CN103800275A - Whitening anti-aging cosmetic and preparation method thereof - Google Patents

Whitening anti-aging cosmetic and preparation method thereof Download PDF

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Publication number
CN103800275A
CN103800275A CN201410048897.5A CN201410048897A CN103800275A CN 103800275 A CN103800275 A CN 103800275A CN 201410048897 A CN201410048897 A CN 201410048897A CN 103800275 A CN103800275 A CN 103800275A
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extract
whitening
whitening anti
aging
skin
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李美凤
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Qingdao University
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李美凤
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Abstract

The invention discloses a whitening anti-aging cosmetic and a preparation method of the whitening anti-aging cosmetic. The whitening anti-aging cosmetic has the formula comprising an oil phase, a water phase, a functional component and a preservative, wherein the oil phase comprises 15-25% of oil, 0.5-10% of emulsifying agent and 1-5% of co-emulsifier; the water phase comprises 30-75% of ionized water, 0.5-8% of emulsifying agent, 3-8% of humectant, 0-3% of alkaline agent, 0-1.5% of thickening agent and 0-0.5% of emulsion stabilizer; the functional component comprises 0.5-1.5% of pomegranate bark extract, 0.5-3% of spirulina extract, 0.5-3% of corn super oxide dismutase extract and 1-5% of fruit acid mixture; the whitening anti-aging cosmetic comprises 0.3-2% of preservative. The whitening anti-aging cosmetic is prepared by reasonably compounding the active ingredients, and has the effects of whitening skin and resisting senility. The active ingredients are embedded, so that the problems of dispersity and stability of the active ingredients can be effectively solved; furthermore, the release speed of the active ingredients is effectively delayed, so that the aims of being effective for a long time and safe to use can be achieved.

Description

A kind of whitening anti-aging cosmetics and preparation method thereof
Technical field
The present invention relates to cosmetic field, establish especially and a kind of cosmetics simultaneously with whitening and anti-senescence function and preparation method thereof.
Background technology
Cosmetic industry has entered a New Times, far beyond in the past simple and crude moisturizing state, has entered the research and development new stage.The sales volume of individual's skin care product keeps the trend rising year by year in recent years, and the product consumption especially with wrinkle removing and repair function increases rapid especially.
Skin aging is a kind of nature and general process, and aging causes the change of skin function on physiology, and this change is irreversible variation, is also the problem of women worry of much liking to be beautiful.Cause the factor of skin aging to comprise inherent gene variation, the variation of hormone level etc., also comprise external ultraviolet injury, free-radical oxidation etc.The impact that its medium-term and long-term daylight (ultraviolet) irradiates or smoking brings is the most remarkable, and daylight light can produce active oxygen (ROS), superoxide anion (O 2 -), hydroxyl radical free radical (OH), hydrogen peroxide (H 2o 2), singlet oxygen ( 1o 2), nitric oxide (NO), lipid peroxide (LPO) etc., these materials cause various genetic transfer factor activations, thereby promote the generation of the skin aging problems such as wrinkle or mottle.In addition in atmosphere, finely ground particles can cause skin oxidation, thereby causes skin to occur prematurely aging, and promotes the generation of wrinkle or mottle etc.
Skin aging shows xerosis cutis, coarse, pliability is poor, tired, gloomy, there is microgroove, mottle etc. in skin, mainly be summed up as skin and lack moisture, cell viability decline, Exposure to Sunlight damage etc., therefore in the formula of anti-aging cosmetics, should comprise and strengthen moisturizing and repair skin barrier function component; There is promotion cell viability, promote collagen and elastic cell synthetic, strengthen the component of skin elasticity; There is the component of effective removing oxygen-derived free radicals function; Have sun-proofly, alleviate the component of the skin injury causing because of Exposure to Sunlight.
Whitening function cosmetics from come out since be subject to liking to be beautiful both at home and abroad always personage pay close attention to.The cosmetics of now more and more kinds have all had whitening function in various degree, and whitening class cosmetics have experienced from the covering whitening of physical property and disturbed and metabolic " cooperative effect " whitening normally of blocking-up melanin to chemical.In the epidermal area of human body skin, in basal layer, exist a large amount of melanocytes, these cells can be manufactured melanin, and the endocrine of external environment condition and health all can affect greatly the metabolism of melanocyte.Thereby for example when will activating tryrosinase wherein during to skin, the ultraviolet radiation in extraneous sunlight make melanin quickening formation, skin now there will be mottle or the phenomenon such as tanned.Whitening composition in cosmetics is mainly to suppress radical pair melanin form and maintain tyrosinase inhibitor activity, or makes tegumentary chromatophore accelerate metabolism, reduces pigmentation and cutin and generates, and improves skin autoprotection ability.But the extraneous factor such as sunshine and environmental pollution is also skin-lightening cosmetic need to be considered in the time carrying out recipe design.
Develop safely, have no side effect for meeting, meet the cosmetics that go back to nature and require, natural animal-plant extract and biological preparation become the first-selection of functional additive.In anti-aging product, cell growth factor, low molecular polypeptide, aminoacid, enzyme are conventional antidotal agents.And arbutin, kojic acid, fruit acid, vitamin A, vitamin C are the normal whitening compositions using at present domestic and international skin-lightening cosmetic in whitening product.The soda acid sensitivity of above-mentioned most preparation to the cosmetics course of processing, therefore, how making same cosmetics when white-skinned face function is provided, play antidotal effect, is the problem that Many researchers is paid close attention to, and such cosmetics also will have very large market potential and using value.
Summary of the invention
The present invention cannot exist for solving whitening component and anti-aging in conventional cosmetics in same system; and the problem of whitening component and anti-aging less stable; providing a kind of carries out whitening component and anti-aging after embedding; add in same cosmetics series; the cosmetics simultaneously with whitening and defying age double effects are provided; this product is little to the zest of skin, and active component is longer to the guard time of skin, the personage's that conveniently likes to be beautiful use.
The present invention includes two parts, i.e. whitening anti-aging cosmetic formulations and preparation method thereof.The formula of whitening anti-aging cosmetics is made up of four parts.
1) oil phase: oils and fats 15-25%, emulsifying agent 0.5-10%, co-emulsifier 1-5%.
2) water: deionized water 30-75%, emulsifying agent 0.5-8%, wetting agent 3-8%, alkaline agent 0-3%, thickening agent 0-1.5%, emulsion stabilizer 0-0.5%.
3) functional component: Pericarpium Granati extract 0.5-1.5%, spirulina extract 0.5-3%, Semen Maydis superoxide dismutase extract 0.5-3%, fruit acid mixture 1-5%.
4) antiseptic 0.3-2%.
Oils and fats in oil phase described in above-mentioned whitening anti-aging cosmetic formulations comprises animal raw fat, as stearic acid, lanoline, spermaceti, ermine oil; Vegetative grease, as Oleum Cocois, olive oil, Jojoba oil, Oleum Ricini, almond oil, Fructus Maydis oil; Mineral oil, as white oil; Synthetic ester oil, as dimethicone, phenyl methyl silicone oil, cyclomethicone, amino-silicone, isopropyl palmitate, stearic acid butyl alcohol ester.Preferred scheme is the mixture of at least two quasi-greases in animal raw fat, vegetative grease and synthetic ester oil three quasi-greases.Emulsifying agent in oil phase comprises one or more the mixture in glyceryl monostearate, sorbitan oleate, anhydrosorbitol monostearate, sorbitan-monopalmityl ester, fatty alcohol-polyoxyethylene ether etc.Co-emulsifier in oil phase comprises hexadecanol, octadecanol.
Emulsifying agent described in above-mentioned whitening anti-aging cosmetic formulations comprises one or more the mixture in stearic acid sodium glutamate, polyoxyethylene hexadecanol ether, polyoxyethylene ether sorbitan stearate, polyoxyethylene ether sorbitan palmitate, fatty alcohol-polyoxyethylene ether, peregal etc.Wetting agent in water comprises one or more in glycerol, 1,3-PD, 1,3 butylene glycol, Sorbitol.Alkaline agent in water has the one in potassium hydroxide, sodium hydroxide, triethanolamine, diethanolamine, ethanolamine.Thickening agent in water comprises one or more in stearyl dimethyl amine oxide, HANSHENGJIAO, Radix Acaciae senegalis, carboxymethyl cellulose, hydroxyethyl-cellulose, guar gum etc.Stabilizing agent in water comprises sodium ethylene diamine tetracetate, sodium citrate.
Pericarpium Granati extract described in above-mentioned whitening anti-aging cosmetic formulations is that Pericarpium Granati is pulverized, utilize organic lixiviate active component wherein under ultrasound wave assosting effect that is dissolved in, subsequently with the active carbon processing of decolouring, filter and remove after active carbon, organic solvent is removed in distilling under reduced pressure can obtain extract.Obtaining extract phospholipid carries out embedding treatment and obtains the embedding Pericarpium Granati extract that particle diameter is 1-20 μ m.
Spirulina extract described in above-mentioned whitening anti-aging cosmetic formulations is that spirulina is carried out after ultrasonic disruption, utilizes phosphate buffered solution lixiviate active component wherein, adopts subsequently the sub-chromatography purification of gel column concentrated, obtains extract product.Obtaining extract phospholipid carries out embedding treatment and obtains the embedding spirulina extract that particle diameter is 1-20 μ m.
Semen Maydis superoxide dismutase extract described in above-mentioned whitening anti-aging cosmetic formulations is to pulverize making beating after corn soaking is germinateed, utilize the superoxide dismutase in phosphate buffered solution lixiviate Semen Maydis pulp, the temperature that raises is subsequently utilized the superoxide dismutase product of heating denaturalization purification.Obtain extract gelatin and carry out embedding treatment, obtaining particle diameter is the embedding Semen Maydis superoxide dismutase extract of 1-20 μ m.
Fruit acid mixture described in above-mentioned whitening anti-aging cosmetic formulations comprises lactic acid, kojic acid, citric acid, malic acid, tartaric acid.Fruit acid mixture is through phospholipid embedding treatment, and obtaining particle diameter is 1-20 μ m embedding fruit acid mixture.
Described in above-mentioned whitening anti-aging cosmetic formulations, antiseptic comprises one or more in methyl parahydroxybenzoate, nipasol, butoben, diazolidinyl urea.
Whitening anti-aging cosmetics preparation method of the present invention is made up of following steps.
5) by above-mentioned 1) in all materials join in reaction pot A, warming while stirring is all dissolved to all materials, keeps 20-30min.
6) by above-mentioned 2) in all materials join in reaction pot B, warming while stirring 80-90 ℃, keep 20-30min.By 5) dissolve material be added in reaction pot B, stir 20-30min.
7) material in reaction pot B is cooled to 40-50 ℃, adds 3) and 4) in material, insulated and stirred 20-30min, slow cooling, to room temperature, obtains whitening anti-aging cosmetics.
In the whitening anti-aging cosmetics that said method is produced, various bioactive ingredients all pass through embedding treatment, can be dispersed in emulsion system fast through phospholipid or gelatin embedding extract after treatment, and can be in alkalescence cosmetics stable existence.Embedding treatment can slow down the rate of release of active component simultaneously, reaches long-term, slow releasing effect, reduces the stimulation of active component to skin.
Said method is produced senile-resistant efficacy in cosmetics and is mainly derived from and in Pericarpium Granati, contains a large amount of Punica granatum L. polyphenol, anthocyanidin, ellagic acid, they are scavenger and the trapping agent of free radical, reduce and in and the free radical that produces in metabolic processes of organism, slow down the aging of skin.Punica granatum L. polyphenol can react with the protein in hydrogen bond and the effect such as hydrophobic and skin, produces astriction, and this reaction can make skin tight, reduces wrinkle.Meanwhile, all contain a large amount of active sods in spirulina and corn extract, it is extremely strong antioxidant, can eliminate the free radical of injured skin, can slow down the aging of skin.Superoxide dismutase also can promote collagen protein to form, and accelerates the metabolism of skin, makes skin high resilience.The all right blood circulation promoting of gamma-Linolenic acid in spirulina extract and the mixture of fruit acid, promotes cell viability, slow down aging.
White-skinned face function in said method production cosmetics is mainly derived from fruit acid mixture and superoxide dismutase acts on rapidly at the epidermal area of skin, accelerates the metabolism of keratodermatitis, keeps the elasticity of skin surface.In spirulina extract, contained gamma-Linolenic acid reacts the kojic acid list gamma-Linolenic acid fat generating and can be used as the inhibitor of tryrosinase with kojic acid, has the effect that anti-melanin generates, and is the functional factor effectively brightening in cosmetics.In Pericarpium Granati and spirulina extract, contain a large amount of vitamin Cs and vitamin E, vitamin C and vitamin E are classical reductant-oxidants, and the effectively activity of restraint of tyrosinase reduces melanin and generates in skin, reaches profound whitening effect.
The active component of above-mentioned cosmetics comes from natural extract, and rationally composite by active component has whitening and senile-resistant efficacy simultaneously.Active component, by embedding treatment, has effectively solved dispersibility and the stability problem of active component, also can effectively delay the rate of release of active component simultaneously, reaches object permanently effective, safe handling.
Below in conjunction with example, content of the present invention is described.
Specific embodiment
Embodiment 1
Whitening anti-aging frost formula 1 is as follows.The crowd that these cosmetics are applicable to neutral skin quality used in autumn and winter season.
Figure BSA0000101089200000041
Production method is as described below, and all materials in above-mentioned oil are joined in reaction pot A, and warming while stirring to all materials all dissolve, and keeps 20min.All materials in above-mentioned water are joined in reaction pot B, and warming while stirring 80-90 ℃, keeps 30min.The material that reaction pot A has been dissolved is slowly added in reaction pot B, stirring reaction 30min.Be cooled to 40 ℃, add functional additive and antiseptic, insulated and stirred 30min, slow cooling, to room temperature, obtains whitening anti-aging frost.
Embodiment 2
It is 2 as follows that whitening anti-aging defrost is filled a prescription.The crowd that these cosmetics are applicable to dryness skin quality used in autumn and winter season.
Figure BSA0000101089200000051
Production method is as described below, and all materials in above-mentioned oil are joined in reaction pot A, and warming while stirring to all materials all dissolve, and keeps 20min.All materials in above-mentioned water are joined in reaction pot B, and warming while stirring 80-90 ℃, keeps 30min.The material that reaction pot A has been dissolved is added in reaction pot B, stirs 20min.Be cooled to 40 ℃, add functional additive and antiseptic, insulated and stirred 30min, slow cooling, to room temperature, obtains whitening anti-aging frost.
Embodiment 3
Whitening anti-aging emulsion formulations 3 is as follows.The crowd that these cosmetics are applicable to different skin quality uses at spring and summer season.
Figure BSA0000101089200000052
Figure BSA0000101089200000061
Production method is as described below, and all materials in above-mentioned oil are joined in reaction pot A, and warming while stirring to all materials all dissolve, and keeps 20min.All materials in above-mentioned water are joined in reaction pot B, and warming while stirring 80-90 ℃, keeps 30min.The material that reaction pot A has been dissolved is added in reaction pot B, stirs 20min.Be cooled to 40 ℃, add functional additive and antiseptic, insulated and stirred 30min, slow cooling, to room temperature, obtains whitening anti-aging emulsion.

Claims (2)

1. whitening anti-aging cosmetics and preparation method thereof, is characterized in that formula is made up of four parts
1) composition of oil phase comprises oils and fats 15-25%, emulsifying agent 0.5-10%, co-emulsifier 1-5%;
2) composition of water comprises deionized water 30-75%, emulsifying agent 0.5-8%, wetting agent 3-8%, alkaline agent 0-3%, thickening agent 0-1.5%, emulsion stabilizer 0-0.5%;
3) functional component comprises Pericarpium Granati extract 0.5-1.5%, spirulina extract 0.5-3%, Semen Maydis superoxide dismutase extract 0.5-3%, fruit acid mixture 1-5%;
4) antiseptic 0.3-2%.
2. a kind of whitening anti-aging cosmetics according to claim 1 and preparation method thereof, it is characterized in that Pericarpium Granati extract, spirulina extract and fruit acid mixture are phospholipid embedding treatment product, Semen Maydis superoxide dismutase extract is gelatin embedding treatment product.
CN201410048897.5A 2014-02-08 2014-02-08 Whitening anti-aging cosmetic and preparation method thereof Pending CN103800275A (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104116677A (en) * 2014-07-30 2014-10-29 广州丹奇日用化工厂有限公司 Cosmetic composition and preparation method thereof
CN105769670A (en) * 2016-03-24 2016-07-20 松原市颖奇经贸有限责任公司 Skin anti-aging essence and preparation method and application thereof
CN105853342A (en) * 2016-05-17 2016-08-17 集美大学 Use of polyphenol extract from spirulina as tyrosinase inhibitor
CN108578350A (en) * 2018-05-04 2018-09-28 深圳市兰亭科技股份有限公司 A kind of care composition and preparation method thereof containing spirulina extract
CN108743468A (en) * 2018-06-16 2018-11-06 赖辉武 It is a kind of can the clear acne spot removal and skin care frost of beauty treatment tune skin formula and preparation method thereof
CN111084387A (en) * 2019-12-24 2020-05-01 李晨悦 Multifunctional nutritional composition, preparation method thereof and health food

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CN101336874A (en) * 2008-08-18 2009-01-07 贝侬生化(苏州工业园区)有限公司 Water-solubility active extract in fruit skin, preparation method and use thereof
CN102370591A (en) * 2010-08-24 2012-03-14 上海博天尼化妆品有限公司 Pomegranate rind extract method and application of pomegranate rind extract
CN102475674A (en) * 2010-11-29 2012-05-30 吴克 Exfoliating scrubbing serum
CN102475672A (en) * 2010-11-29 2012-05-30 吴克 Under-eye dark circle whitening and wrinkle-resisting cream
CN102475671A (en) * 2010-11-29 2012-05-30 吴克 Cream preparation for eliminating pseudo wrinkle of eye

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1570093A (en) * 2003-07-23 2005-01-26 韩伯钧 Extraction method for SOD complex enzyme fine powder from corn
CN101336874A (en) * 2008-08-18 2009-01-07 贝侬生化(苏州工业园区)有限公司 Water-solubility active extract in fruit skin, preparation method and use thereof
CN102370591A (en) * 2010-08-24 2012-03-14 上海博天尼化妆品有限公司 Pomegranate rind extract method and application of pomegranate rind extract
CN102475674A (en) * 2010-11-29 2012-05-30 吴克 Exfoliating scrubbing serum
CN102475672A (en) * 2010-11-29 2012-05-30 吴克 Under-eye dark circle whitening and wrinkle-resisting cream
CN102475671A (en) * 2010-11-29 2012-05-30 吴克 Cream preparation for eliminating pseudo wrinkle of eye

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104116677A (en) * 2014-07-30 2014-10-29 广州丹奇日用化工厂有限公司 Cosmetic composition and preparation method thereof
CN105769670A (en) * 2016-03-24 2016-07-20 松原市颖奇经贸有限责任公司 Skin anti-aging essence and preparation method and application thereof
CN105769670B (en) * 2016-03-24 2018-10-16 松原市颖奇经贸有限责任公司 A kind of skin anti-aging essence and the preparation method and application thereof
CN105853342A (en) * 2016-05-17 2016-08-17 集美大学 Use of polyphenol extract from spirulina as tyrosinase inhibitor
CN105853342B (en) * 2016-05-17 2019-05-03 集美大学 Purposes of the polyphenol extract as tyrosinase inhibitor a kind of in spirulina
CN108578350A (en) * 2018-05-04 2018-09-28 深圳市兰亭科技股份有限公司 A kind of care composition and preparation method thereof containing spirulina extract
CN108743468A (en) * 2018-06-16 2018-11-06 赖辉武 It is a kind of can the clear acne spot removal and skin care frost of beauty treatment tune skin formula and preparation method thereof
CN111084387A (en) * 2019-12-24 2020-05-01 李晨悦 Multifunctional nutritional composition, preparation method thereof and health food

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