Summary of the invention
Based on this, the object of the present invention is to provide a kind of antidotal cosmetic composition, said composition can effectively to free radical resisting, minimizing wrinkle of skin, delay skin aging.
For solving the problems of the technologies described above, the present invention is achieved through the following technical solutions:
A kind of anti-aging cosmetics compositions, described anti-aging cosmetics compositions contains Radix potentillae anserinae extracting solution, Fructus Hippophae extracting solution, Folium Hippophae extracting solution, crocus sativus and Herba Cistanches extracting solution.
In the anti-aging cosmetics compositions of the preferred embodiment of the present invention, the mass ratio that described anti-aging cosmetics contains Radix potentillae anserinae extracting solution, Fructus Hippophae extracting solution, Folium Hippophae extracting solution, crocus sativus and Herba Cistanches extracting solution is preferably (1 ~ 10%): (1 ~ 10%): (1 ~ 10%): (1 ~ 10%): (1 ~ 10%).The mass fraction summation of described Radix potentillae anserinae extracting solution, Fructus Hippophae extracting solution, Folium Hippophae extracting solution, crocus sativus and Herba Cistanches extracting solution is 0.5 ~ 5%.
A kind of anti-aging cosmetics compositions, it comprises the component of following mass percent:
In a preferred embodiment of the invention, described defying age plant extraction liquid is the mixed liquor of Radix potentillae anserinae extracting solution, Fructus Hippophae extracting solution, Folium Hippophae extracting solution, crocus sativus and Herba Cistanches extracting solution.The mass ratio of described Radix potentillae anserinae extracting solution, Fructus Hippophae extracting solution, Folium Hippophae extracting solution, crocus sativus and Herba Cistanches extracting solution is (1 ~ 10%): (1 ~ 10%): (1 ~ 10%): (1 ~ 10%): (1 ~ 10%).
In a preferred embodiment of the invention, described emulsifying agent is a kind of in hydrolecithin, lecithin, glyceryl stearate, PEG-100 stearate, sorbitan stearate, polysorbate-20, polysorbate-60, Polyoxyethylene Sorbitan Monooleate, ceteareth-25, ceteareth-6, methyl sesquistearate, PEG-20 methyl sesquistearate, Pyrusussuriensis smooth olive oil acid esters, cetearyl glucoside or their mixing.Preferred further, described emulsifying agent is the mixing of the smooth olive oil acid esters of Pyrusussuriensis, cetearyl glucoside, and the mass ratio of the smooth olive oil acid esters of described Pyrusussuriensis, cetearyl glucoside is (1 ~ 2): (0.5 ~ 1).The smooth olive oil acid esters of Pyrusussuriensis, cetearyl glucoside be by the sorbitol of natural origin, olive oil, spermol, stearyl alcohol, glucose by the obtained emulsifying agent of esterification, be a kind of originate natural, be conducive to that effect thing absorbs, non-stimulated liquid crystal emulsifier.
In a preferred embodiment of the invention, described vegetable oil is a kind of in Oleum Hippophae, Ginger Root oil, soybean oil, safflower oil, olive oil, Radix Oenotherae erythrosepalae oil, Rosehips oil, American Avocado Tree oil, Jojoba oil, Oleum Vitis viniferae, white Limnanthes Alba Seed Oil, Butyrospermum parkii fruit fatty oil, cocoa seed fat, macadimia nut seed oil, camellia seed oil, Petiolus Trachycarpi oil, palm-kernel oil, Rosa Canina fruit oil, Semen Tritici aestivi germ oil, Semen pruni armeniacae oil or their mixing.Preferred further, described vegetable oil is the mixing of Ginger Root oil, Oleum Hippophae, Oleum Vitis viniferae and Butyrospermum parkii fruit fatty oil, and described Ginger Root oil, Oleum Hippophae, Oleum Vitis viniferae and Butyrospermum parkii fruit fatty oil mass ratio are (0.1 ~ 1): (1 ~ 2): (3 ~ 6): (2 ~ 5).Ginger Root oil, extract obtained by the fresh rhizome of Zingiberaceae herbaceos perennial Rhizoma Zingiberis Recens, Ginger Root oil can impel the increase of dermal blood flow, has the effect of short infiltration.Oleum Hippophae contains the unsaturated fatty acid of more than 50% content, as the multiple beneficial such as linoleic acid, linolenic acid fatty acid, also containing a small amount of nutrient substance such as vitamin E, carotenoid, vitamin A, plant sterol, catechin, flavone compound.The unsaturated fatty acid content that Oleum Vitis viniferae contains is up to 90%, and its Linoleic acid up to more than 75%, and contains vitamin A, E, D, K, P and various trace elements.Butyrospermum parkii fruit fatty oil is soft solid oils and fats under a kind of room temperature, its fusing point is close to skin temperature, easily melt when smearing, the triglyceride of Butyrospermum parkii fruit contained by fatty oil are up to 80%, unsaponifiable matters about 9 ~ 13%, have good skin moistening, antiinflammatory, short effect of oozing, promoting wound healing, Butyrospermum parkii fruit fatty oil also has slight ultraviolet blocking-up effect in addition.Oleum Hippophae, Oleum Vitis viniferae and Butyrospermum parkii fruit fatty oil combination can play skin nutrition, promote infiltration, slow down aging effect.
16/18 alcohol of the present invention, be the mixture of C16 alcohol and C18 alcohol, preferably, C16 alcohol: when the mass ratio of C18 alcohol is 4:6, can make system stability increase.Its source is by Oleum Gossypii semen, Petiolus Trachycarpi oil through ester exchange, then high pressure adds hydrogen reduction and obtains.It plays thick stabilization in this formula.
1,3-PD of the present invention, is obtained through biofermentation by the sugar of corn source, originates natural.1,3-PD is a kind of excellent penetrating agent, and it and Ginger Root oil have synergism, can better promote that composite skin care product enters deep layer and body circulation through skin surface.In compositions of the present invention, both containing 1, ammediol, again containing Ginger Root oil, advantageously in the permeance property improving working substance in Fructus Lycii, Fructus Mori, Semen Coicis extracting solution, promotes that human body is for the absorption of working substance in Radix potentillae anserinae, Fructus Hippophae, Folium Hippophae, Stigma Croci and Herba Cistanches extracting solution.
In a preferred embodiment of the invention, described antiseptic can be pentanediol, hexanediol, glycerol caprylate, imidazolidinyl urea, DMDM Hydantoin, Methylisothiazolinone, parabens.Preferred further, described antiseptic is the mixing of hexanediol and glycerol caprylate, and the mass ratio of described hexanediol and glycerol caprylate is (0.3 ~ 0.6): (0.1 ~ 0.5).
Radix potentillae anserinae extracting solution of the present invention, Fructus Hippophae extracting solution, Folium Hippophae extracting solution, crocus sativus and Herba Cistanches extracting solution, can be prepared, preferably with preparation prepared by following method by conventional production technology:
(1) plant (Radix potentillae anserinae, Fructus Hippophae, Folium Hippophae, Stigma Croci and Herba Cistanches or their mixing) is shredded, be immersed in about 24 hours (soaking in Mel of the medicinal herbs 3kg of 1kg) in Mel, then dry.
(2) plant dry in step (1) is joined in the ethanol of 75%, adopt frequency to be the ultrasonic Treatment 3-5 minute of 20kHZ, under backflow and dipping, carry out extraction 4 ~ 8h.Subsequently, with filter cloth, extracting solution is filtered, more namely centrifugalize obtains Medicinal Herbs Extract.
The way of Chinese medicine processed with honey is adopted in above-mentioned steps (1), with soaking in Mel Radix potentillae anserinae, Fructus Hippophae, Folium Hippophae, Stigma Croci and Herba Cistanches or their mixing, enhance the dissolving of working substance in Radix potentillae anserinae, Fructus Hippophae, Folium Hippophae, Stigma Croci and Herba Cistanches or their mixing, thus improve the extraction quantity of working substance; Mel inherently has promotion cell regeneration, the effect of cosmetology, can increase the skin-care effect of extracting solution; Mel has the effect of anti-inflammation, can promote the shelf life of extracting solution.
Composite skin care product of the present invention can by the preparation of conventional production technology, preferred following preparation method, and it comprises the following steps:
1) mentioned emulsifier, 16/18 alcohol, vegetable oil are dropped into oil phase pot, be heated to 70 ~ 85 DEG C, heat preservation for standby use after waiting all components to melt.
2) above-mentioned glycerol, 1,3-PD, HANSHENGJIAO, hyaluronate sodium, water are dropped into emulsifying pot, be heated to 70 ~ 85 DEG C, be incubated 15 ~ 30 minutes.
3) by step 1) in oil phase suction step 2) emulsifying pot in, homogenizing (homogenizing stir speed (S.S.) is 3000rpm) insulated and stirred (stir speed (S.S.) is 30rpm) 15 ~ 45 minutes after 3 ~ 15 minutes.
4) under 102 ~ 108MPa pressure, 81 ~ 82 DEG C of temperature conditions, by high pressure homogenizer circulation homogenizing 8 ~ 9 times, control homogenizer outlet temperature lower than 85 DEG C, obtain the microemulsion of particle diameter at below 100nm.
5) by step 4) in emulsion be cooled to 40 ~ 45 DEG C, add above-mentioned defying age plant extraction liquid, preservative component, stir.
The preparation method of the nanoemulsions obtained by above-mentioned technique, have employed 2 homogenizing methods, use for the 1st time common homogenizer to obtain emulsified body, adopt for the 2nd time high pressure homogenizer to obtain nanoemulsions, obtained nanoemulsions particle diameter evenly, long-time stability of placing is better.Preparation process is simple and convenient, constant product quality, and large-scale industrial is produced convenient.
Compared with prior art, anti-apolexis composition prepared by the present invention is selected from five kind of plant raw materials, form through effective ratio science is composite, its main active is divided into two kinds: one to be the natural anti-oxidation factor that is main active with flavone, vitamins, as potentilla anserina extract, seabuckthorn fruit extract, Stigma Croci extract, Herba Cistanches extract; Two is the ultra-violet absorption factors that are main active with quinones, terpenoid, as Folium Hippophae extract and Herba Cistanches extract.Above-mentioned two class active skull cap components create good cooperative effect after ratio of the present invention is composite, on the one hand by free radical resisting effect of the Natural antioxidant, free radical unnecessary in purged body, reduce inherent cell injury, on the other hand by the ultra-violet absorption factor, effective absorption ultraviolet, reduce external cell injury, after both scientific combination are composite, the characteristic of each component plays complementation, coordinative role, produce cooperative effect, its defying age performance is much better than unicity antidotal agent, skin permeability is strong, good stability, pure natural, safe and non-stimulating, have nutrition concurrently and moisten effect, through repetition test, component proportion of the present invention can reach maximum product efficacy, can effectively to free radical resisting, reduce wrinkle of skin, delay skin aging, there is good defying age ability.
The preparation of embodiment 5 anti-apolexis composition
The present invention is prepared described anti-apolexis composition, with the addition of defying age plant extraction liquid obtained by embodiment 1 ~ 4 respectively for enforcement group I ~ IV, and be provided with matched group I ~ IV, the defying age plant extraction liquid that matched group I ~ IV uses obtains respectively as follows:
Matched group I:(1) take Radix potentillae anserinae 0.1 part, Fructus Hippophae 4 parts, Folium Hippophae 6 parts, Stigma Croci 5 parts and Herba Cistanches 4 parts.(2) plant (Radix potentillae anserinae, Fructus Hippophae, Folium Hippophae, Stigma Croci and Herba Cistanches or their mixing) is shredded, be immersed in about 24 hours (soaking in Mel of the medicinal herbs 3kg of 1kg) in Mel, then dry.(3) plant dry in step (2) is joined in the ethanol of 75%, adopt frequency to be the ultrasonic Treatment 4 minutes of 20kHZ, under backflow and dipping, carry out extraction 5h.Subsequently, with filter cloth, extracting solution is filtered, more namely centrifugalize obtains Medicinal Herbs Extract.
Matched group II: (1) takes Radix potentillae anserinae 5 parts, Fructus Hippophae 0.1 part, Folium Hippophae 6 parts, Stigma Croci 5 parts and Herba Cistanches 4 parts.(2) plant (Radix potentillae anserinae, Fructus Hippophae, Folium Hippophae, Stigma Croci and Herba Cistanches or their mixing) is shredded, be immersed in about 24 hours (water soaking of the medicinal herbs 3kg of 1kg) in water, then dry.(3) plant dry in step (2) is joined in the ethanol of 75%, adopt frequency to be the ultrasonic Treatment 4 minutes of 20kHZ, under backflow and dipping, carry out extraction 5h.Subsequently, with filter cloth, extracting solution is filtered, more namely centrifugalize obtains Medicinal Herbs Extract.
Matched group III: (1) takes Radix potentillae anserinae 5 parts, Fructus Hippophae 4 parts, Folium Hippophae 0.1 part, Stigma Croci 5 parts and Herba Cistanches 4 parts.(2) plant (Radix potentillae anserinae, Fructus Hippophae, Folium Hippophae, Stigma Croci and Herba Cistanches or their mixing) is shredded, be immersed in about 24 hours (water soaking of the medicinal herbs 3kg of 1kg) in water, then dry.(3) plant dry in step (2) is joined in the ethanol of 75%, adopt frequency to be the ultrasonic Treatment 4 minutes of 20kHZ, under backflow and dipping, carry out extraction 5h.Subsequently, with filter cloth, extracting solution is filtered, more namely centrifugalize obtains Medicinal Herbs Extract.
Matched group IV: (1) takes Radix potentillae anserinae 5 parts, Fructus Hippophae 4 parts, Folium Hippophae 6 parts, Stigma Croci 5 parts and Herba Cistanches 0.1 part.(2) plant (Radix potentillae anserinae, Fructus Hippophae, Folium Hippophae, Stigma Croci and Herba Cistanches or their mixing) is shredded, be immersed in about 24 hours (soaking in Mel of the medicinal herbs 3kg of 1kg) in Mel, then dry.(3) plant dry in step (2) is joined in the ethanol of 75%, adopt frequency to be the ultrasonic Treatment 4 minutes of 20kHZ, under backflow and dipping, carry out extraction 5h.Subsequently, with filter cloth, extracting solution is filtered, more namely centrifugalize obtains Medicinal Herbs Extract.
A kind of composite skin care product, it is made up of the component of following table mass percent:
Preparation technology:
1) above-mentioned A phase is dropped into oil phase pot, be heated to 80 DEG C, heat preservation for standby use after waiting all components to melt.
2) above-mentioned B phase is dropped into emulsifying pot, be heated to 70 DEG C, be incubated 130 minutes.
3) by step 1) in A phase suction step 2) emulsifying pot in, homogenizing (homogenizing stir speed (S.S.) is 3000rpm) insulated and stirred (stir speed (S.S.) is 30rpm) 45 minutes after 3 minutes.
4) under 102MPa pressure, 81 DEG C of temperature conditions, by high pressure homogenizer circulation homogenizing 9 times, control homogenizer outlet temperature lower than 85 DEG C, obtain the microemulsion of particle diameter at below 100nm.
5) by step 4) in emulsion be cooled to 40 DEG C, add above-mentioned C phase component, stir.
The composite skin care product that above-described embodiment is obtained, each embodiment is respectively after 20 personnel continuously 30 days on probation, and result is as follows:
The above, it is only preferred embodiment of the present invention, not any pro forma restriction is done to the present invention, therefore all contents not departing from technical solution of the present invention, according to technical spirit of the present invention to any simple modification made for any of the above embodiments, equivalent variations and modification, all still belong in the scope of technical solution of the present invention.