CN105726456A

CN105726456A - Herbaceous plant nutritive water based on emulsified microcapsule and preparation method of herbaceous plant nutritive water

Info

Publication number: CN105726456A
Application number: CN201610113396.XA
Authority: CN
Inventors: 胡海威; 丁靓; 闫永平; 郑辉; 严辉
Original assignee: SUZHOU ITIC MEDCHEM CO Ltd
Current assignee: Guangzhou Happiness Cosmetics Co ltd
Priority date: 2016-03-01
Filing date: 2016-03-01
Publication date: 2016-07-06
Anticipated expiration: 2036-03-01
Also published as: CN105726456B

Abstract

The invention provides herbaceous plant nutritive water based on an emulsified microcapsule and a preparation method of the herbaceous plant nutritive water. The preparation method comprises the following specific steps: mixing hydrogenated vegetable oil, low erucic acid rapeseed oil , siloxane, microcrystalline wax and diglycerol, heating and uniformly stirring, and performing heat reservation and sterilization to obtain an oil phase; adding ethylene glycol, propylene glycol, glycine betaine, urea, poly-sodium glutamate, triethanolamine, caprylhydroxamic acid and hexylene glycol into deionized water, heating and uniformly stirring, performing heat preservation and sterilization to obtain a water phase; adding the oil phase into the water phase, performing heating, homogenization and low-speed stirring, adding cetyl ethyl hexanoate and stearic acid, then slowly adding PEG-40 hydrogenated castor oil and a microcapsule wall material, cooling, adding tremella, centella asiatica, polygonum cuspidatum, scutellaria baicalensis, tea leaves, glycyrrhiza glabra, female chrysanthemum, rosemary leaves, beer saccharomycete and grape fruit cell extract active components, and adding chondrus crispus extracts, bio-saccharide gum-1, diglycerol, palmitoyl tripeptide-1 and essence for mixing to obtain the herbaceous plant nutritive water based on the emulsified microcapsule.

Description

A kind of herbaceous plant nutritive water of emulsifying microcapsule and preparation method thereof

Technical field:

The invention belongs to daily cosmetics technical field, be specifically related to a kind of emulsifying microcapsule herbaceous plant nutritive water and Its preparation method.

Background technology:

Skin is one of organ of people's bulk area maximum, and skin is made up of epidermis, corium and subcutaneous tissue, and epidermis is skin Skin outermost one layer, can be divided into horny layer, clear layer, granular layer, prickle cell layer and basal layer from inside to outside, and skin The quality of skin i.e. shows as the buffer capacity of acid or alkali environment to external world, if the pH value of skin be chronically at 5.0-5.6 it Outward, the skin quality of skin rescues back change, ultimately results in the aging of skin, the raw infringement such as speckle, melanin pigmentation.Therefore need Select the skin care item being suitable for keep skin ph value between 5.0-5.6, make skin maintain optimum state, really reach To beautiful healthy effect.

Surfactant is the transparent skin-care product with water as solvent, and it has the effect that cream kind cosmetics are same, can make skin Keep soft, moisten, regulate and improve the physiological function of skin, be broadly divided into nutritive water, cosmetic water, shrinkage water, Makeup remover etc..Nutritive water is also referred to as balance liquid, is a kind of neutral astringent, and its character connects with the pH value of people very much Closely, based on plant component, comprise many nutritional labelings and multivitamin, the acid-base value of energy balance skin, shrink Pore, supplements nutrition and the moisture of skin, increases the resistance of skin, slow down cutaneous pigmentation.

A kind of protecting containing plant extract disclosed in Chinese patent CN 103251530B (publication date 2013.8.21) Skin frost, by protective skin cream raw material add pure natural green tea extract, licorice root extract, Herba Rosmarini Officinalis extract, Scutellariae,radix extract, Flos Chrysanthemi extract and Herba Centellae extract, this six Plant Extracts shows antiinflammatory, improves and exempt from The effect of epidemic disease power, can suppress inflammation in reality comprehensively, has class effects of antibiotics to there is no safety and has no side effect, also has simultaneously There are antioxidation, the cooperative effect of machine moisturizing of releiving, baby can be suitable for and use.Chinese patent CN 102068389A is (open Day 2011.5.25) disclosed in microemulsified feature of environmental protection facial treatment milk and preparation method, including emulsifying agent, oil-phase component, merit Effect composition, preservative and essence, wherein oil-phase component includes food grade white mineral oil, refined plant oil etc., water-phase component Including efficient moisture-retention agent, propylene glycol, glycerol etc., functional component includes biocatalyzer and chlorophyll, passes through microemulsified Technology is distributed in well-proportioned to biocatalyzer and chlorophyll in facial treatment milk, it is easy to be absorbed by the skin, and biological The carbon dioxide that catalyst and chlorophyll can absorb in air is converted into oxygen, obtains that stability is high, permeability is strong Environment-friendly type microemulsified facial treatment milk.

From above-mentioned prior art, skin care item based on natural plant extracts and emulsifying technology are the most more Common, but the research of surfactant based on this technology especially nutritive water is the most few.The present invention is based on frost and emulsion Concentration is denser, is unfavorable for the feature absorbed rapidly of skin, the present invention is directed to tea disclosed in currently available technology and extracts Thing, licorice root extract, Herba Rosmarini Officinalis extract, scutellariae,radix extract, Flos Chrysanthemi extract and Herba Centellae extract this six Plant Extracts, and combine the nutritive water that emulsifying technology preparation can quickly be absorbed by the skin, thus fast and effeciently change The problems such as the kind moisture content of skin, microgroove and the colour of skin.

Summary of the invention:

The technical problem to be solved in the present invention is to provide a kind of herbaceous plant nutritive water based on emulsifying microcapsule and preparation thereof Method, uses Tremella extract, Herba Centellae extract, polygoni cuspidati,radix extract, scutellariae,radix extract, Folium Camelliae sinensis to extract Thing, Glycyrrhiza glabra L. root extract, Flos Chrysanthemi extract, rosemary leaf extract, cereuisiae fermentum and uva cell Extract is as active component, in conjunction with microcapsule technology and micro-emulsion technology, obtains draft based on emulsifying microcapsule and plants Thing nutritive water.Fractions of active ingredient is scattered in molten by herbaceous plant nutritive water based on emulsifying microcapsule prepared by the method Liquid, part is coated on microcapsule, in conjunction with microcapsule technology, makes the active component moment existed in solution by skin institute Absorb, and microcapsule through the stimulation of extraneous factor by its abrupt release, reach the purpose of slow release.

For solving above-mentioned technical problem, the technical scheme is that

A kind of herbaceous plant nutritive water based on emulsifying microcapsule, it is characterised in that described grass based on emulsifying microcapsule This plant nutrient water includes that deionized water, ethylene glycol, propylene glycol, glycine betaine, carbamide, polyglutamic acid sodium, ring five gather Dimethyl siloxane, polydimethylsiloxane, phenyl trimethicone, spermol ethylhexoate, hydrogenation are planted Thing oil, stearic acid, low erucic acid rapeseed oil, microwax, allantoin, Chondrus crispus extract, biological carbohydrate gum-1, Diglycerol, palmityl tripeptides-1, beta glucan, Tremella extract, Herba Centellae extract, polygoni cuspidati,radix extract, Scutellariae,radix extract, Folium Camelliae sinensis extract, Glycyrrhiza glabra L. root extract, Flos Chrysanthemi extract, rosemary leaf extract, Carbomer, triethanolamine, 1,2-hexanediol, decoyl hydroximic acid, 1,3-propylene glycol, hexanediol, cereuisiae fermentum, Uva cell extract, Cremophor RH40 and daily essence.

Preferably, the component of described herbaceous plant nutritive water based on emulsifying microcapsule by weight, including: go from Sub-water 35-45 part, ethylene glycol 5-8 part, propylene glycol 4-9 part, glycine betaine 5-10 part, carbamide 3-6 part, polyglutamic Acid sodium 2-5 part, ring five polydimethylsiloxane 1-3 part, polydimethylsiloxane 2-5 part, the poly-trimethyl silicane of phenyl Oxygen alkane 3-4 part, spermol ethylhexoate 6-9 part, hydrogenated vegetable oil 1-2 part, stearic acid 8-12 part, low erucic acid Oleum Brassicae campestris 3-7 part, microwax 2-4 part, allantoin 3-5 part, Chondrus crispus extract 8-13 part, biological carbohydrate gum -15-7 part, diglycerol 4-9 part, palmityl tripeptides-13-6 part, beta glucan 8-15 part, Tremella extract 6-12 Part, Herba Centellae extract 4-8 part, polygoni cuspidati,radix extract 5-9 part, scutellariae,radix extract 7-13 part, Folium Camelliae sinensis extract 8-14 part, Glycyrrhiza glabra L. root extract 3-7 part, Flos Chrysanthemi extract 5-10 part, rosemary leaf extract 7-14 part, Carbomer 10-16 part, triethanolamine 4-8 part, 1,2-hexanediol 9-10 part, decoyl hydroximic acid 6-8 part, 1,3-third Glycol 7-10 part, hexanediol 5-8 part, cereuisiae fermentum 5-8 part, uva cell extract 9-16 part, PEG-40 Castor oil hydrogenated 5-10 part and daily essence 3-8 part.

Preferably, described herbaceous plant nutritive water based on emulsifying microcapsule also includes microcapsule, described microcapsule bag Including core and wall material, described wall material is made up of beta cyclodextrin and bud dextrin, and described core includes Tremella extract, amasss Snow grass extract, polygoni cuspidati,radix extract, scutellariae,radix extract, Folium Camelliae sinensis extract, Glycyrrhiza glabra L. root extract, Flos Matricariae chamomillae Flower extract, rosemary leaf extract, cereuisiae fermentum and uva cell extract active component.

The present invention also provides for the preparation method of a kind of herbaceous plant nutritive water based on emulsifying microcapsule, it is characterised in that: Comprise the following steps:

(1) by hydrogenated vegetable oil, low erucic acid rapeseed oil, ring five polydimethylsiloxane, polydimethylsiloxane, benzene The poly-trimethicone of base, microwax and diglycerol mixing, 70-80 DEG C of heated and stirred is uniform, insulated sterilizing 15-20min, obtains oil phase；

(2) by ethylene glycol, propylene glycol, glycine betaine, carbamide, polyglutamic acid sodium, triethanolamine, 1,2-hexanediol, Decoyl hydroximic acid, 1,3-PD, hexanediol add in deionized water, and 80-90 DEG C of heated and stirred is uniform, and insulation is gone out Bacterium 15-20min, obtains aqueous phase；

(3) oil phase step (1) prepared adds in aqueous phase prepared by step (2), 80-90 DEG C of homogenizing stirring of heating Stirring at low speed again, after adding spermol ethylhexoate, stearic acid, carbamide and carbomer, homogenizing stirs again, more slowly Adding Cremophor RH40 and microcapsule wall material, be cooled to 35-40 DEG C, addition Tremella extract, Herba Centellae carry Take thing, polygoni cuspidati,radix extract, scutellariae,radix extract, Folium Camelliae sinensis extract, Glycyrrhiza glabra L. root extract, Flos Chrysanthemi extraction Thing, rosemary leaf extract, cereuisiae fermentum and uva cell extract active component, add Chondrus crispus Extract, beta glucan, biological carbohydrate gum-1, diglycerol, palmityl tripeptides-1 and essence, stirring at low speed mixing is all Even, obtain herbaceous plant nutritive water based on emulsifying microcapsule.

Preferred as technique scheme, in described step (1) or step (2), insulated sterilizing is ultraviolet disinfection.

Preferred as technique scheme, in described step (3), the rotating speed of homogenizing stirring is 3500-5000rpm/min, the time is 30-50min.

Preferred as technique scheme, in described step (3), the rotating speed of stirring at low speed is 500-1000rpm/min, the time is 10-30min.

Preferred as technique scheme, in described step (3), herbaceous plant nutritive water based on emulsifying microcapsule The particle diameter of middle microcapsule is 1-2 μm,

Preferred as technique scheme, in described step (3), microcapsule wall material can also be chitosan, Sargassum Acid sodium.

Compared with prior art, the method have the advantages that

(1) rich in various active composition, Tremella in herbaceous plant nutritive water based on emulsifying microcapsule prepared by the present invention Extract, Herba Centellae extract, polygoni cuspidati,radix extract, scutellariae,radix extract, Folium Camelliae sinensis extract, Glycyrrhiza glabra L. root carry Take thing, Flos Chrysanthemi extract, rosemary leaf extract, cereuisiae fermentum and uva cell extract active component, Wherein tea extract, licorice root extract, Herba Rosmarini Officinalis extract, scutellariae,radix extract, Flos Chrysanthemi extract and Herba Centellae Extract, this six Plant Extracts table all has antiinflammatory, improves the effect of immunity, can suppress ten several inflammation comprehensively Disease, has class effects of antibiotics to there is no safety and has no side effect, also have antioxidation, the collaborative merit of machine moisturizing of releiving simultaneously Effect, can be suitable for baby and use, and the present invention also added Tremella, Rhizoma Polygoni Cuspidati, cereuisiae fermentum and uva on the basis of secondary The extract of cell, can promote protein and Nucleic acid, improves immunity, in beer yeast fungus extract Containing abundant Antioxidative Factors, skin elasticity can be increased, improve the immunity of human body, prevent skin aging, make skin Skin becomes fine and smooth, moistening, glossy.Uva extract has the effect eliminating free radical, can suppress melanic Being formed, oxidation resistance is big, also has pore and shrinks and the effect of convergence, and skin tightening effect is good.Therefore prepared by the present invention Nutritive water Middle nutrition composition enrich, each composition cooperate can reach moisturizing, moisten, whitening, compact, light The multiple efficacies such as speckle, antiinflammatory, and without toxicity.

(2) possibly together with multiple auxiliary agent, Qi Zhongwei in herbaceous plant nutritive water based on emulsifying microcapsule prepared by the present invention The fine crystalline structure of brilliant wax can connect solvent and oil, reaches the purpose of thickening, skin moistening.Ring five polydimethylsiloxanes Alkane, polydimethylsiloxane, phenyl trimethicone provide water resistant, antioxidation, softness, dry and comfortable effect, To no skin irritation, bright color superior performance.In stearic acid and bases solution and the anionic emulsifying of rear generation Oil/water type emulsified body based on agent.Skin and extraneous dry air isolation, waving of regulation of skin transepidermal water can be made Send out, thus protect skin, will not be dried, chap or coarse, and can be by skin transient absorption, similar snowflake.

(3) can possibly together with microcapsule, microcapsule in herbaceous plant nutritive water based on emulsifying microcapsule prepared by the present invention Using the certain active substance of cladding as core, microcapsule is attached to skin surface, by core wink after environmental stimuli Between discharge, make the nutrient substance of active component continue to act on skin, reach the effect of long-effective protection.

Detailed description of the invention:

The present invention is described in detail, in illustrative examples and the explanation of this present invention below in conjunction with specific embodiment It is used for explaining the present invention, but not as a limitation of the invention.

Embodiment 1:

(1) by weight, by the hydrogenated vegetable oil of 1 part, the low erucic acid rapeseed oil of 3 parts, the poly-diformazan of ring five of 1 part Radical siloxane, the polydimethylsiloxane of 2 parts, the phenyl trimethicone of 3 parts, the microwax of 2 parts and 4 parts Diglycerol mixing, 70 DEG C of heated and stirred are uniform, are incubated ultraviolet disinfection 15min, obtain oil phase.

(2) by weight, by the ethylene glycol of 5 parts, the propylene glycol of 4 parts, the glycine betaine of 5 parts, the carbamide of 3 parts, The polyglutamic acid sodium of 2 parts, the triethanolamine of 4 parts, the 1,2-hexanediol of 9 parts, the decoyl hydroximic acid of 6 parts, 7 parts 1,3-PD, the hexanediol of 5 parts add in the deionized water of 35 parts, and 80 DEG C of heated and stirred are uniform, are incubated ultraviolet Sterilizing 15min, obtains aqueous phase.

(3) by weight, oil phase step (1) prepared adds in aqueous phase prepared by step (2), and 80 DEG C add Temperature, 3500rpm/min homogenizing stirring 30min, then 500rpm/min stirring at low speed 10min, add the spermol of 6 parts 3500rpm/min homogenizing stirring again after the carbomer of ethylhexoate, the stearic acid of 8 parts, the carbamide of 3 parts and 10 parts 30min, is slow added into the Cremophor RH40 of 5 parts and the beta cyclodextrin of 8 parts and bud dextrin microcapsule wall material, Be cooled to 35 DEG C, add the Tremella extract of 6 parts, the Herba Centellae extract of 4 parts, the polygoni cuspidati,radix extract of 5 parts, 7 The scutellariae,radix extract of part, the Folium Camelliae sinensis extract of 8 parts, the Glycyrrhiza glabra L. root extract of 3 parts, the Flos Chrysanthemi of 5 parts extract Thing, the rosemary leaf extract of 7 parts, cereuisiae fermentum part of 5 parts, the uva cell extract activity of 9 parts become Point, add the Chondrus crispus extract of 8 parts, the biological carbohydrate gum-1 of 5 parts, the beta glucan of 8 parts, 4 parts double Glycerol, the palmityl tripeptides-1 of 3 parts and the essence of 3 parts, 500rpm/min stirring at low speed 10min, mix homogeneously, Obtain herbaceous plant nutritive water based on emulsifying microcapsule.

Embodiment 2:

(1) by weight, by the hydrogenated vegetable oil of 2 parts, the low erucic acid rapeseed oil of 7 parts, the poly-diformazan of ring five of 3 parts Radical siloxane, the polydimethylsiloxane of 5 parts, the phenyl trimethicone of 4 parts, the microwax of 4 parts and 9 parts Diglycerol mixing, 80 DEG C of heated and stirred are uniform, are incubated ultraviolet disinfection 20min, obtain oil phase.

(2) by weight, by the ethylene glycol of 8 parts, the propylene glycol of 9 parts, the glycine betaine of 10 parts, the carbamide of 6 parts, The polyglutamic acid sodium of 5 parts, the triethanolamine of 8 parts, the 1,2-hexanediol of 10 parts, the decoyl hydroximic acid of 8 parts, 10 parts 1,3-PD, the hexanediol of 8 parts add in the deionized water of 45 parts, 90 DEG C of heated and stirred are uniform, insulation purple Outside line sterilizing 20min, obtains aqueous phase.

(3) by weight, oil phase step (1) prepared adds in aqueous phase prepared by step (2), and 90 DEG C add Temperature, 5000rpm/min homogenizing stirring 50min, then 1000rpm/min stirring at low speed 30min, add the spermaceti of 9 parts After the carbomer of alcohol ethylhexoate, the stearic acid of 12 parts and 16 parts, 5000rpm/min homogenizing stirs 50min again, then It is slowly added to the Cremophor RH40 of 10 parts and the sodium alginate micro gel cyst wall material of 15 parts, is cooled to 40 DEG C, adds Enter the Tremella extract of 12 parts, the Herba Centellae extract of 8 parts, the polygoni cuspidati,radix extract of 9 parts, the scutellariae,radix of 13 parts carry Take thing, the Folium Camelliae sinensis extract of 14 parts, the Glycyrrhiza glabra L. root extract of 7 parts, the Flos Chrysanthemi extract of 10 parts, 14 parts Rosemary leaf extract, cereuisiae fermentum part of 8 parts, the uva cell extract active component of 16 parts, add The Chondrus crispus extract of 13 parts, the biological carbohydrate gum-1 of 7 parts, the beta glucan of 15 parts, the diglycerol of 9 parts, 6 The palmityl tripeptides-1 of part and the essence of 8 parts, 1000rpm/min stirring at low speed 30min, mix homogeneously, obtain base Herbaceous plant nutritive water in emulsifying microcapsule.

Embodiment 3:

(1) by weight, by the hydrogenated vegetable oil of 1.5 parts, the low erucic acid rapeseed oil of 5 parts, the ring five poly-two of 2 parts Methylsiloxane, the polydimethylsiloxane of 3 parts, the phenyl trimethicone of 3.5 parts, the microwax of 3 parts and The diglycerol mixing of 6 parts, 75 DEG C of heated and stirred are uniform, are incubated ultraviolet disinfection 17min, obtain oil phase.

(2) by weight, by the ethylene glycol of 7 parts, the propylene glycol of 6 parts, the glycine betaine of 8 parts, the carbamide of 5 parts, The polyglutamic acid sodium of 3 parts, the triethanolamine of 6 parts, the 1,2-hexanediol of 9.5 parts, the decoyl hydroximic acid of 7 parts, 8 parts 1,3-PD, the hexanediol of 7 parts add in the deionized water of 40 parts, 85 DEG C of heated and stirred are uniform, are incubated ultraviolet Line sterilizing 18min, obtains aqueous phase.

(3) by weight, oil phase step (1) prepared adds in aqueous phase prepared by step (2), 80-90 DEG C Heat, 4500rpm/min homogenizing stirring 35min, then 800rpm/min stirring at low speed 20min, add the spermaceti of 8 parts After the carbomer of alcohol ethylhexoate, the stearic acid of 10 parts and 14 parts, 4000rpm/min homogenizing stirs 30min again, then It is slowly added to the Cremophor RH40 of 8 parts and the beta cyclodextrin of 12 parts and bud dextrin microcapsule wall material, is cooled to 38 DEG C, add the Tremella extract of 8 parts, the Herba Centellae extract of 6 parts, the polygoni cuspidati,radix extract of 7 parts, the Huang of 10 parts A kind of reed mentioned in ancient books root extract, the Folium Camelliae sinensis extract of 12 parts, the Glycyrrhiza glabra L. root extract of 5 parts, the Flos Chrysanthemi extract of 8 parts, 11 The rosemary leaf extract of part, cereuisiae fermentum part of 6 parts, the uva cell extract active component of 13 parts, then Add the Chondrus crispus extract of 11 parts, the biological carbohydrate gum-1 of 6 parts, the beta glucan of 12 parts, 5 parts double sweet Oil, the palmityl tripeptides-1 of 4 parts and the essence of 5 parts, 800rpm/min stirring at low speed 15min, mix homogeneously, To herbaceous plant nutritive water based on emulsifying microcapsule.

Embodiment 4:

(1) by weight, by the hydrogenated vegetable oil of 1 part, the low erucic acid rapeseed oil of 6 parts, the poly-diformazan of ring five of 1 part Radical siloxane, the polydimethylsiloxane of 3 parts, the phenyl trimethicone of 3 parts, the microwax of 3 parts and 9 parts Diglycerol mixing, 80 DEG C of heated and stirred are uniform, are incubated ultraviolet disinfection 15min, obtain oil phase.

(2) by weight, by the ethylene glycol of 6 parts, the propylene glycol of 5 parts, the glycine betaine of 5 parts, the carbamide of 5 parts, The polyglutamic acid sodium of 3 parts, the triethanolamine of 6 parts, the 1,2-hexanediol of 9 parts, the decoyl hydroximic acid of 6 parts, 9 parts 1,3-PD, the hexanediol of 6 parts add in the deionized water of 40 parts, and 90 DEG C of heated and stirred are uniform, are incubated ultraviolet Sterilizing 15min, obtains aqueous phase.

(3) by weight, oil phase step (1) prepared adds in aqueous phase prepared by step (2), and 90 DEG C add Temperature, 4500rpm/min homogenizing stirring 40min, then 800rpm/min stirring at low speed 30min, add the spermol of 8 parts After the carbomer of ethylhexoate, the stearic acid of 8 parts and 14 parts, 5000rpm/min homogenizing stirs 30min again, then delays The slow Cremophor RH40 adding 7 parts and the chitosan microcapsules wall material of 12 parts, be cooled to 35 DEG C, adds 8 Part Tremella extract, the Herba Centellae extract of 4 parts, the polygoni cuspidati,radix extract of 6 parts, the scutellariae,radix extract of 8 parts, The Folium Camelliae sinensis extract of 10 parts, the Glycyrrhiza glabra L. root extract of 5 parts, the Flos Chrysanthemi extract of 5 parts, the leaf of Herba Rosmarini Officinalis of 8 parts Extract, cereuisiae fermentum part of 6 parts, the uva cell extract active component of 14 parts, add the wrinkle of 9 parts Ripple chondrus extract, the biological carbohydrate gum-1 of 6 parts, the beta glucan of 12 parts, the diglycerol of 5 parts, the Petiolus Trachycarpi of 4 parts Acyl tripeptides-1 and the essence of 6 parts, 700rpm/min stirring at low speed 25min, mix homogeneously, obtain based on the micro-glue of emulsifying The herbaceous plant nutritive water of capsule.

Embodiment 5:

(1) by weight, by the hydrogenated vegetable oil of 2 parts, the low erucic acid rapeseed oil of 3 parts, the poly-diformazan of ring five of 3 parts Radical siloxane, the polydimethylsiloxane of 2 parts, the phenyl trimethicone of 4 parts, the microwax of 4 parts and 4 parts Diglycerol mixing, 80 DEG C of heated and stirred are uniform, are incubated ultraviolet disinfection 20min, obtain oil phase.

(2) by weight, by the ethylene glycol of 8 parts, the propylene glycol of 4 parts, the glycine betaine of 10 parts, the carbamide of 6 parts, The polyglutamic acid sodium of 2 parts, the triethanolamine of 8 parts, the 1,2-hexanediol of 9 parts, the decoyl hydroximic acid of 6 parts, 7 parts 1,3-PD, the hexanediol of 5 parts add in the deionized water of 35 parts, and 90 DEG C of heated and stirred are uniform, are incubated ultraviolet Sterilizing 15min, obtains aqueous phase.

(3) by weight, oil phase step (1) prepared adds in aqueous phase prepared by step (2), and 90 DEG C add Temperature, 5000rpm/min homogenizing stirring 30min, then 1000rpm/min stirring at low speed 10min, add the spermaceti of 9 parts After the carbomer of alcohol ethylhexoate, the stearic acid of 12 parts and 10 parts, 5000rpm/min homogenizing stirs 30min again, then It is slowly added to the Cremophor RH40 of 10 parts and the chitosan microcapsules wall material of 15 parts, is cooled to 40 DEG C, add The Tremella extract of 12 parts, the Herba Centellae extract of 8 parts, the polygoni cuspidati,radix extract of 5 parts, the scutellariae,radix of 13 parts extract Thing, the Folium Camelliae sinensis extract of 14 parts, the Glycyrrhiza glabra L. root extract of 7 parts, the Flos Chrysanthemi extract of 5 parts, the fan of 7 parts change Herba Pelargonii Graveolentis extract, the cereuisiae fermentum of 8 parts, the uva cell extract active component of 9 parts, add the wrinkle of 8 parts Ripple chondrus extract, the biological carbohydrate gum-1 of 5 parts, the beta glucan of 8 parts, the diglycerol of 9 parts, the palmityl of 6 parts Tripeptides-1 and the essence of 8 parts, 1000rpm/min stirring at low speed 10min, mix homogeneously, obtain based on the micro-glue of emulsifying The herbaceous plant nutritive water of capsule.

Embodiment 6:

(1) by weight, by the hydrogenated vegetable oil of 1 part, the low erucic acid rapeseed oil of 4 parts, the poly-diformazan of ring five of 3 parts Radical siloxane, the polydimethylsiloxane of 3 parts, the phenyl trimethicone of 3 parts, the microwax of 4 parts and 4 parts Diglycerol mixing, 80 DEG C of heated and stirred are uniform, are incubated ultraviolet disinfection 20min, obtain oil phase.

(2) by weight, by the ethylene glycol of 8 parts, the propylene glycol of 8 parts, the glycine betaine of 8 parts, the carbamide of 4 parts, The polyglutamic acid sodium of 4 parts, the triethanolamine of 8 parts, the 1,2-hexanediol of 10 parts, the decoyl hydroximic acid of 8 parts, 7 parts 1,3-PD, the hexanediol of 8 parts add in the deionized water of 40 parts, and 80 DEG C of heated and stirred are uniform, are incubated ultraviolet Sterilizing 20min, obtains aqueous phase.

(3) by weight, oil phase step (1) prepared adds in aqueous phase prepared by step (2), and 80 DEG C add Temperature, 4000rpm/min homogenizing stirring 40min, then 800rpm/min stirring at low speed 20min, add the spermol of 8 parts After the carbomer of ethylhexoate, the stearic acid of 8 parts and 16 parts, 4000rpm/min homogenizing stirs 50min again, then delays The slow Cremophor RH40 adding 8 parts and the beta cyclodextrin of 8 parts and bud dextrin microcapsule wall material, be cooled to 40 DEG C, add the Tremella extract of 8 parts, the Herba Centellae extract of 88 parts, the polygoni cuspidati,radix extract of 8 parts, the Huang of 8 parts A kind of reed mentioned in ancient books root extract, the Folium Camelliae sinensis extract of 12 parts, the Glycyrrhiza glabra L. root extract of 6 parts, the Flos Chrysanthemi extract of 5 parts, 8 The rosemary leaf extract of part, the cereuisiae fermentum of 7 parts, the uva cell extract active component of 16 parts, then add Enter the Chondrus crispus extract of 8 parts, the biological carbohydrate gum-1 of 5 parts, the beta glucan of 8 parts, the diglycerol of 8 parts, 4 The palmityl tripeptides-1 of part and the essence of 4 parts, 1000rpm/min stirring at low speed 30min, mix homogeneously, obtain base Herbaceous plant nutritive water in emulsifying microcapsule.

After testing, the microcapsule of herbaceous plant nutritive water based on emulsifying microcapsule prepared by embodiment 1-6 particle diameter, The test of thermostability, tolerance to cold, skinfeel, antibiotic property, moisture retention, whitening result as follows:

As seen from the above table, herbaceous plant nutritive water stable uniformity based on emulsifying microcapsule prepared by the present invention, clearly Moisturizing, the most sticky, also there is moisturizing antibacterial, permanent and whitening effect.

The principle of above-described embodiment only illustrative present invention and effect thereof, not for limiting the present invention.Any ripe Above-described embodiment all can be modified under the spirit and the scope of the present invention or change by the personage knowing this technology Become.Therefore, art has usually intellectual such as without departing from disclosed spirit and technology All equivalences completed under thought are modified or change, and must be contained by the claim of the present invention.

Claims

null1. a herbaceous plant nutritive water based on emulsifying microcapsule，It is characterized in that，Described herbaceous plant nutritive water based on emulsifying microcapsule includes deionized water、Ethylene glycol、Propylene glycol、Glycine betaine、Carbamide、Polyglutamic acid sodium、Ring five polydimethylsiloxane、Polydimethylsiloxane、Phenyl trimethicone、Spermol ethylhexoate、Hydrogenated vegetable oil、Stearic acid、Low erucic acid rapeseed oil、Microwax、Allantoin、Chondrus crispus extract、Biological carbohydrate gum-1、Diglycerol、Palmityl tripeptides-1、Beta glucan、Tremella extract、Herba Centellae extract、Polygoni cuspidati,radix extract、Scutellariae,radix extract、Folium Camelliae sinensis extract、Glycyrrhiza glabra L. root extract、Flos Chrysanthemi extract、Rosemary leaf extract、Carbomer、Triethanolamine、1,2-hexanediol、Decoyl hydroximic acid、1,Ammediol、Hexanediol、Cereuisiae fermentum、Uva cell extract、Cremophor RH40 and daily essence.
nullA kind of herbaceous plant nutritive water based on emulsifying microcapsule the most according to claim 1，It is characterized in that，The component of described herbaceous plant nutritive water based on emulsifying microcapsule is by weight，Including: deionized water 35-45 part、Ethylene glycol 5-8 part、Propylene glycol 4-9 part、Glycine betaine 5-10 part、Carbamide 3-6 part、Polyglutamic acid sodium 2-5 part、Ring five polydimethylsiloxane 1-3 part、Polydimethylsiloxane 2-5 part、Phenyl trimethicone 3-4 part、Spermol ethylhexoate 6-9 part、Hydrogenated vegetable oil 1-2 part、Stearic acid 8-12 part、Low erucic acid rapeseed oil 3-7 part、Microwax 2-4 part、Allantoin 3-5 part、Chondrus crispus extract 8-13 part、Biological carbohydrate gum-15-7 part、Diglycerol 4-9 part、Palmityl tripeptides-13-6 part、Beta glucan 8-15 part、Tremella extract 6-12 part、Herba Centellae extract 4-8 part、Polygoni cuspidati,radix extract 5-9 part、Scutellariae,radix extract 7-13 part、Folium Camelliae sinensis extract 8-14 part、Glycyrrhiza glabra L. root extract 3-7 part、Flos Chrysanthemi extract 5-10 part、Rosemary leaf extract 7-14 part、Carbomer 10-16 part、Triethanolamine 4-8 part、1,2-hexanediol 9-10 part、Decoyl hydroximic acid 6-8 part、1,Ammediol 7-10 part、Hexanediol 5-8 part、Cereuisiae fermentum 5-8 part、Uva cell extract 9-16 part、Cremophor RH40 5-10 part and daily essence 3-8 part.
A kind of herbaceous plant nutritive water based on emulsifying microcapsule the most according to claim 1, it is characterized in that, described herbaceous plant nutritive water based on emulsifying microcapsule also includes microcapsule, described microcapsule includes core and wall material, described wall material is made up of beta cyclodextrin and bud dextrin, and described core includes Tremella extract, Herba Centellae extract, polygoni cuspidati,radix extract, scutellariae,radix extract, Folium Camelliae sinensis extract, Glycyrrhiza glabra L. root extract, Flos Chrysanthemi extract, rosemary leaf extract, cereuisiae fermentum and uva cell extract active component.
4. the preparation method of a herbaceous plant nutritive water based on emulsifying microcapsule, it is characterised in that: comprise the following steps:

(1) hydrogenated vegetable oil, low erucic acid rapeseed oil, ring five polydimethylsiloxane, polydimethylsiloxane, phenyl trimethicone, microwax and diglycerol being mixed, 70-80 DEG C of heated and stirred is uniform, and insulated sterilizing 15-20min obtains oil phase；

(2) by ethylene glycol, propylene glycol, glycine betaine, carbamide, polyglutamic acid sodium, triethanolamine, 1,2-hexanediol, decoyl hydroximic acid, 1,3-PD, hexanediol add in deionized water, and 80-90 DEG C of heated and stirred is uniform, insulated sterilizing 15-20min, obtains aqueous phase；

(3) oil phase step (1) prepared adds in aqueous phase prepared by step (2), 80-90 DEG C of homogenizing of heating stirs stirring at low speed again, add spermol ethylhexoate, stearic acid, homogenizing stirring again after carbamide and carbomer, it is slow added into Cremophor RH40 and microcapsule wall material, it is cooled to 35-40 DEG C, add Tremella extract, Herba Centellae extract, polygoni cuspidati,radix extract, scutellariae,radix extract, Folium Camelliae sinensis extract, Glycyrrhiza glabra L. root extract, Flos Chrysanthemi extract, rosemary leaf extract, cereuisiae fermentum and uva cell extract active component, add Chondrus crispus extract, biological carbohydrate gum-1, beta glucan, diglycerol, palmityl tripeptides-1 and essence, stirring at low speed mix homogeneously, obtain herbaceous plant nutritive water based on emulsifying microcapsule.
The preparation method of a kind of herbaceous plant nutritive water based on emulsifying microcapsule the most according to claim 4, it is characterised in that: in described step (1) or step (2), insulated sterilizing is ultraviolet disinfection.
The preparation method of a kind of herbaceous plant nutritive water based on emulsifying microcapsule the most according to claim 4, it is characterised in that: in described step (3), the rotating speed of homogenizing stirring is 3500-5000rpm/min, and the time is 30-50min.
The preparation method of a kind of herbaceous plant nutritive water based on emulsifying microcapsule the most according to claim 4, it is characterised in that: in described step (3), the rotating speed of stirring at low speed is 500-1000rpm/min, and the time is 10-30min.
The preparation method of a kind of herbaceous plant nutritive water based on emulsifying microcapsule the most according to claim 4, it is characterised in that: in described step (3), in herbaceous plant nutritive water based on emulsifying microcapsule, the particle diameter of microcapsule is 1-2 μm.
The preparation method of a kind of herbaceous plant nutritive water based on emulsifying microcapsule the most according to claim 1, it is characterised in that: in described step (3), microcapsule wall material can also be chitosan, sodium alginate.