CN105726456B - A kind of herbaceous plant nutritive water and preparation method thereof of emulsification microcapsules - Google Patents
A kind of herbaceous plant nutritive water and preparation method thereof of emulsification microcapsules Download PDFInfo
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- CN105726456B CN105726456B CN201610113396.XA CN201610113396A CN105726456B CN 105726456 B CN105726456 B CN 105726456B CN 201610113396 A CN201610113396 A CN 201610113396A CN 105726456 B CN105726456 B CN 105726456B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/56—Compounds, absorbed onto or entrapped into a solid carrier, e.g. encapsulated perfumes, inclusion compounds, sustained release forms
Abstract
The present invention provides a kind of herbaceous plant nutritive water and preparation method thereof based on emulsification microcapsules, the specific steps are：Hydrogenated vegetable oil, Canola Oil, siloxanes, microwax and diglycerol are mixed, heating stirring is uniform, and insulated sterilizing obtains oil phase；Ethylene glycol, propylene glycol, glycine betaine, urea, polyglutamic acid sodium, triethanolamine, decoyl hydroximic acid, hexylene glycol are added in deionized water, heating stirring is uniform, and insulated sterilizing obtains water phase；During the oil phase is added to the aqueous phase, heat homogeneous stirring at low speed again, after cetanol ethylhexoate, stearic acid is added, it is slow added into Cremophor RH40 and microcapsule wall material, cooling, white fungus, centella, giant knotweed, radix scutellariae, tealeaves, glycyrrhiza glabra, Flos Chrysanthemi, rosemary leave, saccharomyces cerevisiae and uva cell extract active constituent is added, add Chondrus crispus extract, biological carbohydrate gum -1, diglycerol, palmityl tripeptides -1, essence, mixing obtains the herbaceous plant nutritive water based on emulsification microcapsules.
Description
Technical field：
The invention belongs to daily cosmetics technical fields, and in particular to it is a kind of emulsification microcapsules herbaceous plant nutritive water and
Preparation method.
Background technology：
Skin is one of maximum organ of human body area, and skin is made of epidermis, corium and subcutaneous tissue, and epidermis is skin
One layer of outermost, can be divided into cuticula, hyaline layer, stratum granulosum, stratum spinosum epidermidis and basal layer from inside to outside, and the quality of skin is
The buffer capacity to extraneous acid or alkali environment is shown as, if the pH value of skin is chronically at except 5.0-5.6, the skin quality of skin is rescued
It returns and changes, eventually lead to the damages such as aging, raw spot, the melanin pigmentation of skin.Therefore it needs that suitable skin care item is selected to keep
Skin ph value makes skin maintain optimum state between 5.0-5.6, is really achieved the effect of beautiful health.
Surfactant is the transparent skin-care product using water as solvent, it has the similarly effect of cream kind cosmetics, can make skin
The physiological function for keeping soft, moist, adjust and improving skin, is broadly divided into nutritive water, toner, shrinkage water, makeup remover etc..
Nutritive water is also referred to as equilibrium liquid, is a kind of neutral toner, its property and the pH value of people are very close, are with plant component
It is main, include many nutritional ingredients and multivitamin, can balance skin acid-base value, pore refining, supplement the nutrition of skin with
Moisture increases the resistance of skin, slows down cutaneous pigmentation.
A kind of skin care containing plant extracts disclosed in Chinese patent CN 103251530B (publication date 2013.8.21)
Frost is carried by adding pure natural green-tea extract, licorice root extract, Rosmarinus officinalis extract, scutellariae,radix in face cream raw material
Object, chrysanthemum extract and Gotu Kola P.E are taken, this six Plant Extracts shows effect that is anti-inflammatory, improving immunity, energy
Inhibit inflammation in practice comprehensively, there is class effects of antibiotics to have no safe without side-effects, while also there is anti-oxidant, machine moisturizing of releiving
Cooperative effect, baby can be suitble to use.Microemulsified disclosed in Chinese patent CN 102068389A (publication date 2011.5.25)
Feature of environmental protection facial treatment milk and preparation method, including emulsifier, oil-phase component, functional component, preservative and essence, wherein oil phase at
It includes food grade White Mineral Oil, refined plant oil etc. to divide, and water-phase component includes efficient moisture-retention agent, propylene glycol, glycerine etc., functional component
Including biocatalyst and chlorophyll, skin care milk is distributed in by biocatalyst and chlorophyll are well-proportioned by micro-emulsion technology
In liquid, it is easy to be absorbed by the skin, and the carbon dioxide that biocatalyst and chlorophyll can absorb in air is converted into oxygen,
Obtain the environment-friendly type microemulsified facial treatment milk that stability is high, permeability is strong.
By the above-mentioned prior art it is found that the skin care item based on natural plant extracts and emulsifying technology on the market more
It is common, but the research of the especially nutritive water of the surfactant based on the technology is not much.The present invention is based on the concentration of frost and lotion
Denser, the characteristics of being unfavorable for the rapid absorption of skin, the present invention is for tea extraction, licorice disclosed in currently available technology
This six Plant Extracts of extract, Rosmarinus officinalis extract, radix scutellariae root extract, chrysanthemum extract and Gotu Kola P.E, and
The nutritive water that can be quickly absorbed by the skin is prepared in conjunction with emulsifying technology, to fast and effeciently improve moisture content, the microgroove of skin
And the problems such as colour of skin.
Invention content：
The technical problem to be solved in the present invention is to provide a kind of herbaceous plant nutritive waters and its system based on emulsification microcapsules
Preparation Method, using dried tremella extract, Gotu Kola P.E, giant knotweed root extract, radix scutellariae root extract, tea extract, light fruit
Licorice root extract, german chamomile flower extract, rosemary leaf extract, saccharomyces cerevisiae and uva cell extract are as activity
Ingredient obtains the herbaceous plant nutritive water based on emulsification microcapsules in conjunction with microcapsules technology and micro-emulsion technology.It is prepared by this method
Based on emulsification microcapsules herbaceous plant nutritive water fractions of active ingredient is scattered in solution, be partly coated on microcapsules, tie
Microcapsules technology is closed, the active constituent moment to exist in solution is made to be less readily available for absorption by the skin, and thorn of the microcapsules through extraneous factor
It goads its abrupt release into action, achievees the purpose that sustained release.
In order to solve the above technical problems, the technical scheme is that：
A kind of herbaceous plant nutritive water based on emulsification microcapsules, which is characterized in that the grass based on emulsification microcapsules
This plant nutrient water includes deionized water, ethylene glycol, propylene glycol, glycine betaine, urea, polyglutamic acid sodium, five poly dimethyl silicon of ring
It is oxygen alkane, dimethyl silicone polymer, phenyl trimethicone, cetanol ethylhexoate, hydrogenated vegetable oil, stearic acid, low
Erucic acid rapeseed oil, microwax, allantoin, Chondrus crispus extract, biological carbohydrate gum -1, diglycerol, palmityl tripeptides -1, β-Portugal
Glycan, dried tremella extract, Gotu Kola P.E, giant knotweed root extract, radix scutellariae root extract, tea extract, glycyrrhiza glabra root
Extract, german chamomile flower extract, rosemary leaf extract, carbomer, triethanolamine, 1,2- hexylene glycols, decoyl hydroximic acid, 1,3-
Propylene glycol, hexylene glycol, saccharomyces cerevisiae, uva cell extract, Cremophor RH40 and daily essence.
Preferably, it is described based on emulsification microcapsules herbaceous plant nutritive water component by weight, including：Deionization
35-45 parts of water, 5-8 parts of ethylene glycol, 4-9 parts of propylene glycol, 5-10 parts of glycine betaine, 3-6 parts of urea, 2-5 parts of polyglutamic acid sodium, ring five
1-3 parts of dimethyl silicone polymer, 2-5 parts of dimethyl silicone polymer, 3-4 parts of phenyl trimethicone, cetanol ethyl hexyl
6-9 parts of acid esters, 1-2 parts of hydrogenated vegetable oil, 8-12 parts of stearic acid, 3-7 parts of Canola Oil, 2-4 parts of microwax, allantoin 3-
5 parts, 8-13 parts of Chondrus crispus extract, biological -15-7 parts of carbohydrate gum, 4-9 parts of diglycerol, -13-6 parts of palmityl tripeptides, β-Portugal
8-15 parts of glycan, 6-12 parts of dried tremella extract, 4-8 parts of Gotu Kola P.E, 5-9 parts of giant knotweed root extract, radix scutellariae root extract
7-13 parts, 8-14 parts of tea extract, 3-7 parts of glycyrrhiza glabra root extract, 5-10 parts of german chamomile flower extract, rosemary leave extraction
7-14 parts of object, 10-16 parts of carbomer, 4-8 parts of triethanolamine, 9-10 parts of 1,2- hexylene glycols, 6-8 parts of decoyl hydroximic acid, 1,3- third
7-10 parts of glycol, 5-8 parts of hexylene glycol, 5-8 parts of saccharomyces cerevisiae, 9-16 parts of uva cell extract, PEG-40 hydrogenated castors
Oily 5-10 parts and 3-8 parts of daily essence.
Preferably, further include microcapsules in the herbaceous plant nutritive water based on emulsification microcapsules, the microcapsules packet
Core material and wall material are included, the wall material is made of beta cyclodextrin and bud dextrin, and the core material includes that dried tremella extract, centella carry
Object, giant knotweed root extract, radix scutellariae root extract, tea extract, glycyrrhiza glabra root extract, german chamomile flower extract, fan is taken to change
Herba Pelargonii Graveolentis extract, saccharomyces cerevisiae and uva cell extract active constituent.
The present invention also provides a kind of preparation methods of the herbaceous plant nutritive water based on emulsification microcapsules, it is characterised in that：
Include the following steps：
(1) hydrogenated vegetable oil, Canola Oil, ring five dimethyl silicone polymer, dimethyl silicone polymer, phenyl are gathered
Trimethicone, microwax and diglycerol mixing, 70-80 DEG C of heating stirring is uniform, and insulated sterilizing 15-20min obtains oil
Phase；
(2) by ethylene glycol, propylene glycol, glycine betaine, urea, polyglutamic acid sodium, triethanolamine, 1,2- hexylene glycols, decoyl hydroxyl
Oxime acid, 1,3-PD, hexylene glycol are added in deionized water, and 80-90 DEG C of heating stirring is uniform, and insulated sterilizing 15-20min is obtained
To water phase；
(3) oil phase for preparing step (1) is added in water phase prepared by step (2), and 80-90 DEG C of heating homogeneous stirring is low again
Speed stirring is added after cetanol ethylhexoate, stearic acid, urea and carbomer homogeneous stirring again, is slow added into PEG-40
Rilanit special and microcapsule wall material are cooled to 35-40 DEG C, and dried tremella extract, Gotu Kola P.E, polygoni cuspidati,radix extraction is added
Object, radix scutellariae root extract, tea extract, glycyrrhiza glabra root extract, german chamomile flower extract, rosemary leaf extract, beer
Saccharomycete and uva cell extract active constituent, add Chondrus crispus extract, beta glucan, biological carbohydrate gum -1,
Diglycerol, palmityl tripeptides -1 and essence, stirring at low speed are uniformly mixed, and obtain the herbaceous plant nutrition based on emulsification microcapsules
Water.
As a preferred embodiment of the above technical solution, in the step (1) or step (2), insulated sterilizing is ultraviolet disinfection.
As a preferred embodiment of the above technical solution, in the step (3), the rotating speed of homogeneous stirring is 3500-5000r/min,
Time is 30-50min.
As a preferred embodiment of the above technical solution, in the step (3), the rotating speed of stirring at low speed is 500-1000r/min, when
Between be 10-30min.
As a preferred embodiment of the above technical solution, in the step (3), in the herbaceous plant nutritive water based on emulsification microcapsules
The grain size of microcapsules is 1-2 μm,
As a preferred embodiment of the above technical solution, in the step (3), microcapsule wall material is chitosan, sodium alginate.
Compared with prior art, the invention has the advantages that：
(1) a variety of active ingredients, white fungus are rich in the herbaceous plant nutritive water based on emulsification microcapsules prepared by the present invention
Extract, Gotu Kola P.E, giant knotweed root extract, radix scutellariae root extract, tea extract, glycyrrhiza glabra root extract, mother
Chrysanthemum extract, rosemary leaf extract, saccharomyces cerevisiae and uva cell extract active constituent, wherein tea extraction,
Licorice root extract, Rosmarinus officinalis extract, radix scutellariae root extract, chrysanthemum extract and Gotu Kola P.E, this six kinds of plants carry
Taking object table all has the effect of anti-inflammatory, raising immunity, can inhibit ten several inflammation comprehensively, have class effects of antibiotics to have no safety
It is without side-effects, while also there is anti-oxidant, machine moisturizing of releiving cooperative effect, baby can be suitble to use, the present invention is on secondary basis
On also added the extract of white fungus, giant knotweed, saccharomyces cerevisiae and uva cell, protein and biological nucleic acid can be promoted to close
At improving immunity, abundant Antioxidative Factors contained in brewer's yeast fungus extract, skin elasticity can be increased, improve human body
Immunity, prevent skin aging, skin made to become fine and smooth, moistening, glossy.Grape berry extract, which has, eliminates free radical
Effect, can inhibit the formation of melanin, and oxidation resistance is big, also have contraction and convergent effect, skin tightening effect good pore.Cause
Rich in nutrition content in nutritive water prepared by this present invention, each ingredient cooperate can reach moisturizing, moisten, whitening, compact,
The multiple efficacies such as light spot, anti-inflammatory, and without toxicity.
(2) auxiliary agent there are many also containing in the herbaceous plant nutritive water based on emulsification microcapsules prepared by the present invention, wherein micro-
The fine crystalline structure of brilliant wax can connect solvent and oil, achieve the purpose that thickening, moisturizing.Ring five dimethyl silicone polymer is gathered
Dimethyl siloxane, phenyl trimethicone provide water resistant, anti-oxidant, soft, dry and comfortable effect, non-stimulated to skin
Property, bright color superior performance.Oil/water type based on the anionic emulsifier that stearic acid and bases solution generate after neutralizing
Emulsified body.Skin can be made to be isolated with extraneous dry air, the volatilization of skin epidermis moisture is adjusted, to protect skin, Bu Zhigan
Dry, chap or coarse, and can be by skin transient absorption, similar snowflake.
(3) also contain microcapsules in the herbaceous plant nutritive water based on emulsification microcapsules prepared by the present invention, microcapsules can
To coat certain active material as core material, microcapsules are attached to skin surface, release core material moment after environmental stimuli
It puts, makes the nutriment of active constituent continue to act on skin, have the function that long-effective protection.
Specific implementation mode：
Below in conjunction with specific embodiment, the present invention will be described in detail, herein illustrative examples and explanation of the invention
For explaining the present invention, but it is not as a limitation of the invention.
Embodiment 1：
(1) by weight, by 1 part of hydrogenated vegetable oil, 3 parts of Canola Oil, 1 part of five poly dimethyl silicon of ring
Oxygen alkane, 2 parts of dimethyl silicone polymer, 3 parts of phenyl trimethicone, 2 parts of microwax and 4 parts of diglycerol are mixed
It closes, 70 DEG C of heating stirrings are uniform, keep the temperature ultraviolet disinfection 15min, obtain oil phase.
(2) by weight, by 5 parts of ethylene glycol, 4 parts of propylene glycol, 5 parts of glycine betaine, 3 parts of urea, 2 parts poly-
Sodium glutamate, 4 parts of triethanolamine, 9 parts of 1,2- hexylene glycols, 6 parts of decoyl hydroximic acid, 7 parts of 1,3- propylene glycol, 5 parts
Hexylene glycol is added in 35 parts of deionized water, and 80 DEG C of heating stirrings are uniform, keeps the temperature ultraviolet disinfection 15min, obtains water phase.
(3) by weight, the oil phase prepared by step (1) is added in water phase prepared by step (2), 80 DEG C of heatings,
3500r/min homogeneous stirs 30min, then 500r/min stirring at low speed 10min, be added 6 parts cetanol ethylhexoate, 8 parts
Stearic acid, 3500r/min homogeneous stirs 30min again after 3 parts of urea and 10 parts of carbomer, be slow added into 5 parts
Cremophor RH40 and 8 parts of beta cyclodextrin and bud dextrin microcapsule wall material are cooled to 35 DEG C, and 6 parts of white fungus extraction is added
Object, 4 parts of Gotu Kola P.E, 5 parts of giant knotweed root extract, 7 parts of radix scutellariae root extract, 8 parts of tea extract, 3 parts
Glycyrrhiza glabra root extract, 5 parts of german chamomile flower extract, 7 parts of rosemary leaf extract, 5 parts saccharomyces cerevisiae part, 9
Part uva cell extract active constituent, add 8 parts of Chondrus crispus extract, 5 parts of biological carbohydrate gum -1,8 parts
Beta glucan, 4 parts of diglycerol, 3 parts of palmityl tripeptides -1 and 3 parts of essence, 500r/min stirring at low speed 10min, mix
It closes and uniformly obtains the herbaceous plant nutritive water based on emulsification microcapsules.
Embodiment 2：
(1) by weight, by 2 parts of hydrogenated vegetable oil, 7 parts of Canola Oil, 3 parts of five poly dimethyl silicon of ring
Oxygen alkane, 5 parts of dimethyl silicone polymer, 4 parts of phenyl trimethicone, 4 parts of microwax and 9 parts of diglycerol are mixed
It closes, 80 DEG C of heating stirrings are uniform, keep the temperature ultraviolet disinfection 20min, obtain oil phase.
(2) by weight, by 8 parts of ethylene glycol, 9 parts of propylene glycol, 10 parts of glycine betaine, 6 parts of urea, 5 parts
Polyglutamic acid sodium, 8 parts of triethanolamine, 10 parts of 1,2- hexylene glycols, 8 parts of decoyl hydroximic acid, 10 parts of 1,3- propylene glycol, 8
The hexylene glycol of part is added in 45 parts of deionized water, and 90 DEG C of heating stirrings are uniform, keeps the temperature ultraviolet disinfection 20min, obtains water phase.
(3) by weight, the oil phase prepared by step (1) is added in water phase prepared by step (2), 90 DEG C of heatings,
5000r/min homogeneous stirs 50min, then 1000r/min stirring at low speed 30min, the cetanol ethylhexoate of 9 parts of addition, 12
5000r/min homogeneous stirs 50min again after the stearic acid and 16 parts of carbomer of part, is slow added into 10 parts of PEG-40 hydrogenations
Castor oil and 15 parts of sodium alginate micro gel cyst wall material are cooled to 40 DEG C, and 12 parts of dried tremella extract, 8 parts of centella is added
Extract, 9 parts of giant knotweed root extract, 13 parts of radix scutellariae root extract, 14 parts of tea extract, 7 parts of glycyrrhiza glabra root
Extract, 10 parts of german chamomile flower extract, 14 parts of rosemary leaf extract, 8 parts saccharomyces cerevisiae part, 16 parts of uva
It is poly- to add 13 parts of Chondrus crispus extract, 7 parts of biological carbohydrate gum -1,15 parts of β-Portugal for cell extract active constituent
Sugar, 9 parts of diglycerol, 6 parts of palmityl tripeptides -1 and 8 parts of essence, 1000r/min stirring at low speed 30min are uniformly mixed,
Obtain the herbaceous plant nutritive water based on emulsification microcapsules.
Embodiment 3：
(1) by weight, by 1.5 parts of hydrogenated vegetable oil, 5 parts of Canola Oil, 2 parts of five poly dimethyl of ring
Siloxanes, 3 parts of dimethyl silicone polymer, 3.5 parts of phenyl trimethicone, 3 parts of microwax and 6 parts of diglycerol
Mixing, 75 DEG C of heating stirrings are uniform, keep the temperature ultraviolet disinfection 17min, obtain oil phase.
(2) by weight, by 7 parts of ethylene glycol, 6 parts of propylene glycol, 8 parts of glycine betaine, 5 parts of urea, 3 parts poly-
Sodium glutamate, 6 parts of triethanolamine, 9.5 parts of 1,2- hexylene glycols, 7 parts of decoyl hydroximic acid, 8 parts of 1,3- propylene glycol, 7 parts
Hexylene glycol be added in 40 parts of deionized water, 85 DEG C of heating stirrings are uniform, keep the temperature ultraviolet disinfection 18min, obtain water phase.
(3) by weight, the oil phase prepared by step (1) is added in water phase prepared by step (2), 80-90 DEG C of heating,
4500r/min homogeneous stirs 35min, then 800r/min stirring at low speed 20min, be added 8 parts cetanol ethylhexoate, 10 parts
Stearic acid and 14 parts of carbomer after again 4000r/min homogeneous stir 30min, be slow added into 8 parts PEG-40 hydrogenation castor
Sesame oil and 12 parts of beta cyclodextrin and bud dextrin microcapsule wall material are cooled to 38 DEG C, and 8 parts of dried tremella extract, 6 parts of product is added
The careless extract of snow, 7 parts of giant knotweed root extract, 10 parts of radix scutellariae root extract, 12 parts of tea extract, 5 parts of light fruit are sweet
Grass roots extract, 8 parts of german chamomile flower extract, 11 parts of rosemary leaf extract, 6 parts saccharomyces cerevisiae part, 13 parts of Portugal
Grape fruit cell extract active constituent adds 11 parts of Chondrus crispus extract, 6 parts of biological carbohydrate gum -1,12 parts of β -
Glucan, 5 parts of diglycerol, 4 parts of palmityl tripeptides -1 and 5 parts of essence, 800r/min stirring at low speed 15min, mixing are equal
It is even, obtain the herbaceous plant nutritive water based on emulsification microcapsules.
Embodiment 4：
(1) by weight, by 1 part of hydrogenated vegetable oil, 6 parts of Canola Oil, 1 part of five poly dimethyl silicon of ring
Oxygen alkane, 3 parts of dimethyl silicone polymer, 3 parts of phenyl trimethicone, 3 parts of microwax and 9 parts of diglycerol are mixed
It closes, 80 DEG C of heating stirrings are uniform, keep the temperature ultraviolet disinfection 15min, obtain oil phase.
(2) by weight, by 6 parts of ethylene glycol, 5 parts of propylene glycol, 5 parts of glycine betaine, 5 parts of urea, 3 parts poly-
Sodium glutamate, 6 parts of triethanolamine, 9 parts of 1,2- hexylene glycols, 6 parts of decoyl hydroximic acid, 9 parts of 1,3- propylene glycol, 6 parts
Hexylene glycol is added in 40 parts of deionized water, and 90 DEG C of heating stirrings are uniform, keeps the temperature ultraviolet disinfection 15min, obtains water phase.
(3) by weight, the oil phase prepared by step (1) is added in water phase prepared by step (2), 90 DEG C of heatings,
4500r/min homogeneous stirs 40min, then 800r/min stirring at low speed 30min, be added 8 parts cetanol ethylhexoate, 8 parts
Stearic acid and 14 parts of carbomer after again 5000r/min homogeneous stir 30min, be slow added into 7 parts PEG-40 hydrogenation castor
Sesame oil and 12 parts of chitosan microcapsules wall material are cooled to 35 DEG C, and 8 parts of dried tremella extract, the extraction of 4 parts of centella is added
Object, 6 parts of giant knotweed root extract, 8 parts of radix scutellariae root extract, 10 parts of tea extract, the extraction of 5 parts of glycyrrhiza glabra root
Object, 5 parts of german chamomile flower extract, 8 parts of rosemary leaf extract, 6 parts saccharomyces cerevisiae part, 14 parts of uva cell carry
Take object active constituent, add 9 parts Chondrus crispus extract, 6 parts of biological carbohydrate gum -1,12 parts of beta glucan, 5 parts
Diglycerol, 4 parts of palmityl tripeptides -1 and 6 parts of essence, 700r/min stirring at low speed 25min are uniformly mixed, and are obtained based on breast
The herbaceous plant nutritive water of microcapsules.
Embodiment 5：
(1) by weight, by 2 parts of hydrogenated vegetable oil, 3 parts of Canola Oil, 3 parts of five poly dimethyl silicon of ring
Oxygen alkane, 2 parts of dimethyl silicone polymer, 4 parts of phenyl trimethicone, 4 parts of microwax and 4 parts of diglycerol are mixed
It closes, 80 DEG C of heating stirrings are uniform, keep the temperature ultraviolet disinfection 20min, obtain oil phase.
(2) by weight, by 8 parts of ethylene glycol, 4 parts of propylene glycol, 10 parts of glycine betaine, 6 parts of urea, 2 parts
Polyglutamic acid sodium, 8 parts of triethanolamine, 9 parts of 1,2- hexylene glycols, 6 parts of decoyl hydroximic acid, 7 parts of 1,3- propylene glycol, 5 parts
Hexylene glycol be added in 35 parts of deionized water, 90 DEG C of heating stirrings are uniform, keep the temperature ultraviolet disinfection 15min, obtain water phase.
(3) by weight, the oil phase prepared by step (1) is added in water phase prepared by step (2), 90 DEG C of heatings,
5000r/min homogeneous stirs 30min, then 1000r/min stirring at low speed 10min, the cetanol ethylhexoate of 9 parts of addition, 12
5000r/min homogeneous stirs 30min again after the stearic acid and 10 parts of carbomer of part, is slow added into 10 parts of PEG-40 hydrogenations
Castor oil and 15 parts of chitosan microcapsules wall material are cooled to 40 DEG C, 12 parts of dried tremella extract are added, 8 parts of centella carries
Object, 5 parts of giant knotweed root extract, 13 parts of radix scutellariae root extract, 14 parts of tea extract, 7 parts of glycyrrhiza glabra root is taken to carry
Object, 5 parts of german chamomile flower extract, 7 parts of rosemary leaf extract, 8 parts of saccharomyces cerevisiae, 9 parts of uva cell is taken to carry
Take object active constituent, add 8 parts Chondrus crispus extract, 5 parts of biological carbohydrate gum -1,8 parts of beta glucan, 9 parts
Diglycerol, 6 parts of palmityl tripeptides -1 and 8 parts of essence, 1000r/min stirring at low speed 10min are uniformly mixed, are based on
Emulsify the herbaceous plant nutritive water of microcapsules.
Embodiment 6：
(1) by weight, by 1 part of hydrogenated vegetable oil, 4 parts of Canola Oil, 3 parts of five poly dimethyl silicon of ring
Oxygen alkane, 3 parts of dimethyl silicone polymer, 3 parts of phenyl trimethicone, 4 parts of microwax and 4 parts of diglycerol are mixed
It closes, 80 DEG C of heating stirrings are uniform, keep the temperature ultraviolet disinfection 20min, obtain oil phase.
(2) by weight, by 8 parts of ethylene glycol, 8 parts of propylene glycol, 8 parts of glycine betaine, 4 parts of urea, 4 parts poly-
Sodium glutamate, 8 parts of triethanolamine, 10 parts of 1,2- hexylene glycols, 8 parts of decoyl hydroximic acid, 7 parts of 1,3- propylene glycol, 8 parts
Hexylene glycol is added in 40 parts of deionized water, and 80 DEG C of heating stirrings are uniform, keeps the temperature ultraviolet disinfection 20min, obtains water phase.
(3) by weight, the oil phase prepared by step (1) is added in water phase prepared by step (2), 80 DEG C of heatings,
4000r/min homogeneous stirs 40min, then 800r/min stirring at low speed 20min, be added 8 parts cetanol ethylhexoate, 8 parts
Stearic acid and 16 parts of carbomer after again 4000r/min homogeneous stir 50min, be slow added into 8 parts PEG-40 hydrogenation castor
Sesame oil and 8 parts of beta cyclodextrin and bud dextrin microcapsule wall material are cooled to 40 DEG C, and 8 parts of dried tremella extract, 88 parts of product is added
The careless extract of snow, 8 parts of giant knotweed root extract, 8 parts of radix scutellariae root extract, 12 parts of tea extract, 6 parts of glycyrrhiza glabra
Root extract, 5 parts of german chamomile flower extract, 8 parts of rosemary leaf extract, 7 parts of saccharomyces cerevisiae, 16 parts of uva are thin
Born of the same parents' extract active constituent, add 8 parts Chondrus crispus extract, 5 parts of biological carbohydrate gum -1,8 parts of beta glucan, 8
The diglycerol, 4 parts of palmityl tripeptides -1 and 4 parts of essence of part, 1000r/min stirring at low speed 30min are uniformly mixed, obtain
Herbaceous plant nutritive water based on emulsification microcapsules.
After testing, the grain size, resistance to of the microcapsules for the herbaceous plant nutritive water based on emulsification microcapsules that prepared by embodiment 1-6
Hot, cold resistance, the examination of skin sensing, antibiotic property, moisture retention, the result of whitening are as follows：
As seen from the above table, the herbaceous plant nutritive water stable uniformity based on emulsification microcapsules that prepared by the present invention, clearly
Moisturizing, it is not sticky, also there is antibacterial, permanent moisturizing and whitening effect.
The above-described embodiments merely illustrate the principles and effects of the present invention, and is not intended to limit the present invention.It is any ripe
The personage for knowing this technology can all carry out modifications and changes to above-described embodiment without violating the spirit and scope of the present invention.Cause
This, institute is complete without departing from the spirit and technical ideas disclosed in the present invention by those of ordinary skill in the art such as
At all equivalent modifications or change, should by the present invention claim be covered.
Claims (7)
1. a kind of herbaceous plant nutritive water based on emulsification microcapsules, which is characterized in that the draft based on emulsification microcapsules
The component of plant nutrient water by weight, including：35-45 parts of deionized water, 5-8 parts of ethylene glycol, 11-19 parts of propylene glycol, sweet tea
5-10 parts of dish alkali, 3-6 parts of urea, 2-5 parts of polyglutamic acid sodium, 1-3 parts of ring five dimethyl silicone polymer, dimethyl silicone polymer 2-
5 parts, 3-4 parts of phenyl trimethicone, 6-9 parts of cetanol ethylhexoate, 1-2 parts of hydrogenated vegetable oil, stearic acid 8-12
Part, 3-7 parts of Canola Oil, 2-4 parts of microwax, 3-5 parts of allantoin, 8-13 parts of Chondrus crispus extract, biological carbohydrate gum-
1 5-7 parts, 4-9 parts of diglycerol, -1 3-6 parts of palmityl tripeptides, 8-15 parts of beta glucan, 6-12 parts of dried tremella extract, centella
4-8 parts of extract, 5-9 parts of giant knotweed root extract, 7-13 parts of radix scutellariae root extract, 8-14 parts of tea extract, glycyrrhiza glabra root
3-7 parts of extract, 5-10 parts of german chamomile flower extract, 7-14 parts of rosemary leaf extract, 10-16 parts of carbomer, triethanolamine 4-8
Part, 6-8 parts of decoyl hydroximic acid, 14-18 parts of hexylene glycol, 5-8 parts of saccharomyces cerevisiae, 9-16 parts of uva cell extract, PEG-
3-8 parts of 40 5-10 parts of rilanit specials and daily essence；
Wherein, the herbaceous plant nutritive water based on emulsification microcapsules includes microcapsules, the microcapsules include core material with
Wall material, the wall material are made of beta cyclodextrin and bud dextrin, and the core material includes dried tremella extract, Gotu Kola P.E, giant knotweed
Root extract, radix scutellariae root extract, tea extract, glycyrrhiza glabra root extract, german chamomile flower extract, rosemary leave extraction
Object, saccharomyces cerevisiae and uva cell extract active constituent.
2. a kind of preparation method of the herbaceous plant nutritive water based on emulsification microcapsules, it is characterised in that：Include the following steps：
(1) by hydrogenated vegetable oil, Canola Oil, ring five dimethyl silicone polymer, dimethyl silicone polymer, the poly- front three of phenyl
Radical siloxane, microwax and diglycerol mixing, 70-80 DEG C of heating stirring is uniform, and insulated sterilizing 15-20min obtains oil phase；
(2) ethylene glycol, propylene glycol, glycine betaine, urea, polyglutamic acid sodium, triethanolamine, decoyl hydroximic acid, hexylene glycol are added
In deionized water, 80-90 DEG C of heating stirring is uniform, and insulated sterilizing 15-20min obtains water phase；
(3) oil phase for preparing step (1) is added in water phase prepared by step (2), and low speed stirs again for 80-90 DEG C of heating homogeneous stirring
It mixes, homogeneous stirring again is added after cetanol ethylhexoate, stearic acid, urea and carbomer, be slow added into PEG-40 hydrogenations
Castor oil and microcapsule wall material are cooled to 35-40 DEG C, and dried tremella extract, Gotu Kola P.E, giant knotweed root extract, Huang is added
A kind of reed mentioned in ancient books root extract, tea extract, glycyrrhiza glabra root extract, german chamomile flower extract, rosemary leaf extract, saccharomyces cerevisiae
With uva cell extract active constituent, add Chondrus crispus extract, biological carbohydrate gum -1, beta glucan, diglycerol,
Palmityl tripeptides -1 and essence, stirring at low speed are uniformly mixed, and obtain the herbaceous plant nutritive water based on emulsification microcapsules.
3. a kind of preparation method of herbaceous plant nutritive water based on emulsification microcapsules according to claim 2, feature
It is：In the step (1) or step (2), insulated sterilizing is ultraviolet disinfection.
4. a kind of preparation method of herbaceous plant nutritive water based on emulsification microcapsules according to claim 2, feature
It is：In the step (3), the rotating speed of homogeneous stirring is 3500-5000r/min, time 30-50min.
5. a kind of preparation method of herbaceous plant nutritive water based on emulsification microcapsules according to claim 2, feature
It is：In the step (3), the rotating speed of stirring at low speed is 500-1000r/min, time 10-30min.
6. a kind of preparation method of herbaceous plant nutritive water based on emulsification microcapsules according to claim 2, feature
It is：In the step (3), the grain size of microcapsules is 1-2 μm in the herbaceous plant nutritive water based on emulsification microcapsules.
7. a kind of preparation method of herbaceous plant nutritive water based on emulsification microcapsules according to claim 2, feature
It is：In the step (3), microcapsule wall material is made of beta cyclodextrin and bud dextrin.
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