CN106176450A - A kind of plant biological source nanospray nursing eye glue and preparation method thereof - Google Patents
A kind of plant biological source nanospray nursing eye glue and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/042—Gels
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
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- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/88—Polyamides
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
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- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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- A61K2800/21—Emulsions characterized by droplet sizes below 1 micron
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
Abstract
The present invention provides a kind of plant biological source nanospray nursing eye glue to specifically include that Aesculus hippocastanum L. seed extract, XIAOMIJIAO berry extract, Fructus Citri grandis extract, uva extract, Tremella extract, Herba Centellae extract, polygoni cuspidati,radix extract, scutellariae,radix extract, Folium Camelliae sinensis extract, Glycyrrhiza glabra L. root extract, Flos Chrysanthemi extract, rosemary leaf extract and Herba portulacae extract mixtures, acetyl group hexapeptide 8, palmityl tripeptides 1, Chondrus crispus, beta glucan, biological carbohydrate gum 1, methyl-monosilane alcohol hydroxyproline ester aspartic acid, dimethyldisilane alcohol hyaluronic acid ester and cereuisiae fermentum mixture, and other auxiliary agents.Nursing eye glue prepared by the present invention uses microwave distillation condensation extractive technique, cladding and nanospray technology to combine and prepare the comprehensive care eye glue that absorbance is good.
Description
Technical field
The invention belongs to daily cosmetics technical field, be specifically related to a kind of plant biological source nanospray nursing eye glue and
Its preparation method.
Background technology
Along with the quickening day by day of contemporary work rhythm of life, and the going from bad to worse of work living environment, people are to self
Cleaning with maintenance increasingly pay close attention to.The skin of eye makes one of skin that human body is the thinnest, and the thickness on the top layer of eye part skin is only
/ to five/3rds of hi skin of face thickness, and, the skin around eyelid does not contains sebum, elastin laminin and glue
The protection of former albumen, the muscle of circumference of eyes to be blinked up to ten thousand times every day in addition, and therefore, the skin of eye is particularly easy to fatigue,
Dimness, old and feeble, lose elasticity, the eye problems such as black eye, eye pouch, microgroove, edema, fat granule occur.
For the skin nursing products of circumference of eyes, kind on the market is the most varied.Chinese patent CN
A kind of anti-black eye lipid nanoparticle emulsion and preparation method thereof disclosed in 102772338B, this product includes that olibanoresin extracts
Thing, Aesculus hippocastanum L. seed extract, the mixture of tetrahydrochysene piperine, stearic acid monoglycerides or Vegetable oil lipoprotein or stearic acid monoglycerides
With the mixture of Vegetable oil lipoprotein, lecithin and polyglyceryl fatty acid ester, sucrose stearate, aliphatic alcohol polyether, anhydrous sorbitol
Fatty acid ester, the emulsifying agent of polyoxyethylene ether sorbitan fatty acid ester and preservative, main functional component is for be wrapped simultaneously
Three kinds of active component of envelope, and particle diameter is nanoscale, can increase the absorbance of skin, dispersibility and good stability.China is specially
One disclosed in profit CN 103494752A is used for improving black-eyed roe elite eye cream, and this roe elite eye cream comprises Acipenser Sinensis
Sub-elite, vitamin E, vitamin C, pantothenylol, strong aspartic acid, butchers broom root extract, Herba Centellae extract and Sargassum are extracted
Thing, utilizes sturgeon roe living cells elite and active components of plants and injection Vitamin B_6, reaches to remove black eye, remove eyeprint, supplements glue
Effect of former albumen.
From above-mentioned prior art, mostly current existing eyeware products and solution for lenses and contact lenses is bio-extract, plant extract
Simply carry out formula, and the simple effective ingredient relying on functional materials acts on eye skin, and according to crowd's eye
The difference of the myoplasm of skin, the consumption of effective ingredient is difficult to hold, and the many meetings of effective ingredient amount cause fat granule, and effective ingredient amount is few
It is difficult to again reach nursing efficacy.Applicant of the present invention by comprehensive utilization various plants effective ingredient and biological effective components,
Coordinating nanometer cladding and atomization technique, play synergism between the two, utilize on product structure is functional, prepares a
Eye comprehensive care product.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of plant biological source nanospray nursing eye glue and preparation side thereof
Method, selects Aesculus hippocastanum L. seed, XIAOMIJIAO fruit, Fructus Citri grandis, uva, Tremella, Herba Centellae, polygoni cuspidati,radix, scutellariae,radix, Folium Camelliae sinensis, light fruit
Licorice, Flos Chrysanthemi, leaf of Herba Rosmarini Officinalis and Herba portulacae, as plant source, are combined with biogenic extract, at nanospray device
Reason forms plant biological source nanospray nursing eye glue.Eye part skin can comprehensively be protected by nursing eye glue prepared by the method
Reason, and beneficially eye part skin absorbs, functional good, have no side effect.
For solving above-mentioned technical problem, the technical scheme is that
A kind of plant biological source nanospray nursing eye glue, it is characterised in that described plant biological source nanospray is nursed
Eye glue includes following components:
Component A: Aesculus hippocastanum L. seed extract, XIAOMIJIAO berry extract, Fructus Citri grandis extract, uva extract, Tremella
Extract, Herba Centellae extract, polygoni cuspidati,radix extract, scutellariae,radix extract, Folium Camelliae sinensis extract, Glycyrrhiza glabra L. root extract, mother
Flos Chrysanthemi extract, rosemary leaf extract and Herba portulacae extract;
B component: Argireline, palmityl tripeptides-1, Chondrus crispus, beta glucan, biological carbohydrate gum-1, methyl silicon
Alkanol hydroxyproline ester aspartic acid, dimethyldisilane alcohol hyaluronic acid ester and cereuisiae fermentum;
C component: Cremophor ELP, PEG-40 Oleum Ricini, plant sterol, carbomer, ascorbic acid methyl-monosilane alcohol fruit
Glue acid esters, hydroxyethyl cellulose, carbamide and allantoin;
D component: butanediol, propylene glycol, diglycerol, PEG-4000, glycine betaine, nicotiamide, polyglutamic acid sodium, three second
Hydramine, 1,2-hexanediol, decoyl hydroximic acid, 1,3-propylene glycol, hexanediol and deionized water.
Preferred as technique scheme, nanospray nursing eye glue in described plant biological source is colloid substance, also may be used
To comprise preservative and essence.
Preferred as technique scheme, the mass ratio of described component A, B component, C component and D component is 15-30:5-
20:20-30:30-50.
Preferred as technique scheme, the component in described component A, by weight, and including: Aesculus hippocastanum L. seed
Extract 5-12 part, XIAOMIJIAO berry extract 3-9 part, Fructus Citri grandis extract 4-10 part, uva extract 2-5 part, Tremella extract
Thing 3-6 part, Herba Centellae extract 4-8 part, polygoni cuspidati,radix extract 2-6 part, scutellariae,radix extract 1-4 part, Folium Camelliae sinensis extract 1-3
Part, Glycyrrhiza glabra L. root extract 1-4 part, Flos Chrysanthemi extract 2-4 part, rosemary leaf extract 1-3 part and Herba portulacae extract
1-3 part.
Preferred as technique scheme, the component in described B component, by weight, and including: Argireline
3-10 part, palmityl tripeptides-1 2-8 part, Chondrus crispus 3-6 part, beta glucan 2-7 part, biological carbohydrate gum-1 3-8 part, methyl
Silanol hydroxyproline ester aspartic acid 4-5 part, dimethyldisilane alcohol hyaluronic acid ester 2-6 part and cereuisiae fermentum 3-7
Part.
Preferred as technique scheme, the component in described C component, by weight, and including: carbomer 10-15
Part, hydroxyethyl cellulose 8-12 part, carbamide 3-7 part, allantoin 5-12 part, Cremophor ELP 1-3 part, PEG-40 Oleum Ricini 2-
5 parts, plant sterol 4-10 part, ascorbic acid methyl-monosilane alcohol pectate 5-8 part.
Preferred as technique scheme, the component in described D component, by weight, and including: butanediol 5-10
Part, propylene glycol 2-7 part, diglycerol 3-6 part, PEG-4000 4-8 part, glycine betaine 4-8 part, nicotiamide 3-6 part, polyglutamic
Acid sodium 5-7 part, triethanolamine 4-9 part, 1,2-hexanediol 3-7 part, decoyl hydroximic acid 2-5 part, 1,3-propylene glycol 1-5 part, oneself two
Alcohol 2-5 part, deionized water 50-80 part.
The present invention also provides for the preparation method of a kind of plant biological source nanospray nursing eye glue, it is characterised in that: include
Following steps:
(1) by Aesculus hippocastanum L. seed, XIAOMIJIAO fruit, Fructus Citri grandis, uva, Tremella, Herba Centellae, polygoni cuspidati,radix, scutellariae,radix, tea
Leaf, Glycyrrhiza glabra L. root, Flos Chrysanthemi, leaf of Herba Rosmarini Officinalis and Herba portulacae are cleaned and are dried, and are placed in microwave device by masking foil cladding, microwave
Radiation 5-10min, after taking out cooling, shreds, and immerses in ethanol water solvent, adds thermal distillation condensation, takes plant distillate, by plant
Distillate is concentrated to give component A;
(2) by Cremophor ELP, PEG-40 Oleum Ricini, plant sterol, carbomer, ascorbic acid methyl-monosilane alcohol pectin
Acid esters, hydroxyethyl cellulose, carbamide and allantoin add in deionized water, are quickly stirred until homogeneous formation colloid substance, instill
Component A prepared by step (1), stirring forms functional colloid substance;
(3) by butanediol, propylene glycol, diglycerol, PEG-4000, glycine betaine, nicotiamide, polyglutamic acid sodium, three second
Hydramine, 1,2-hexanediol, decoyl hydroximic acid, 1,3-PD, hexanediol add in deionized water, are sufficiently mixed, and form carrier
Solution;
(4) functional colloid substance prepared by step (2) and Argireline, palmityl tripeptides-1, ripple angle fork
Dish, beta glucan, biological carbohydrate gum-1, methyl-monosilane alcohol hydroxyproline ester aspartic acid, dimethyldisilane alcohol hyaluronic acid
Ester and cereuisiae fermentum, homogenizing stirs, and forms function solution;
(5) function solution step (4) prepared loads in device for atomizing liquid, and the atomization of function solution is entered step
(3) in the carrier solution prepared, mix homogeneously, stand, obtain plant biological source nanospray nursing eye glue.
As in the preferred described step (2) of technique scheme, in functional colloid substance, component A is by colloid substance bag
Cover.
As in the preferred described step (5) of technique scheme, the atomizing particle size of function solution is micro/nano level.
Compared with prior art, the method have the advantages that
(1) plant source in prepared by the present invention plant biological source nanospray nursing eye glue is Aesculus hippocastanum L. seed, little
Meter Jiao Guo, Fructus Citri grandis, uva, Tremella, Herba Centellae, polygoni cuspidati,radix, scutellariae,radix, Folium Camelliae sinensis, Glycyrrhiza glabra L. root, Flos Chrysanthemi, leaf of Herba Rosmarini Officinalis
And Herba portulacae, wherein Aesculus hippocastanum L., leaf of Herba Rosmarini Officinalis can promote the circulation of skin, eliminate eye pouch, and Herba Centellae, Tremella can be mended
Filling collagen protein, dispel microgroove, polygoni cuspidati,radix, Folium Camelliae sinensis, Glycyrrhiza glabra L. root, Flos Chrysanthemi can be with antioxidation, whitening, eliminate black eye,
Bright color, scutellariae,radix and Herba portulacae extract can be with anti-inflammations, and XIAOMIJIAO fruit and Fructus Citri grandis can promote the new old generation of skin
Thank, make skin rejuvenate, pore refining.The skin of eye can be entered by the plant source effective ingredient therefore contained in the present invention
Row comprehensive care, solves the Varied problems such as eye skin black eye, eye pouch, microgroove, colour of skin dimness, and composition is all natural goods
Matter, environmental protection, nontoxic non-stimulated to skin.
(2) biogenic in the plant biological source nanospray nursing eye glue that prepared by the present invention is Argireline, palm fibre
Palmitic acid acyl tripeptides-1, Chondrus crispus, beta glucan, biological carbohydrate gum-1, methyl-monosilane alcohol hydroxyproline ester aspartic acid, diformazan
Base disilane alcohol hyaluronic acid ester and cereuisiae fermentum, can supplement the collagen protein of eye part skin, moisturizing lock water, improve skin
Immunity, make skin gloss water tender high-elastic.
(3) the plant biological source nanospray nursing eye glue that prepared by the present invention uses by carbomer and hydroxyethyl cellulose
Botanical components is coated with by the colloid substance prepared Deng raw material, is coated togather by various plants source material, has colloid
The structure alternately existed with plant source effective ingredient, carries out alternating action to eye part skin, makes the absorption that eye part skin can be releived,
And use nanospray technology, plant source and biogenic effective ingredient are prepared as micro-nano colloidal particle, disperse uniformly
In eye glue, make nanospray nursing eye glue not only absorbance high, and free of a burden to skin, fat granule will not be formed.
(4) additionally, in the plant biological source nanospray nursing eye glue prepared of the present invention plant source effective ingredient use micro-
Wave technology combines with distillation condensation technology, improves the extraction ratio of plant source effective ingredient, and efficiency is high, preparation method letter
Single.
Detailed description of the invention
The present invention is described in detail, in illustrative examples and the explanation of this present invention below in conjunction with specific embodiment
It is used for explaining the present invention, but not as a limitation of the invention.
Embodiment 1:
(1) by Aesculus hippocastanum L. seed, XIAOMIJIAO fruit, Fructus Citri grandis, uva, Tremella, Herba Centellae, polygoni cuspidati,radix, scutellariae,radix, tea
Leaf, Glycyrrhiza glabra L. root, Flos Chrysanthemi, leaf of Herba Rosmarini Officinalis and Herba portulacae are cleaned and are dried, and are placed in microwave device by masking foil cladding, microwave
Radiation 5-10min, after taking out cooling, shreds, is 1g:5ml by solid-liquid ratio, immerses in the ethanol water solvent of 60%, adds thermal distillation
Condensation, takes plant distillate, plant distillate is concentrated to give the component A that mass fraction of solids is 15%.Wherein, component A
Composition, by weight, Aesculus hippocastanum L. seed extract 5 parts, XIAOMIJIAO berry extract 3 parts, Fructus Citri grandis extract 4 parts, uva
Extract 2 parts, Tremella extract 3 parts, Herba Centellae extract 4 parts, polygoni cuspidati,radix extract 2 parts, scutellariae,radix extract 1 part, Folium Camelliae sinensis
Extract 1 part, Glycyrrhiza glabra L. root extract 1 part, Flos Chrysanthemi extract 2 parts, rosemary leaf extract 1 part and Herba portulacae extract
1 part.
(2) by weight, by carbomer 10 parts, hydroxyethyl cellulose 8 parts, 3 parts of carbamide, allantoin 5 parts, PEG-35 castor
Going of 1 part of Oleum Sesami, PEG-40 Oleum Ricini 2 parts, plant sterol 4 parts, ascorbic acid methyl-monosilane alcohol pectate 5 parts addition 50 parts
In ionized water, quickly it is stirred until homogeneous formation colloid substance, is C component.
(3) by butanediol 5 parts, propylene glycol 2 parts, diglycerol 3 parts, PEG-4000 4 parts, glycine betaine 4 parts, nicotiamide 3
Part, 5 parts of polyglutamic acid sodium, triethanolamine 4 parts, 1,2-hexanediol 3 parts, decoyl hydroximic acid 2 parts, 1,3-propylene glycol 1 part, hexanediol
2 parts add in deionized water 50 parts, are sufficiently mixed, and form carrier solution, i.e. D component.
(4) by Argireline 3 parts, palmityl tripeptides-1 2 part, Chondrus crispus 3 parts, beta glucan 2 parts, biology
Carbohydrate gum-1 3 part, methyl-monosilane alcohol hydroxyproline ester aspartic acid 4 parts, dimethyldisilane alcohol hyaluronic acid ester 2 parts and beer
Brewer yeast bacterium 3 parts is mixed to form B component.
(5) by weight, will instill the component A of 15 parts in the C component of 20 parts, stirring, component A is coated with by C component, shape
Functional colloid substance, by functional colloid substance and the B component of 30 parts, homogenizing stirs, and forms function solution, and function is molten
Liquid loads in device for atomizing liquid, is entered by function solution mist chemical conversion micro/nano level granule in the D component of 30 parts, mix homogeneously,
Stand, obtain plant biological source nanospray nursing eye glue.
Embodiment 2:
(1) by Aesculus hippocastanum L. seed, XIAOMIJIAO fruit, Fructus Citri grandis, uva, Tremella, Herba Centellae, polygoni cuspidati,radix, scutellariae,radix, tea
Leaf, Glycyrrhiza glabra L. root, Flos Chrysanthemi, leaf of Herba Rosmarini Officinalis and Herba portulacae are cleaned and are dried, and are placed in microwave device by masking foil cladding, microwave
Radiation 5-10min, after taking out cooling, shreds, is 1g:10ml by solid-liquid ratio, immerses in the ethanol water solvent of 80%, adds thermal distillation
Condensation, takes plant distillate, plant distillate is concentrated to give the component A that mass fraction of solids is 25%.Wherein, component A
Composition, by weight, Aesculus hippocastanum L. seed extract 12 parts, XIAOMIJIAO berry extract 9 parts, Fructus Citri grandis extract 10 parts, Fructus Vitis viniferae
Berry extract 5 parts, Tremella extract 6 parts, Herba Centellae extract 8 parts, polygoni cuspidati,radix extract 6 parts, scutellariae,radix extract 4 parts, tea
Leaf extract 3 parts, Glycyrrhiza glabra L. root extract 4 parts, Flos Chrysanthemi extract 4 parts, rosemary leaf extract 3 parts and Herba portulacae extract
Thing 3 parts.
(2) by weight, by carbomer 15 parts, hydroxyethyl cellulose 12 parts, 7 parts of carbamide, allantoin 12 parts, PEG-35
Oleum Ricini 3 parts, PEG-40 Oleum Ricini 5 parts, plant sterol 10 parts, ascorbic acid methyl-monosilane alcohol pectate 8 parts add 80 parts
Deionized water in, be quickly stirred until homogeneous formation colloid substance, be C component.
(3) by butanediol 10 parts, propylene glycol 7 parts, diglycerol 6 parts, PEG-4000 8 parts, glycine betaine 8 parts, nicotiamide
6 parts, 7 parts of polyglutamic acid sodium, triethanolamine 9 parts, 1,2-hexanediol 7 parts, decoyl hydroximic acid 5 parts, 1,3-propylene glycol 5 parts, oneself two
Alcohol 5 parts adds in deionized water 80 parts, is sufficiently mixed, and forms carrier solution, i.e. D component.
(4) by Argireline 10 parts, palmityl tripeptides-1 8 part, Chondrus crispus 6 parts, beta glucan 7 parts, life
Thing carbohydrate gum-18 parts, methyl-monosilane alcohol hydroxyproline ester aspartic acid 5 parts, dimethyldisilane alcohol hyaluronic acid ester 6 parts and beer
Brewer yeast bacterium 7 parts is mixed to form B component.
(5) by weight, will instill the component A of 30 parts in the C component of 30 parts, stirring, component A is coated with by C component, shape
Functional colloid substance, by functional colloid substance and the B component of 50 parts, homogenizing stirs, and forms function solution, and function is molten
Liquid loads in device for atomizing liquid, is entered by function solution mist chemical conversion micro/nano level granule in the D component of 50 parts, mix homogeneously,
Stand, obtain plant biological source nanospray nursing eye glue.
Embodiment 3:
(1) by Aesculus hippocastanum L. seed, XIAOMIJIAO fruit, Fructus Citri grandis, uva, Tremella, Herba Centellae, polygoni cuspidati,radix, scutellariae,radix, tea
Leaf, Glycyrrhiza glabra L. root, Flos Chrysanthemi, leaf of Herba Rosmarini Officinalis and Herba portulacae are cleaned and are dried, and are placed in microwave device by masking foil cladding, microwave
Radiation 7min, after taking out cooling, shreds, is 1g:8ml by solid-liquid ratio, immerses in the ethanol water solvent of 70%, adds thermal distillation cold
Solidifying, take plant distillate, plant distillate is concentrated to give the component A that mass fraction of solids is 20%.Wherein, the group of component A
Becoming, by weight, Aesculus hippocastanum L. seed extract 8 parts, XIAOMIJIAO berry extract 6 parts, Fructus Citri grandis extract 7 parts, uva carry
Take thing 3 parts, Tremella extract 4 parts, Herba Centellae extract 6 parts, polygoni cuspidati,radix extract 4 parts, scutellariae,radix extract 3 parts, Folium Camelliae sinensis carry
Take thing 2 parts, Glycyrrhiza glabra L. root extract 2 parts, Flos Chrysanthemi extract 3 parts, rosemary leaf extract 2 parts and Herba portulacae extract 2
Part.
(2) by weight, by carbomer 12 parts, hydroxyethyl cellulose 10 parts, 5 parts of carbamide, allantoin 7 parts, PEG-35
Oleum Ricini 2 parts, PEG-40 Oleum Ricini 3 parts, plant sterol 6 parts, ascorbic acid methyl-monosilane alcohol pectate 6 parts add 70 parts
In deionized water, quickly it is stirred until homogeneous formation colloid substance, is C component.
(3) by butanediol 7 parts, propylene glycol 4 parts, diglycerol 4 parts, PEG-4000 6 parts, glycine betaine 5 parts, nicotiamide 4
Part, 6 parts of polyglutamic acid sodium, triethanolamine 6 parts, 1,2-hexanediol 4 parts, decoyl hydroximic acid 3 parts, 1,3-propylene glycol 3 parts, hexanediol
3 parts add in deionized water 60 parts, are sufficiently mixed, and form carrier solution, i.e. D component.
(4) by Argireline 5 parts, palmityl tripeptides-1 4 part, Chondrus crispus 4 parts, beta glucan 4 parts, biology
Carbohydrate gum-1 6 part, methyl-monosilane alcohol hydroxyproline ester aspartic acid 4 parts, dimethyldisilane alcohol hyaluronic acid ester 3 parts and beer
Brewer yeast bacterium 4 parts is mixed to form B component.
(5) by weight, will instill the component A of 25 parts in the C component of 25 parts, stirring, component A is coated with by C component, shape
Functional colloid substance, by functional colloid substance and the B component of 40 parts, homogenizing stirs, and forms function solution, and function is molten
Liquid loads in device for atomizing liquid, is entered by function solution mist chemical conversion micro/nano level granule in the D component of 45 parts, mix homogeneously,
Stand, obtain plant biological source nanospray nursing eye glue.
Embodiment 4:
(1) by Aesculus hippocastanum L. seed, XIAOMIJIAO fruit, Fructus Citri grandis, uva, Tremella, Herba Centellae, polygoni cuspidati,radix, scutellariae,radix, tea
Leaf, Glycyrrhiza glabra L. root, Flos Chrysanthemi, leaf of Herba Rosmarini Officinalis and Herba portulacae are cleaned and are dried, and are placed in microwave device by masking foil cladding, microwave
Radiation 10min, after taking out cooling, shreds, is 1g:5ml by solid-liquid ratio, immerses in the ethanol water solvent of 75%, adds thermal distillation cold
Solidifying, take plant distillate, plant distillate is concentrated to give the component A that mass fraction of solids is 15%.Wherein, the group of component A
Becoming, by weight, Aesculus hippocastanum L. seed extract 10 parts, XIAOMIJIAO berry extract 4 parts, Fructus Citri grandis extract 8 parts, uva carry
Take thing 3 parts, Tremella extract 4 parts, Herba Centellae extract 6 parts, polygoni cuspidati,radix extract 3 parts, scutellariae,radix extract 2 parts, Folium Camelliae sinensis carry
Take thing 2 parts, Glycyrrhiza glabra L. root extract 3 parts, Flos Chrysanthemi extract 2 parts, rosemary leaf extract 1 part and Herba portulacae extract 1
Part.
(2) by weight, by carbomer 12 parts, hydroxyethyl cellulose 10 parts, 4 parts of carbamide, allantoin 8 parts, PEG-35
Oleum Ricini 2 parts, PEG-40 Oleum Ricini 2 parts, plant sterol 5 parts, ascorbic acid methyl-monosilane alcohol pectate 7 parts add 75 parts
In deionized water, quickly it is stirred until homogeneous formation colloid substance, is C component.
(3) by butanediol 8 parts, propylene glycol 3 parts, diglycerol 4 parts, PEG-4000 5 parts, glycine betaine 5 parts, nicotiamide 5
Part, 5 parts of polyglutamic acid sodium, triethanolamine 5 parts, 1,2-hexanediol 5 parts, decoyl hydroximic acid 5 parts, 1,3-propylene glycol 5 parts, hexanediol
5 parts add in deionized water 50 parts, are sufficiently mixed, and form carrier solution, i.e. D component.
(4) by Argireline 7 parts, palmityl tripeptides-1 7 part, Chondrus crispus 3 parts, beta glucan 7 parts, biology
Carbohydrate gum-17 parts, methyl-monosilane alcohol hydroxyproline ester aspartic acid 5 parts, dimethyldisilane alcohol hyaluronic acid ester 5 parts and medicated beer
5 parts of yeast is mixed to form B component.
(5) by weight, will instill the component A of 15 parts in the C component of 30 parts, stirring, component A is coated with by C component, shape
Functional colloid substance, by functional colloid substance and the B component of 30 parts, homogenizing stirs, and forms function solution, and function is molten
Liquid loads in device for atomizing liquid, is entered by function solution mist chemical conversion micro/nano level granule in the D component of 30 parts, mix homogeneously,
Stand, obtain plant biological source nanospray nursing eye glue.
Embodiment 5:
(1) by Aesculus hippocastanum L. seed, XIAOMIJIAO fruit, Fructus Citri grandis, uva, Tremella, Herba Centellae, polygoni cuspidati,radix, scutellariae,radix, tea
Leaf, Glycyrrhiza glabra L. root, Flos Chrysanthemi, leaf of Herba Rosmarini Officinalis and Herba portulacae are cleaned and are dried, and are placed in microwave device by masking foil cladding, microwave
Radiation 5-10min, after taking out cooling, shreds, is 1g:7ml by solid-liquid ratio, immerses in the ethanol water solvent of 65%, adds thermal distillation
Condensation, takes plant distillate, plant distillate is concentrated to give the component A that mass fraction of solids is 25%.Wherein, component A
Composition, by weight, Aesculus hippocastanum L. seed extract 12 parts, XIAOMIJIAO berry extract 5 parts, Fructus Citri grandis extract 4 parts, uva
Extract 3 parts, Tremella extract 4 parts, Herba Centellae extract 5 parts, polygoni cuspidati,radix extract 3 parts, scutellariae,radix extract 3 parts, Folium Camelliae sinensis
Extract 3 parts, Glycyrrhiza glabra L. root extract 1 part, Flos Chrysanthemi extract 3 parts, rosemary leaf extract 1 part and Herba portulacae extract
2 parts.
(2) by weight, by carbomer 13 parts, hydroxyethyl cellulose 10 parts, 4 parts of carbamide, allantoin 8 parts, PEG-35
Oleum Ricini 2 parts, PEG-40 Oleum Ricini 4 parts, plant sterol 7 parts, ascorbic acid methyl-monosilane alcohol pectate 6 parts add 70 parts
In deionized water, quickly it is stirred until homogeneous formation colloid substance, is C component.
(3) by butanediol 10 parts, propylene glycol 5 parts, diglycerol 4 parts, PEG-4000 4 parts, glycine betaine 5 parts, nicotiamide
6 parts, 7 parts of polyglutamic acid sodium, triethanolamine 8 parts, 1,2-hexanediol 7 parts, decoyl hydroximic acid 4 parts, 1,3-propylene glycol 3 parts, oneself two
Alcohol 2 parts adds in deionized water 75 parts, is sufficiently mixed, and forms carrier solution, i.e. D component.
(4) by Argireline 3 parts, palmityl tripeptides-1 4 part, Chondrus crispus 5 parts, beta glucan 6 parts, biology
Carbohydrate gum-1 7 part, methyl-monosilane alcohol hydroxyproline ester aspartic acid 4 parts, dimethyldisilane alcohol hyaluronic acid ester 5 parts and beer
Brewer yeast bacterium 6 parts is mixed to form B component.
(5) by weight, will instill the component A of 24 parts in the C component of 28 parts, stirring, component A is coated with by C component, shape
Functional colloid substance, by functional colloid substance and the B component of 42 parts, homogenizing stirs, and forms function solution, and function is molten
Liquid loads in device for atomizing liquid, is entered by function solution mist chemical conversion micro/nano level granule in the D component of 45 parts, mix homogeneously,
Stand, obtain plant biological source nanospray nursing eye glue.
Embodiment 6:
(1) by Aesculus hippocastanum L. seed, XIAOMIJIAO fruit, Fructus Citri grandis, uva, Tremella, Herba Centellae, polygoni cuspidati,radix, scutellariae,radix, tea
Leaf, Glycyrrhiza glabra L. root, Flos Chrysanthemi, leaf of Herba Rosmarini Officinalis and Herba portulacae are cleaned and are dried, and are placed in microwave device by masking foil cladding, microwave
Radiation 5-10min, after taking out cooling, shreds, is 1g:6ml by solid-liquid ratio, immerses in the ethanol water solvent of 80%, adds thermal distillation
Condensation, takes plant distillate, plant distillate is concentrated to give the component A that mass fraction of solids is 17%.Wherein, component A
Composition, by weight, Aesculus hippocastanum L. seed extract 7 parts, XIAOMIJIAO berry extract 6 parts, Fructus Citri grandis extract 8 parts, uva
Extract 3 parts, Tremella extract 4 parts, Herba Centellae extract 5 parts, polygoni cuspidati,radix extract 3 parts, scutellariae,radix extract 3 parts, Folium Camelliae sinensis
Extract 2 parts, Glycyrrhiza glabra L. root extract 2 parts, Flos Chrysanthemi extract 3 parts, rosemary leaf extract 2 parts and Herba portulacae extract
1 part.
(2) by weight, by carbomer 12 parts, hydroxyethyl cellulose 10 parts, 4 parts of carbamide, allantoin 8 parts, PEG-35
Oleum Ricini 2 parts, PEG-40 Oleum Ricini 4 parts, plant sterol 8 parts, ascorbic acid methyl-monosilane alcohol pectate 7 parts add 70 parts
In deionized water, quickly it is stirred until homogeneous formation colloid substance, is C component.
(3) by butanediol 8 parts, propylene glycol 5 parts, diglycerol 3 parts, PEG-4000 5 parts, glycine betaine 5 parts, nicotiamide 4
Part, 6 parts of polyglutamic acid sodium, triethanolamine 8 parts, 1,2-hexanediol 4 parts, decoyl hydroximic acid 4 parts, 1,3-propylene glycol 3 parts, hexanediol
3 parts add in deionized water 60 parts, are sufficiently mixed, and form carrier solution, i.e. D component.
(4) by Argireline 4 parts, palmityl tripeptides-1 6 part, Chondrus crispus 5 parts, beta glucan 4 parts, biology
Carbohydrate gum-1 5 part, methyl-monosilane alcohol hydroxyproline ester aspartic acid 5 parts, dimethyldisilane alcohol hyaluronic acid ester 5 parts and beer
Brewer yeast bacterium 6 parts is mixed to form B component.
(5) by weight, will instill the component A of 20 parts in the C component of 30 parts, stirring, component A is coated with by C component, shape
Functional colloid substance, by functional colloid substance and the B component of 40 parts, homogenizing stirs, and forms function solution, and function is molten
Liquid loads in device for atomizing liquid, is entered by function solution mist chemical conversion micro/nano level granule in the D component of 50 parts, mix homogeneously,
Stand, obtain plant biological source nanospray nursing eye glue.
After testing, the plant biological source nanospray nursing whitening of eye glue that prepared by embodiment 1-6, moisturizing, antibacterial, dispel black
Eyelet, eyeprint of dispelling, dispel eye pouch and fat granule result as follows:
Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Embodiment 6 | |
Free radical scavenging activity (%) | 46.5 | 52.3 | 50.1 | 51.2 | 50.7 | 52.4 |
Use the moisturizing rate (%) after 1h | 74.2 | 75.6 | 77.0 | 72.4 | 73.9 | 75.2 |
Antibiotic rate (%) | 80.2 | 83.6 | 80.4 | 81.5 | 81.9 | 82.7 |
Whitening effect after using 30 days | Well | Good | Good | Well | Good | Well |
Eyeprint effect of dispelling after using 30 days | Good | Good | Well | Good | Good | Well |
Eye pouch effect of dispelling after using 30 days | Good | Well | Well | Good | Good | Well |
Elimination black eye effect after using 30 days | Well | Good | Good | Well | Good | Well |
Eye fat granule situation after using 30 days | Nothing | Slightly | Nothing | Nothing | Nothing | Slightly |
As seen from the above table, plant biological source nanospray nursing eye glue has good whitening that prepared by the present invention, moisturizing,
Antibacterial, black eye of dispelling, eyeprint of dispelling, eye pouch of dispelling are respond well, and almost without fat granule produce.
The principle of above-described embodiment only illustrative present invention and effect thereof, not for limiting the present invention.Any ripe
Above-described embodiment all can be modified under the spirit and the scope of the present invention or change by the personage knowing this technology.Cause
This, have usually intellectual such as complete with institute under technological thought without departing from disclosed spirit in art
All equivalences become are modified or change, and must be contained by the claim of the present invention.
Claims (10)
1. a plant biological source nanospray nursing eye glue, it is characterised in that described plant biological source nanospray nursing eye
Glue includes following components:
Component A: Aesculus hippocastanum L. seed extract, XIAOMIJIAO berry extract, Fructus Citri grandis extract, uva extract, Tremella extract
Thing, Herba Centellae extract, polygoni cuspidati,radix extract, scutellariae,radix extract, Folium Camelliae sinensis extract, Glycyrrhiza glabra L. root extract, Flos Chrysanthemi
Extract, rosemary leaf extract and Herba portulacae extract;
B component: Argireline, palmityl tripeptides-1, Chondrus crispus, beta glucan, biological carbohydrate gum-1, methyl-monosilane alcohol
Hydroxyproline ester aspartic acid, dimethyldisilane alcohol hyaluronic acid ester and cereuisiae fermentum;
C component: Cremophor ELP, PEG-40 Oleum Ricini, plant sterol, carbomer, ascorbic acid methyl-monosilane alcohol pectic acid
Ester, hydroxyethyl cellulose, carbamide and allantoin;
D component: butanediol, propylene glycol, diglycerol, PEG-4000, glycine betaine, nicotiamide, polyglutamic acid sodium, three ethanol
Amine, 1,2-hexanediol, decoyl hydroximic acid, 1,3-propylene glycol, hexanediol and deionized water.
A kind of plant biological source the most according to claim 1 nanospray nursing eye glue, it is characterised in that described plant is raw
Thing source nanospray nursing eye glue is colloid substance, it is also possible to comprise preservative and essence.
A kind of plant biological source the most according to claim 1 nanospray nursing eye glue, it is characterised in that described component A,
The mass ratio of B component, C component and D component is 15-30:5-20:20-30:30-50.
A kind of plant biological source the most according to claim 1 nanospray nursing eye glue, it is characterised in that described component A
In component, by weight, including: Aesculus hippocastanum L. seed extract 5-12 part, XIAOMIJIAO berry extract 3-9 part, Fructus Citri grandis carry
Take thing 4-10 part, uva extract 2-5 part, Tremella extract 3-6 part, Herba Centellae extract 4-8 part, polygoni cuspidati,radix extract 2-
6 parts, scutellariae,radix extract 1-4 part, Folium Camelliae sinensis extract 1-3 part, Glycyrrhiza glabra L. root extract 1-4 part, Flos Chrysanthemi extract 2-4
Part, rosemary leaf extract 1-3 part and Herba portulacae extract 1-3 part.
A kind of plant biological source the most according to claim 1 nanospray nursing eye glue, it is characterised in that described B component
In component, by weight, including Argireline 3-10 part, palmityl tripeptides-1 2-8 part, Chondrus crispus 3-6
Part, beta glucan 2-7 part, biological carbohydrate gum-1 3-8 part, methyl-monosilane alcohol hydroxyproline ester aspartic acid 4-5 part, dimethyl
Disilane alcohol hyaluronic acid ester 2-6 part and cereuisiae fermentum 3-7 part.
A kind of plant biological source the most according to claim 1 nanospray nursing eye glue, it is characterised in that described C component
In component, by weight, including carbomer 10-15 part, hydroxyethyl cellulose 8-12 part, carbamide 3-7 part, allantoin 5-
12 parts, Cremophor ELP 1-3 part, PEG-40 Oleum Ricini 2-5 part, plant sterol 4-10 part, ascorbic acid methyl-monosilane alcohol fruit
Glue acid esters 5-8 part.
A kind of plant biological source the most according to claim 1 nanospray nursing eye glue, it is characterised in that described D component
In component, by weight, including butanediol 5-10 part, propylene glycol 2-7 part, diglycerol 3-6 part, PEG-4000 4-
8 parts, glycine betaine 4-8 part, nicotiamide 3-6 part, polyglutamic acid sodium 5-7 part, triethanolamine 4-9 part, 1,2-hexanediol 3-7 part, pungent
Acyl hydroximic acid 2-5 part, 1,3-propylene glycol 1-5 part, hexanediol 2-5 part, deionized water 50-80 part.
8. the preparation method of a plant biological source nanospray nursing eye glue, it is characterised in that: comprise the following steps:
(1) by Aesculus hippocastanum L. seed, XIAOMIJIAO fruit, Fructus Citri grandis, uva, Tremella, Herba Centellae, polygoni cuspidati,radix, scutellariae,radix, Folium Camelliae sinensis, light
Really licorice, Flos Chrysanthemi, leaf of Herba Rosmarini Officinalis and Herba portulacae are cleaned and are dried, and are placed in microwave device by masking foil cladding, microwave radiation
5-10min, after taking out cooling, shreds, and immerses in ethanol water solvent, adds thermal distillation condensation, takes plant distillate, is distilled by plant
Liquid is concentrated to give component A;
(2) by Cremophor ELP, PEG-40 Oleum Ricini, plant sterol, carbomer, ascorbic acid methyl-monosilane alcohol pectic acid
Ester, hydroxyethyl cellulose, carbamide and allantoin add in deionized water, are quickly stirred until homogeneous formation colloid substance, instill step
Suddenly the component A that prepared by (1), stirring forms functional colloid substance;
(3) by butanediol, propylene glycol, diglycerol, PEG-4000, glycine betaine, nicotiamide, polyglutamic acid sodium, triethanolamine,
1,2-hexanediol, decoyl hydroximic acid, 1,3-PD, hexanediol add in deionized water, are sufficiently mixed, and form carrier solution;
(4) functional colloid substance prepared by step (2) and Argireline, palmityl tripeptides-1, Chondrus crispus, β-
Glucosan, biological carbohydrate gum-1, methyl-monosilane alcohol hydroxyproline ester aspartic acid, dimethyldisilane alcohol hyaluronic acid ester and beer
Brewer yeast bacterium, homogenizing stirs, and forms function solution;
(5) function solution step (4) prepared loads in device for atomizing liquid, and the atomization of function solution is entered step (3)
In the carrier solution of preparation, mix homogeneously, stand, obtain plant biological source nanospray nursing eye glue.
The preparation method of a kind of plant biological source the most according to claim 8 nanospray nursing eye glue, it is characterised in that:
In described step (2), in functional colloid substance, component A is coated with by colloid substance.
The preparation method of a kind of plant biological source the most according to claim 8 nanospray nursing eye glue, its feature exists
In: in described step (5), the atomizing particle size of function solution is micro/nano level.
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