CN104873419A - Multi-plant composition and extract thereof as well as preparation and application of microcapsule - Google Patents
Multi-plant composition and extract thereof as well as preparation and application of microcapsule Download PDFInfo
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- CN104873419A CN104873419A CN201510255077.8A CN201510255077A CN104873419A CN 104873419 A CN104873419 A CN 104873419A CN 201510255077 A CN201510255077 A CN 201510255077A CN 104873419 A CN104873419 A CN 104873419A
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Abstract
The invention discloses a multi-plant composition and an extract thereof as well as a preparation method and application of a microcapsule. The multi-plant composition comprises the following six natural plants folium ginkgo, mother chrysanthemum, honeysuckle, liquorice, dandelion and oat as natural plant active components at the mass ratio of (0.5-1) to (0.5-1) to (0.5-1) to (1-3) to (2-4) to (4-6); composite plant composition powder is prepared from the six natural plant extracts through a series of separation and purification processes; and in addition, the composition microcapsule is obtained from the composite plant composition powder by a liposome embedding technology. The obtained composite plant composition microcapsule is good in stability, does not change the physical and chemical properties of cosmetics when applied to the cosmetics, is stable in color, has the effects of resisting allergy, relieving the skin, resisting inflammation, resisting irritation and relieving itching, is obvious and lasting in efficiency and has slow-release property.
Description
Technical field
The invention belongs to cosmetics preparation field, particularly the Synthesis and applications of one kind of multiple vegetable compositions and extract thereof, microcapsule.
Background technology
Microcapsule technology be a kind of utilize natural or synthesis macromolecular material, by solid or liquid substance embedding get up, formed have semipermeable or sealing cyst membrane microencapsulation technology.Microcapsule technology can improve the physical property being wrapped material, and active component and external environment are completely cut off and comes, enhanced stability, reduces volatility, extends storage life, has Co ntrolled release function in addition.This technical research starts from the 50's of 20th century, is first applied in no carbon paper by microcapsule by the U.S., have passed through the fast development of decades afterwards, so far the method for existing more than 200 kind of micro encapsulation.The fields such as medicine, food, chemical industry and printing industry are widely used at present.
As everyone knows, in the formula of Traditional makeup, the interpolation of bioactive ingredients (as: plant extraction liquid) can cause the instability of following several respects properties of product: a) physical characteristic of product; B) chemical composition of product; C) biological activity; D) degraded of other compositions in formula; E) shortening of the shelf-life of product.
Summary of the invention
The object of this invention is to provide the Synthesis and applications of one kind of multiple composition of plant extracts and microcapsule thereof, wherein, have employed microcapsule technology, enable the composition of biologically active labile in cosmetics, maintain its activity, do not affect again effect of other composition in formula simultaneously.
Adopt up-to-date plant compounded combination technique, extraction process is innovated, composite extract synergetic name shows, and after microcapsule technology process, be applied in cosmetics and solve a series of problem, such as: plant extract addition is high, cosmetics physicochemical property changes, active matter easy in inactivation etc. utilizes advanced micro-capsule package technology to prepare antieczematic slow release child skin-protection product, can be widely used in child's cosmetic field.
The object of the invention is to be achieved through the following technical solutions:
One kind of multiple vegetable compositions, the raw material of described compositions comprises Folium Ginkgo, Flos Chrysanthemi Indici, Flos Lonicerae, Radix Glycyrrhizae, Herba Taraxaci and Herba bromi japonici, and the ratio of weight and number of described each raw material is:
Folium Ginkgo 0.5 ~ 1
Flos Chrysanthemi Indici 0.5 ~ 1
Flos Lonicerae 0.5 ~ 1
Radix Glycyrrhizae 1 ~ 3
Herba Taraxaci 2 ~ 4
Herba bromi japonici 4 ~ 6.
Described various plants compositions extracts the plant extract obtained, and extracting method comprises the following steps:
1) filter out 6 above-mentioned kind of plant, Folium Ginkgo, Flos Chrysanthemi Indici, Flos Lonicerae, Radix Glycyrrhizae, Herba Taraxaci and Herba bromi japonici, pulverization process is carried out respectively in 6 described kind of plant effect positions, cross 20 mesh sieves, obtain 6 kind of plant flours, for subsequent use;
2) by above-mentioned steps 1) the 6 kind of plant flours that obtain mix by above-mentioned ratio of weight and number, obtain plant flour mixture;
3) 10g step 2 is got) the described plant flour mixture that obtains, according to solid-liquid ratio 1:10, in described plant flour mixture, add deionized water and stirring even, leaves standstill 30min, decoct 30min or ethanol extraction 1h, filter and obtain supernatant A and filtering residue;
4) filtering residue that obtains of step 3) is according to solid-liquid ratio 1:10, and in described filtering residue, add deionized water and stirring even, leaves standstill 30min, decoct 30min or ethanol extraction 1h, filter and obtain supernatant B, merge supernatant A and supernatant B, obtain supernatant;
5) centrifugal segregation magazine precipitation, obtains supernatant again after concentrated, is settled to 10ml, namely obtains the plant extract of described various plants compositions; Described method for concentration is rotary distillation, reclaims ethanol.
Another object of the present invention is achieved through the following technical solutions:
A kind of microcapsule containing above-mentioned plant extract.
The preparation method of described plant extract microcapsule, adopts supercritical fluid spray drying method to prepare described plant extract microcapsule, said method comprising the steps of:
The wall material of described plant extract microcapsule is gelatin, arabic gum, cellulose, carboxymethyl cellulose, hydroxy methocel, beta glucan, maltose, sucrose, chitosan, lactalbumin wherein one or more, described plant extract as core, by wall material and core according to the ratio of ratio of weight and number 4 ~ 10:1 containing supercritical CO
2mix in the high-pressure bottle of fluid, pressure condition: 15 ~ 30MPa, temperature conditions: 40 ~ 80 DEG C, flow-control is at 10 ~ 30Lh
-1, the described plant extract microcapsule namely obtained.
Another preparation method of described plant extract microcapsule, adopts liposome legal system for described plant extract microcapsule, said method comprising the steps of:
The wall material of described plant extract microcapsule is one or more in lecithin, cholesterol, phosphatidylcholine, ceramide, olive oil, described plant extract is as core, the mixed proportion of described wall material and core is 4 ~ 10:1, the water of wall material, core and both mixture 10 ~ 20 times amount is heated to 60 DEG C-90 DEG C respectively, high pressure homogenize emulsifying, the described plant extract microcapsule namely obtained.
Another object of the present invention is achieved through the following technical solutions:
An application for described plant extract microcapsule, described plant extract microcapsule can be added in cosmetics.
Another object of the present invention is achieved through the following technical solutions:
With the addition of cream frost or the emulsion of described plant extract microcapsule, described cream frost or the raw material of emulsion and the ratio of weight and number of each raw material are:
A phase:
Cetostearyl alcohol 2 ~ 4
Monoglyceride 0.5 ~ 2
White oil 3 ~ 5
Ring five polydimethylsiloxane (C 345) 1 ~ 2
Emulsifying agent 1 ~ 3
Co-emulsifier 0.5 ~ 2
Thickening agent 1 ~ 2
B phase:
Deionized water 67 ~ 87
Glycerol 3 ~ 5
EDTA-2NA 0.1~1
C phase:
Antiseptic 0.1 ~ 1
Vegetable composition microcapsule 1 ~ 5
Essence 0.1 ~ 1.
Described cream frost or the preparation method of emulsion, comprise the following steps:
Respectively each for A phase raw material is added to oil phase still under room temperature, the each raw material of B phase is added to aqueous phase still, and be heated to more than 85 DEG C respectively, dissolving stirs, and then A phase is mixed with B phase, emulsifying when temperature remains on more than 85 DEG C, slowly stirs when being cooled to 45 DEG C and adds C phase, stirs and namely obtains described cream frost or newborn.
Further, described emulsifying agent is cetearyl alcohol ether-6; Described co-emulsifier is cetearyl alcohol ether-25; Described thickening agent is carbomer; Described antiseptic is one or both the mixture in Bronopol or IPBC.
Another object of the present invention is achieved through the following technical solutions:
With the addition of essence or the surfactant of described plant extract microcapsule, the raw material of described essence or surfactant and the ratio of weight and number of each raw material are:
Glycerol 3 ~ 5
Propylene glycol 2 ~ 4
Hydroxyethyl-cellulose (HEC) 0.1 ~ 1
Hyaluronate sodium 0.01 ~ 0.5
Vegetable composition microcapsule 1 ~ 5
Deionized water 81 ~ 94
Antiseptic 0.1 ~ 1
Essence 0.1 ~ 1
Solubilizing agent 0.1 ~ 1.
Described essence or the preparation method of surfactant, comprise the following steps:
First HEC powder deionized water is dissolved as the HEC solution of 1 ~ 3% concentration, vegetable composition microcapsule propylene glycol is pre-dispersed or molten in advance with deionized water is the aqueous solution of 0.5 ~ 2% concentration, then add remaining each raw material successively, stir, namely obtain described essence or surfactant.
the present invention's beneficial effect is compared to existing technology:
1, the present invention adopts up-to-date plant compounded combination, innovates the extraction process of described plant extract simultaneously, and composite extract synergetic name shows;
2, microcapsule technology is applied to cosmetic industry by the present invention, is wrapping in microcapsule, and then adds these microcapsules to cosmetics by the composition (as natural extract liquid etc.) of biologically active labile.Like this, both improve the addition of plant extract, maintained the activity of bioactive ingredients, do not changed again the physicochemical property of cosmetics, and do not affect effect of other composition in formula;
3, the ordinary cosmetics containing kindred plant extract, i.e. the cosmetics of not encapsulated process, when room temperature is placed, within 8 ~ 12 months, just there will be metachromatism, shelf life of products was at about 1 year; And the cosmetics that the present invention is prepared by micro-capsule package technology, shelf life of products rises appreciably, and the shelf-life is compared above-mentioned ordinary cosmetics and at least can extend 1 year, product stable in physicochemical property, and the shelf-life was at about 2 ~ 3 years;
4, the present invention utilizes advanced micro-capsule package technology to prepare antieczematic slow release child skin-protection product, can be widely used in child's cosmetic field.
Detailed description of the invention
Embodiment 1
One kind of multiple vegetable compositions, the raw material of described compositions comprises Folium Ginkgo, Flos Chrysanthemi Indici, Flos Lonicerae, Radix Glycyrrhizae, Herba Taraxaci and Herba bromi japonici, and the ratio of weight and number of described each raw material is:
Folium Ginkgo 0.5 ~ 1
Flos Chrysanthemi Indici 0.5 ~ 1
Flos Lonicerae 0.5 ~ 1
Radix Glycyrrhizae 1 ~ 3
Herba Taraxaci 2 ~ 4
Herba bromi japonici 4 ~ 6.
Described various plants compositions extracts the plant extract obtained, and extracting method comprises the following steps:
1) filter out 6 above-mentioned kind of plant, Folium Ginkgo, Flos Chrysanthemi Indici, Flos Lonicerae, Radix Glycyrrhizae, Herba Taraxaci and Herba bromi japonici, pulverization process is carried out respectively in 6 described kind of plant effect positions, cross 20 mesh sieves, obtain 6 kind of plant flours, for subsequent use;
2) by above-mentioned steps 1) the 6 kind of plant flours that obtain mix by above-mentioned ratio of weight and number, obtain plant flour mixture;
3) 10g step 2 is got) the described plant flour mixture that obtains, according to solid-liquid ratio 1:10, in described plant flour mixture, add deionized water and stirring even, leaves standstill 30min, decoct 30min or ethanol extraction 1h, filter and obtain supernatant A and filtering residue;
4) filtering residue that obtains of step 3) is according to solid-liquid ratio 1:10, and in described filtering residue, add deionized water and stirring even, leaves standstill 30min, decoct 30min or ethanol extraction 1h, filter and obtain supernatant B, merge supernatant A and supernatant B, obtain supernatant;
5) centrifugal segregation magazine precipitation, obtains supernatant again after concentrated, is settled to 10ml, namely obtains the plant extract of described various plants compositions; Described method for concentration is rotary distillation, reclaims ethanol.
Embodiment 2
Present embodiments provide one kind of multiple vegetable compositions, be the preferred version on embodiment 1 basis, raw materials used quality is identical with embodiment 1, and the ratio of weight and number of each raw material described is:
Folium Ginkgo 0.8, Flos Chrysanthemi Indici 0.8, Flos Lonicerae 0.8, Radix Glycyrrhizae 2, Herba Taraxaci 3, Herba bromi japonici 5.
Embodiment 3
Present embodiments provide one kind of multiple vegetable compositions, be the preferred version on embodiment 1 basis, raw materials used quality is identical with embodiment 1, and the ratio of weight and number of each raw material described is:
Folium Ginkgo 1, Flos Chrysanthemi Indici 1, Flos Lonicerae thing 1, Radix Glycyrrhizae 2, Herba Taraxaci 3, Herba bromi japonici 5.
Embodiment 4
A kind of plant extract microcapsule containing the various plants extract described in embodiment 1.
The preparation method of described plant extract microcapsule, adopts supercritical fluid spray drying method to prepare described plant extract microcapsule, said method comprising the steps of:
The wall material of described plant extract microcapsule is gelatin, arabic gum, cellulose, carboxymethyl cellulose, hydroxy methocel, beta glucan, maltose, sucrose, chitosan, lactalbumin wherein one or more, by the various plants extractive composition described in wall material and embodiment 1 according to the ratio of ratio of weight and number 4 ~ 10:1 containing supercritical CO
2mix in the high-pressure bottle of fluid, pressure condition: 15 ~ 30MPa, temperature conditions: 40 ~ 80 DEG C, flow-control is at 10 ~ 30Lh
-1, the described plant extract microcapsule namely obtained.
Another preparation method of described plant extract microcapsule, adopts liposome legal system for described plant extract microcapsule, said method comprising the steps of:
The wall material of described plant extract microcapsule is one or more in lecithin, cholesterol, phosphatidylcholine, ceramide, olive oil, described plant extract is as core, the mixed proportion of described wall material and core is 4 ~ 10:1, the water of wall material, core and both mixture 10 ~ 20 times amount is heated to 60 DEG C-90 DEG C respectively, high pressure homogenize emulsifying, the described plant extract microcapsule namely obtained.
Embodiment 5
With the addition of cream frost or the emulsion of the plant extract microcapsule described in embodiment 4, described cream frost or the raw material of emulsion and the ratio of weight and number of each raw material are:
A phase:
Cetostearyl alcohol 2 ~ 4
Monoglyceride 0.5 ~ 2
White oil 3 ~ 5
C 345 1~2
Emulsifying agent 1 ~ 3
Co-emulsifier 0.5 ~ 2
Thickening agent 1 ~ 2
B phase:
Deionized water 67 ~ 87
Glycerol 3 ~ 5
EDTA-2NA 0.1~1
C phase:
Antiseptic 0.1 ~ 1
Vegetable composition microcapsule 1 ~ 5
Essence 0.1 ~ 1.
Described cream frost or the preparation method of emulsion, comprise the following steps:
Respectively each for A phase raw material is added to oil phase still under room temperature, the each raw material of B phase is added to aqueous phase still, and be heated to more than 85 DEG C respectively, dissolving stirs, and then A phase is mixed with B phase, emulsifying when temperature remains on more than 85 DEG C, slowly stirs when being cooled to 45 DEG C and adds C phase, stirs and namely obtains described cream frost or newborn.
Observe and add vegetable composition microcapsule and the cosmetics directly adding identical working substance (non-micro encapsulation), the cream that with the addition of described plant extract microcapsule prepared by the present embodiment is white or emulsion appearance is finer and smoother, color in normal temperature storage to 28 day, without variable color.And directly add the cosmetics of identical working substance (non-micro encapsulation), in normal temperature storage after 28 days, mastic darkens.
Adopt Konica CM-5 spectral photometric colour measuring meter measurement products colourity situation of change, sample one is for adding the product of plant extract microcapsule formula, sample two is the product of the formula directly adding plant extract, the sample not adding the formula of any form plant extract is adopted to make blank, measure the difference situation of change of these two groups of samples at the normal temperature storage colourity of 14 days, 28 days, 3 months, 6 months, 12 months and blank sample respectively, result is as follows:
As can be seen here, sample one (namely adding the sample of plant microcapsule) contrasts with blank product with sample two (adding the sample of non-micro encapsulation plant extract), the two all has the phenomenon darkened, sample one is slightly less than the change of sample second colors, along with the prolongation of time, sample two is increasing with the aberration of reference substance, and sample product of the same colour changes not quite substantially, illustrate that the product adding vegetable composition microcapsule improves in colour stability greatly with the sample of the plant society adding non-micro encapsulation.
Consumer's Experience in addition, the cream frost that with the addition of described plant extract microcapsule prepared by the present embodiment or emulsion, the effect of antagonism skin sensitivity is better than the cosmetics directly adding identical working substance (non-micro encapsulation) greatly, and effect is more lasting, possesses certain moistening effect simultaneously.
Embodiment 6
With the addition of essence or the surfactant of described plant extract microcapsule, the raw material of described essence or surfactant and the ratio of weight and number of each raw material are:
Glycerol 3 ~ 5
Propylene glycol 2 ~ 4
HEC 0.1~1
Hyaluronate sodium 0.01 ~ 0.5
Vegetable composition microcapsule 1 ~ 5
Deionized water 81 ~ 94
Antiseptic 0.1 ~ 1
Essence 0.1 ~ 1
Solubilizing agent 0.1 ~ 1.
Further, described solubilizing agent is LRI; Described antiseptic is a kind of in Bronopol or IPBC or both mixture.
Described essence or the preparation method of surfactant, comprise the following steps:
First HEC powder deionized water is dissolved as the HEC solution of 1 ~ 3% concentration, vegetable composition microcapsule propylene glycol is pre-dispersed or molten in advance with deionized water is the aqueous solution of 0.5 ~ 2% concentration, then add remaining each raw material successively, stir, namely obtain described essence or surfactant.
Compared with the water of the essence of prepared by the present embodiment with the addition of described plant extract microcapsule or surfactant and the vegetable composition containing non-micro encapsulation or elite, product heat-resistant stability prepared by the present embodiment and storage at normal temperature stability strengthen, product colour is comparatively stable, and can effectively alleviate sensitivity skin rubescent, itch or harsh feeling, effect is lasting, life-time service can make skin more smooth, and sensitivity reduces.
Claims (10)
1. one kind of multiple vegetable compositions, is characterized in that, the raw material of described compositions comprises Folium Ginkgo, Flos Chrysanthemi Indici, Flos Lonicerae, Radix Glycyrrhizae, Herba Taraxaci and Herba bromi japonici, and the ratio of weight and number of described each raw material is:
Folium Ginkgo 0.5 ~ 1
Flos Chrysanthemi Indici 0.5 ~ 1
Flos Lonicerae 0.5 ~ 1
Radix Glycyrrhizae 1 ~ 3
Herba Taraxaci 2 ~ 4
Herba bromi japonici 4 ~ 6.
2. extracted the plant extract obtained by various plants compositions according to claim 1, it is characterized in that, extracting method comprises the following steps:
1) filter out 6 kind of plant described in claim 1, Folium Ginkgo, Flos Chrysanthemi Indici, Flos Lonicerae, Radix Glycyrrhizae, Herba Taraxaci and Herba bromi japonici, pulverization process is carried out respectively in 6 described kind of plant effect positions, cross 20 mesh sieves, obtain 6 kind of plant flours, for subsequent use;
2) by above-mentioned steps 1) the 6 kind of plant flours that obtain, and mix according to ratio of weight and number according to claim 1, obtain plant flour mixture;
3) 10g step 2 is got) the described plant flour mixture that obtains, according to solid-liquid ratio 1:10, in described plant flour mixture, add deionized water and stirring even, leaves standstill 30min, decoct 30min or ethanol extraction 1h, filter and obtain supernatant A and filtering residue;
4) filtering residue that obtains of step 3) is according to solid-liquid ratio 1:10, and in described filtering residue, add deionized water and stirring even, leaves standstill 30min, decoct 30min or ethanol extraction 1h, filtration obtains supernatant B, merges supernatant A and supernatant B, obtains the supernatant of plant society extract;
5) supernatant of above-mentioned vegetable composition extract is first precipitated through centrifugal segregation magazine, obtain supernatant again after concentrated, be settled to 10ml, namely obtain the extract of various plants compositions.
3. the microcapsule containing, for example plant extract according to claim 2.
4. a preparation method for plant extract microcapsule as claimed in claim 3, is characterized in that, adopts supercritical fluid spray drying method to prepare described plant extract microcapsule, said method comprising the steps of:
The wall material of described plant extract microcapsule is gelatin, arabic gum, cellulose, carboxymethyl cellulose, hydroxy methocel, beta glucan, maltose, sucrose, chitosan, lactalbumin wherein one or more, plant extract according to claim 2 as core, by wall material and core according to the ratio of ratio of weight and number 4 ~ 10:1 containing supercritical CO
2mix in the high-pressure bottle of fluid, pressure condition: 15 ~ 30MPa, temperature conditions: 40 ~ 80 DEG C, flow-control is at 10 ~ 30Lh
-1, the described plant extract microcapsule namely obtained.
5. a preparation method for plant extract microcapsule as claimed in claim 3, is characterized in that, adopts liposome legal system for described plant extract microcapsule, said method comprising the steps of:
The wall material of described plant extract microcapsule is one or more in lecithin, cholesterol, phosphatidylcholine, ceramide, olive oil, plant extract according to claim 3 is as core, the mixed proportion of described wall material and core is 4 ~ 10:1, the water of wall material, core and both mixture 10 ~ 20 times amount is heated to 60 DEG C-90 DEG C respectively, high pressure homogenize emulsifying, the described plant extract microcapsule namely obtained.
6. an application for plant extract microcapsule as claimed in claim 3, is characterized in that, described plant extract microcapsule can be added in cosmetics.
7. with the addition of cream frost or the emulsion of plant extract microcapsule as claimed in claim 3, it is characterized in that, described cream frost or the raw material of emulsion and the ratio of weight and number of each raw material are:
A phase:
Cetostearyl alcohol 2 ~ 4
Monoglyceride 0.5 ~ 2
White oil 3 ~ 5
C 345 1~2
Emulsifying agent 1 ~ 3
Co-emulsifier 0.5 ~ 2
Thickening agent 1 ~ 2
B phase:
Deionized water 67 ~ 87
Glycerol 3 ~ 5
EDTA-2NA 0.1~1
C phase:
Antiseptic 0.1 ~ 1
Vegetable composition microcapsule 1 ~ 5
Essence 0.1 ~ 1.
8. a preparation method for cream frost as claimed in claim 7 or emulsion, it is characterized in that, described preparation method comprises the following steps:
Respectively each for A phase raw material is added to oil phase still under room temperature, the each raw material of B phase is added to aqueous phase still, and be heated to more than 85 DEG C respectively, dissolving stirs, and then A phase is mixed with B phase, emulsifying when temperature remains on more than 85 DEG C, slowly stirs when being cooled to 45 DEG C and adds C phase, stirs and namely obtains described cream frost or emulsion.
9. with the addition of essence or the surfactant of plant extract microcapsule as claimed in claim 3, it is characterized in that, the raw material of described essence or surfactant and the ratio of weight and number of each raw material are:
Glycerol 3 ~ 5
Propylene glycol 2 ~ 4
HEC 0.1~1
Hyaluronate sodium 0.01 ~ 0.5
Vegetable composition microcapsule 1 ~ 5
Deionized water 81 ~ 94
Antiseptic 0.1 ~ 1
Essence 0.1 ~ 1
Solubilizing agent 0.1 ~ 1.
10. a preparation method for essence as claimed in claim 9 or surfactant, is characterized in that, described preparation method comprises the following steps:
First HEC powder deionized water is dissolved as the HEC solution of 1 ~ 3% concentration, vegetable composition microcapsule propylene glycol is pre-dispersed or molten in advance with deionized water is the aqueous solution of 0.5 ~ 2% concentration, then add remaining each raw material successively, stir, namely obtain described essence or surfactant.
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