CN105496830A - Preparation method of alpinia japonica extract and application thereof in personal care products - Google Patents

Preparation method of alpinia japonica extract and application thereof in personal care products Download PDF

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Publication number
CN105496830A
CN105496830A CN201410495441.3A CN201410495441A CN105496830A CN 105496830 A CN105496830 A CN 105496830A CN 201410495441 A CN201410495441 A CN 201410495441A CN 105496830 A CN105496830 A CN 105496830A
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extract
alpinia japonica
personal care
rhizoma
preparation
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CN201410495441.3A
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Chinese (zh)
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黄爱强
屈红斌
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Healthy Science And Technology Co Ltd In Guangzhou 9958
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Healthy Science And Technology Co Ltd In Guangzhou 9958
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Abstract

The invention provides a preparation method of an alpinia japonica extract for caring hair or skin, and a personal care product composition containing the alpinia japonica extract. The preparation method comprises the following steps: 1) crushing and press-squeezing the alpinia japonica to obtain residue and juice of the alpinia japonica; 2) adding water to the alpinia japonica residue with uniform mixing and allowing the mixture to stand for 30-45 min; 3) collecting water soluble substances with rest alpinia japonica residue for later use; 4) mixing the water soluble substance with the alpinia japonica juice, performing supercritical CO2 extraction and collecting an extract; 5) adding water to the alpinia japonica residue to decoct the alpinia japonica residue for 1-2 h, and filtering the decoction to collect an extract liquid; and 6) mixing the extract and the extract liquid. The preparation method is mild in operation conditions. The alpinia japonica extract has excellent effects of whitening and moisturizing skin when being used in skin care products, and also has excellent hair caring effect when being used in hair caring products.

Description

The preparation method of Rhizoma of Japanse Galangal extract and the application in personal care articles thereof
Technical field
The invention belongs to personal care articles field, be specifically related to a kind of preparation method of the Rhizoma of Japanse Galangal extract for personal care articles and the personal care articles containing this Rhizoma of Japanse Galangal extract.
Background technology
Alpinia japonica (Thunb.) Miq. (Classification system: Alpiniajaponica (Thunb.) Miq.), another name is: nine Jiang Lian, Folium Zingiberis Herba Epimedii, Herba Polygoni Runcinati, Rhizoma Zingiberis Recens seven, Rhizoma Alpiniae Officinarum, JIZHUALIAN, be born in sylvan life, dark and damp place, limit, field, all have distribution all over the world." detailed outline " cloud: " Alpinia japonica (Thunb.) Miq., raw south.Leaf, like Rhizoma Zingiberis Recens, spends redness of the skin or complexion, very pungent; Son is like Semen Alpiniae Katsumadai, and root is as Rhizoma Polliae Japonicae." Su Songyun " and Flos Alpiniae japonicae, stem and leaf all Rhizoma Zingiberis Recens also, but root can't bear food, be and Flos Amomi Rotundus random small ear mutually.Between Folium Arachidis hypogaeae, make fringe as wheat grain, light red color." Alpinia japonica (Thunb.) Miq. is rich in the composition such as flavonoid, diarylheptanoids.Its fruit hyoscine, is armaticity stomachic, controls dyspepsia, stomachache, vomiting, eructation, chronic dysentery.In Zhejiang, Fujian also have report use for Fructus Amomi with these product.Rhizome is warm in nature, acrid in the mouth, energy regulating QI to relieve pain, and Eradicates wets, detumescence, promoting blood circulation to remove obstruction in the collateral, treating rheumatic arthritis, peratodynia, traumatic injury.Function cures mainly: warming middle-JIAO; Cold expelling; Dispel the wind; Invigorate blood circulation.
Alpinia japonica (Thunb.) Miq., as compound Chinese herbal medicinal ingredients, uses more in current medicine, such as, apply in the treatment and sanitary health drug of oral disease.But at present, do not see the relevant report be applied to by Rhizoma of Japanse Galangal extract in personal care articles, particularly in the skin care item and hair products of whitening skin and preserving moisture skin, yet there are no related application.
Summary of the invention
The present invention is for making up above-mentioned deficiency, a kind of preparation method of the Rhizoma of Japanse Galangal extract for hair nursing or skin protection is provided, its process conditions of the method are gentle, obtained Rhizoma of Japanse Galangal extract is applied in skin care item, can play effect of good whitening and moistening skin, it is applied in treatment also has good hair care effect.
The present invention is for reaching its object, and the technical scheme of employing is as follows:
The invention provides a kind of preparation method of the Rhizoma of Japanse Galangal extract for hair nursing or skin protection, comprise the steps:
1) Alpinia japonica (Thunb.) Miq. is carried out pulverize, squeeze, obtain Rhizoma Zingiberis Recens dregs and Sucus Zingberis;
2) in Rhizoma Zingiberis Recens dregs, add water, the weight ratio of Rhizoma Zingiberis Recens dregs and water is 1:0.7 ~ 3, and the two mixed and leave standstill 30 ~ 45min, collecting the hydrotrope, remaining Rhizoma Zingiberis Recens dregs is for subsequent use;
3) by step 2) hydrotrope that obtains and step 1) the Sucus Zingberis mix homogeneously that obtains, carry out supercritical carbon dioxide extraction, extraction temperature is 35 ~ 50 DEG C, extracting pressure is 20 ~ 50MPa, extraction time is 1 ~ 3h, carbon dioxide flow rate is 10 ~ 25L/h, and extraction terminates rear collection extract;
4) to step 2) Rhizoma Zingiberis Recens dregs in add water, the consumption of water is 2 ~ 4 times of Rhizoma Zingiberis Recens dregs weight, decocts 1 ~ 2 hour, collecting by filtration extracting solution;
5) combining step 3) extract that obtains and step 4) extracting solution that obtains.
Further, described Alpinia japonica (Thunb.) Miq. is fresh Alpinia japonica (Thunb.) Miq..
Further, step 3) in, when being separated after supercritical carbon dioxide extraction terminates, separation temperature controlled to be 35 ~ 55 DEG C, it is 3 ~ 10MPa that separating pressure controls.
The present invention also provides a kind of personal care composition, is added with plant extract in its formula, and described plant extract includes or is only Rhizoma of Japanse Galangal extract, and described Rhizoma of Japanse Galangal extract obtains according to preparation method as described above.
It is the Rhizoma of Japanse Galangal extract of 5% ~ 20% that described personal care composition wherein contains mass content.Rhizoma of Japanse Galangal extract prepared by the present invention addition in personal care composition controls in this scope, well can play its whitening skin and preserving moisture effect, or hair care effect.
Further, described personal care composition is the skin care compositions with whitening and/or moistening effect.Described skincare product compositions is bath gel, protective skin cream, emulsion or essence etc.
Further, described personal care composition is have antipruritic and/or improve hair washing or the Haircare composition of hair quality effect, such as shampoo, shampoo, hair conditioner, hairdressing gel etc.
Rhizoma of Japanse Galangal extract of the present invention, its extract part is the rhizome of Alpinia japonica (Thunb.) Miq..
Technical scheme provided by the invention has following beneficial effect: Rhizoma of Japanse Galangal extract prepared by method of the present invention, its extraction process is simple, containing abundant Alpinia japonica (Thunb.) Miq. active component in extract, be applied in hair products, it can play good hair care and to take care of hair effect, not only can improve hair quality, and also have good effect to scalp itch; In addition, be applied in skin-protection product, such as, in protective skin cream, also there is good skin moistening and whitening effect.This extract its there is pure natural, non-stimulated advantage, can be widely used in multiple personal care product.
The present invention is before extraction, the Sucus Zingberis of Alpinia japonica (Thunb.) Miq. and Rhizoma Zingiberis Recens dregs are processed respectively, be conducive to the natural constituent in more convenient efficient reservation Alpinia japonica (Thunb.) Miq., Sucus Zingberis is extracted with supercritical extraction technology, its operative temperature is low, the probability that the activity of effective ingredient in Alpinia japonica (Thunb.) Miq. is destroyed can be reduced preferably, reduce the degraded of active component; And further decoction is carried out to Rhizoma Zingiberis Recens dregs and extract, to a greater extent by the extracts active ingredients that contains in Alpinia japonica (Thunb.) Miq. out, the utilization rate of Alpinia japonica (Thunb.) Miq. effective ingredient can be improved.Extraction process of the present invention is compared with traditional Alpinia japonica (Thunb.) Miq. extraction process, a large amount of organic solvents can be saved, save extraction cost on the one hand, avoid organic solvent residual on the other hand, thus minimizing increases its irritating probability because of organic solvent remaining in extract.
Detailed description of the invention
Below in conjunction with embodiment, technical scheme of the present invention is described further.
Embodiment 1 Rhizoma of Japanse Galangal extract preparation example
Prepare Rhizoma of Japanse Galangal extract in accordance with the following steps:
1) fresh Alpinia japonica (Thunb.) Miq. is carried out pulverize, squeeze, obtain Rhizoma Zingiberis Recens dregs and Sucus Zingberis;
2) in Rhizoma Zingiberis Recens dregs, add water, the weight ratio of Rhizoma Zingiberis Recens dregs and water is 1:0.7, and the two mixed and leave standstill 30 ~ 45min, collecting the hydrotrope, remaining Rhizoma Zingiberis Recens dregs is for subsequent use;
3) by step 2) hydrotrope that obtains and step 1) the Sucus Zingberis mix homogeneously that obtains, carry out supercritical carbon dioxide extraction, extraction temperature is 35 DEG C, extracting pressure is 20MPa, extraction time is 3h, carbon dioxide flow rate is 10L/h, after extraction terminates, separation temperature is controlled to be 35 DEG C, separating pressure controls, for 3MPa, to collect extract.
4) to step 2) Rhizoma Zingiberis Recens dregs in add water, the consumption of water is 2 times of Rhizoma Zingiberis Recens dregs weight, decocts 1 hour, collecting by filtration extracting solution;
5) combining step 3) extract that obtains and step 4) extracting solution that obtains.
Embodiment 2 Rhizoma of Japanse Galangal extract preparation example
Prepare Rhizoma of Japanse Galangal extract in accordance with the following steps:
1) fresh Alpinia japonica (Thunb.) Miq. is carried out pulverize, squeeze, obtain Rhizoma Zingiberis Recens dregs and Sucus Zingberis;
2) in Rhizoma Zingiberis Recens dregs, add water, the weight ratio of Rhizoma Zingiberis Recens dregs and water is 1:3, and the two mixed and leave standstill 30 ~ 45min, collecting the hydrotrope, remaining Rhizoma Zingiberis Recens dregs is for subsequent use;
3) by step 2) hydrotrope that obtains and step 1) the Sucus Zingberis mix homogeneously that obtains, carry out supercritical carbon dioxide extraction, extraction temperature is 50 DEG C, extracting pressure is 50MPa, extraction time is 1h, carbon dioxide flow rate is 25L/h, after extraction terminates, separation temperature is controlled to be 55 DEG C, separating pressure controls, for 10MPa, to collect extract.
4) to step 2) Rhizoma Zingiberis Recens dregs in add water, the consumption of water is 4 times of Rhizoma Zingiberis Recens dregs weight, decocts 2 hours, collecting by filtration extracting solution;
5) combining step 3) extract that obtains and step 4) extracting solution that obtains.
Embodiment 3 Rhizoma of Japanse Galangal extract preparation example
Prepare Rhizoma of Japanse Galangal extract in accordance with the following steps:
1) fresh Alpinia japonica (Thunb.) Miq. is carried out pulverize, squeeze, obtain Rhizoma Zingiberis Recens dregs and Sucus Zingberis;
2) in Rhizoma Zingiberis Recens dregs, add water, the weight ratio of Rhizoma Zingiberis Recens dregs and water is 1::2, and the two mixed and leave standstill 30 ~ 45min, collecting the hydrotrope, remaining Rhizoma Zingiberis Recens dregs is for subsequent use;
3) by step 2) hydrotrope that obtains and step 1) the Sucus Zingberis mix homogeneously that obtains, carry out supercritical carbon dioxide extraction, extraction temperature is 44 DEG C, extracting pressure is 35MPa, extraction time is 2h, carbon dioxide flow rate is 15L/h, after extraction terminates, separation temperature is controlled to be 45 DEG C, separating pressure controls, for 6MPa, to collect extract.
4) to step 2) Rhizoma Zingiberis Recens dregs in add water, the consumption of water is 3 times of Rhizoma Zingiberis Recens dregs weight, decocts 2 hours, collecting by filtration extracting solution;
5) combining step 3) extract that obtains and step 4) extracting solution that obtains.
Embodiment 4 one kinds of bath gel
Described bath gel obtains according to the formula of following mass percentage: Rhizoma of Japanse Galangal extract 5%, Methylisothiazolinone 0.04%, essence 0.5%, deionized water surplus that sodium laureth sulfate 10%, coconut oleoyl amine 3%, cocamido propyl betaine 4.0%, EDETATE SODIUM 0.6%, citric acid 0.1%, sodium chloride 0.2%, embodiment 1 are obtained.
Preparation method is: sodium laureth sulfate, coconut oleoyl amine, cocamido propyl betaine, EDETATE SODIUM, citric acid, sodium chloride, deionized water are heated to 80 DEG C and stir, until dissolve completely; Then be cooled to less than 40 DEG C, add Rhizoma of Japanse Galangal extract, Methylisothiazolinone, essence wherein, stir, to be cooledly can carry out fill to room temperature.
Embodiment 5 one kinds of whitening skin and preserving moisture frosts
Described whitening skin and preserving moisture frost obtains according to the formula of following mass percentage: glyceryl monostearate 2.5%, octadecanol 1.5%, white oil 5%, olive oil 3%, dimethicone 1%, caprylic/capric triglyceride 4%, glycerol 6%, iso-octyl palmitate 4%, tridecyl alcohol trimellitate 5%, EDETATE SODIUM 0.05%, propylene glycol 3%, the Rhizoma of Japanse Galangal extract 10% that embodiment 2 is obtained, squalane 2%, essence 0.5%, Methylisothiazolinone 0.05%, deionized water surplus.
Its conveniently cream frost preparation method be prepared, specifically can carry out in accordance with the following steps: glyceryl monostearate, octadecanol, white oil, olive oil, dimethicone, caprylic/capric triglyceride, iso-octyl palmitate, tridecyl alcohol trimellitate, EDETATE SODIUM are mixed as oil phase and are warming up to 85 DEG C and dissolves completely to raw material; Using glycerol, squalane 2%, propylene glycol 3%, deionized water as aqueous phase, be warming up to 85 DEG C complete to material dissolution; Then carry out emulsifying by aqueous phase and oil phase suction emulsifying pot, treat that material is cooled to less than 45 DEG C, add remaining material wherein, stir, to be cooledly can carry out fill to room temperature.
Embodiment 6 one kinds of shampoos
Described shampoo is prepared according to the formula of following mass percentage: Rhizoma of Japanse Galangal extract 15%, castor oil-base maleic acid esters 0.5%, Methylisothiazolinone 0.01%, sodium chloride 1%, citric acid 0.02%, deionized water surplus that sodium laureth sulfate 5%, dodecyldimethylammonium hydroxide inner salt 4%, coconut oleoyl amine DEA2%, polyquaternary ammonium salt-70.5%, embodiment 3 are obtained.
Be prepared as follows: sodium laureth sulfate, dodecyldimethylammonium hydroxide inner salt, coconut oleoyl amine DEA, polyquaternary ammonium salt-7, deionized water are heated to 85 DEG C, stir, treat that it is cooled to 45 DEG C, add castor oil-base maleic acid esters, Methylisothiazolinone, Rhizoma of Japanse Galangal extract, stir again, then add sodium chloride and citric acid, stir evenly acquisition shampoo.
Embodiment 7 Yi Zhong hairdressing gel
Suo Shu hairdressing gel is prepared (following percentage ratio is mass percent) according to following formula: Rhizoma of Japanse Galangal extract 7%, essence 0.3%, Kazon 0.05%, water surplus prepared by 18 hexadecanol 8%, isopropyl palmitate 5%, ceteareth-6 and stearyl alcohol 4%, ceteareth-253%, dimethicone 3%, hexadecyltrimethylammonium chloride 4%, embodiment 1.
18 hexadecanol, isopropyl palmitate, ceteareth-6 and stearyl alcohol, ceteareth-25, dimethicone are mixed and heated to 85 DEG C, each component is dissolved completely, for subsequent use as oil phase; Then by water and cetyl front three ammonium chloride mix and blend, 85 DEG C are heated to, until material dissolves completely, for subsequent use as aqueous phase; Then by oil phase and aqueous phase mixing and emulsifying, homogenizing 5 minutes at 80 DEG C, then continues stirring and emulsifying 15 minutes; Lower the temperature afterwards, when temperature is down to below 45 DEG C, rest materials is added wherein, and stirs; Last vacuum outgas discharging.
The product that above-described embodiment 4 ~ 7 is obtained, through cutaneous safety test, confirms skin non-stimulated, can not cause erythema, desquamation, twinge and the untoward reaction such as scorching hot, can feel at ease to use.
The Rhizoma of Japanse Galangal extract used in the present invention, can as the both effectiveness raw material of whitening, moisturizing, hair care personal care articles, and its type of service does not have particular/special requirement, and it may be used for the cosmetics of the various different dosage forms such as water preparation, cream, emulsion.
Whitening and moistening effect
The cream containing Rhizoma of Japanse Galangal extract obtained to embodiment 5 below, the result that its whitening and moistening effect carry out testing is introduced.The tested crowd of this test is healthy volunteer 20 people, age 30 ~ 40 years old.The use of given the test agent is use 20 days continuously.Experimenter's left forearm smears blank frost (this blank white formula is substantially identical with embodiment 5, and difference is only not add Rhizoma of Japanse Galangal extract in formula), and right forearm smears the product of the embodiment of the present invention 5.
The acquisition of experimental data: CK company skinanalysis apparatus MexameterMX18 (melanin and haemachrome test probe) detection of skin melanin; The effect of SKICON200 type keratodermatitis water content measuring instrument test skin hydration.
Assessment result: melanin is the common standard passing judgment on skin black and white, and the colour of skin gets over brilliant white, and melanin value is lower.By continuous monitoring, find that its colour of skin of position of smearing the product of the embodiment of the present invention 5 is more even brilliant white, and not there is significant change in the position of smearing blank frost.By SKICON200 type keratodermatitis water content measuring instrument monitoring skin hydration, found that its skin average electrical of position of the product smearing the embodiment of the present invention 5 has increase trend, then not there is significant change in the position of smearing blank frost.
Experimental result shows, the cream frost containing Rhizoma of Japanse Galangal extract of the present invention, its whitening and moisture-keeping functions are obviously better than not containing the skin care item of Rhizoma of Japanse Galangal extract of the present invention.
Hair care effect is evaluated
Prepare blank shampoo, the preparation of this blank shampoo is substantially the same manner as Example 6, and difference is only wherein not add Rhizoma of Japanse Galangal extract.
The shampoo of embodiment 6 and the experiment number of blank shampoo are 20 women, all have the easy pruritus of scalp, hair dries up, be easy to the symptom of pulling apart.
Using method: the experimenter of experimental group and matched group washes weekly three times respectively, experimental group and matched group use the shampoo of embodiment 6 and blank shampoo respectively, use two months continuously.
Experimental result finds, the subject of matched group all feeds back its symptom and does not improve sign, and experimental group has the subject of 85% to feed back symptom that its hair easily itches be improved significantly, and experimental group has its hair of the subject feedback of 80% obviously more submissive, combing is convenient, and hairline is more tough.Visible, the shampoo containing Rhizoma of Japanse Galangal extract of the present invention, it has antipruritic, the effect of improving hair quality preferably.
The above, it is only preferred embodiment of the present invention, not any pro forma restriction is done to the present invention, therefore all contents not departing from technical solution of the present invention, according to technical spirit of the present invention to any simple modification made for any of the above embodiments, equivalent variations and modification, all still belong in the scope of technical solution of the present invention.

Claims (9)

1., for a preparation method for the Rhizoma of Japanse Galangal extract of hair nursing or skin protection, it is characterized in that, comprise the steps:
1) Alpinia japonica (Thunb.) Miq. is carried out pulverize, squeeze, obtain Rhizoma Zingiberis Recens dregs and Sucus Zingberis;
2) in Rhizoma Zingiberis Recens dregs, add water, the weight ratio of Rhizoma Zingiberis Recens dregs and water is 1:0.7 ~ 3, and the two mixed and leave standstill 30 ~ 45min, collecting the hydrotrope, remaining Rhizoma Zingiberis Recens dregs is for subsequent use;
3) by step 2) hydrotrope that obtains and step 1) the Sucus Zingberis mix homogeneously that obtains, carry out supercritical carbon dioxide extraction, extraction temperature is 35 ~ 50 DEG C, extracting pressure is 20 ~ 50MPa, extraction time is 1 ~ 3h, carbon dioxide flow rate is 10 ~ 25L/h, and extraction terminates rear collection extract;
4) to step 2) Rhizoma Zingiberis Recens dregs in add water, the consumption of water is 2 ~ 4 times of Rhizoma Zingiberis Recens dregs weight, decocts 1 ~ 2 hour, collecting by filtration extracting solution;
5) combining step 3) extract that obtains and step 4) extracting solution that obtains.
2. preparation method according to claim 1, is characterized in that, described Alpinia japonica (Thunb.) Miq. is fresh Alpinia japonica (Thunb.) Miq..
3. preparation method according to claim 1, is characterized in that, step 3) in, when being separated after supercritical carbon dioxide extraction terminates, separation temperature controlled to be 35 ~ 55 DEG C, it is 3 ~ 10MPa that separating pressure controls.
4. a personal care composition, is characterized in that, is added with plant extract in its formula, and described plant extract includes Rhizoma of Japanse Galangal extract, and described Rhizoma of Japanse Galangal extract obtains according to the preparation method as described in any one of claims 1 to 3.
5. personal care composition according to claim 4, is characterized in that, it is the Rhizoma of Japanse Galangal extract of 5% ~ 20% that described personal care composition wherein contains mass content.
6. personal care composition according to claim 4, is characterized in that, described personal care composition is the skin care compositions with whitening and/or moistening effect.
7. personal care composition according to claim 6, is characterized in that, described skin care compositions is bath gel, protective skin cream, emulsion or essence.
8. personal care composition according to claim 4, is characterized in that, described personal care composition is have antipruritic and/or improve hair washing, the Haircare composition of hair quality effect.
9. personal care composition according to claim 8, is characterized in that, described Haircare composition is hairdressing gel.
CN201410495441.3A 2014-09-24 2014-09-24 Preparation method of alpinia japonica extract and application thereof in personal care products Pending CN105496830A (en)

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CN106038418A (en) * 2016-07-21 2016-10-26 陈琼燕 Rhizoma Alpiniae Japonicae and tea seed cake shampoo and preparation method thereof
CN106074306A (en) * 2016-08-04 2016-11-09 碌柚葉(香港)有限公司 A kind of for skin and the compositions of hair maintenance and application
CN106109280A (en) * 2016-05-24 2016-11-16 安徽俊达食品有限公司 A kind of Sucus Zingberis shampoo production technology
CN106109281A (en) * 2016-05-24 2016-11-16 安徽俊达食品有限公司 A kind of Sucus Zingberis bath gel production technology
CN111135135A (en) * 2020-02-11 2020-05-12 广州栋方生物科技股份有限公司 Ginger powder with mite removing and acne removing effects and preparation method and application thereof

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106109280A (en) * 2016-05-24 2016-11-16 安徽俊达食品有限公司 A kind of Sucus Zingberis shampoo production technology
CN106109281A (en) * 2016-05-24 2016-11-16 安徽俊达食品有限公司 A kind of Sucus Zingberis bath gel production technology
CN106038418A (en) * 2016-07-21 2016-10-26 陈琼燕 Rhizoma Alpiniae Japonicae and tea seed cake shampoo and preparation method thereof
CN106074306A (en) * 2016-08-04 2016-11-09 碌柚葉(香港)有限公司 A kind of for skin and the compositions of hair maintenance and application
CN111135135A (en) * 2020-02-11 2020-05-12 广州栋方生物科技股份有限公司 Ginger powder with mite removing and acne removing effects and preparation method and application thereof
CN111135135B (en) * 2020-02-11 2022-08-02 广州栋方生物科技股份有限公司 Ginger powder with mite removing and acne removing effects and preparation method and application thereof

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