CN104116677A - Cosmetic composition and preparation method thereof - Google Patents
Cosmetic composition and preparation method thereof Download PDFInfo
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- CN104116677A CN104116677A CN201410371364.0A CN201410371364A CN104116677A CN 104116677 A CN104116677 A CN 104116677A CN 201410371364 A CN201410371364 A CN 201410371364A CN 104116677 A CN104116677 A CN 104116677A
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Abstract
The invention discloses a cosmetic composition comprising the following components in parts by weight: 2-20 parts of plant extracting solution, 3-11 parts of moisturizing agent, 0.2-0.4 part of thickening agent, 0.1-0.5 part of emulsifying agent, 0.1-2 parts of silica, 0.03-0.07 part of potassium hydroxide, 0.055-0.88 part of pH regulator, 0.8-4 parts of preservative and 60-90 parts of water, wherein the moisturizing agent comprises a tsaoko amomum fruit extracting solution and a pomegranate peel extracting solution; the preservative comprises a common vladimiria root extracting solution. The cosmetic composition disclosed by the invention applies a mixed solution of the tsaoko amomum fruit extracting solution and the pomegranate peel extracting solution into the cosmetic composition, and can be used for effectively whitening the skin and resisting ultraviolet rays.
Description
Technical field
The present invention relates to cosmetic field, particularly relate to a kind of cosmetic composition with sun-proof white-skinned face function and preparation method thereof.
Background technology
Cosmetics are to smear, spray or other similar methods, impose on any position of human body surface (skin, fingernail, lip, the ripe film in oral cavity etc.), with the product that reaches clean, eliminates bad smell, skin protection, beauty treatment and modification object.
No matter be hot summer or warm winter, face skin long term exposure is in the environment of ultraviolet radiation.The melanin of Skin Cell forms, and is skin change, low and deep, dry.To how there is so skin whitening, effectively shielding of ultraviolet.This will be an important problem.
Along with the development of cosmetics industry, natural plants series products due to use safety, action temperature and, the advantage such as successful welcome.Be generally to obtain by corresponding processing the plant extract that contains effective ingredient, and add in cosmetics.
At present, the sun-proof whitening of cosmetics is on the market not obvious, and very easily causes allergic phenomena.Therefore, selecting which kind of plant, and being applied to of its safety reached to better sun-proof whitening effect in cosmetics, and can make skin obviously pale, effectively resist ultraviolet, is problem demanding prompt solution.
Summary of the invention
Based on this, the object of the present invention is to provide a kind of cosmetic composition.
Concrete technical scheme is as follows:
A kind of cosmetic composition, by weight, comprises following component:
Wherein, above-mentioned wetting agent comprises Fructus Tsaoko extracting solution and Pericarpium Granati extracting solution, and antiseptic comprises Radix Vladimiriae extracting solution.
In an embodiment, described plant extraction liquid is that weight part ratio is (1～10): the Fructus Tsaoko extracting solution of (1～10) and the mixing of Pericarpium Granati extracting solution therein.
In an embodiment, the weight part ratio of described Fructus Tsaoko extracting solution and Pericarpium Granati extracting solution is (5～8): (5～10) therein.
In an embodiment, described wetting agent is that weight part ratio is (0.1～1): the trehalose of (2～10), the mixing of glycerol therein.
In an embodiment, described thickening agent is that weight part ratio is (0.1～0.2): the transparent HANSHENGJIAO of (0.1～0.2) and the mixing of carbomer therein.
In an embodiment, described emulsifying agent is fine jade wax stearyl Fructus Canarii albi oils and fats/sorbitol Fructus Canarii albi oils and fats therein.
In an embodiment, described pH adjusting agent is that mass parts ratio is (0.005～0.08): the sodium hydroxide of (0.05～0.8) and the mixing of water therein.
In an embodiment, described antiseptic is that weight part ratio is (0.3～1): the mixing of the sodium benzoate/potassium sorbate of (0.5～3) and Radix Vladimiriae extracting solution therein.
In an embodiment, the weight portion of described Radix Vladimiriae extracting solution is 1～2 part therein.
Fructus Tsaoko extracting solution of the present invention, Pericarpium Granati extracting solution and Radix Vladimiriae extracting solution can be by conventional alcohol extracting method preparations, preferably following extracting method: it is in 50% ethanol that dry plant (Radix Vladimiriae, Pericarpium Granati, Fructus Tsaoko) is joined to mass ratio, under backflow and dipping, extract 1～3h, extract 1～3 time; Subsequently, extracting solution is filtered with filter cloth, obtain filtrate.Mix the filtrate of 1～3 time and be concentrated into dry plant (Radix Vladimiriae, Pericarpium Granati, Fructus Tsaoko) extracting solution.
The preparation method of above-mentioned cosmetic composition, comprises the following steps:
(1) first use the glycerol in wetting agent scattered thickening agent, add emulsifying pot, then add wetting agent, skinfeel regulator, the emulsifying agent of plant extraction liquid, remainder, be heated to 75～85 DEG C, insulated and stirred 10～20 minutes, stir speed (S.S.) is 20～40rpm, then homogenizing 2～5 minutes, stir speed (S.S.) is 2000～4000rpm, cools, and obtains A phase;
(2) by complete pH adjusting agent mixed dissolution, obtain B phase;
(3) A of step (1) is cooled to 65～70 DEG C mutually, adds the B phase in step (2), stir, continue cooling;
(4) when the temperature in step (3) near 40～45 DEG C, add antiseptic, stir, cosmetic composition.
Fructus Tsaoko is the dry mature fruit of Zingiberaceae Amomum herbaceos perennial Fructus Tsaoko, another name SEMEN TSAOKO, Fructus Tsaoko, and Fructus Tsaoko has cultivation on Yunnan Province of China, Guangxi, Guizhou, Sichuan and other places, and Yunnan is main product ground.The cinnamate extracting from Fructus Tsaoko has strong absorption to ultraviolet light.Fructus Tsaoko extracting solution is in the present invention as natural sun-prevention agent, and control skin irradiates the infringement causing because of short wave ultraviolet light UVB and long wave ultraviolet light UVA.In the present invention as sunscreen.
Pericarpium Granati is the dry peel of Punica granatum L..Punica Punicaceae Punica plant, a kind of machaka or dungarunga, if if having pomegranate pomegranate, pellet, golden small-mouthed jar, the another names such as gold Pang, Tu Lin.Punica granatum L. is mainly distributed in Ji Wen torrid areas, subtropical zone, all has Punica granatum L. plantation in each department, China north and south.Pericarpium Granati extracting solution is to the strong inhibition of the active demonstration of B-16 melanocyte, in the present invention as cosmetics whitening additive.
The Silicon stone adding in cosmetic composition of the present invention is that skinfeel regulator can make people be combined and improve skin condition with physiology from psychology, increases moisture of skin; The effect of pH adjusting agent is that cosmetic composition of the present invention is had the good acid-base value of skin effect.
Radix Vladimiriae is the dry root of Compositae Dolomiaea plant Radix Vladimiriae.Its equal plant gray wool Radix Vladimiriae is close with Radix Vladimiriae performance, mostly is mutual use.Radix Vladimiriae is Chinese medicine and Tibetan medicine cross-reference kind, in the dry root of medicinal Radix Vladimiriae and gray wool Radix Vladimiriae, Tibetan medicine is only used the dry root of Radix Vladimiriae.River Fructus Foeniculi mostly is wild, grow in the high mountain of height above sea level 3000～4500m, mainly be distributed in the Abazangzuqiangzu autonomous region of western Sichuan, Tibetan Autonomous Prefecture of Garze, the ground such as Yaan, Xichang, Yi Autonomous Prefecture of Liangshan and Eastern Tibet, there is a small amount of growth Deqin County, Tibetan autonomous prefecture, Deqen in Yunnan Province, Linxia Region of Gansu Province.Radix Vladimiriae has inhibitory action to staphylococcus aureus, dysentery bacterium and bacillus pyocyaneus, and dermatophytes is also had to inhibitory action.Stronger to gram positive bacteria comparison gram-negative bacteria and saccharomycetic bacteriostasis and sterilization effect.Because it has good bactericidal effect.Use as antiseptic in the present invention.But antibacterial is killed in the prevention that act as of antiseptic, and protection product is avoided microbial contamination, extends the product shelf phase; Prevent that consumer's use is subject to the product of microbial contamination and causes possible infection, guarantees safety.
The following composition title that the application occurs is the title of INCI (International Nomenclaure Cosmetic Ingredient, i.e. international cosmetic raw material name) defined: fine jade wax stearyl Fructus Canarii albi oils and fats/sorbitol Fructus Canarii albi oils and fats and sodium benzoate/potassium sorbate.
Advantage of the present invention is as follows:
Compared with prior art, cosmetic composition of the present invention can make Skin Cell have obvious inhibition to B-16 melanocyte activity, effectively resists ultraviolet, the beautiful coloured silk that makes that skin and muscles are fair; Separately, in the present invention, use natural botanical extraction liquid to use as antiseptic, and reached good effect.
Detailed description of the invention
Below in conjunction with specific embodiment, present techniques scheme is described further.
Embodiment 1
The preparation of plant extraction liquid
It is in 50% ethanol that dry Fructus Tsaoko is joined to mass ratio, reflux and dipping under extract 2.5h, extract 3 times; Subsequently, extracting solution is filtered with filter cloth, obtain filtrate.Mix the filtrate of 3 times and be concentrated into dry Fructus Tsaoko extracting solution.
It is in 50% ethanol that dry Pericarpium Granati is joined to mass ratio, reflux and dipping under extract 1.5h, extract 2 times; Subsequently, extracting solution is filtered with filter cloth, obtain filtrate.Mix the filtrate of 2 times and be concentrated into dry Pericarpium Granati extracting solution.
It is in 50% ethanol that dry plant Radix Vladimiriae is joined to mass ratio, reflux and dipping under extract 2h, extract 2 times; Subsequently, extracting solution is filtered with filter cloth, obtain filtrate.Mix filtrate repeatedly and be concentrated into dry Radix Vladimiriae extracting solution.
Embodiment 2
The preparation of cosmetic composition
One, the formula of cosmetic composition
The cosmetic combinations composition formula of experimental example 1～3 and comparative example 1～3 is in table 1.
Table 1
The cosmetic combinations composition formula of experimental example 4～6 and comparative example 4～6 is in table 2.
Table 2
The cosmetic combinations composition formula of experimental example 7～12 is in table 3.
Table 3
The cosmetic combinations composition formula of experimental example 13～18 is in table 4.
Table 4
Two, the preparation of cosmetic composition
The cosmetic composition of above-mentioned experimental example 1-18 and comparative example 1-6 makes by following preparation method:
(1) first use the glycerol in wetting agent scattered thickening agent, add emulsifying pot, then add wetting agent, skinfeel regulator, the emulsifying agent of plant extraction liquid, remainder, be heated to 80 DEG C, insulated and stirred 15 minutes, stir speed (S.S.) is 30rpm, then homogenizing 3 minutes, stir speed (S.S.) is 3000rpm, cools, and obtains A phase;
(2) by complete pH adjusting agent mixed dissolution, obtain B phase;
(3) A of step (1) is cooled to 70 DEG C mutually, adds the B phase in step (2), stir, continue cooling;
(4) when the temperature in step (3) near 40 DEG C, add antiseptic, stir, cosmetic composition.
Embodiment 3
The effect experiment of sun-proof whitening function
The cosmetic composition that experimental example 1～6 in above-mentioned table 1 and table 2 and comparative example 1～6 are made, through 100 personnel of 20～55 years old 30 days on probation continuously, the sun-proof whitening effect of prepared cosmetic composition in the various embodiments described above was evaluated in relative analysis respectively.Wherein, described sun-proof whitening effect is antitan agent, jaundice, low and deep, coarse etc. improvement situation, the results are shown in Table 5.
Table 5
The cosmetic composition of above-mentioned experimental example 1-12 and comparative example 1-6 is not all found zest and allergic phenomena in process on probation.
As known from Table 5: in experimental example, each cosmetic composition is obviously high than the improvement degree of each product in matched group to the improvement degree of antitan agent, jaundice, dimness, mottle etc.; And the weight portion of Fructus Tsaoko extracting solution and Pericarpium Granati extracting solution is larger, improvement degree is higher, and the weight portion of Pericarpium Granati extracting solution is 5～10 o'clock, and the cost performance of cosmetic composition is the highest.
Embodiment 4
Anti-corrosive properties test
The protective system efficiency evaluation method that this experiment is recommended with reference to U.S.'s cosmetics, toilet articles and essence association (CTFA), the anticorrosion single challenge experiment of classical 28 days by a definite date of recommending with CTFA.
1. challenge microorganism: antibacterial and mycete
2. mode and the quantity of inoculation
(1) mode of inoculation: adopt combined inoculation.Because natural microorganism has mixed raw feature of living together, so the situation of the realistic pollution of combined inoculation.
(2) quantity of inoculation: each strain is inoculated in suitable culture medium, cultivates in 37 DEG C (antibacterials) and 28 DEG C of (mycete) incubators.Antibacterial culturing 48 hours, mycotic culture, after 72 hours, is selected typical bacterium colony and in the fluid medium of sterilizing, is made certain density antibacterial and mycete mixing suspension, is placed in refrigerator cold-storage for subsequent use.Antibacterial: every gram of suspension bacteria containing amount is 1 × 10
6cFU/g or CFU/ml; Mycete is that every gram of suspension bacteria containing amount is 1 × 10
5cFU/g or CFU/ml.
3. Microbial Challenge experiment
Take each 100 grams of experimental example 13～18 cosmetic samples, add in the container of sterilizing, add mixed cell and mould bacteria suspension, fully mix.Every gram of sample is 1 × 10 containing amount of bacteria
6cFU/g or CFU/ml; Be 1 × 10 containing mycete amount
5cFU/g or CFU/ml.Then be placed at 28 DEG C.Connecing 0,7,14,21,28 day sample analysis of bacterium: accurately take 10 grams of samples, be added in the conical flask that contains glass pellet and 90ml sterile saline, fully concussion mixes, and this suspension is 1:10 diluent, and then dilutes successively by 1:10 with normal saline.At 37 DEG C, antibacterial, cultivate 48 hours; At 28 DEG C, mycete, cultivate 72 hours, by bacteria containing amount in dull and stereotyped tilt-pour process counting sample.
4. evaluation methodology
In 28 days samples, contain antibacterial or mycete at 10CFU/g～100CFU/g (CFU/ml), but the protective system that shows this sample has the stronger effect of killing to microorganism, test by challenge, below within the 7th day, dropping to 1000CFU/g (CFU/m1), be considered as passing through, other is considered as not passing through.
5. experimental result
Inoculation 0,7,14,2l and 28 days sampling detects, the anticorrosion test result of experimental example 13～18 cosmetic combinations matter sample is in table 6.
Table 6
As known from Table 6: in experimental example, each cosmetic composition has certain antiseptic effect; The weight portion of Radix Vladimiriae extracting solution is larger, and antiseptic effect is more obvious; Show that Radix Vladimiriae extracting solution has good antisepsis.In the time that the weight portion of Radix Vladimiriae extracting solution is 1～2, the antisepsis of Radix Vladimiriae extracting solution is better, and cost performance is the highest.
The above embodiment has only expressed several embodiment of the present invention, and it describes comparatively concrete and detailed, but can not therefore be interpreted as the restriction to the scope of the claims of the present invention.It should be pointed out that for the person of ordinary skill of the art, without departing from the inventive concept of the premise, can also make some distortion and improvement, these all belong to protection scope of the present invention.Therefore, the protection domain of patent of the present invention should be as the criterion with claims.
Claims (10)
1. a cosmetic composition, is characterized in that, by weight, comprises following component:
Wherein, described plant extraction liquid is the mixing of Fructus Tsaoko extracting solution and Pericarpium Granati extracting solution, and antiseptic comprises Radix Vladimiriae extracting solution.
2. cosmetic composition according to claim 1, is characterized in that, described plant extraction liquid is that weight part ratio is (1～10): the Fructus Tsaoko extracting solution of (1～10) and the mixing of Pericarpium Granati extracting solution.
3. cosmetic composition according to claim 2, is characterized in that, the weight part ratio of described Fructus Tsaoko extracting solution and Pericarpium Granati extracting solution is (5～8): (5～10).
4. according to cosmetic composition described in claim 1-3 any one, it is characterized in that described wetting agent is that weight part ratio is (0.1～1): the trehalose of (2～10), the mixing of glycerol.
5. according to cosmetic composition described in claim 1-3 any one, it is characterized in that, described thickening agent is that weight part ratio is (0.1～0.2): the transparent HANSHENGJIAO of (0.1～0.2) and the mixing of carbomer.
6. according to cosmetic composition described in claim 1-3 any one, it is characterized in that, described emulsifying agent is fine jade wax stearyl Fructus Canarii albi oils and fats/sorbitol Fructus Canarii albi oils and fats.
7. according to cosmetic composition described in claim 1-3 any one, it is characterized in that, described pH adjusting agent is that mass parts ratio is (0.005～0.08): the sodium hydroxide of (0.05～0.8) and the mixing of water.
8. according to cosmetic composition described in claim 1-3 any one, it is characterized in that, described antiseptic is that weight part ratio is (0.3～1): the mixing of the sodium benzoate/potassium sorbate of (0.5～3) and Radix Vladimiriae extracting solution.
9. cosmetic composition according to claim 7, is characterized in that, the weight portion of described Radix Vladimiriae extracting solution is 1～2 part.
10. a preparation method for cosmetic composition described in claim 1-8 any one, is characterized in that, comprises the following steps:
(1) first use the glycerol in wetting agent scattered thickening agent, add emulsifying pot, then add wetting agent, skinfeel regulator, the emulsifying agent of plant extraction liquid, remainder, be heated to 75～85 DEG C, insulated and stirred 10～20 minutes, stir speed (S.S.) is 20～40rpm, then homogenizing 2～5 minutes, stir speed (S.S.) is 2000～4000rpm, cools, and obtains A phase;
(2) by complete pH adjusting agent mixed dissolution, obtain B phase;
(3) A of step (1) is cooled to 65～70 DEG C mutually, adds the B phase in step (2), stir, continue cooling;
(4) when the temperature in step (3) near 40～45 DEG C, add antiseptic, stir, cosmetic composition.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108653142A (en) * | 2018-07-01 | 2018-10-16 | 佛山文森特知识产权服务有限公司 | A kind of moisture-keeping composition |
| CN112569139A (en) * | 2021-02-05 | 2021-03-30 | 东晟源研究院(广州)有限公司 | Soothing gel containing anti-inflammatory repairing composition and preparation method thereof |
| CN114588093A (en) * | 2021-12-27 | 2022-06-07 | 华南农业大学 | Application of amomum tsao-ko in preparing shampoo |
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| CN103462873A (en) * | 2013-09-26 | 2013-12-25 | 广州丹奇日用化工厂有限公司 | Skin care product with functions of maintaining beauty and keeping young and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108653142A (en) * | 2018-07-01 | 2018-10-16 | 佛山文森特知识产权服务有限公司 | A kind of moisture-keeping composition |
| CN112569139A (en) * | 2021-02-05 | 2021-03-30 | 东晟源研究院(广州)有限公司 | Soothing gel containing anti-inflammatory repairing composition and preparation method thereof |
| CN114588093A (en) * | 2021-12-27 | 2022-06-07 | 华南农业大学 | Application of amomum tsao-ko in preparing shampoo |
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Application publication date: 20141029 |