CN104873419B - The preparation and application of one kind of multiple plant compositions and its extract, microcapsules - Google Patents
The preparation and application of one kind of multiple plant compositions and its extract, microcapsules Download PDFInfo
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- CN104873419B CN104873419B CN201510255077.8A CN201510255077A CN104873419B CN 104873419 B CN104873419 B CN 104873419B CN 201510255077 A CN201510255077 A CN 201510255077A CN 104873419 B CN104873419 B CN 104873419B
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Abstract
The invention discloses one kind of multiple plant compositions and its extract, the preparation method and application of microcapsules.Described plant composition includes six kinds of ginkgo leaf, chrysanthemum indicum, honeysuckle, radix glycyrrhizae, dandelion and oat natural plant active components, and six kinds of natural plants weight ratios are 0.5 ~ 1:0.5~1:0.5~1:1~3:2~4:4 ~ 6, six kinds of natural plant extracts obtain plant complex composition powder by a series of separation purifying technique, and the compound botanical composition powder uses liposome embedded technology in addition, obtains said composition microcapsules.The plant complex composition microcapsule stability that the present invention obtains is good, does not change the physicochemical property of cosmetics added in cosmetics, colour stable, have the function that antiallergic releive, anti-inflammatory, anti-irritant and antipruritic, effect is obvious and persistently, has slow release.
Description
Technical field
The invention belongs to cosmetics preparation field, more particularly to one kind of multiple plant compositions and its extract, microcapsules
Preparation and application.
Background technology
Microcapsules technology is a kind of using natural or synthesis high polymer material, and solid or liquid substance are embedded
Come, form with semipermeable or seal the microencapsulation technology of cyst membrane.Microcapsules technology can improve the thing of wrapped material
Rationality matter, active component is completely cut off with external environment and come, strengthen stability, reduce volatility, extend storage life, additionally have
There is control release function.This technical research starts from the 50's of 20th century, is first applied to microcapsules by the U.S. carbon-free
In carbon paper, the fast development of decades is have passed through afterwards, so far the existing method of more than 200 kinds of microencapsulation.It is wide at present
It is general to be applied to the fields such as medicine, food, chemical industry and printing industry.
It is well known that in the formula of Traditional makeup, bioactive ingredients(Such as:Plant extraction liquid)Addition can cause
Following several respects properties of product it is unstable:a)The physical characteristic of product;b)The chemical composition of product;c)The activity of biology;d)
The degraded of other compositions in formula;e)The shortening of the shelf-life of product.
The content of the invention
It is an object of the invention to provide the preparation and application of one kind of multiple composition of plant extracts and its microcapsules, its
In, microcapsules technology is employed, the composition of biologically active labile is maintained its activity, while not shadow again in cosmetics
The effect of ringing other compositions in formula.
Using newest plant compounded combination technique, extraction process innovation, compounding extract synergetic is obvious, and passes through
After microcapsules technology processing, apply and solve a series of problem in cosmetics, such as:Plant extracts addition is high, changes
Cosmetic physicochemical property changes, and active matter easy in inactivation etc. prepares antieczematic sustained release children's skin care using advanced micro-capsule package technology
Product, it can be widely applied to cosmetics for children field.
The purpose of the present invention is achieved through the following technical solutions:
One kind of multiple plant compositions, the raw material of the composition include ginkgo leaf, chrysanthemum indicum, honeysuckle, radix glycyrrhizae, Pu Gong
English and oat, the ratio of weight and number of each raw material are:
Ginkgo leaf 0.5 ~ 1
Chrysanthemum indicum 0.5 ~ 1
Honeysuckle 0.5 ~ 1
Radix glycyrrhizae 1 ~ 3
Dandelion 2 ~ 4
Oat 4 ~ 6.
Described various plants composition extracts obtained plant extracts, and extracting method comprises the following steps:
1)6 kinds of above-mentioned plants are filtered out, ginkgo leaf, chrysanthemum indicum, honeysuckle, radix glycyrrhizae, dandelion and oat will be described
6 kinds of plant effect positions carry out pulverization process respectively, cross 20 mesh sieves, obtain 6 kinds of plant flours, standby;
2)By above-mentioned steps 1)6 kinds of obtained plant flours are mixed by above-mentioned ratio of weight and number, obtain the mixing of plant flour
Thing;
3)Take 10g steps 2)The obtained plant flour mixture, according to solid-liquid ratio 1:10, mixed to the plant flour
In compound add deionized water stir, stand 30min, decoct 30min or ethanol extraction 1h, be filtrated to get supernatant A and
Filter residue;
4)Step 3)Obtained filter residue is according to solid-liquid ratio 1:10, into the filter residue, addition deionized water stirs, quiet
30min is put, 30min or ethanol extraction 1h is decocted, is filtrated to get supernatant B, merges supernatant A and supernatant B, obtain supernatant
Liquid;
5)Centrifugation removes contamination precipitation, obtain supernatant it is concentrated again after, be settled to 10ml, that is, obtain described more plantations
The plant extracts of compositions;The method for concentration is rotary distillation, reclaims ethanol.
It is another object of the present invention to what is be achieved through the following technical solutions:
A kind of microcapsules containing above-mentioned plant extracts.
The preparation method of described plant extracts microcapsules, the plant is prepared using supercritical fluid spray drying process
Extract microcapsules, it the described method comprises the following steps:
The wall material of the plant extracts microcapsules is gelatin, Arabic gum, cellulose, carboxymethyl cellulose, methylol
Cellulose, beta glucan, maltose, sucrose, chitosan, lactalbumin it is therein one or more, described plant extracts make
For core, by wall material and core according to ratio of weight and number 4 ~ 10:1 ratio is containing supercritical CO2In the high-pressure bottle of fluid
Mixing, pressure condition:15 ~ 30MPa, temperature conditionss:40 ~ 80 DEG C, flow is controlled in 10 ~ 30Lh-1, that is, the described plant that obtains
Thing extract microcapsules.
Another preparation method of described plant extracts microcapsules, the plant extract is prepared using liposome method
Thing microcapsules, the described method comprises the following steps:
The wall material of the plant extracts microcapsules is lecithin, cholesterol, phosphatidyl choline, ceramide, olive oil
In one or more, for described plant extracts as core, the mixed proportion of the wall material and core is 4 ~ 10:1, by wall
Material, the water of 10 ~ 20 times of amounts of core and both mixtures are separately heated to 60 DEG C -90 DEG C, high-pressure homogeneous emulsification, that is, the institute obtained
The plant extracts microcapsules stated.
It is another object of the present invention to what is be achieved through the following technical solutions:
A kind of application of the plant extracts microcapsules, the plant extracts microcapsules can be added in cosmetics.
It is another object of the present invention to what is be achieved through the following technical solutions:
A kind of cream or emulsion that with the addition of described plant extracts microcapsules, the raw material of the cream or emulsion and each
The ratio of weight and number of raw material is:
A phases:
Cetostearyl alcohol 2 ~ 4
Monoglyceride 0.5 ~ 2
White oil 3 ~ 5
Ring five dimethyl silicone polymer(C 345) 1~2
Emulsifying agent 1 ~ 3
Assistant for emulsifying agent 0.5 ~ 2
Thickener 1 ~ 2
B phases:
Deionized water 67 ~ 87
Glycerine 3 ~ 5
EDTA-2NA 0.1~1
C phases:
Preservative 0.1 ~ 1
Plant composition microcapsules 1 ~ 5
Essence 0.1 ~ 1.
Described cream or the preparation method of emulsion, comprise the following steps:
Each raw material of A phases is added to oil phase kettle respectively under normal temperature, each raw material of B phases is added to aqueous phase kettle, and is separately heated to
More than 85 DEG C, dissolving stirs, and then again mixes A phases with B, emulsifying when temperature is maintained at more than 85 DEG C, slowly
Stirring adds C phases when being cooled to 45 DEG C, stirs and obtains described cream or breast.
Further, the emulsifying agent is cetearyl alcohol ether -6;The assistant for emulsifying agent is cetearyl alcohol ether -25;The increasing
Thick dose is carbomer;The preservative is one or both of Bronopol or IPBC mixture.
It is another object of the present invention to what is be achieved through the following technical solutions:
A kind of Essence or surfactant that with the addition of described plant extracts microcapsules, the Essence or surfactant
The ratio of weight and number of raw material and each raw material is:
Glycerine 3 ~ 5
Propane diols 2 ~ 4
Hydroxyethyl cellulose(HEC) 0.1~1
Sodium Hyaluronate 0.01 ~ 0.5
Plant composition microcapsules 1 ~ 5
Deionized water 81 ~ 94
Preservative 0.1 ~ 1
Essence 0.1 ~ 1
Solubilizer 0.1 ~ 1.
Described Essence or the preparation method of surfactant, comprise the following steps:
HEC powder is first dissolved as to the HEC solution of 1 ~ 3% concentration, plant composition microcapsules propane diols with deionized water
It is pre-dispersed or be pre-dissolved with deionized water as the aqueous solution of 0.5 ~ 2% concentration, remaining each raw material is then sequentially added, is stirred,
Obtain described Essence or surfactant.
Present invention beneficial effect compared with prior art is:
1st, the present invention uses newest plant compounded combination, while innovates the extraction process of the plant extracts, compounds
Extract synergetic is obvious;
2nd, microcapsules technology is applied to cosmetic industry by the present invention, by the composition of biologically active labile(As naturally carried
Take liquid etc.)Wrap up in microcapsules, these microcapsules are then added to cosmetics again.So, plant extracts is both improved
Addition, maintain the activity of bioactive ingredients, and do not change the physicochemical property of cosmetics, and do not influence its in formula
The effect of its composition;
3rd, the ordinary cosmetics containing kindred plant extract, i.e., the cosmetics of unencapsulated processing, during room temperature, 8 ~
Metachromatism just occurs within 12 months, shelf life of products was at 1 year or so;And the present invention is prepared by micro-capsule package technology
Cosmetics, shelf life of products rises appreciably, and the shelf-life can at least extend 1 year compared to above-mentioned ordinary cosmetics, product physics and chemistry
Property is stable, and the shelf-life was at 2 ~ 3 years or so;
4th, the present invention prepares antieczematic sustained release children's skin-protection product using advanced micro-capsule package technology, can answer extensively
For cosmetics for children field.
Embodiment
Embodiment 1
One kind of multiple plant compositions, the raw material of the composition include ginkgo leaf, chrysanthemum indicum, honeysuckle, radix glycyrrhizae, Pu Gong
English and oat, the ratio of weight and number of each raw material are:
Ginkgo leaf 0.5 ~ 1
Chrysanthemum indicum 0.5 ~ 1
Honeysuckle 0.5 ~ 1
Radix glycyrrhizae 1 ~ 3
Dandelion 2 ~ 4
Oat 4 ~ 6.
Described various plants composition extracts obtained plant extracts, and extracting method comprises the following steps:
1)6 kinds of above-mentioned plants are filtered out, ginkgo leaf, chrysanthemum indicum, honeysuckle, radix glycyrrhizae, dandelion and oat will be described
6 kinds of plant effect positions carry out pulverization process respectively, cross 20 mesh sieves, obtain 6 kinds of plant flours, standby;
2)By above-mentioned steps 1)6 kinds of obtained plant flours are mixed by above-mentioned ratio of weight and number, obtain the mixing of plant flour
Thing;
3)Take 10g steps 2)The obtained plant flour mixture, according to solid-liquid ratio 1:10, mixed to the plant flour
In compound add deionized water stir, stand 30min, decoct 30min or ethanol extraction 1h, be filtrated to get supernatant A and
Filter residue;
4)Step 3)Obtained filter residue is according to solid-liquid ratio 1:10, into the filter residue, addition deionized water stirs, quiet
30min is put, 30min or ethanol extraction 1h is decocted, is filtrated to get supernatant B, merges supernatant A and supernatant B, obtain supernatant
Liquid;
5)Centrifugation removes contamination precipitation, obtain supernatant it is concentrated again after, be settled to 10ml, that is, obtain described more plantations
The plant extracts of compositions;The method for concentration is rotary distillation, reclaims ethanol.
Embodiment 2
One kind of multiple plant compositions are present embodiments provided, are the preferred schemes on the basis of embodiment 1, it is raw materials used
Quality it is same as Example 1, the ratio of weight and number of each raw material is:
Ginkgo leaf 0.8, chrysanthemum indicum 0.8, honeysuckle 0.8, radix glycyrrhizae 2, dandelion 3, oat 5.
Embodiment 3
One kind of multiple plant compositions are present embodiments provided, are the preferred schemes on the basis of embodiment 1, it is raw materials used
Quality it is same as Example 1, the ratio of weight and number of each raw material is:
Ginkgo leaf 1, chrysanthemum indicum 1, honeysuckle thing 1, radix glycyrrhizae 2, dandelion 3, oat 5.
Embodiment 4
A kind of plant extracts microcapsules of the various plants extract containing described in embodiment 1.
The preparation method of described plant extracts microcapsules, the plant is prepared using supercritical fluid spray drying process
Extract microcapsules, it the described method comprises the following steps:
The wall material of the plant extracts microcapsules is gelatin, Arabic gum, cellulose, carboxymethyl cellulose, methylol
Cellulose, beta glucan, maltose, sucrose, chitosan, lactalbumin it is therein one or more, by wall material and the institute of embodiment 1
The various plants extractive composition stated is according to ratio of weight and number 4 ~ 10:1 ratio is containing supercritical CO2The high pressure-volume of fluid
Mixed in device, pressure condition:15 ~ 30MPa, temperature conditionss:40 ~ 80 DEG C, flow is controlled in 10 ~ 30Lh-1, that is, what is obtained is described
Plant extracts microcapsules.
Another preparation method of described plant extracts microcapsules, the plant extract is prepared using liposome method
Thing microcapsules, the described method comprises the following steps:
The wall material of the plant extracts microcapsules is lecithin, cholesterol, phosphatidyl choline, ceramide, olive oil
In one or more, for described plant extracts as core, the mixed proportion of the wall material and core is 4 ~ 10:1, by wall
Material, the water of 10 ~ 20 times of amounts of core and both mixtures are separately heated to 60 DEG C -90 DEG C, high-pressure homogeneous emulsification, that is, the institute obtained
The plant extracts microcapsules stated.
Embodiment 5
A kind of cream or emulsion that with the addition of the plant extracts microcapsules described in embodiment 4, the cream or emulsion
The ratio of weight and number of raw material and each raw material is:
A phases:
Cetostearyl alcohol 2 ~ 4
Monoglyceride 0.5 ~ 2
White oil 3 ~ 5
C 345 1~2
Emulsifying agent 1 ~ 3
Assistant for emulsifying agent 0.5 ~ 2
Thickener 1 ~ 2
B phases:
Deionized water 67 ~ 87
Glycerine 3 ~ 5
EDTA-2NA 0.1~1
C phases:
Preservative 0.1 ~ 1
Plant composition microcapsules 1 ~ 5
Essence 0.1 ~ 1.
Described cream or the preparation method of emulsion, comprise the following steps:
Each raw material of A phases is added to oil phase kettle respectively under normal temperature, each raw material of B phases is added to aqueous phase kettle, and is separately heated to
More than 85 DEG C, dissolving stirs, and then again mixes A phases with B, emulsifying when temperature is maintained at more than 85 DEG C, slowly
Stirring adds C phases when being cooled to 45 DEG C, stirs and obtains described cream or breast.
Observation addition plant composition microcapsules are with being directly added into identical working substance(Non- microencapsulation)Cosmetics, this reality
Apply the cream that with the addition of described plant extracts microcapsules prepared by example or emulsion appearance is finer and smoother, color is stored up in normal temperature
Deposit to 28 days, no discoloration.And it is directly added into identical working substance(Non- microencapsulation)Cosmetics, after normal temperature storage 28 days, cream
Body darkens.
Volume production product colourity situation of change is measured using Konica CM-5 spectral photometric colour measurings, sample one is micro- to add plant extracts
The product of capsule formula, sample two are the product for the formula for being directly added into plant extracts, are carried using any form plant is not added with
Take the sample of the formula of thing to make blank control, measure respectively two groups of samples normal temperature storage 14 days, 28 days, 3 months, 6 months,
The colourity of 12 months and the difference situation of change of blank sample are as a result as follows:
As can be seen here, sample one(Add the sample of plant microcapsules)With sample two(Non- microencapsulation plant is added to carry
Take the sample of thing)Being compareed with blank product, the two has the phenomenon to darken, and sample one is more slightly smaller than the change of sample second colors, with
The extension of time, the aberration of sample two and reference substance is increasing, and sample production of the same colour substantially change is little, illustrates addition
The sample of plant society of the product of plant composition microcapsules with adding non-microencapsulation carries significantly in terms of colour stability
It is high.
Other Consumer's Experience, the cream or breast that with the addition of described plant extracts microcapsules prepared by the present embodiment
Liquid, the sensitive effect of confrontation skin, which is significantly better than, is directly added into identical working substance(Non- microencapsulation)Cosmetics, and effect is more
Persistently, it is provided simultaneously with certain moistening effect.
Embodiment 6
A kind of Essence or surfactant that with the addition of described plant extracts microcapsules, the Essence or surfactant
The ratio of weight and number of raw material and each raw material is:
Glycerine 3 ~ 5
Propane diols 2 ~ 4
HEC 0.1~1
Sodium Hyaluronate 0.01 ~ 0.5
Plant composition microcapsules 1 ~ 5
Deionized water 81 ~ 94
Preservative 0.1 ~ 1
Essence 0.1 ~ 1
Solubilizer 0.1 ~ 1.
Further, the solubilizer is LRI;The preservative is the mixed of one or both of Bronopol or IPBC
Compound.
Described Essence or the preparation method of surfactant, comprise the following steps:
HEC powder is first dissolved as to the HEC solution of 1 ~ 3% concentration, plant composition microcapsules propane diols with deionized water
It is pre-dispersed or be pre-dissolved with deionized water as the aqueous solution of 0.5 ~ 2% concentration, remaining each raw material is then sequentially added, is stirred,
Obtain described Essence or surfactant.
The Essence that with the addition of described plant extracts microcapsules or surfactant manufactured in the present embodiment are with containing not micro- glue
The water or elite of the plant composition of encapsulated are compared, product heat-resistant stability and storage at normal temperature stability prepared by the present embodiment
Enhancing, product colour is relatively stable, and can effectively alleviate that sensitiveness skin is rubescent, itches or harsh feeling, efficacy lasting, makes for a long time
With that can make, skin is more smooth, and sensitiveness reduces.
Claims (8)
- A kind of 1. microcapsules containing plant extracts, it is characterised in that the plant extracts for extracting to obtain by plant composition, The raw material of the plant composition is made up of ginkgo leaf, chrysanthemum indicum, honeysuckle, radix glycyrrhizae, dandelion and oat, each raw material Ratio of weight and number is:Ginkgo leaf 0.5 ~ 1Chrysanthemum indicum 0.5 ~ 1Honeysuckle 0.5 ~ 1Radix glycyrrhizae 1 ~ 3Dandelion 2 ~ 4Oat 4 ~ 6;Extracting method comprises the following steps:1)Filter out 6 kinds of above-mentioned plants, ginkgo leaf, chrysanthemum indicum, honeysuckle, radix glycyrrhizae, dandelion and oat, by described 6 kinds Plant effect position carries out pulverization process respectively, crosses 20 mesh sieves, obtains 6 kinds of plant flours, standby;2)By above-mentioned steps 1)6 kinds of obtained plant flours, and mixed according to above-mentioned ratio of weight and number, obtain plant flour and mix Compound;3)Take 10g steps 2)The obtained plant flour mixture, according to solid-liquid ratio 1:10, to the plant flour mixture Middle addition deionized water stirs, and stands 30min, decocts 30min or ethanol extraction 1h, is filtrated to get supernatant A and filter residue;4)Step 3)Obtained filter residue is according to solid-liquid ratio 1:10, into the filter residue, addition deionized water stirs, and stands 30min, 30min or ethanol extraction 1h is decocted, supernatant B is filtrated to get, merges supernatant A and supernatant B, obtain plant society The supernatant of extract;5)The supernatant of above-mentioned plant composition extract is first removed into contamination precipitation through centrifugation, it is concentrated again to obtain supernatant Afterwards, 10ml is settled to, that is, obtains the extract of various plants composition.
- 2. a kind of preparation method of plant extracts microcapsules as claimed in claim 1, it is characterised in that using shooting flow Spray body seasoning prepares the plant extracts microcapsules, the described method comprises the following steps:The wall material of the plant extracts microcapsules is gelatin, Arabic gum, cellulose, carboxymethyl cellulose, hydroxylmethyl cellulose Element, beta glucan, maltose, sucrose, chitosan, lactalbumin it is therein one or more, the plant described in claim 1 carries Thing is taken as core, by wall material and core according to ratio of weight and number 4 ~ 10:1 ratio is containing supercritical CO2The high pressure of fluid Mixed in container, pressure condition:15 ~ 30MPa, temperature conditionss:40 ~ 80 DEG C, flow is controlled in 10 ~ 30Lh-1, that is, the institute that obtains The plant extracts microcapsules stated.
- 3. a kind of preparation method of plant extracts microcapsules as claimed in claim 1, it is characterised in that using liposome bag Pack prepares the plant extracts microcapsules, the described method comprises the following steps:The wall material of the plant extracts microcapsules is 1 in lecithin, cholesterol, phosphatidyl choline, ceramide, olive oil Kind or it is a variety of, plant extracts described in claim 1 is used as core, and the mixed proportion of the wall material and core is 4 ~ 10:1, The water of 10 ~ 20 times of wall material, core and both mixtures amounts is separately heated to 60 DEG C -90 DEG C, high-pressure homogeneous emulsification, that is, obtained Described plant extracts microcapsules.
- 4. a kind of application of plant extracts microcapsules as claimed in claim 1, it is characterised in that the plant extracts is micro- Capsule can be added in cosmetics.
- 5. a kind of cream or emulsion that with the addition of plant extracts microcapsules as claimed in claim 1, it is characterised in that described The ratio of weight and number of the raw material and each raw material of cream or emulsion is:A phases:Cetostearyl alcohol 2 ~ 4Monoglyceride 0.5 ~ 2White oil 3 ~ 5C 345 1~2Emulsifying agent 1 ~ 3Assistant for emulsifying agent 0.5 ~ 2Thickener 1 ~ 2B phases:Deionized water 67 ~ 87Glycerine 3 ~ 5EDTA-2NA 0.1~1C phases:Preservative 0.1 ~ 1Plant composition microcapsules 1 ~ 5Essence 0.1 ~ 1.
- A kind of 6. preparation method of cream as claimed in claim 5 or emulsion, it is characterised in that the preparation method include with Lower step:Each raw material of A phases is added to oil phase kettle respectively under normal temperature, each raw material of B phases is added to aqueous phase kettle, and is separately heated to 85 DEG C More than, dissolving is stirred, and then A phases are mixed with B again, emulsifying when temperature is maintained at more than 85 DEG C, are slowly stirred C phases are added when being cooled to 45 DEG C, stirs and obtains described cream or emulsion.
- A kind of 7. Essence or surfactant that with the addition of plant extracts microcapsules as claimed in claim 1, it is characterised in that The raw material of the Essence or surfactant and the ratio of weight and number of each raw material are:Glycerine 3 ~ 5Propane diols 2 ~ 4HEC 0.1~1Sodium Hyaluronate 0.01 ~ 0.5Plant composition microcapsules 1 ~ 5Deionized water 81 ~ 94Preservative 0.1 ~ 1Essence 0.1 ~ 1Solubilizer 0.1 ~ 1.
- A kind of 8. preparation method of Essence as claimed in claim 7 or surfactant, it is characterised in that the preparation method bag Include following steps:HEC powder is first dissolved as to the HEC solution of 1 ~ 3% concentration with deionized water, plant composition microcapsules propane diols divides in advance Dissipate or be pre-dissolved with deionized water as the aqueous solution of 0.5 ~ 2% concentration, then sequentially add remaining each raw material, stir, produce To described Essence or surfactant.
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