagen, thereby reducing both collagen and elasticity.

COSMOL 222 (S) is a diisostearyl malate with an INCI name and has a high viscosity and is excellent in pigment dispersibility, dye solubility and wax solubility.

The DUB SSOD is referred to as octyldodecyl stearoyl stearate and the molecular formula is C ₅₆ H ₁₁₀ O ₄ . The DUB SSOD improves the feeling of use of the cosmetic composition and imparts a moisturizing function.

The Dermosoft GMCY is called glyceryl monocaprylate and the molecular formula is C ₁₁ H ₂₂ O ₄ . It does not dissolve well in water but has a property of being easily hydrolyzed under strong acidic or strong basic conditions and has excellent dispersing, emulsifying and antibacterial functions and is used as a dispersant and emulsifier in personal care products.

The Sensiva SC 50 is referred to as ethylhexyl glycerin and the molecular formula is C ₁₁ H ₂₄ O ₃ . The Sensiva SC 50 has an antibacterial function and various skin regulating functions.

The aqueous solution of white ginseng polysaccharide means a water-soluble polysaccharide extracted from white ginseng, that is, dried ginseng. Generally, it can extract about 7% of white ginseng polysaccharide from white ginseng and increase skin cell ATP energy.

The above-mentioned Baekhwa reed NS has the effects of improving wrinkles and preventing sagging of skin, and is excellent in anti-inflammatory effect, antiviral, antibacterial and antifungal effect.

The essential oil base refers to a fragrance oil extracted from flowers, seeds, leaves, stems, roots, byproducts, etc. of plants, or by using a part or a plant. The essential oil base stimulates the body to stimulate metabolic functions, relaxes fatigue, relaxes the mind and body, stimulates endocrine secretion, improves mood, increases the white blood cell count, and improves immune function. It is very beneficial to the human body. And it has fat-soluble property to dissolve well in fat.

The consonants are five kinds of herbal extracts of lotus, lily, jade, peony, and rhubarb, and have the effect of controlling moisturizing action, preventing aging, improving elasticity and controlling skin balance.

The consonant herb extracts are five kinds of herbal extracts of Seiho, Yinhyeon, Nuyin, Candy, and Chaesuncho.

The fat-soluble melt is preferably 7.0 to 11.0% by weight, more preferably 8.0 to 10.0% by weight, based on the total weight of the powder cosmetic composition. The fat soluble solubility is less than 7.0% by weight based on the total weight of the powder cosmetic composition, and the ultraviolet ray shielding effect is insignificant, resulting in deterioration of the skin wrinkle improving function. When the content exceeds 11.0% by weight, skin irritation occurs, There arises a problem that may affect the stability of the formulation.

Table 4 shows the content ratios when only five components are used according to one embodiment of the present invention. Table 5 shows the ratios of the raw materials constituting the fat-soluble liquor according to another embodiment of the present invention It represents the content ratio when 10 components are used.

Raw material Content ratio (% by weight) Ethylhexyl methoxycinnamate 38.5 to 60.2 COSMOL 222 (S) 8.0 to 15.0 DUB SSOD 30.0 to 42.0 Dermosoft GMCY 0.8 to 1.5 Sensiva SC 50 1.0 to 3.0

Raw material Content ratio (% by weight) Ethylhexyl methoxycinnamate 31.920 to 60.480 COSMOL 222 (S) 8.000 ~ 15.000 DUB SSOD 28,000 ~ 40,000 White ginseng aqueous solution 0.005 to 0.020 Baekhwaso private NS 0.005 to 0.020 A consonant 0.005 to 0.020 Consonant Corps 0.005 to 0.020 Dermosoft GMCY 0.500 ~ 2.000 Sensiva SC 50 1.000 ~ 3.000 Essential oil base 2.000 ~ 8.000

The step (S3) of mixing the fat-soluble melt of the present invention is carried out by mixing ethylhexyl methoxycinnamate, COSMOL 222 (S) and DUB SSOD in the ingredients of Table 4 at 70 to 90 ° C, The mixture is dispersed at 75 to 80 ° C and then added to the mixture prepared in step S2. In addition, Dermosoft GMCY is preferably added to the mixture at 450 to 600 rpm for 5 to 20 seconds, Mix for 8 to 15 seconds at 500 to 550 rpm. In addition, it is preferable to further add Sensiva SC 50 and mix at a speed of 900 to 1,500 rpm for 100 to 200 seconds, more preferably at a speed of 1,000 to 1,300 rpm for 130 to 180 seconds.

In another embodiment, the step (S3) of mixing the fat soluble solubles comprises adding ethylhexyl methoxycinnamate, COSMOL 222 (S), DUB SSOD, white ginseng polysaccharide aqueous solution, The mixture is further dispersed at 70 to 90 ° C, more preferably at 75 to 80 ° C, and then added to the mixture prepared in the step (S2). In addition, a consonant, a consonant bowel and Dermosoft GMCY It is preferable to mix for 5 to 20 seconds at the rpm rate, more preferably for 8 to 15 seconds at the rate of 500 to 550 rpm. In addition, it is preferable to add Sensiva SC 50 and an essential oil base at a speed of 900 to 1,500 rpm for 100 to 200 seconds, more preferably at a speed of 1,000 to 1,300 rpm for 130 to 180 seconds.

(S4) of adding a pigment to the mixture prepared in the step (S3) of mixing the fat-soluble mixture and coloring the mixture. The pigment is used to complement the color of the extender pigments and is excellent in water resistance (water repellency), dispersibility and expandability, and is composed of OTS-2 RED R-516L, OTS-2 YELLOW LLXLO and OTS-2 BLACK BL-100 .

The OTS-2 RED R-516L is red iron oxide and has a contact angle to water of 153 °.

The OTS-2 YELLOW LLXLO is yellow iron oxide and has a contact angle to water of 155 °.

The OTS-2 BLACK BL-100 is black iron oxide and has a contact angle to water of 159 DEG.

The coloring matter is preferably 0.5 to 2.0 wt%, more preferably 0.8 to 1.5 wt%, based on the total weight of the powder cosmetic composition. If the amount of the coloring matter is less than 0.5% by weight based on the total weight of the powder cosmetic, there is a problem that the function of complementing the color of the extender pigment is poor. When the amount exceeds 2.0% by weight, the color of the powder becomes cloudy.

Table 6 shows the content ratios of OTS-2 RED R-516L, OTS-2 YELLOW LLXLO and OTS-2 BLACK BL-100.

Raw material Content ratio (% by weight) OTS-2 RED R-516L 15.0 to 23.0 OTS-2 YELLOW LLXLO 72.0 to 84.0 OTS-2 BLACK BL-100 1.0 to 5.0

The step (S4) of adding and dyeing the coloring matter of the present invention is performed by mixing the components of Table 6 into the mixture prepared in the step (S3) of mixing the fat-soluble melt and mixing the components at a speed of 300 to 1,000 rpm for 30 to 300 seconds , And more preferably at a speed of 400 to 700 rpm for 60 to 180 seconds.

(S5) of putting the mixture prepared in the coloring step (S4) into a pulverizer and pulverizing the mixture is carried out. In the pulverizing step S5, it is preferable that the mixture is pulverized at a speed of 9,500 to 14,000 rpm for 150 to 450 seconds in order to prepare the mixture prepared in the coloring step (S4) into a pulverizer, Milling at a speed of 11,000 to 13,000 rpm for 250 to 350 seconds. If the speed is less than 9,500 rpm, the mixture of the raw materials can not be uniformly mixed and the raw materials are bundled together. If the speed is more than 13,000 rpm, heat is generated due to frictional force, There is a problem that the function of the seafood is deteriorated.

Hereinafter, the present invention will be described in detail with reference to Examples and Experimental Examples.

However, the following examples and experimental examples are merely illustrative of the present invention, and the content of the present invention is not limited to the following examples and experimental examples.

< Example  1> Manufacture of powder cosmetics according to the conventional manufacturing method Example

(1) mixing an extender pigment;

30.0 wt% of TR-2 AS (Snow crystal powder), 6.000 wt% of Micro TiO ₂ (Sericite) SS, 12.000 wt% of Softitan 60, 9.000 wt% of SILICA BEAD SS, 6.000% by weight of GANZPEARL GMX-0610A is added and mixed at a speed of 500 rpm for 130 seconds to prepare an extender pigment mixture.

(2) mixing a fat-soluble melt;

6.000% by weight of ethylhexyl methoxycinnamate, 5.000% by weight of DUB SSOD and 2.000% by weight of essential oil base were dispersed at 80 占 폚 in terms of the total weight of the powder cosmetic composition, The mixture is added to the pigment and mixed for 130 seconds at a speed of 1,000 rpm.

(3) mixing a water soluble melt;

2.000 wt.% Of niacinamide and 2.500 wt.% Of water were dispersed at 80 DEG C with respect to the total weight of the powder cosmetic composition, and the aqueous solution of niacinamide obtained after the external dispersion was added to the mixture obtained in the step (2) Mix for 130 seconds at speed.

(4) coloring by adding a dye;

0.250 wt% of OTS-2 RED R-516L, 1.000 wt% of OTS-2 YELLOW LLXLO and 100 wt% of OTS-2 BLACK BL-100 were added to the mixture prepared in the step (3) Mix for 90 seconds at rpm speed.

(5) pulverizing;

To prepare the mixture prepared in the step (4) as a powder, the mixture was pulverized at a speed of 12,000 rpm for 300 seconds to obtain a mixture of the dual functional materials.

< Example  2> In the powder cosmetic manufacturing method according to the present invention for improving the stability of a dual functional material, Example

(S1) 21.210% by weight of TALC FM SSA, 32.000% by weight of TR-2 AS (Snow Crystal powder), 15,000% by weight of Softitan 60 and 6.000% by weight of Z-COTE HP1 were mixed in a mixer at a rate of 240 rpm Mix for 10 seconds. Then, 10.000% by weight of SILICA BEAD SS is added and mixed at a speed of 620 rpm for 160 seconds to prepare an extender pigment mixture.

(S2) 2.000% by weight of niacinamide and 2.500% by weight of water are dispersed at 80 DEG C with respect to the total weight of the powder cosmetic composition, and the aqueous solution of niacinamide obtained after the external dispersion is added to the extender pigment obtained in the step (S1) Mix for 10 seconds at a speed of 540 rpm and mix for another 160 seconds at a speed of 1,200 rpm.

(S3) 4.000% by weight of ethylhexyl methoxycinnamate, 1.000% by weight of COSMOL 222 (S) and 3.000% by weight of DUB SSOD were dispersed at 80 ° C in the total weight of the powder cosmetic composition, ), 1.000% by weight of Dermosoft GMCY is added and mixed at a rate of 540 rpm for 10 seconds. Then add 1000 wt% Sensiva SC 50 and mix for another 160 seconds at 1,200 rpm.

(S4) 0.250% by weight of OTS-2 RED R-516L, 1.000% by weight of OTS-2 YELLOW LLXLO and 100% by weight of OTS-2 BLACK BL-100% by weight based on the total weight of the powder cosmetic composition And mixed at a speed of 600 rpm for 90 seconds.

(S5) In order to prepare the mixture prepared in the step (S4) as a powder, the mixture was put into a pulverizer and pulverized at a speed of 12,000 rpm for 300 seconds to obtain a mixture of the dual functional materials.

< Example  3 > Another object of the present invention is to provide a powder cosmetic composition for improving the stability of a dual functional material of the present invention, Example

(S1) 15.406% by weight of TALC FM SSA, 5.000% by weight of FTL-300, 30.000% by weight of TR-2 AS, 30,000% by weight of Micro TiO ₂ (Sericite) SS, By weight and Z-COTE HP1 2.000% by weight are mixed in a mixer at a speed of 240 rpm for 10 seconds. Then, 3.000% by weight of FP-OMC, 7.000% by weight of SILICA BEAD SS, 3.000% by weight of EA-209, 4.000% by weight of GANZPEARL GMX-0610A and 1.000% by weight of KSP-300 were added and mixed for 160 seconds at a speed of 620 rpm An extender pigment mixture is prepared.

(S2) 2.000% by weight of niacinamide and 2.500% by weight of water are dispersed at 80 DEG C with respect to the total weight of the powder cosmetic composition, and the aqueous solution of niacinamide obtained after the external dispersion is added to the extender pigment obtained in the step (S1) Mix for 10 seconds at a speed of 540 rpm and mix for another 160 seconds at a speed of 1,200 rpm.

(S3) 4.000 wt.% Of ethylhexyl methoxycinnamate, 1.000 wt.% Of COSMOL 222 (S), 3.000 wt.% Of DUB SSOD, 0.001 wt.% Of white ginseng polysaccharide solution, 0.001 wt. Was added to the mixture prepared in the above step (S2), 0.001 wt% of a consonant portion, 0.001 wt% of a consonant portion, 0.100 wt% of Dermosoft GMCY was added, and the mixture was stirred at 540 rpm for 10 seconds Mix. Then 0.200% by weight of Sensiva SC 50 and 0.500% by weight of essential oil base are further added and mixed for another 160 seconds at a speed of 1,200 rpm.

 (S4) 0.250% by weight of OTS-2 RED R-516L, 1.000% by weight of OTS-2 YELLOW LLXLO and 100% by weight of OTS-2 BLACK BL-100% by weight based on the total weight of the powder cosmetic composition And mixed at a speed of 600 rpm for 90 seconds.

(S5) In order to prepare the mixture prepared in the step (S4) as a powder, the mixture was put into a pulverizer and pulverized at a speed of 12,000 rpm for 300 seconds to obtain a mixture of the dual functional materials.

< Experimental Example  1> Example  1 of existing powder cosmetics manufacturing method and Example  2 of the present invention, the stability of the dual functional material of the present invention is improved. Examples  practice Yes  3 &lt; / RTI &gt; of the dual functional material of the present invention, In the embodiment  Comparison of the effects of powder cosmetics manufactured by

In order to confirm the effect of the powder cosmetics manufactured by the powder cosmetic manufacturing method with improved stability of the dual functional material of the present invention, the powder cosmetics manufactured by <Example 1> to <Example 3> The effect of wrinkles was evaluated in 50 women aged 20 to 40 years. The sensory evaluation of the feeling, whitening effect, and wrinkle improvement effect was carried out by a questionnaire consisting of 5 points scale, and it was rated as 5 excellent, 4 good, 3 average, 2 poor and 1 very poor. The evaluation scores are shown in Table 7 below.

Evaluation items According to Example 1
powder According to the embodiment 2
powder According to Example 3
powder Feeling (spreadability, touch) 2.38 4.17 4.81 Whitening effect 2.47 4.36 4.84 Wrinkle improvement effect 2.89 4.58 4.88

As described above, the present invention is only one embodiment of the powder cosmetic manufacturing method in which the stability of the dual functional material is improved, and the present invention is not limited to the above embodiments. It will be understood by those skilled in the art that various changes in form and details may be made therein without departing from the spirit and scope of the present invention as defined by the appended claims and their equivalents. .

Claims (28)

Mixing the extender pigments (Sl);
Mixing a water soluble melt with the mixture prepared in the step (S1) (S2);
Mixing the fat-soluble melt with the mixture prepared in the step (S2) (S3);
Adding a dye to the mixture prepared in the step (S3) and coloring the mixture (S4);
And a step (S5) of grinding the mixture prepared in the step (S4) into a pulverizer,
In step S3, the fat soluble solubles are ethylhexyl methoxycinnamate, COSMOL 222 (S), DUB SSOD, Dermosoft GMCY, Sensiva SC 50, white ginseng polysaccharide aqueous solution, , And a consonant-protective step. The method for manufacturing a powder cosmetic according to claim 1, (S1) mixing the extender pigment with 80.0-89.5 wt% of the total weight of the powder cosmetic composition;
(S2) mixing 3.0 to 7.0% by weight of the water-soluble lysate with respect to the total weight of the powder cosmetic composition to the mixture prepared in the step (S1);
(S3) mixing 7.0 to 11.0 wt% of the fat-soluble melt with respect to the total weight of the powder cosmetic composition to the mixture prepared in the step (S2);
(S4) adding 0.5 to 2.0% by weight of a coloring matter to the mixture prepared in the step (S3) based on the total weight of the powdered cosmetic composition to color;
And a step (S5) of grinding the mixture prepared in the step (S4) into a pulverizer,
In step S3, the fat soluble solubles are ethylhexyl methoxycinnamate, COSMOL 222 (S), DUB SSOD, Dermosoft GMCY, Sensiva SC 50, white ginseng polysaccharide aqueous solution, , And a consonant-protective step. The method for manufacturing a powder cosmetic according to claim 1, 3. The method according to claim 1 or 2,
Wherein the water soluble melt comprises niacinamide in step (S2). &Lt; RTI ID = 0.0 &gt; 15. &lt; / RTI &gt; delete 3. The method according to claim 1 or 2,
Wherein the extender pigment comprises TALC FM SSA, TR-2 AS (Snow crystal powder), Softitan 60, Z-COTE HP1 and SILICA BEAD SS in the step (S1) Method of manufacturing cosmetics. 6. The method of claim 5,
The stability of the dual functional material, characterized in that the extender pigment further comprises FTL-300, Micro TiO2 (Sericite) SS, FP-OMC, EA-209, GANZPEARL GMX-0610A and KSP- Method for manufacturing improved powder cosmetics. 6. The method of claim 5,
Wherein the TALC FM SSA is composed of 98% talc and 2% dimethicone. 6. The method of claim 5,
Wherein the Softitan 60 is composed of 55% titanium dioxide, 40% silica, and 5% triethoxy caprylylsilane. 6. The method of claim 5,
Wherein the Z-COTE HP1 is composed of 96% zinc oxide and 4% triethoxycapryllylsilane. The method according to claim 6,
Wherein the FP-OMC is composed of 60% methyl methacrylate crosspolymer and 40% ethyl hexyl methoxycinnamate, wherein the stability of the dual functional material is improved. 3. The method according to claim 1 or 2,
The extender pigment contained 20.0 ~ 28.0 wt% of TALC FM SSA, 34.0 ~ 62.0 wt% of TR-2 AS (snow crystal powder), 1.0 ~ 5.0 wt% of Softitan 60, 12.0 ~ 18.0 wt% of Z- SILICA BEAD SS in an amount of 5.0 to 15.0 wt% based on the total weight of the cosmetic composition. 3. The method according to claim 1 or 2,
Wherein the extender pigment comprises 3.0 to 7.0 wt% of FTL-300, 3.0 to 7.0 wt% of Micro TiO2 (Sericite) SS, 1.5 to 5.0 wt% of FP-OMC, 1.5 to 5.0 wt% of EA-209, GANZPEARL GMX- 06-10A and KSP-300 in an amount of 2.5 to 7.0% by weight and KSP-300 in an amount of 0.5 to 2.0% by weight, based on the total weight of the cosmetic composition. 3. The method according to claim 1 or 2,
The extender pigment was mixed with TALC FM SSA, TR-2 AS (Snow crystal powder), Z-COTE HP1 and Softitan 60 in a mixer at a speed of 200 to 300 rpm for 5 to 20 seconds and then SILICA BEAD SS Characterized in that the mixing is performed at a speed of 580 to 680 rpm for 100 to 250 seconds, thereby improving the stability of the dual functional material. 3. The method according to claim 1 or 2,
The extender pigment is added to a mixer at a rate of 200 to 300 rpm and mixed with 5 to 20 parts by weight of TALC FM SSA, FTL-300, TR-2 AS (Snow crystal powder), Micro TiO ₂ (Sericite) SS, Softitan 60 and Z- Characterized in that it is mixed for from 100 to 250 seconds at a speed of 580 to 680 rpm after addition of FP-OMC, SILICA BEAD SS, EA-209, GANZPEARL GMX-0610A and KSP- A method for manufacturing powder cosmetics with improved stability. 3. The method according to claim 1 or 2,
Wherein the water soluble lysate contains 38.0 to 52.0% by weight of niacinamide and 48.0 to 62.0% by weight of water, wherein the stability of the dual functional material is improved. 3. The method according to claim 1 or 2,
The aqueous dissolution product is prepared by separately dispersing niacinamide and water at 70 to 90 ° C, adding the mixture to the mixture prepared in step (S1), mixing the mixture at 450 to 600 rpm for 5 to 20 seconds, To 1500 rpm for 100 to 200 seconds. &Lt; RTI ID = 0.0 &gt; 15. &lt; / RTI &gt; delete delete 3. The method according to claim 1 or 2,
Wherein the consonant comprises five herbal extracts of lotus, lily, jade, peony, and rhubarb. 3. The method according to claim 1 or 2,
Wherein the consonant suppressing unit comprises five herbal extracts, namely, Sephora, Rhinoceros, Nuyin, Passerinus, and Chaetzchecho. 3. The method according to claim 1 or 2,
The fat-soluble melt contains 38.5 to 60.2% by weight of ethylhexyl methoxycinnamate, 8.0 to 15.0% by weight of COSMOL 222 (S), 30.0 to 42.0% by weight of DUB SSOD, 0.8 to 1.5% by weight of Dermosoft GMCY % And Sensiva SC 50 from 1.0 to 3.0% by weight, based on the total weight of the cosmetic composition. 3. The method according to claim 1 or 2,
Wherein the fat soluble solubles contain 0.005-0.020 wt.% Of white ginseng aqueous solution, 0.005-0.020 wt.% Of whitening agent NS, 2.000-8.000 wt.% Of essential oil base, 0.005-0.020 wt.% Of consonant tone and 0.005-0.020 wt. By weight based on the total weight of the cosmetic composition. 3. The method according to claim 1 or 2,
The fat-soluble melt is prepared by separately dispersing ethylhexyl methoxycinnamate, COSMOL 222 (S) and DUB SSOD at 70 to 90 ° C, and then adding the mixture to the mixture prepared in step (S2) Dermosoft GMCY is added thereto and mixed at a speed of 450 to 600 rpm for 5 to 20 seconds, followed by addition of Sensiva SC 50, followed by mixing at a speed of 900 to 1,500 rpm for 100 to 200 seconds. Method for manufacturing improved powder cosmetics. 3. The method according to claim 1 or 2,
The fat-soluble melt is prepared by separately dispersing ethylhexyl methoxycinnamate, COSMOL 222 (S), DUB SSOD, white ginseng polysaccharide aqueous solution and Baekhwasa specimen NS at 70 to 90 ° C, The mixture was then mixed at a speed of 450 to 600 rpm for 5 to 20 seconds. Sensiva SC 50 and an essential oil base were further added to the mixture at 900 to 1,500 rpm Wherein the blending is performed at a speed of 100 to 200 seconds. 3. The method according to claim 1 or 2,
Wherein the coloring agent comprises OTS-2 RED R-516L, OTS-2 YELLOW LLXLO and OTS-2 BLACK BL-100. 3. The method according to claim 1 or 2,
Wherein the coloring matter comprises 15.0 to 23.0 wt% of OTS-2 RED R-516L, 72.0 to 84.0 wt% of OTS-2 YELLOW LLXLO and 1.0 to 5.0 wt% of OTS-2 BLACK BL-100 Wherein the stability of the material is improved. 3. The method according to claim 1 or 2,
ODS-2 YELLOW LLXLO, OTS-2 YELLOW LLXLO and OTS-2 BLACK BL-100 are added to the mixture prepared in the step (S3) of mixing the fat soluble solubles at a speed of 300 to 1,000 rpm, Wherein the mixture is mixed for 300 seconds, and the stability of the dual functional material is improved. 3. The method according to claim 1 or 2,
Wherein the pulverizing step (S5) comprises pulverizing the mixture prepared in the coloring step (S4) in a pulverizer at a speed of 9,500 to 14,000 rpm for 150 to 450 seconds. Gt;

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