CN109674666A - It is a kind of containing beta glucan-coriander essential oil microcapsules deodorization hand cleanser and preparation method thereof - Google Patents
It is a kind of containing beta glucan-coriander essential oil microcapsules deodorization hand cleanser and preparation method thereof Download PDFInfo
- Publication number
- CN109674666A CN109674666A CN201910038431.XA CN201910038431A CN109674666A CN 109674666 A CN109674666 A CN 109674666A CN 201910038431 A CN201910038431 A CN 201910038431A CN 109674666 A CN109674666 A CN 109674666A
- Authority
- CN
- China
- Prior art keywords
- essential oil
- beta glucan
- coriander
- oil microcapsules
- deodorization
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/11—Encapsulated compositions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q15/00—Anti-perspirants or body deodorants
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Dermatology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Cosmetics (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses a kind of containing beta glucan-coriander essential oil microcapsules deodorization hand cleanser and preparation method thereof, the deodorization hand cleanser containing beta glucan-coriander essential oil microcapsules is composed of the following components: beta glucan-coriander essential oil microcapsules, surfactant, antibacterial agent, thickener, pH adjusting agent, essence, preservative, surplus are deionized water.The preparation method of the deodorization hand cleanser of the present invention containing beta glucan-coriander essential oil microcapsules includes the following steps: that beta glucan-coriander essential oil microcapsules, surfactant, antibacterial agent, thickener are added to the water by (1), stirring and dissolving；(2) essence is then added and modulates specific odor type, stirring and dissolving；System pH 5.5-7 is adjusted to the cooling pH adjusting agent that is added of system；(3) preservative is added, is made after cooling containing beta glucan-coriander essential oil microcapsules deodorization hand cleanser.Deodorization effect of the present invention is obvious, and has both the effect of skin moisturizing.
Description
Technical field
The invention belongs to daily use chemicals articles for washing technical field, it is related to a kind of going containing beta glucan-coriander essential oil microcapsules
Raw meat hand cleanser and preparation method thereof.
Background technique
The fresh water such as fish, shrimp, crab or seawater aquatic products are an important composition parts of people's daily life Chinese meal diet material,
It is delicious in taste, it is full of nutrition；However all there is these aquatic products a kind of special fishy smell to add in processing and diet processes
Work person and consumer are difficult to avoid that hand or other positions of body can be stained with certain fishy smell.Common cleaning method is to pass through
Detergent (perfumed soap or common hand cleanser) is selected to clean hand, or the common perilla leaf water cleaning to boil, to reach covering hand
Or the fishy smell at other positions of body；However these methods cannot all completely remove in gastronomical process or in processor or disappear after diet
The fishy smell retained with the person of expense.Currently, hand cleanser in the market is mainly clean type, degerming type etc., these products are for aquatic products
Fishy smell caused by product all only has certain effect in removal ability, and cannot completely remove.Currently, there are no special in the market
Deodorization hand cleanser.
Natural plant composition is no lack of application in terms of removing fishy smell, such as some pungent perfume (or spice) being commonly used in gastronomical process
Material: ginger, purple perilla, coriander etc.；It is inspired by this, inventor team is especially smart to the effective component of these spice plants
Oily position carried out except raw meat solution raw meat in terms of research, with crab shell enzymic hydrolysates be tested raw material, with thiobarbituricacidα- (TBA)
Value is that chemical index reacts deodorization degree, as a result, it has been found that the extraction of essential oil object of each raw material is more than water extract, alcohol extract and other effects
By force, and wherein the extraction of essential oil object effect of coriander is best, and deodorization effect reaches 76.6%, remote super coriander water extract (deodorization effect
35.2%) and alcohol extract for (deodorization effect is 27.7%).Coriander (Coriandrum sativum L) also known as caraway, coriandrum
It is a kind of annual or biennial herbaceous plant Deng, Umbelliferae coriander category, is the seasoning vegetable on widely known dining table.
Main component includes linalool, laurene, australene, limonene etc. in coriander essential oil, is such as added in deodorization hand sanitizer formula,
The deodorization effect of product will be greatly enhanced, and carry natural coriander faint scent, understands experience sense more preferably after use.
But natural plant essential oils dissolubility in aqueous phase system is very low, and property is also unstable, and it is readily volatilized, after being heated
Oxidizable decomposition；In order to be applied in daily chemical products formula, it must just improve the water-soluble and steady of coriander essential oil
It is qualitative.Traditional method at present, can be using miscible with chemical cosolvent/solubilizer, to make its dispersion for water insoluble active ingredient
Into aqueous phase system；But this method can make the cosolvent/solubilizer for increasing a large amount of nonfunctional effect in product end system, and
And bring and stick greasy feeling using rear skin, it is clear that will not be welcome by consumer；And it is a kind of that essential oil, which is prepared into microcapsules,
Relatively conventional stable state chemical industry skill.Wall material the selection of material mostly uses such as cyclodextrin, Arabic gum when being typically prepared microcapsules, this
A little wall material raw material not functional result, and from the beta glucan of agrobacterium fermentation preparation (preparation method referring to
The patent No.: 201010146371.2；Inventor: Zhang Jianfa, Xiu Aihui, Zhu Bin；Patent name: agrobacterium ZX09 uses soil
It water-soluble natural beta glucan and preparation method thereof of bacillus ZX09 production and is reducing in the application specifications on blood glucose
Embodiment 3.) there is excellent filming performance, it is a kind of excellent natural thickener and moisturizer；Such as it is applied to hand cleanser
Product can be made to have the effect of moistening skin-care in formula
Lack at present it is a kind of have both deodorization effect and can moistening skin-care containing beta glucan-coriander essential oil microcapsules deodorization
Hand cleanser and preparation method thereof.
Summary of the invention
The technical problem to be solved by the present invention is in view of the deficiencies of the prior art, provide one kind to have both deodorization effect and can grow
Moisten skin care containing beta glucan-coriander essential oil microcapsules deodorization hand cleanser and preparation method thereof.
The present invention is achieved by the following technical solutions: one kind of the invention contains beta glucan-coriander essential oil microcapsules
Deodorization hand cleanser, the deodorization hand cleanser containing beta glucan-coriander essential oil microcapsules is by weight percentage by following components
Composition:
Further, the deodorization hand cleanser containing beta glucan-coriander essential oil microcapsules is by weight percentage by following
Group is grouped as:
Further, the surfactant is fatty alcohol polyoxyethylene ether sulfate, aliphatic alcohol sulfate, alkylbenzene
One of sulfonate or a variety of combinations；The antibacterial agent is p-chloro-m-xylol PCMX, chlorhexidine gluconate
Deng one of or a variety of combinations；The moisturizer be one of glycerol, propylene glycol, butanediol or polyethylene glycol 20 or
A variety of combinations.
Further, the surfactant is sodium sulfate of polyethenoxy ether of fatty alcohol AES, lauryl sodium sulfate
Or one of neopelex or a variety of combinations；
The thickener is cellulose thickener, carboxymethyl class thickener, polyethylene glycol stearate diester or card wave
One of nurse or a variety of combinations；
The pH adjusting agent is one of citric acid, sodium citrate or triethanolamine or a variety of combinations；Described
Preservative is the combination of one or both of isothiazolinone or Phenoxyethanol.
The preparation method of the deodorization hand cleanser of the present invention containing beta glucan-coriander essential oil microcapsules, including it is as follows
Step:
(1) each component is weighed according to the mass percent, beta glucan-coriander essential oil microcapsules is added to temperature
For in 50-60 DEG C of deionized water, stirring is sufficiently dissolved；
(2) surfactant, antibacterial agent, thickener, stirring, sufficiently dissolution is then added；Essence is added and modulates specific perfume (or spice)
Type, stirring and dissolving；PH adjusting agent is added when system is cooled to 25-35 DEG C and adjusts system pH 5.5-7；
(3) appropriate preservative is added, after cooling and standings, the effect of containing beta glucan-coriander essential oil microcapsules type is made and kills
Bacterium thimerosal.
Further, in step (1), it is 55 DEG C that 5g beta glucan-coriander essential oil microcapsules, which are added to temperature,
In 77.7g deionized water, stirring is sufficiently dissolved；Then 15g surfactant, 0.2g antibacterial agent, 1.5g thickener is added, stirs
It mixes, sufficiently dissolves；The stirring rate is 35-55r/min；
In step (2), 0.1g essence is added and modulates specific odor type, stirring and dissolving；Addition when system is cooled to 30 DEG C
0.3g pH adjusting agent adjusts system pH 5.5-7；
In step (3), 0.2g preservative is added, after cooling and standings, the micro- containing beta glucan-coriander essential oil of 100g is made
The effect of capsule type disinfection solution.
Beta glucan of the present invention-coriander essential oil microcapsules preparation method, includes the following steps:
(1) it weighs appropriate coriander essential oil and dissolves in obtained coriander essential oil solution, the matter of the coriander essential oil and solvent in solvent
Amount ratio is 1:1-3,
(2) it is added dropwise under stirring in the beta glucan solution that temperature is 35-65 DEG C, concentration is 3-10%, wherein
The mass ratio of coriander essential oil solution and beta glucan solution is 1:6-25；In the high-pressure homogeneous 40-85min of 15-30MPa, contained
The beta glucan lotion of coriander essential oil；
(3) it is then spray-dried, aspiration pressure 5.0-6.5kg/cm2, 165-185 DEG C of inlet air temperature, feeding temperature
55-65 DEG C, white is obtained to light yellow powder object, beta glucan-coriander essential oil microcapsules are made by 75-85 DEG C of leaving air temp.
Further, in step (1), coriander essential oil 100g is accurately weighed, is dissolved in 200mL dehydrated alcohol；
In step (2), the beta glucan aqueous solution of 6.5-8.5L mass fraction 7.0% is added dropwise under stirring
In, emulsifying temperature is 50-55 DEG C, the high-pressure homogeneous 60min of 20MPa, obtains the beta glucan lotion of the essential oil containing coriander；
It in step (3), is then spray-dried, aspiration pressure 5.0-6kg/cm2, 170-180 DEG C of inlet air temperature, into
80-85 DEG C of leaving air temp, beta glucan-coriander essential oil microcapsules are made in 55-60 DEG C of material temperature degree.
Further, the solvent is any one in dehydrated alcohol, propylene glycol or glycerine.
Application of the beta glucan of the present invention-coriander essential oil microcapsules in filed of daily-use chemical industry.
Coriander essential oil of the present invention is the volatile essential oil that mature coriander cauline leaf is prepared by steam distillation, outside
Seeing clear has coriander characteristic perfume, physicochemical property are as follows: relative density 0.87g/mL, diopter 1.4632, optical activity-
6°。
The utility model has the advantages that product of the present invention deodorization effect is thorough, beta glucan-coriander essential oil microcapsules and has both and make hand skin
The moist effect of skin, safety and stability, smell is pleasant, wide application of the crowd, and product is colourless transparent liquid, nontoxic, nonirritant, nothing
Corrosivity has natural coriander faint scent；Without to the harmful substance of human skin, belong to green, safe and environment-friendly daily use chemicals are used
Product.
Compared with prior art, the present invention has the advantage that
(1) it currently, related beta glucan not yet appears in the newspapers for the research that wall material embedding prepares coriander essential oil microcapsules, produces
Beta glucan-coriander essential oil microcapsules of product addition are this deodorization hand cleanser especial manufacture, and wherein coriander essential oil has aobvious
The deodorization of work acts on；Coriander essential oil is embedded by beta glucan to form microcapsules after, water solubility greatly increases, and bioactivity is more
Stablize, while the effect of deodorization effect and beta glucan skin-moisturizing, skin that coriander essential oil has is integrated, generates synergy
Effect, is added to and makes the deodorization of this money deodorization hand cleanser and soothing effect more significant in system, and it is clear to carry natural coriander
Perfume (or spice) will not feel drying and dehydrating using rear skin, and skin sense is more preferably.
(2) hand cleanser is adjusted by beta glucan-coriander essential oil microcapsules, surfactant, antibacterial agent, thickener, pH
Agent, essence, preservative and deionized water are proportionally prepared, which is that one kind can remove fishy smell and taste
Moisten skin care.Volunteer try out sensory evaluation the experimental results showed that, type deodorization is washed the effect of containing beta glucan-coriander essential oil microcapsules
Hand liquid is while having excellent deodorization effect；Compared to the product that other same types contain only plant extracts ingredient, after use
Skin sense is more preferably.
Specific embodiment
Following embodiment only exists in illustrative purpose, limits the scope of the invention without being intended to.
Embodiment 1
Of the invention is a kind of containing beta glucan-coriander essential oil microcapsules deodorization hand cleanser, described to contain beta glucan-coriander
The deodorization hand cleanser of essential oil microcapsules is composed of the following components by weight percentage:
The surfactant is fatty alcohol polyoxyethylene ether sulfate, two kinds of combination in aliphatic alcohol sulfate；
The antibacterial agent is p-chloro-m-xylol PCMX；The moisturizer is glycerol, propylene glycol, butanediol and polyethylene glycol
Four kinds of combination in 20.
The surfactant is sodium sulfate of polyethenoxy ether of fatty alcohol AES；
The thickener is polyethylene glycol stearate diester and two kinds of carbomer of combination；
The pH adjusting agent is triethanolamine；The preservative is isothiazolinone.
The preparation method of the deodorization hand cleanser containing beta glucan-coriander essential oil microcapsules of the invention, including such as
Lower step:
(1) each component is weighed according to the mass percent, beta glucan-coriander essential oil microcapsules is added to temperature
For in 60 DEG C of deionized waters, stirring is sufficiently dissolved；
(2) surfactant, antibacterial agent, thickener, stirring, sufficiently dissolution is then added；Essence is added and modulates specific perfume (or spice)
Type, stirring and dissolving；PH adjusting agent is added when system is cooled to 25 DEG C and adjusts system pH 7；
(3) appropriate preservative is added, after cooling and standings, the effect of containing beta glucan-coriander essential oil microcapsules type is made and kills
Bacterium thimerosal.
Beta glucan of the present invention-coriander essential oil microcapsules preparation method, includes the following steps:
(1) coriander essential oil 100g is accurately weighed, is dissolved in 200g dehydrated alcohol and coriander essential oil solution is made；
(2) it is added dropwise under stirring in the beta glucan solution that temperature is 35 DEG C, concentration is 7%, wherein coriander essence
The mass ratio of oil solution and beta glucan solution is 1:6；In the high-pressure homogeneous 40min of 15MPa, the β-Portugal for obtaining the essential oil containing coriander is poly-
Sugared lotion；
(3) it is then spray-dried, aspiration pressure 5.5kg/cm2, 165 DEG C of inlet air temperature, 55 DEG C of feeding temperature, outlet air
80 DEG C of temperature, obtaining white to light yellow powder object is beta glucan-coriander essential oil microcapsules.
With coriander essential oil microcapsules prepared by this technique, granularity is good, and embedding rate reaches 64.5%, the stability series of aqueous solution
Number is 87.2%, and viscosity is 24.6cp/20 DEG C.The coriander essential oil of microencapsulation has preferable water solubility, and retains simple and elegant
Coriander faint scent.Microencapsulation is a kind of physical modification means, refers to the chemical structure for not changing compound itself, uses certain material
(wall material) embeds it, is a kind of safe and simple modification hand having no toxic side effect to increase its dissolubility and stability
Section；The later compound of microencapsulation, application range will be widened significantly.Beta glucan has been used to embed coriander essential oil and obtain
Success is made beta glucan-coriander essential oil microcapsules, and is applied in daily chemical products；This beta glucan-coriander essential oil is micro-
Capsule not only in hand cleanser field, the application of other daily chemicals fields also should be in protection scope.
Embodiment 2
Embodiment 2 the difference from embodiment 1 is that:
Of the invention is a kind of containing beta glucan-coriander essential oil microcapsules deodorization hand cleanser, described to contain beta glucan-coriander
The deodorization hand cleanser of essential oil microcapsules is composed of the following components by weight percentage:
The surfactant is aliphatic alcohol sulfate, two kinds of alkylbenzene sulfonate of combination；The antibacterial agent is
Chlorhexidine gluconate；The moisturizer is propylene glycol and two kinds of butanediol of combination.
The surfactant is lauryl sodium sulfate and two kinds of neopelex of combination；
The thickener is cellulose thickener, two kinds of combination in carboxymethyl class thickener；
The pH adjusting agent is sodium citrate；The preservative is isothiazolinone.
The preparation method of the deodorization hand cleanser of the present invention containing beta glucan-coriander essential oil microcapsules, including it is as follows
Step:
(1) each component is weighed according to the mass percent, beta glucan-coriander essential oil microcapsules is added to temperature
For in 50 DEG C of deionized waters, stirring is sufficiently dissolved；
(2) surfactant, antibacterial agent, thickener, stirring, sufficiently dissolution is then added；Essence is added and modulates specific perfume (or spice)
Type, stirring and dissolving；PH adjusting agent is added when system is cooled to 35 DEG C and adjusts system pH 5.5；
(3) appropriate preservative is added, after cooling and standings, the effect of containing beta glucan-coriander essential oil microcapsules type is made and kills
Bacterium thimerosal.
Beta glucan of the present invention-coriander essential oil microcapsules preparation method, includes the following steps:
(1) coriander essential oil 100g is weighed, dissolves in and coriander essential oil solution is made in the propylene glycol of 100g,
(2) it is added dropwise under stirring in the beta glucan solution that temperature is 45 DEG C, concentration is 5%, wherein coriander essence
The mass ratio of oil solution and beta glucan solution is 1:10；In the high-pressure homogeneous 60min of 30MPa, β-Portugal of the essential oil containing coriander is obtained
Glycan lotion；
(3) it is then spray-dried, aspiration pressure 5kg/cm2, 175 DEG C of inlet air temperature, 60 DEG C of feeding temperature, wind-warm syndrome out
75 DEG C of degree, obtaining white to light yellow powder object is beta glucan-coriander essential oil microcapsules.
Embodiment 3
Embodiment 3 the difference from embodiment 1 is that:
The present invention is a kind of containing beta glucan-coriander essential oil microcapsules deodorization hand cleanser, it is characterised in that: described to contain β-Portugal
Glycan-coriander essential oil microcapsules deodorization hand cleanser is composed of the following components by weight percentage:
The surfactant is aliphatic alcohol sulfate；The antibacterial agent is chlorhexidine gluconate；The guarantor
Humectant is butanediol, two kinds of combination in polyethylene glycol 20.
The surfactant is lauryl sodium sulfate；
The thickener is cellulose thickener, two kinds of polyethylene glycol stearate diester of combination；
The pH adjusting agent is citric acid；The preservative is isothiazolinone and two kinds of Phenoxyethanol of combination.
The preparation method of the deodorization hand cleanser of the present invention containing beta glucan-coriander essential oil microcapsules, including it is as follows
Step:
(1) mass percent described in accordance with the claim 1 weighs each component, by beta glucan-coriander essential oil microcapsules
It is added in the deionized water that temperature is 55 DEG C, stirring, sufficiently dissolution；
(2) surfactant, antibacterial agent, thickener, stirring, sufficiently dissolution is then added；Essence is added and modulates specific perfume (or spice)
Type, stirring and dissolving；PH adjusting agent is added when system is cooled to 30 DEG C and adjusts system pH 6；
(3) appropriate preservative is added, after cooling and standings, the effect of containing beta glucan-coriander essential oil microcapsules type is made and kills
Bacterium thimerosal.
Beta glucan of the present invention-coriander essential oil microcapsules preparation method, includes the following steps:
(1) coriander essential oil 100g is weighed, dissolves in and coriander essential oil solution is made in the glycerine of 300g,
(2) it is added dropwise under stirring in the beta glucan solution that temperature is 65 DEG C, concentration is 10%, wherein coriander essence
The mass ratio of oil solution and beta glucan solution is 1:25；In the high-pressure homogeneous 85min of 25MPa, β-Portugal of the essential oil containing coriander is obtained
Glycan lotion；
(3) it is then spray-dried, aspiration pressure 6.5kg/cm2,185 DEG C of inlet air temperature, 65 DEG C of feeding temperature, outlet air
85 DEG C of temperature, obtaining white to light yellow powder object is beta glucan-coriander essential oil microcapsules.
Embodiment 4 (median)
Of the invention is a kind of containing beta glucan-coriander essential oil microcapsules deodorization hand cleanser, described to contain beta glucan-coriander
The effect of essential oil microcapsules, type disinfection solution was composed of the following components by weight percentage:
The preparation method of the deodorization hand cleanser of the present invention containing beta glucan-coriander essential oil microcapsules, including it is as follows
Step:
(1) 5g beta glucan-coriander essential oil microcapsules are added in the 82.7g deionized water that temperature is 55 DEG C, stirring,
Sufficiently dissolution；Then 15g surfactant, 0.2g antibacterial agent, 1.5g thickener is added, stirring is sufficiently dissolved；The stirring speed
Rate is 45r/min.
(2) 0.1g essence is added and modulates specific odor type, 0.3gpH regulator adjusting body is added when system is cooled to 30 DEG C
It is pH to 5.5-7；
(3) 0.2g preservative is added, going containing beta glucan-coriander essential oil microcapsules for 100g is obtained after cooling and standings
Raw meat hand cleanser.
Embodiment 5 (low value)
Embodiment 5 and the difference of embodiment 4 are: of the invention a kind of to go containing beta glucan-coriander essential oil microcapsules
Raw meat hand cleanser, the deodorization hand cleanser containing beta glucan-coriander essential oil microcapsules are composed of the following components by weight percentage:
The preparation method of the deodorization hand cleanser of the present invention containing beta glucan-coriander essential oil microcapsules, including it is as follows
Step:
(1) 2.0g beta glucan-coriander essential oil microcapsules are added in the 92.43g deionized water that temperature is 60 DEG C, are stirred
It mixes, sufficiently dissolves；Then 5.0g surfactant, 0.05g antibacterial agent, 0.5g thickener is added, stirring is sufficiently dissolved；It is described
Stirring rate is 35r/min.
(2) it is added without essence, it is 5.5-7 that system pH is measured when system is cooled to 25 DEG C, therefore also it is not necessary that pH tune is added
Save agent；
(3) be added 0.02g preservative, after cooling and standings i.e. obtain 100g containing beta glucan-coriander essential oil microcapsules
Deodorization hand cleanser.
Embodiment 6 (high level)
Embodiment 6 and the difference of embodiment 4 are: of the invention a kind of to go containing beta glucan-coriander essential oil microcapsules
Raw meat hand cleanser, the effect of containing beta glucan-coriander essential oil microcapsules type disinfection solution is by weight percentage by with the following group
It is grouped as:
Of the invention is a kind of containing beta glucan-coriander essential oil microcapsules deodorization hand cleanser, described to contain beta glucan-coriander
The effect of essential oil microcapsules, type disinfection solution was composed of the following components by weight percentage:
The preparation method of the deodorization hand cleanser of the present invention containing beta glucan-coriander essential oil microcapsules, including it is as follows
Step:
(1) 10g beta glucan-coriander essential oil microcapsules are added in the 64.7g deionized water that temperature is 60 DEG C, are stirred
It mixes, sufficiently dissolves；Then 20g surfactant, 0.5g antibacterial agent, 3.0g thickener is added, stirring is sufficiently dissolved；It is described to stir
Mixing rate is 55r/min.
(2) 0.3g essence is added and modulates specific odor type, 1.0gpH regulator adjusting body is added when system is cooled to 35 DEG C
It is pH to 5.5-7；
(3) 0.5g preservative is added, going containing beta glucan-coriander essential oil microcapsules for 100g is obtained after cooling and standings
Raw meat hand cleanser.
Study on the stability, physicochemical and microbial index, bacteriostasis is carried out to deodorization hand cleanser made from embodiment 4-6 to survey
Examination and deodorization measure of merit.
Test 1: study on the stability
2 parts of the deodorization hand cleanser sample of Example 4-6 preparation respectively, is respectively placed in 40 DEG C of ± 2 DEG C of perseverances by 100 grams every part
Temperature 24 hours and is placed in -15 DEG C ± 2 DEG C constant temperature 24 hours, takes out and restores to 25 DEG C of room temperature to observe.
The deodorization hand cleanser sample of embodiment 4-6 preparation is without layering and without metachromatism, haze-free after testing, with examination
It is identical before testing.Therefore, product stability meets the requirements.
Test 2: related physical and chemical index test
The embodiment 4-6 deodorization prepared is washed according to the relevant regulations of table 1 in GB19877.1-2005 (extraordinary hand cleanser)
The test of hand liquid sample progress physical and chemical index.Embodiment 4-6 preparation deodorization hand cleanser sample be all satisfied arsenic (in 1% solution with
As meter, mg/kg)≤0.1, heavy metal (in 1% solution in terms of Pb, mg/kg)≤1 complies fully with requirement.
The embodiment 4-6 deodorization prepared is washed according to the relevant regulations of table 2 in GB19877.1-2005 (extraordinary hand cleanser)
The test of hand liquid sample progress microbiological indicator.Deodorization hand cleanser sample total plate count≤100cfu/g of embodiment 4-6 preparation,
Comply with standard regulation≤200cfu/g requirement；Coliform is not detected simultaneously, also complies with standard requirements.
Test 3, bacteriostasis test
Deodorization hand cleanser prepared by embodiment 4-6 according to table 2 in GB19877.1-2005 (extraordinary hand cleanser) regulation
It is detected, 99% is all larger than to the bacteriostasis rate of Staphylococcus aureus, Escherichia coli, comply fully with wanting for standard regulation >=50%
It asks.
Test 4, the experiment of deodorization effect assessment
Given the test agent: the deodorization hand cleanser of embodiment 4-6 preparation
Test method:
Step 1: fish-bone crab shell enzyme hydrolysis stoste is prepared.It collects the wastes → such as fish-bone and crab shell after eating plus water is high
Press softening → mashing filtering → enzymatic hydrolysis → hydrolysising original liquid.The stoste has ichthyophagy crab category feature stink smell.
Step 2: choosing 60 consumers (men and women is fifty-fifty, and the age is unlimited), and it is former that hand is immersed the hydrolysis of fish-bone crab shell first
It is impregnated 3 minutes in liquid, hand, which shares equally, is infected with consumer's obviously recognizable stink smell；Then after hand volatilizes naturally, make respectively
The hand cleanser prepared with embodiment 4-6 is conscientiously cleaned 1 minute by science principle of washing one's hands, after hand volatilizes naturally again, consumption
Person voluntarily evaluates the effect of removal hand stink smell.
As a result as shown in table 1 below:
Table 1
| Remove stink smell effect | Embodiment 4 | Embodiment 5 | Embodiment 6 |
| It is fully erased | 27 | 21 | 35 |
| Preferably remove | 29 | 33 | 22 |
| It removes unobvious | 4 | 6 | 3 |
| Total number | 60 | 60 | 60 |
| Effective ratio | 93.3% | 90.0% | 95% |
As shown in table 1, volunteer to test by consumer, deodorization hand cleanser prepared by the present invention, deodorization satisfaction rate reaches
90% or more, therefore products of the present invention is fully able to reach the deodorization effect made consumer satisfaction.
The basic principles, main features and advantages of the present invention have been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, the present invention
Claimed range is delineated by the appended claims, the specification and equivalents thereof from the appended claims.
Claims (10)
1. a kind of containing beta glucan-coriander essential oil microcapsules deodorization hand cleanser, it is characterised in that:-the Yuan containing beta glucan
The deodorization hand cleanser of Sui essential oil microcapsules is composed of the following components by weight percentage:
2. according to claim 1 containing beta glucan-coriander essential oil microcapsules deodorization hand cleanser, it is characterised in that: institute
It is composed of the following components by weight percentage to state the deodorization hand cleanser containing beta glucan-coriander essential oil microcapsules:
3. according to claim 1 containing beta glucan-coriander essential oil microcapsules deodorization hand cleanser, it is characterised in that: institute
The surfactant stated is one of fatty alcohol polyoxyethylene ether sulfate, aliphatic alcohol sulfate, alkylbenzene sulfonate or more
The combination of kind；The antibacterial agent is one of p-chloro-m-xylol PCMX, chlorhexidine gluconate etc. or a variety of
Combination；The moisturizer is one of glycerol, propylene glycol, butanediol or polyethylene glycol 20 or a variety of combinations.
4. according to claim 2 containing beta glucan-coriander essential oil microcapsules deodorization hand cleanser, it is characterised in that: institute
The surfactant stated is in sodium sulfate of polyethenoxy ether of fatty alcohol AES, lauryl sodium sulfate or neopelex
One or more combinations；
The thickener is in cellulose thickener, carboxymethyl class thickener, polyethylene glycol stearate diester or carbomer
One or more combinations；
The pH adjusting agent is one of citric acid, sodium citrate or triethanolamine or a variety of combinations；The anti-corrosion
Agent is the combination of one or both of isothiazolinone or Phenoxyethanol.
5. the preparation method of the deodorization hand cleanser described in claim 1 containing beta glucan-coriander essential oil microcapsules, feature exist
In including the following steps:
(1) mass percent described in accordance with the claim 1 weighs each component, and beta glucan-coriander essential oil microcapsules are added
In the deionized water for being 50-60 DEG C to temperature, stirring, sufficiently dissolution；
(2) surfactant, antibacterial agent, thickener, stirring, sufficiently dissolution is then added；Essence is added and modulates specific odor type, stirs
Mix dissolution；PH adjusting agent is added when system is cooled to 25-35 DEG C and adjusts system pH 5.5-7；
(3) appropriate preservative is added, after cooling and standings, the effect of containing beta glucan-coriander essential oil microcapsules type sterilization is made and disappears
Venom.
6. it is according to claim 5 containing beta glucan-coriander essential oil microcapsules the effect of type disinfection solution preparation side
Method, it is characterised in that:
In step (1), 5g beta glucan-coriander essential oil microcapsules are added in the 77.7g deionized water that temperature is 55 DEG C,
Stirring is sufficiently dissolved；Then 15g surfactant, 0.2g antibacterial agent, 1.5g thickener is added, stirring is sufficiently dissolved；It is described
Stirring rate is 35-55r/min；
In step (2), 0.1g essence is added and modulates specific odor type, stirring and dissolving；0.3g is added when system is cooled to 30 DEG C
PH adjusting agent adjusts system pH 5.5-7；
In step (3), 0.2g preservative is added, after cooling and standings, 100g is made contains beta glucan-coriander essential oil microcapsules
The effect of type disinfection solution.
7. beta glucan described in claim 1-coriander essential oil microcapsules preparation method, it is characterised in that including walking as follows
It is rapid:
(1) it weighs appropriate coriander essential oil and dissolves in obtained coriander essential oil solution, the mass ratio of the coriander essential oil and solvent in solvent
For 1:1-3,
(2) it is added dropwise under stirring in the beta glucan solution that temperature is 35-65 DEG C, concentration is 3-10%, wherein coriander
The mass ratio of essential oil solution and beta glucan solution is 1:6-25；In the high-pressure homogeneous 40-85min of 15-30MPa, obtains and contain coriander
The beta glucan lotion of essential oil；
(3) it is then spray-dried, aspiration pressure 5.0-6.5kg/cm2,165-185 DEG C of inlet air temperature, feeding temperature 55-65
DEG C, 75-85 DEG C of leaving air temp, white is obtained to light yellow powder object, beta glucan-coriander essential oil microcapsules are made.
8. beta glucan according to claim 7-coriander essential oil microcapsules preparation method, it is characterised in that: in step
Suddenly in (1), coriander essential oil 100g is accurately weighed, is dissolved in 200mL dehydrated alcohol；
In step (2), it is added dropwise under stirring in the beta glucan aqueous solution of 6.5-8.5L mass fraction 7.0%,
Emulsifying temperature is 50-55 DEG C, the high-pressure homogeneous 60min of 20MPa, obtains the beta glucan lotion of the essential oil containing coriander；
It in step (3), is then spray-dried, aspiration pressure 5.0-6kg/cm2,170-180 DEG C of inlet air temperature, charging temperature
80-85 DEG C of leaving air temp, beta glucan-coriander essential oil microcapsules are made in 55-60 DEG C of degree.
9. beta glucan according to claim 1-coriander essential oil microcapsules preparation method, it is characterised in that: described
Solvent is any one in dehydrated alcohol, propylene glycol or glycerine.
10. the described in any item beta glucans of claim 7 to 9-coriander essential oil microcapsules are in the application of filed of daily-use chemical industry.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910038431.XA CN109674666B (en) | 2019-01-16 | 2019-01-16 | Fishy smell removing hand sanitizer containing beta-glucan-coriander essential oil microcapsules and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910038431.XA CN109674666B (en) | 2019-01-16 | 2019-01-16 | Fishy smell removing hand sanitizer containing beta-glucan-coriander essential oil microcapsules and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109674666A true CN109674666A (en) | 2019-04-26 |
| CN109674666B CN109674666B (en) | 2022-03-08 |
Family
ID=66193166
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910038431.XA Active CN109674666B (en) | 2019-01-16 | 2019-01-16 | Fishy smell removing hand sanitizer containing beta-glucan-coriander essential oil microcapsules and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109674666B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111281819A (en) * | 2020-04-02 | 2020-06-16 | 上海应用技术大学 | Bacteriostatic hand sanitizer containing fingered citron-rose essential oil microcapsules and preparation method thereof |
| CN114344204A (en) * | 2020-09-21 | 2022-04-15 | 山西焦煤运城盐化集团有限责任公司 | Foam hand sanitizer with caraway extract as fishy smell removing component and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2002083827A1 (en) * | 2001-04-13 | 2002-10-24 | Japan Tobacco Inc. | Process for producing glucan capsules having flavor component enclosed therein |
| CN104873419A (en) * | 2015-05-19 | 2015-09-02 | 天津郁美净集团有限公司 | Multi-plant composition and extract thereof as well as preparation and application of microcapsule |
| CN105997699A (en) * | 2016-06-30 | 2016-10-12 | 江苏敖广日化集团股份有限公司 | Fishy smell removal liquid soap |
| CN105997964A (en) * | 2016-04-18 | 2016-10-12 | 中华全国供销合作总社南京野生植物综合利用研究院 | Efficacy type sterilization and disinfection liquid containing natural citral-bletilla striata polysaccharide polymer and preparation method thereof |
-
2019
- 2019-01-16 CN CN201910038431.XA patent/CN109674666B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2002083827A1 (en) * | 2001-04-13 | 2002-10-24 | Japan Tobacco Inc. | Process for producing glucan capsules having flavor component enclosed therein |
| CN104873419A (en) * | 2015-05-19 | 2015-09-02 | 天津郁美净集团有限公司 | Multi-plant composition and extract thereof as well as preparation and application of microcapsule |
| CN105997964A (en) * | 2016-04-18 | 2016-10-12 | 中华全国供销合作总社南京野生植物综合利用研究院 | Efficacy type sterilization and disinfection liquid containing natural citral-bletilla striata polysaccharide polymer and preparation method thereof |
| CN105997699A (en) * | 2016-06-30 | 2016-10-12 | 江苏敖广日化集团股份有限公司 | Fishy smell removal liquid soap |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111281819A (en) * | 2020-04-02 | 2020-06-16 | 上海应用技术大学 | Bacteriostatic hand sanitizer containing fingered citron-rose essential oil microcapsules and preparation method thereof |
| CN114344204A (en) * | 2020-09-21 | 2022-04-15 | 山西焦煤运城盐化集团有限责任公司 | Foam hand sanitizer with caraway extract as fishy smell removing component and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN109674666B (en) | 2022-03-08 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104173250B (en) | Skin-nourishing liquid soap containing natural bacteriostatic components and preparation method thereof | |
| CN104094977A (en) | Composition with insect-expelling sterilization disinfection effects and application thereof | |
| CN105326681B (en) | A kind of anti-bacterial hand lotion containing Folium Artemisiae Argyi extract and preparation method thereof | |
| CN105342932B (en) | A kind of all natural multifunctional liquid soap and its production method containing carboxymethyl chitosan | |
| CN105779165A (en) | Washing composition as well as preparation method and application of washing composition | |
| CN104818140A (en) | Antibacterial dishwashing detergent | |
| CN110184135A (en) | A kind of antibacterial dish washing liquid of propolis and preparation method thereof | |
| CN107624758A (en) | A kind of complex composition containing parahydroxyacet-ophenone and preparation method and application | |
| CN104789383A (en) | Antibacterial washing liquid | |
| CN109674666A (en) | It is a kind of containing beta glucan-coriander essential oil microcapsules deodorization hand cleanser and preparation method thereof | |
| CN103493847B (en) | Environment-friendly immersing and spraying liquid and preparation method thereof | |
| CN109135946A (en) | A kind of edible detergent and preparation method thereof | |
| CN108078815A (en) | A kind of disposable hand cleanser of natural bacteriostatic and preparation method thereof | |
| CN104490714A (en) | Natural high polymer based water-free hand sanitizer | |
| CN110373284A (en) | A kind of natural plant extracts perfumed soap and preparation method thereof | |
| CN109010178B (en) | Shower gel and production process thereof | |
| CN106728630A (en) | A kind of anti-inflammation composition and privates care product | |
| CN106591011B (en) | A kind of antibacterial soap and preparation method thereof | |
| CN108559656A (en) | A kind of plant type antibacterial bacteriostatic liquid detergent with pomelo fragrant smell | |
| CN105087180A (en) | Antibacterial and anti-mildew cleaning and treating agent for towels | |
| CN109463401A (en) | A kind of wooden essential oil and preparation method thereof | |
| CN108451799A (en) | A kind of hand cleanser and preparation method thereof | |
| CN105726358A (en) | Antibacterial bath cream containing cybopogon essential oil and preparing method thereof | |
| CN109247343A (en) | A kind of thimerosal and preparation method thereof containing tea tree ethereal oil | |
| CN111481597B (en) | Female herbal bacteriostatic care solution and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |