CN104173250B - Skin-nourishing liquid soap containing natural bacteriostatic components and preparation method thereof - Google Patents
Skin-nourishing liquid soap containing natural bacteriostatic components and preparation method thereof Download PDFInfo
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- CN104173250B CN104173250B CN201410466170.9A CN201410466170A CN104173250B CN 104173250 B CN104173250 B CN 104173250B CN 201410466170 A CN201410466170 A CN 201410466170A CN 104173250 B CN104173250 B CN 104173250B
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- 239000007788 liquid Substances 0.000 title claims abstract description 55
- 239000000344 soap Substances 0.000 title claims abstract description 30
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 230000003385 bacteriostatic Effects 0.000 title claims abstract description 15
- 210000003491 Skin Anatomy 0.000 claims abstract description 40
- 239000012153 distilled water Substances 0.000 claims abstract description 19
- -1 fatty acid glycinate Chemical class 0.000 claims abstract description 17
- PEDCQBHIVMGVHV-UHFFFAOYSA-N glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000000284 extract Substances 0.000 claims abstract description 15
- KWIUHFFTVRNATP-UHFFFAOYSA-N Trimethylglycine Chemical compound C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 claims abstract description 12
- 235000014113 dietary fatty acids Nutrition 0.000 claims abstract description 12
- 239000000194 fatty acid Substances 0.000 claims abstract description 12
- 229920002907 Guar gum Polymers 0.000 claims abstract description 11
- 150000004665 fatty acids Chemical class 0.000 claims abstract description 11
- 239000000665 guar gum Substances 0.000 claims abstract description 11
- 229960002154 guar gum Drugs 0.000 claims abstract description 11
- 235000010417 guar gum Nutrition 0.000 claims abstract description 11
- 229940093429 Polyethylene Glycol 6000 Drugs 0.000 claims abstract description 10
- 240000007170 Cocos nucifera Species 0.000 claims abstract description 7
- 235000013162 Cocos nucifera Nutrition 0.000 claims abstract description 7
- WXMKPNITSTVMEF-UHFFFAOYSA-M Sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims abstract description 6
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims abstract description 6
- 229960003237 betaine Drugs 0.000 claims abstract description 6
- 235000019864 coconut oil Nutrition 0.000 claims abstract description 6
- 239000003240 coconut oil Substances 0.000 claims abstract description 6
- 235000010234 sodium benzoate Nutrition 0.000 claims abstract description 6
- 239000004299 sodium benzoate Substances 0.000 claims abstract description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 37
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 29
- 239000000203 mixture Substances 0.000 claims description 26
- 241000628997 Flos Species 0.000 claims description 19
- 238000010438 heat treatment Methods 0.000 claims description 19
- 238000003756 stirring Methods 0.000 claims description 14
- 230000002522 swelling Effects 0.000 claims description 13
- 238000004140 cleaning Methods 0.000 claims description 11
- 150000001768 cations Chemical class 0.000 claims description 10
- 239000012467 final product Substances 0.000 claims description 10
- QIQXTHQIDYTFRH-UHFFFAOYSA-M stearate Chemical compound CCCCCCCCCCCCCCCCCC([O-])=O QIQXTHQIDYTFRH-UHFFFAOYSA-M 0.000 claims description 9
- RTZKZFJDLAIYFH-UHFFFAOYSA-N diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 8
- 238000001914 filtration Methods 0.000 claims description 8
- HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 8
- 210000000582 Semen Anatomy 0.000 claims description 7
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Vitamin C Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 6
- 229960005070 ascorbic acid Drugs 0.000 claims description 6
- 239000003921 oil Substances 0.000 claims description 6
- 235000019198 oils Nutrition 0.000 claims description 6
- DXDTUQXKMVJYAM-UHFFFAOYSA-N 2-aminoacetic acid;potassium Chemical compound [K].NCC(O)=O DXDTUQXKMVJYAM-UHFFFAOYSA-N 0.000 claims description 5
- 239000004141 Sodium laurylsulphate Substances 0.000 claims description 5
- 125000003368 amide group Chemical group 0.000 claims description 5
- SFNALCNOMXIBKG-UHFFFAOYSA-N ethylene glycol monododecyl ether Chemical compound CCCCCCCCCCCCOCCO SFNALCNOMXIBKG-UHFFFAOYSA-N 0.000 claims description 5
- PMZURENOXWZQFD-UHFFFAOYSA-L na2so4 Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 5
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 5
- 235000019333 sodium laurylsulphate Nutrition 0.000 claims description 5
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 5
- 235000011152 sodium sulphate Nutrition 0.000 claims description 5
- 238000000605 extraction Methods 0.000 claims description 4
- 239000000706 filtrate Substances 0.000 claims description 4
- 239000003208 petroleum Substances 0.000 claims description 4
- 238000001556 precipitation Methods 0.000 claims description 4
- 238000001291 vacuum drying Methods 0.000 claims description 4
- 239000003643 water by type Substances 0.000 claims description 4
- 240000002254 Ananas comosus Species 0.000 claims description 3
- 235000007119 Ananas comosus Nutrition 0.000 claims description 3
- 244000111489 Gardenia augusta Species 0.000 claims description 3
- 235000018958 Gardenia augusta Nutrition 0.000 claims description 3
- 238000002386 leaching Methods 0.000 claims description 3
- 239000002994 raw material Substances 0.000 claims description 3
- 244000144730 Amygdalus persica Species 0.000 claims description 2
- 240000008067 Cucumis sativus Species 0.000 claims description 2
- 235000010799 Cucumis sativus var sativus Nutrition 0.000 claims description 2
- 235000019082 Osmanthus Nutrition 0.000 claims description 2
- 241000333181 Osmanthus Species 0.000 claims description 2
- 235000006040 Prunus persica var persica Nutrition 0.000 claims description 2
- 239000000796 flavoring agent Substances 0.000 claims description 2
- 235000019634 flavors Nutrition 0.000 claims description 2
- 239000003205 fragrance Substances 0.000 claims description 2
- 239000000686 essence Substances 0.000 abstract description 9
- 239000000126 substance Substances 0.000 abstract description 4
- 239000004094 surface-active agent Substances 0.000 abstract description 4
- 241000196324 Embryophyta Species 0.000 abstract description 3
- 235000016709 nutrition Nutrition 0.000 abstract description 3
- 230000035764 nutrition Effects 0.000 abstract description 3
- 241000894006 Bacteria Species 0.000 abstract description 2
- 235000008495 Chrysanthemum leucanthemum Nutrition 0.000 abstract 1
- 244000035851 Chrysanthemum leucanthemum Species 0.000 abstract 1
- 229940079841 SODIUM COPPER CHLOROPHYLLIN Drugs 0.000 abstract 1
- 229930003268 Vitamin C Natural products 0.000 abstract 1
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- 125000002091 cationic group Chemical group 0.000 abstract 1
- KYLOFEQLMQEHBO-JOKPRTCASA-I copper;trisodium;(8Z,17S,18S)-18-(2-carboxylatoethyl)-20-(carboxylatomethyl)-12-ethenyl-7-ethyl-3,13,17-trimethyl-8-(oxidomethylidene)-17,18-dihydroporphyrin-21-ide-2-carboxylate Chemical compound [Na+].[Na+].[Na+].[Cu+2].C1=C([N-]2)C(C)=C(C([O-])=O)C2=C(CC([O-])=O)C([C@H]([C@@H]2C)CCC([O-])=O)=NC2=CC(C(=C2C=C)C)=NC2=CC\2=NC1=C(CC)C/2=C\[O-] KYLOFEQLMQEHBO-JOKPRTCASA-I 0.000 abstract 1
- 150000002148 esters Chemical class 0.000 abstract 1
- 229910052700 potassium Inorganic materials 0.000 abstract 1
- 239000011591 potassium Substances 0.000 abstract 1
- 235000013758 sodium copper chlorophyllin Nutrition 0.000 abstract 1
- 235000019154 vitamin C Nutrition 0.000 abstract 1
- 239000011718 vitamin C Substances 0.000 abstract 1
- 150000003700 vitamin C derivatives Chemical class 0.000 abstract 1
- 239000010497 wheat germ oil Substances 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 19
- 230000000844 anti-bacterial Effects 0.000 description 9
- 239000000047 product Substances 0.000 description 9
- 238000005406 washing Methods 0.000 description 8
- 210000004247 Hand Anatomy 0.000 description 7
- 238000005187 foaming Methods 0.000 description 7
- 230000036740 Metabolism Effects 0.000 description 4
- 230000002708 enhancing Effects 0.000 description 4
- 230000002401 inhibitory effect Effects 0.000 description 4
- 230000004060 metabolic process Effects 0.000 description 4
- 230000035786 metabolism Effects 0.000 description 4
- 206010002198 Anaphylactic reaction Diseases 0.000 description 3
- 208000003455 Anaphylaxis Diseases 0.000 description 3
- 241000588724 Escherichia coli Species 0.000 description 3
- 241000191967 Staphylococcus aureus Species 0.000 description 3
- 230000032683 aging Effects 0.000 description 3
- 230000036592 analgesia Effects 0.000 description 3
- 230000036783 anaphylactic response Effects 0.000 description 3
- 230000003110 anti-inflammatory Effects 0.000 description 3
- 230000003064 anti-oxidating Effects 0.000 description 3
- 230000033228 biological regulation Effects 0.000 description 3
- 238000005119 centrifugation Methods 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 239000002537 cosmetic Substances 0.000 description 3
- 239000003814 drug Substances 0.000 description 3
- 235000011187 glycerol Nutrition 0.000 description 3
- 238000003475 lamination Methods 0.000 description 3
- 201000008125 pain agnosia Diseases 0.000 description 3
- 239000006072 paste Substances 0.000 description 3
- 230000001717 pathogenic Effects 0.000 description 3
- 244000052769 pathogens Species 0.000 description 3
- 239000002689 soil Substances 0.000 description 3
- 230000001954 sterilising Effects 0.000 description 3
- 239000000341 volatile oil Substances 0.000 description 3
- 241001116389 Aloe Species 0.000 description 2
- 210000000589 Cicatrix Anatomy 0.000 description 2
- 208000001848 Dysentery Diseases 0.000 description 2
- OYHQOLUKZRVURQ-IXWMQOLASA-N Linoleic acid Natural products CCCCC\C=C/C\C=C\CCCCCCCC(O)=O OYHQOLUKZRVURQ-IXWMQOLASA-N 0.000 description 2
- 241000293871 Salmonella enterica subsp. enterica serovar Typhi Species 0.000 description 2
- 241000700605 Viruses Species 0.000 description 2
- 229940088594 Vitamin Drugs 0.000 description 2
- 206010048222 Xerosis Diseases 0.000 description 2
- 230000002159 abnormal effect Effects 0.000 description 2
- 235000011399 aloe vera Nutrition 0.000 description 2
- 201000010099 disease Diseases 0.000 description 2
- 238000003379 elimination reaction Methods 0.000 description 2
- 239000006260 foam Substances 0.000 description 2
- 239000003502 gasoline Substances 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 241000411851 herbal medicine Species 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 239000003350 kerosene Substances 0.000 description 2
- 230000002147 killing Effects 0.000 description 2
- 230000014759 maintenance of location Effects 0.000 description 2
- 239000002736 nonionic surfactant Substances 0.000 description 2
- 230000035943 smell Effects 0.000 description 2
- 238000004659 sterilization and disinfection Methods 0.000 description 2
- 230000000638 stimulation Effects 0.000 description 2
- 239000011782 vitamin Substances 0.000 description 2
- 235000013343 vitamin Nutrition 0.000 description 2
- 150000003722 vitamin derivatives Chemical class 0.000 description 2
- 229930003231 vitamins Natural products 0.000 description 2
- 230000037303 wrinkles Effects 0.000 description 2
- 231100001002 xerosis Toxicity 0.000 description 2
- DTOSIQBPPRVQHS-PDBXOOCHSA-N α-linolenic acid Chemical compound CC\C=C/C\C=C/C\C=C/CCCCCCCC(O)=O DTOSIQBPPRVQHS-PDBXOOCHSA-N 0.000 description 2
- GHNRTXCRBJQVGN-UHFFFAOYSA-N 4-dodecan-6-ylbenzenesulfonic acid Chemical compound CCCCCCC(CCCCC)C1=CC=C(S(O)(=O)=O)C=C1 GHNRTXCRBJQVGN-UHFFFAOYSA-N 0.000 description 1
- 241000193830 Bacillus <bacterium> Species 0.000 description 1
- 229940095731 Candida albicans Drugs 0.000 description 1
- 241000222122 Candida albicans Species 0.000 description 1
- HIPIENNKVJCMAP-UHFFFAOYSA-N Chrysanthemol Chemical compound CC(C)=CC1C(CO)C1(C)C HIPIENNKVJCMAP-UHFFFAOYSA-N 0.000 description 1
- 229930008410 Chrysanthemol Natural products 0.000 description 1
- YXMMAVURUUXKKN-UHFFFAOYSA-J Copper chlorophyll sodium Chemical class [Na+].[Na+].[Cu+2].[N-]1C2=C(C=3C(C(C)C(=CC=4C(=C(C=C)C(=C5)N=4)C)N=3)CCC([O-])=O)C(C([O-])=O)C([O-])=C2C(C)=C1C=C1C(CC)=C(C)C5=N1 YXMMAVURUUXKKN-UHFFFAOYSA-J 0.000 description 1
- 206010011409 Cross infection Diseases 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 208000002672 Hepatitis B Diseases 0.000 description 1
- 235000003935 Hippophae Nutrition 0.000 description 1
- 241000229143 Hippophae Species 0.000 description 1
- 206010022114 Injury Diseases 0.000 description 1
- 229960004488 Linolenic Acid Drugs 0.000 description 1
- 210000004185 Liver Anatomy 0.000 description 1
- 206010062080 Pigmentation disease Diseases 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
- 229940034610 Toothpaste Drugs 0.000 description 1
- 240000008529 Triticum aestivum Species 0.000 description 1
- DSNIKOZTDZBWKD-XMNJDQQWSA-N Yejuhua lactone Chemical compound O([C@H]1C2C[C@H]([C@@](C3C1C(=CC3)C)(C)O)OC(=O)C)C(=O)C2(C1(C)C=C2)CC22C1[C@H]1OC(=O)C(=C)C1CC[C@@]2(C)O DSNIKOZTDZBWKD-XMNJDQQWSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000003213 activating Effects 0.000 description 1
- 238000007792 addition Methods 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 235000020661 alpha-linolenic acid Nutrition 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminum Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 235000001014 amino acid Nutrition 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 239000002280 amphoteric surfactant Substances 0.000 description 1
- 125000000129 anionic group Chemical group 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
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- 230000001741 anti-phlogistic Effects 0.000 description 1
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- 239000002585 base Substances 0.000 description 1
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- 239000004064 cosurfactant Substances 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 238000005202 decontamination Methods 0.000 description 1
- 230000003588 decontaminative Effects 0.000 description 1
- 238000005238 degreasing Methods 0.000 description 1
- 230000001934 delay Effects 0.000 description 1
- 238000004332 deodorization Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 201000009910 diseases by infectious agent Diseases 0.000 description 1
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- 230000003670 easy-to-clean Effects 0.000 description 1
- 230000002500 effect on skin Effects 0.000 description 1
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- 230000002124 endocrine Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000001815 facial Effects 0.000 description 1
- 235000021285 flavonoid Nutrition 0.000 description 1
- 150000007955 flavonoid glycosides Chemical class 0.000 description 1
- 150000002215 flavonoids Chemical class 0.000 description 1
- 229930003935 flavonoids Natural products 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 239000000576 food coloring agent Substances 0.000 description 1
- 235000013376 functional food Nutrition 0.000 description 1
- 150000004676 glycans Polymers 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 229910052738 indium Inorganic materials 0.000 description 1
- 235000020778 linoleic acid Nutrition 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000003020 moisturizing Effects 0.000 description 1
- 230000001264 neutralization Effects 0.000 description 1
- 230000003000 nontoxic Effects 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000000050 nutritive Effects 0.000 description 1
- 235000012736 patent blue V Nutrition 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 230000035479 physiological effects, processes and functions Effects 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 230000019612 pigmentation Effects 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 150000004804 polysaccharides Polymers 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
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- 102000004169 proteins and genes Human genes 0.000 description 1
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- 239000003507 refrigerant Substances 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
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- KEAYESYHFKHZAL-UHFFFAOYSA-N sodium Chemical compound [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
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Abstract
The invention discloses skin-nourishing liquid soap containing natural bacteriostatic components and a preparation method thereof. The liquid soap is prepared from the following substances: coconut oil alkyl amidopropyl betaine, sodium copper chlorophyllin, wild chrysanthemum extract, lauryl sodium sulfate, wheat germ oil, cocoanut fatty acid diethanolamide, N-potassium coconut fatty acid glycinate, polyethylene glycol 6000 distearate ester, cationic guar gum, glycerinum, vitamin C, distilled water, sodium benzoate and essence. Compared with the prior art, the liquid soap has the advantages of mild property and high safety; generation of bacteria on the skin surface can be inhibited by adopting a method of combining active substances in natural plants and a mild surfactant; the liquid soap has good stain removing performance, good moistening performance and good nourishing performance; a user feels fresh and comfortable when using the liquid soap, so that a mild and natural bacteriostatic effect can be achieved while stains on hands are removed, nutrition and moisture required by skin can be supplied, and skin can be nourished.
Description
Technical field
The present invention relates to a kind of skin moistening liquid soap and preparation method thereof, particularly to a kind of profit containing natural bacteriostatic composition
Skin handwashing liquid and preparation method thereof.
Background technology
Hand-washing article belongs to one kind of skin cleaner, in China's a period of time very long in the past, the living condition of the people
Relatively backward, beautiful requirement is also stayed at relatively low level, the clean usual of people opponent is fancy soap, soap, laundry
Powder even ground caustic, gasoline, kerosene etc..Although they can reach certain cleaning effect, there is certain stimulation to skin
Effect, and gasoline, kerosene have certain toxicity, alkalescence is too big, degreasing power is too strong, and clean effect is also not satisfactory, for a long time
Lead to pachylosiies, chap, decortication using meeting.Soap is in alkalescence, can make xerosis cutiss after washing, matt, is especially easily stained with
Dirt on hand and antibacterial, become pollution source.Compare with traditional fancy soap, soap, handwashing liquid has the advantage with its uniqueness,
It is even more ruthless very place in some aspects once " fatal weakness " of soap.
First, the solidss such as soap, fancy soap become easily infected by dirt and sterilization on hand, become pollution source.And wash one's hands
The contact surface of liquid and handss is but typically the pump head on bottle, and easy to clean, it is to avoid cross infection probability.Handwashing liquid leads to
Cross hand taken amount, only need to gently press pump head, liquid just flows into the palm of the hand, how much is grasped by oneself, capable of being conveniently and easily taken, also easily saves
About.Handwashing liquid foaming abundancy is fine and smooth, and water excessively is felt well, and can water-saving can save time again.
Second, hand cleanser products composition diversification, the composition of handwashing liquid typically all contains pure glycerin, Aloe, Oleum Hippophae, dimension
The natural plant compositions such as raw element c, ph value is moderate, has reached the requirement of green product.The product property of handwashing liquid belongs to neutral, no
Phosphorus, aluminum, alkali, sodium alkyl benzene sulfonate etc., gentle decontamination, easily accepted by skin, the Aloe that particularly wherein contains, vitamin c
Deng composition, more the effect moistening deeply can be played to the skin of hand although some fancy soaps also have certain taste to hand
The function of profit, but their effect has difficulties in competiting with handwashing liquid.
3rd, sterilizing effect is substantially.Handwashing liquid is to Candida albicans, staphylococcus aureuses, escherichia coli, first
The sterilization rate of the source of disease such as liver, hepatitis B, up to more than 90%, to human body nonirritant, and no anaphylaxiss, protects oneself effectively
With household away from antibacterial and disease, practicality is stronger.
4th, compared with skating and volume is also larger for the solid such as soap, fancy soap, particularly disadvantageous hold in child, old man, and wash
Handss liquid can avoid this problem.Although soap has good dirt-removing power, easily landing, is readily soluble product when in use,
Especially meet hot water, high temperature and water logging, naturally expend higher.
" Chinese herbal medicine " is then the best raw material of functional cosmetics, correctly selects Chinese herbal medicine to add in washing product, has very
Good antibacterial, skin care effect.Chinese medicine elite is dissolved into and washes in shield product, be the Development Trend of modern handwashing liquid.Profit
With sophisticated technologies, extract the essential ingredient in Chinese medicine, so that effective ingredient is fully contacted with skin, preferably play antibacterial, skin moistening
Effect.For busy working clan, elderly population and xerosis cutiss person, the operator often working out of doors, or often
For the personnel of the chemical drugss such as contact acid, bases, wash shield product Shi Ji section using containing the antibacterial, skin care of Chinese medicine elite
Learn again easy method.
Content of the invention
For solving above-mentioned technical problem, the present invention provides a kind of skin moistening liquid soap containing natural bacteriostatic composition and its preparation
Method.
A kind of skin moistening liquid soap containing natural bacteriostatic composition that the present invention provides, by the raw material preparation of following content
Become:
Described sodium copper chlorophllin is prepared by the following method:
Weigh appropriate Folium Bambusae, Folium Bambusae is cleaned and dries, then pulverize, add 75%-95%'s by the solid-liquid ratio of 1:10-15
Ethanol, as leaching extracting solution, heating in water bath 0.5-2h, reduce pressure sucking filtration, and gained filtrate adjusts ph to 10- with the naoh of 5%-10%
13, maintain 1-2.5h with 60 DEG C of -80 DEG C of heating in water bath, use isopyknic petroleum ether extraction concentrated extracting solution 2-5 time every time, fetch water
Layer segment, then uses 0.2-0.5mol/l hcl to adjust ph to 2-4, adds the cuso of 15%-20%4In clear liquid ratio 1:2-
1:4 adds, and 0.5-1.5h is heated in 60 DEG C of -80 DEG C of waters bath with thermostatic control, and 3000r/min is centrifuged 5-10 minute, then washes, uses 5%-
10% naoh adjusts ph to 11-12, takes precipitation, dries, finely ground, obtains final product sodium copper chlorophllin.
Described Flos Chrysanthemi Indici extract is to be prepared by the following method:
Weigh Flos Chrysanthemi Indici appropriate, soak 6-10h, decoct 2 times, each 1h, amount of water first time is 6-30 times, second
Secondary for 6-16 times, collecting decoction, be concentrated into density be 1.01-1.08g/ml, add ethanol, make concentration of alcohol reach 65%-
80%, stir, stand 12-20h, filtration, reclaim ethanol, be concentrated into paste, 40 DEG C -65 DEG C vacuum drying, finely ground, that is,
?.
Described essence is peach flavor, flavoring pineapple essence, Fructus Citri Limoniae essence, green cucumber essence, jasmin essence or osmanthus flower fragrance.
A kind of preparation method of skin moistening liquid soap containing natural bacteriostatic composition that the present invention provides, comprises the following steps:
A) weigh cation guar gum 1-4g, be added in the distilled water of 20-50ml, 60-80 DEG C of heating in water bath, side is heated
Side is stirred, to be mixed uniformly after, standing makes it fully swelling, stand-by；
B) weigh the double stearate 3-6g of polyethylene glycol 6000, be added in 10-30ml distilled water, be heated to 60-80 DEG C,
Heat while stirring, after mix homogeneously, standing makes it fully swelling, stand-by；
C) weigh sodium lauryl sulphate 3-6g, be added in 10-30ml distilled water as solution 1；
D) Brij 35 sodium sulfate 9-13g, Cocoalkyl amido propyl betaine 4- are weighed respectively
8g, cocoanut fatty acid diethanolamide 5-8g, n- coco-nut oil fatty acid glycine potassium 1-4g, Semen Tritici aestivi germ oil 1-6g, glycerol
4-10g stirs, as solution 2；
F) take a large beaker, add sodium copper chlorophllin 1-10g, Flos Chrysanthemi Indici extract 1-10g, then by solution 1, solution 2
Add, be uniformly mixed；
G) swelling good cation guar gum, the double stearate of polyethylene glycol 6000 are added to the large beaker of step f)
In, weigh sodium benzoate 0.8-2g, vitamin c 0.1-0.5g, essence 0.05-0.25g, add the heating of 2-15ml distilled water molten
Solution, to be dissolved after put in the large beaker of step f), stir and obtain final product the skin moistening liquid soap containing natural bacteriostatic composition.
Various composition in the present invention is as follows:
Semen Tritici aestivi germ oil has concentrated the nutrition elite of Semen Tritici aestivi, lives rich in vitamin e, linoleic acid, linolenic acid and multiple physiology
Property component, be valuable functional food, there is very high nutritive value.Particularly vitamin e comparision contents are high, are acknowledged as
A kind of functional grease having much nutrition health-care functions, has endocrine regulation, prevents mottle, black speck and pigmentation；Antioxygen
Change acts on, and reduces lipid peroxide and generates, promotes moisture-retention function of skin, so that skin is moistened, slow down aging；Enhance metabolism and
Skin renewal, crease-resistant, wrinkle resistant, anti-skin aging, elimination cicatrix.Semen Tritici aestivi germ oil is applied to parts of body, after clean skin, takes suitable
Amount is applied in skin surface, gently massages.Its anti-oxidation function, can effective protection skin from natural environment injury.
Flos Chrysanthemi Indici contains yejuhua lactone, chrysanthemol, flavonoid glycoside, flavonoid, half terpenes, polysaccharide, alantol, aminoacid
With trace element etc., tool dispelling wind and heat pathogens, subduing swelling and detoxicating, infection, effect of antiviral.Flos Chrysanthemi Indici water extract and vapor distillation
The aeruginouss volatile oil that method extracts has killing or inhibitory activity to various pathogens, virus.Flos Chrysanthemi Indici extracting solution (water extract)
Volatile oil is better than to the inhibitory activity of staphylococcus aureuses, dysentery bacterium, escherichia coli, Bacillus typhi etc., and has anti-
Inflammation, antioxidation, the activity of Repercusion analgesia.Flos Chrysanthemi Indici extracting solution be applied to all kinds of daily skin care item, it is antibacterial, antiinflammatory, analgesia,
Antioxidative acts on highly significant.
Sodium copper chlorophllin is a kind of natural, food coloring of water solublity, safety non-toxic, is through FAO (Food and Agriculture Organization of the United Nation)
Pigment with the approval use of food additive standard committee of China.This use of a compound is extensive, in medical aspect copper chlorophyll
Sodium salt enhances metabolism to body, has stronger anti-cancer, effect for cancer, in terms of daily-use chemical industry, have deodorization,
Antiphlogistic antibacterial etc. acts on, and is widely used in the aspects such as medicated toothpaste.
Cation guar gum plays good foaming, steady bubble, antistatic and thickening power in washing product, can reduce washing
The zest to skin for the agent.
Substantial amounts of extracted form natural plant composition, sodium copper chlorophllin, Flos Chrysanthemi Indici water extract is with the addition of in this handwashing liquid prescription
And have killing or inhibitory activity Flos Chrysanthemi Indici extracting solution (water extract) to staphylococcus aureuses, dysentery to various pathogens, virus
The inhibitory activity of bacillus, escherichia coli, Bacillus typhi etc. is better than volatile oil, and has the work of antiinflammatory, antioxidation, Repercusion analgesia
Property.Fructus Tritici aestivi Wheat Protein, reduces lipid peroxide and generates, promote moisture-retention function of skin, so that skin is moistened, delays to decline
Always；Enhance metabolism and skin renewal, crease-resistant, wrinkle resistant, anti-skin aging, elimination cicatrix.
On the other hand have selected the stronger anion surfactant of dirt-removing power in hand sanitizer formula as main table
Face activating agent, then coordinate amphoteric surfactant nonionic surfactant as auxiliary surfactant.May be selected two in formula
Property surfactant as cosurfactant, such material generally has good bactericidal action, with anionic surface live
Property agent and nonionic surfactant all have good compatibility, foaming abundancy and stablize, flexibility is good, the stimulation to skin
Property is little, and biological degradability is good, and has good viscosity adjustment effect.
In a word, this handwashing liquid can suppress antibacterial, the growing of funguses, skin care, reach the effect of cleaning skin moistening, can supplement
Moisture, enhances metabolism, and makes skin moisturizing clean.
Handwashing liquid made by the present invention is in sky blue, transparent sparkling and crystal-clear, and viscosity is suitable, and foam is smooth abundant, fine and smooth equal
Even, stretchability is good, cool and comfortable, good stability, fragrant.
Specific embodiment
With reference to embodiment, the present invention will be further described.
The Semen Tritici aestivi germ oil of the present invention is commercially available.
Embodiment 1
1.1 sodium copper chlorophllins are prepared by the following method:
Weigh Folium Bambusae 20g, Folium Bambusae is cleaned and dries, then pulverize, add by the solid-liquid ratio of 1:12 and soak extracting solution, 75%
Ethanol, heating in water bath 0.5h, reduce pressure sucking filtration, and gained filtrate adjusts ph to 11 with 5% naoh, maintains 1h with 75 DEG C of heating in water bath,
Use every time isopyknic petroleum ether extraction concentrated extracting solution 2 times, layer segment of fetching water, then use 0.2mol/l hcl regulation ph to 2,
Add 15% cuso4Add in clear liquid ratio 1:2,75 DEG C of waters bath with thermostatic control heating 1h, 3000r/min centrifugation 8 minutes, then
Washing, the naoh with 5% adjusts ph to 11, takes precipitation, dries, finely ground, obtains final product.
1.2 Flos Chrysanthemi Indici extracting solution are prepared by the following method:
Weigh Flos Chrysanthemi Indici 30g, soak 8h, decoct 2 times, each 1h, amount of water first time is 900ml, is for the second time
480ml, collecting decoction, being concentrated into density is 1.06g/ml, adds ethanol, makes concentration of alcohol reach 75%, stir, standing
15h, filtration, reclaim ethanol, be concentrated into paste, 60 DEG C of vacuum drying, finely ground, obtain final product.
The preparation of 1.3 handwashing liquid
A) weigh cation guar gum 3g, be added in the distilled water of 30ml, 60 DEG C of heating in water bath, heat while stirring,
To be mixed uniformly after, standing makes it fully swelling, stand-by；
B) weigh double stearate 638 4g of polyethylene glycol 6000, be added in 20ml distilled water, be heated to 60 DEG C, Bian Jia
The stirring of hot side, after mix homogeneously, standing makes it fully swelling, stand-by；
C) weigh sodium lauryl sulphate 3g to be added in 20ml distilled water as solution 1；
D) Brij 35 sodium sulfate aes 10g, Cocoalkyl amido propyl betaine are weighed respectively
Cab 6g, cocoanut fatty acid diethanolamide 6501 6g, n- coco-nut oil fatty acid glycine potassium gck-12 3g, Fructus Tritici aestivi
Oily 5g, 4g glycerol, stirs, as solution 2；
F) take a large beaker, weigh sodium copper chlorophllin 6g, Flos Chrysanthemi Indici extract 10g, then solution 1, solution 2 are added,
Use Glass rod mix homogeneously.
G) by swelling good cation guar gum, the double stearate 638 of polyethylene glycol 6000, it is added to the big burning of step f)
In cup, weigh sodium benzoate 1.0g, vitamin c 0.3g, jasmin essence 0.08g, add 15ml distilled water heating for dissolving, treat molten
Add after solution in large beaker, remaining distilled water is added in the large beaker of step f), stirs, obtain skin moistening and wash one's hands
Liquid.
Embodiment 2
The preparation of 2.1 sodium copper chlorophllins
Weigh 50g Folium Bambusae, Folium Bambusae is cleaned and dries, then pulverize, add leaching extracting solution (85% by the solid-liquid ratio of 1:14
Ethanol), heating in water bath 1h, reduce pressure sucking filtration, and gained filtrate adjusts ph to 12 with 5% naoh, maintains 2.0h with 80 DEG C of heating in water bath,
Use every time isopyknic petroleum ether extraction concentrated extracting solution 2 times, layer segment of fetching water, then use 0.2mol/l hcl regulation ph to 2,
Add 15% cuso4Add in clear liquid ratio 1:2,75 DEG C of waters bath with thermostatic control heating 1h, 3000r/min centrifugation 10 minutes, so
After wash, with 5% naoh adjust ph to 12, take precipitation, dry, finely ground, obtain final product.
The preparation of 2.2 Flos Chrysanthemi Indici extracts
Weigh Flos Chrysanthemi Indici 20g, soak 6h, decoct 2 times, each 1h, amount of water first time is 600ml, is for the second time
240ml, collecting decoction, it is concentrated into relatively for 1.06g/ml, add ethanol, make concentration of alcohol reach 75%, stir, standing
12h, filtration, reclaim ethanol, be concentrated into paste, 60 DEG C of vacuum drying, finely ground, obtain final product.
The preparation of 2.3 skin moistening liquid soaps containing natural bacteriostatic composition
A) weigh cation guar gum 2g, be added in the distilled water of 40ml, 80 DEG C of heating in water bath, heat while stirring,
To be mixed uniformly after, standing makes it fully swelling, stand-by；
B) weigh double stearate 638 4g of polyethylene glycol 6000, be added in 20ml distilled water, be heated to 80 DEG C, Bian Jia
The stirring of hot side, after mix homogeneously, standing makes it fully swelling, stand-by；
C) weigh sodium lauryl sulphate 6g, be added in 30ml distilled water as solution 1；
D) Brij 35 sodium sulfate aes 10g, Cocoalkyl amido propyl betaine are weighed respectively
Cab 5g, cocoanut fatty acid diethanolamide 6501 7g, n- coco-nut oil fatty acid glycine potassium gck-12 3g, Fructus Tritici aestivi
Oily 4g, glycerol 5g stir, as solution 2；
F) take a large beaker, add sodium copper chlorophllin 5g, Flos Chrysanthemi Indici extract 5g, then solution 1, solution 2 are added, use
Glass rod mix homogeneously；
G) swelling good cation guar gum, the double stearate 638 of polyethylene glycol 6000 are added to the big burning of step f)
In cup, weigh sodium benzoate 1.0g, vitamin c 0.4g, flavoring pineapple essence 0.1g, add 10ml distilled water heating for dissolving, to be dissolved
Put into afterwards in the large beaker of step f), stir and obtain final product the skin moistening liquid soap containing natural bacteriostatic composition.
Embodiment 3
The physical and chemical index of embodiment 1,2 is as follows:
3.1 character
This product is that viscosity is suitable, and foam is smooth abundant, and color is pleasing, fine and smooth uniformly, stretchability is good, dirt-removing power relatively
Good light blue handwashing liquid.
3.2ph value checks
Dip a small amount of handwashing liquid with the ph reagent paper of moistening, ph is 6-7.
3.3 caloric test
Handwashing liquid is packaged in transparence cosmetic bottle, observes no lamination within two weeks about in 3 DEG C of refrigerator cold-storages.In
24h in 60 DEG C of calorstat, handwashing liquid is no layered, emulsifying is spoiled, the phenomenon such as rotten.
3.4 centrifugal test
Handwashing liquid is packaged in 3000r/min centrifugation 15min, no lamination in tool plug test tube.
3.5 irritation tests, anaphylaxis experiment
White mice back cuts off hair, smears respectively and does not apply in cutting plucked position, with by the handwashing liquid of embodiment 1,2 preparation
Position is compared, and result does not have zest and anaphylaxiss.
1 gram of Example is applied in volunteer (15-65 year, 380 people) gesture and facial expression, observes after spending 30 minutes, does not all occur sending out
Red, dermexanthesis, foaming phenomena.
3.6 room temperatures place experiment
The made handwashing liquid of embodiment 1,2 is placed in bottle for cosmetics, room temperature standing is investigated 6 months, no lamination is used
After feel unchanged, abnormal smells from the patient is unchanged, no denaturalization phenomenon.
3.7 clean effects
Choose volunteer (15-65 year, 80 people), obtained handwashing liquid is used for volunteer on hand, with the mixing of a small amount of water
And repeatedly wash by rubbing with the hands, find foaming abundancy, preferably, volunteers generally feel smooth comfortable to soil release performance, preferably, abnormal smells from the patient is pure and fresh for feel
Pleasant, after washing, dermal sensation is comfortable, non-greasy, and moistening effect is preferable.
Embodiment 4:
This handwashing liquid resultant effect is investigated
Feel to evaluate the effect of the handwashing liquid that embodiment 1 produces following with probation.Using public-opinion poll point system,
Choose 80 25-50 year age bracket women as object on probation, be arbitrarily divided into two groups, respectively washing with embodiment 1 preparation
Handss liquid is washed one's hands.Use 3 times daily, use time is one month.Every using effect total score is divided into best result for 5 points: 5, represents
Very well, very satisfied；4 are divided into preferably；3 are divided into and can accept；Less than 3 points is bad it is impossible to accept.It is below that items are average to obtain
Point.The results are shown in Table 1:
Table 1 resultant effect is investigated
| Using effect | The every average of embodiment 1 | The every average of embodiment 2 |
| Moisture retention | 4.8 | 4.9 |
| Moistness | 4.7 | 4.8 |
| Cooling | 5 | 5 |
| Foaming characteristic | 5 | 5 |
| Soil release performance | 5 | 5 |
| Comfortableness | 4.8 | 4.9 |
In sum, this made handwashing liquid foaming abundancy of the present invention, has good soil release performance, moisture retention, alimentary, makes
Used time feels refrigerant comfortable.
Claims (3)
1. a kind of skin moistening liquid soap containing natural bacteriostatic composition is it is characterised in that be prepared from by the raw material of following content:
Brij 35 sodium sulfate 9-13g
Cocoalkyl amido propyl betaine 4-8g
Sodium copper chlorophllin 1-10g
Flos Chrysanthemi Indici extract 1-10g
Sodium lauryl sulphate 3-6g
Semen Tritici aestivi germ oil 1-6g
Cocoanut fatty acid diethanolamide 5-8g
N- coco-nut oil fatty acid glycine potassium 1-4g
The double stearate 3-6g of polyethylene glycol 6000
Cation guar gum 1-4g
Glycerol 4-10g
Vitamin c 0.1-0.5g
Distilled water 42-125ml
Sodium benzoate 0.8-2g
Essence 0.05-0.25g；
Described sodium copper chlorophllin is prepared by the following method:
Weigh appropriate Folium Bambusae, Folium Bambusae cleaned and dries, then pulverize, add the ethanol of 75%-95% by the solid-liquid ratio of 1:10-15,
As leaching extracting solution, heating in water bath 0.5-2h, reduce pressure sucking filtration, and gained filtrate adjusts ph to 10-13 with the naoh of 5%-10%, uses 60
DEG C of -80 DEG C heating in water bath maintain 1-2.5h, use isopyknic petroleum ether extraction concentrated extracting solution 2-5 time every time, water intaking layer segment,
Then use 0.2-0.5mol/l hcl to adjust ph to 2-4, add the cuso of 15%-20%4Add in clear liquid ratio 1:2-1:4,
0.5-1.5h is heated in 60 DEG C of -80 DEG C of waters bath with thermostatic control, and 3000r/min is centrifuged 5-10 minute, then washes, and is adjusted with the naoh of 5%-10%
Section ph to 11-12, takes precipitation, dries, finely ground, obtains final product sodium copper chlorophllin；
Described Flos Chrysanthemi Indici extract is to be prepared by the following method:
Weigh Flos Chrysanthemi Indici appropriate, soak 6-10h, decoct 2 times, each 1h, amount of water first time is 6-30 times, is for the second time
6-16 times, collecting decoction, being concentrated into density is 1.01-1.08 g/ml, adds ethanol, makes concentration of alcohol reach 65%-80%, stir
Mix uniformly, stand 12-20h, filtration, reclaim ethanol, be concentrated into paste, 40 DEG C -65 DEG C vacuum drying, finely ground, obtain final product.
2. the skin moistening liquid soap containing natural bacteriostatic composition according to claim 1 is it is characterised in that described essence is
Peach flavor, flavoring pineapple essence, Fructus Citri Limoniae essence, green cucumber essence, jasmin essence or osmanthus flower fragrance.
3. a kind of preparation method of the skin moistening liquid soap containing natural bacteriostatic composition described in claim 1 is it is characterised in that institute
The preparation method stated comprises the following steps:
A) weigh cation guar gum 1-4g, be added in the distilled water of 20-50ml, 60-80 DEG C of heating in water bath, stirs in heating
Mix, to be mixed uniformly after, standing makes it fully swelling, stand-by；
B) weigh the double stearate 3-6g of polyethylene glycol 6000, be added in 10-30ml distilled water, be heated to 60-80 DEG C, Bian Jia
The stirring of hot side, after mix homogeneously, standing makes it fully swelling, stand-by；
C) weigh sodium lauryl sulphate 3-6g, be added in 10-30ml distilled water as solution 1；
D) weigh respectively Brij 35 sodium sulfate 9-13g, Cocoalkyl amido propyl betaine 4-8g,
Cocoanut fatty acid diethanolamide 5-8g, n- coco-nut oil fatty acid glycine potassium 1-4g, Semen Tritici aestivi germ oil 1-6g, glycerol 4-
10g stirs, as solution 2；
F) take a large beaker, add sodium copper chlorophllin 1-10g, Flos Chrysanthemi Indici extract 1-10g, then solution 1, solution 2 are added,
It is uniformly mixed；
G) swelling good cation guar gum, the double stearate of polyethylene glycol 6000 are added in the large beaker of step f), claim
Take sodium benzoate 0.8-2g, vitamin c 0.1-0.5g, essence 0.05-0.25g, add 2-15ml distilled water heating for dissolving, treat
Put into after dissolving in the large beaker of step f), stir and obtain final product the skin moistening liquid soap containing natural bacteriostatic composition.
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| CN105411918A (en) * | 2015-12-02 | 2016-03-23 | 济宁医学院 | Bamboo leaf skin-caring foam type hand washing liquid |
| CN105326727A (en) * | 2015-12-11 | 2016-02-17 | 饶雅琴 | Wild chrysanthemum flower washing-free hand sanitizer and preparation method thereof |
| CN106176362A (en) * | 2016-07-25 | 2016-12-07 | 深圳先进技术研究院 | A kind of Herba Sophorae alopecuroidis antibiotic skincare hand cleanser and preparation method thereof |
| CN106983682A (en) * | 2017-03-19 | 2017-07-28 | 长沙协浩吉生物工程有限公司 | A kind of compound method of ferment hand cleanser |
| CN107536754A (en) * | 2017-09-07 | 2018-01-05 | 芜湖皖江知识产权运营中心有限公司 | A kind of gentle tender skin hand cleanser and preparation method thereof |
| CN108403547A (en) * | 2018-04-20 | 2018-08-17 | 朱华伟 | A kind of bacteriostatic hand sanitizer and preparation method thereof |
| CN108324652A (en) * | 2018-04-23 | 2018-07-27 | 安徽科技学院 | A kind of radix echinopsis latifolii bacteriostatic hand sanitizer and preparation method thereof |
| CN108578346A (en) * | 2018-08-01 | 2018-09-28 | 杨林 | A kind of skin care anti-bacterial hand lotion and preparation method thereof |
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| KR20100035005A (en) * | 2008-09-25 | 2010-04-02 | 유한킴벌리 주식회사 | Cosmetic composition for kids with high moisturizing effects |
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