CN104107154A - Cosmetic composition and preparation method thereof - Google Patents
Cosmetic composition and preparation method thereof Download PDFInfo
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- CN104107154A CN104107154A CN201410370153.5A CN201410370153A CN104107154A CN 104107154 A CN104107154 A CN 104107154A CN 201410370153 A CN201410370153 A CN 201410370153A CN 104107154 A CN104107154 A CN 104107154A
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- alpiniae officinarum
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Abstract
The invention discloses a cosmetic composition. The cosmetic composition contains the following ingredients in parts by weight: 5-25 parts of humectant, 0.2-0.4 part of thickener, 0.1-0.5 part of emulsifier, 0.1-2 parts of silica, 0.03-0.07 part of potassium hydroxide, 0.055-0.88 part of pH regulator, 0.8-4 parts of preservative and 60-90 parts of water, wherein the humectant contains a galangal extract solution and a hairy-vein agrimony extract solution, and the preservative contains a tarragon extract solution. According to the cosmetic composition, a mixed solution of the galangal extract solution and the hairy-vein agrimony extract solution is applied to the cosmetic composition, so that the cosmetic composition is used for effectively increasing the moisture of skin and improving the moisture degree of the skin.
Description
Technical field
The present invention relates to cosmetic field, particularly relate to a kind of cosmetic composition with moisture-keeping efficacy and preparation method thereof.
Background technology
Cosmetics are to smear, spray or other similar methods, impose on any position of human body surface (skin, fingernail, lip, the ripe film in oral cavity etc.), with the product that reaches clean, eliminates bad smell, skin protection, beauty treatment and modification object.
When air humidity reduces, keratodermatitis can not regulate enough Moisture factor in time, and the ability of enlivening of oils and fats gland is also reducing, and oils and fats on the face just can reduce, so skin just easily tightens, now and the other microgroove that more there will be of nose.Will how to make fast so skin moisturize, strengthen skin wettability, this will be an important problem.
Along with the development of cosmetics industry, natural plants series products due to use safety, action temperature and, the advantage such as successful welcome.Be generally to obtain by corresponding processing the plant extract that contains effective ingredient, and add in cosmetics.
At present, cosmetics moistening effect is on the market not obvious, and very easily causes allergic phenomena.Therefore, selecting which kind of plant, and being applied to of its safety reached to better moistening effect in cosmetics, and can make skin absorb fast the nutritional labeling in cosmetics, is problem demanding prompt solution.
Summary of the invention
Based on this, the object of the present invention is to provide a kind of cosmetic composition.
Concrete technical scheme is as follows:
A cosmetic composition, by weight, comprises following component:
Wherein, above-mentioned wetting agent comprises Rhizoma Alpiniae Officinarum extracting solution and Herba Agrimoniae extracting solution, and antiseptic comprises Artemisia dracunculus extracting solution.
In an embodiment, described wetting agent is that weight part ratio is (0.1～1): (2～10): (1～10): the mixing of the trehalose of (1～10), glycerol, Rhizoma Alpiniae Officinarum extracting solution and Herba Agrimoniae extracting solution therein.
In an embodiment, the weight part ratio of described Rhizoma Alpiniae Officinarum extracting solution and Herba Agrimoniae extracting solution is (5～8): (5～10) therein.
In an embodiment, described thickening agent is that weight part ratio is (0.1～0.2): the transparent HANSHENGJIAO of (0.1～0.2) and the mixing of carbomer therein.
In an embodiment, described emulsifying agent is fine jade wax stearyl Fructus Canarii albi oils and fats/sorbitol Fructus Canarii albi oils and fats therein.
In an embodiment, described pH adjusting agent is that mass parts ratio is (0.005～0.08): the sodium hydroxide of (0.05～0.8) and the mixing of water therein.
In an embodiment, described antiseptic is that weight part ratio is (0.3～1): the mixing of the sodium benzoate/potassium sorbate of (0.5～3) and Artemisia dracunculus extracting solution therein.
In an embodiment, the weight portion of described Artemisia dracunculus extracting solution is 1～2 part therein.
Rhizoma Alpiniae Officinarum extracting solution of the present invention, Herba Agrimoniae extracting solution and Artemisia dracunculus extracting solution can be prepared by conventional alcohol extracting method, preferred following extracting method: it is in 50% ethanol that dry plant (Artemisia dracunculus, Herba Agrimoniae, Rhizoma Alpiniae Officinarum) is joined to mass ratio, under backflow and dipping, extract 1～3h, extract 1～3 time; Subsequently, with filter cloth, extracting solution is filtered, obtain filtrate.Mix the filtrate of 1～3 time and be concentrated into dry plant (Artemisia dracunculus, Herba Agrimoniae, Rhizoma Alpiniae Officinarum) extracting solution.
The preparation method of above-mentioned cosmetic composition, comprises the following steps:
(1) first use the glycerol in wetting agent scattered thickening agent, add emulsifying pot, then add remaining wetting agent, skinfeel regulator, emulsifying agent, be heated to 75～85 ℃, insulated and stirred 10～20 minutes, stir speed (S.S.) is 20～40rpm, then homogenizing is 2～5 minutes, stir speed (S.S.) is 2000～4000rpm, cools, and obtains A phase;
(2) pH adjusting agent mixed dissolution is complete, obtain B phase;
(3) A of step (1) is cooled to 65～70 ℃ mutually, adds the B phase in step (2), stir, continue cooling;
(4) temperature in step (3) is near 40～45 ℃, adds antiseptic, stir, cosmetic composition.
Rhizoma Alpiniae Officinarum is the dry rhizome of Zingiberaceae Alpinia plants Rhizoma Alpiniae Officinarum, another name Rhizoma Alpiniae Officinarum, little Rhizoma Alpiniae Officinarum etc., as Chinese medicine, go through an edition < < Chinese Pharmacopoeia > > and all record, main product in Fujian, the ground such as Taiwan, Guangdong, Guangxi, Hainan, Yunnan.Rhizoma Alpiniae Officinarum extracting solution has promotion osmosis, when dermal administration, can make very soon skin temperature rise.And the rising of skin temperature can make cutaneous vasodilation, blood flow rate increase, accelerate to have penetrated in-house material disperse, thereby skin absorbability is improved, can make nutrient substance in cosmetic composition of the present invention sooner, be more effectively absorbed by the skin.Wherein, Rhizoma Alpiniae Officinarum extracting solution itself has good moisture-retaining capacity, and glycerol, trehalose and the Herba Agrimoniae extracting solution with cosmetic composition of the present invention with moisture-keeping efficacy are combined, and by the moisture of faster and better increase skin, keeps the wettability of skin.
Herba Agrimoniae is the dry aerial parts of Rosaceae herbaceos perennial Radix Agrimoniae, another name Herba silenes fortunei, Herba Verbenae, Radix Agrimoniae, Herba Salviae Chinensis etc.Herba Agrimoniae all has distribution in most of China area, main product in Zhejiang, the ground such as Jiangsu, Hubei, Heilungkiang.Herba Agrimoniae extracting solution has good inhibitory action to hyaluronidase, and the raising of hyaluronidase activity will be decomposed hyaluronic acid, and reduces the moisture holding capacity of skin, to the inhibition ability of hyaluronidase, is therefore maintaining skin moisture-keeping ability.
The Silicon stone adding in cosmetic composition of the present invention is that skinfeel regulator can make people be combined and improve skin condition with physiology from psychology, increases moisture of skin; The effect of pH adjusting agent is that cosmetic composition of the present invention is had the good acid-base value of skin effect.
Artemisia dracunculus is called narrow leaf Artemisia annua L., Serpentis punt-pole, green pepper punt-pole, for Compositae dragon punt-pole belongs to perennial fruticuli herbaceous plant, has drought-resistant, Salt And Alkali Tolerance, the characteristic such as cold-resistant and barren-resistant.Long Gao China is distributed more widely, and all there is distribution national most areas, especially more with the north and the northwestward.Dragon punt-pole extracting solution has very strong fungistatic effect, can suppress the growth of staphylococcus, streptococcus, the pungent bacterium of Yale and false pseudomonas bacillus.As antiseptic, use in the present invention.But antibacterial is killed in the prevention that act as of antiseptic, and protection product is avoided microbial contamination, extends the product shelf phase; Prevent that consumer's use is subject to the product of microbial contamination and causes possible infection, guarantees safety.
The following composition title that the application occurs is the title of INCI (International Nomenclaure Cosmetic Ingredient, i.e. international cosmetic raw material name) defined: fine jade wax stearyl Fructus Canarii albi oils and fats/sorbitol Fructus Canarii albi oils and fats and sodium benzoate/potassium sorbate.
Advantage of the present invention is as follows:
Compared with prior art, cosmetic composition of the present invention can make skin absorb more quickly and effectively nutritional labeling, increases moisture of skin, keeps skin wettability; Separately, in the present invention, use natural botanical extraction liquid to use as antiseptic, and reached good effect.
The specific embodiment
Below in conjunction with specific embodiment, present techniques scheme is described further.
Embodiment 1
The preparation of plant extraction liquid
It is in 50% ethanol that dry Rhizoma Alpiniae Officinarum is joined to mass ratio, reflux and dipping under extract 2.5h, extract 3 times; Subsequently, with filter cloth, extracting solution is filtered, obtain filtrate.Mix the filtrate of 3 times and be concentrated into dry Rhizoma Alpiniae Officinarum extracting solution.
It is in 50% ethanol that dry Herba Agrimoniae is joined to mass ratio, reflux and dipping under extract 1.5h, extract 2 times; Subsequently, with filter cloth, extracting solution is filtered, obtain filtrate.Mix the filtrate of 2 times and be concentrated into dry Herba Agrimoniae extracting solution.
It is in 50% ethanol that dry plant of tarragon is joined to mass ratio, reflux and dipping under extract 2h, extract 2 times; Subsequently, with filter cloth, extracting solution is filtered, obtain filtrate.Mix filtrate repeatedly and be concentrated into dry Artemisia dracunculus extracting solution.
Embodiment 2
The preparation of cosmetic composition
One, the formula of cosmetic composition
The cosmetic combinations composition formula of experimental example 1～3 and comparative example 1～3 is in Table 1.
Table 1
The cosmetic combinations composition formula of experimental example 4～6 and comparative example 4～6 is in Table 2.
Table 2
The cosmetic combinations composition formula of experimental example 7～12 is in Table 3.
Table 3
The cosmetic combinations composition formula of experimental example 13～18 is in Table 4.
Table 4
Two, the preparation of cosmetic composition
The cosmetic composition of above-mentioned experimental example 1-18 and comparative example 1-6 makes by following preparation method:
(1) first use the glycerol in wetting agent scattered thickening agent, add emulsifying pot, then add remaining wetting agent, skinfeel regulator, emulsifying agent, be heated to 80 ℃, insulated and stirred 15 minutes, stir speed (S.S.) is 30rpm, then homogenizing is 3 minutes, stir speed (S.S.) is 3000rpm, cools, and obtains A phase;
(2) pH adjusting agent mixed dissolution is complete, obtain B phase;
(3) A of step (1) is cooled to 70 ℃ mutually, adds the B phase in step (2), stir, continue cooling;
(4) temperature in step (3) is near 40 ℃, adds antiseptic, stir, cosmetic composition.
Embodiment 3
The effect experiment of moisture-keeping function
The cosmetic composition that experimental example 1～6 in above-mentioned table 1 and table 2 and comparative example 1～6 are made, through 100 personnel of 20～55 years old 30 days on probation continuously, the moistening effect of prepared cosmetic composition in above-mentioned each experimental example was evaluated in relative analysis respectively.Wherein, described moistening effect is xerosis cutis, jaundice, dimness, lax etc. improvement situation, the results are shown in Table 5.
Table 5
The cosmetic composition of above-mentioned experimental example 1-6 and comparative example 1-6 is not all found zest and allergic phenomena in process on probation.
As known from Table 5: in experimental example, each cosmetic composition is obviously high than the improvement degree of each product in matched group to xerosis cutis, jaundice, dimness, lax etc. improvement degree; And the weight portion of Rhizoma Alpiniae Officinarum extracting solution and Herba Agrimoniae extracting solution is larger, improvement degree is higher, and the weight portion of Herba Agrimoniae extracting solution is 5～10 o'clock, and the cost performance of cosmetic composition is the highest.
Embodiment 4
Promote chemosmotic effect experiment
By the cosmetic composition that in above-mentioned table 3, experimental example 7～12 makes, on probation through 100 personnel of 20～35 respectively.In the on probation obvious number of moistening effect that records respectively for 0,7,14,21,28 day.The results are shown in Table 6.
Table 6
The obvious number of moistening effect
The cosmetic composition of above-mentioned experimental example 7～12 is not all found zest and allergic phenomena in process on probation.
As known from Table 6: in experimental example, each cosmetic composition has certain moistening effect; The weight portion of Rhizoma Alpiniae Officinarum extracting solution is larger, and moistening effect is more obvious; Show that Rhizoma Alpiniae Officinarum extracting solution has good urging to ooze effect, make skin absorb fast nutritional labeling, reach good moisturizing degree.When the weight portion of Rhizoma Alpiniae Officinarum extracting solution is 5～8, the short effect of oozing of Rhizoma Alpiniae Officinarum extracting solution is better, and cost performance is the highest.
Embodiment 5
Anti-corrosive properties test
The protective system efficiency evaluation method that this experiment is recommended with reference to U.S.'s cosmetics, toilet articles and essence association (CTFA), the anticorrosion single challenge experiment of classical 28 days by a definite date of recommending with CTFA.
1. challenge microorganism: antibacterial and mycete
2. mode and the quantity inoculated
(1) mode of inoculation: adopt combined inoculation.Because natural microorganism has mixed raw feature of living together, so the situation of the realistic pollution of combined inoculation.
(2) quantity of inoculation: each strain is inoculated in suitable culture medium, cultivates in 37 ℃ (antibacterials) and 28 ℃ of (mycete) incubators.Antibacterial culturing 48 hours, mycotic culture, after 72 hours, is selected typical bacterium colony and in the fluid medium of sterilizing, is made certain density antibacterial and mycete mixing suspension, is placed in refrigerator cold-storage standby.Antibacterial: every gram of suspension bacteria containing amount is 1 * 10
6cFU/g or CFU/ml; Mycete is that every gram of suspension bacteria containing amount is 1 * 10
5cFU/g or CFU/ml.
3. Microbial Challenge experiment
Take each 100 grams of experimental example 13～18 cosmetic samples, add in the container of sterilizing, add mixed cell and mould bacteria suspension, fully mix.Every gram of sample is 1 * 10 containing amount of bacteria
6cFU/g or CFU/ml; Containing mycete amount, be 1 * 10
5cFU/g or CFU/ml.Then be placed at 28 ℃.Connecing 0,7,14,21,28 day sample analysis of bacterium: accurately take 10 grams of samples, be added in the conical flask that contains glass pellet and 90ml sterile saline, fully concussion mixes, and this suspension is 1:10 diluent, and then dilutes successively by 1:10 with normal saline.At 37 ℃, antibacterial, cultivate 48 hours; At 28 ℃, mycete, cultivate 72 hours, by bacteria containing amount in dull and stereotyped tilt-pour process counting sample.
4. evaluation methodology
In 28 days samples, contain antibacterial or mycete at 10CFU/g～100CFU/g (CFU/ml), but the protective system that shows this sample has the stronger effect of killing to microorganism, by challenge, test, at the 7th day, drop to below 1000CFU/g (CFU/m1), be considered as by, other is considered as not passing through.
5. experimental result
Inoculation 0,7,14,2l and 28 days sampling detects, the anticorrosion test result of experimental example 13～18 cosmetic combinations matter sample is in Table 7.
Table 7
As known from Table 7: in experimental example, each cosmetic composition has certain antiseptic effect; The weight portion of Artemisia dracunculus extracting solution is larger, and antiseptic effect is more obvious; Show that Artemisia dracunculus extracting solution has good antisepsis.When the weight portion of Artemisia dracunculus extracting solution is 1～2, the antisepsis of Artemisia dracunculus extracting solution is better, and cost performance is the highest.
The above embodiment has only expressed several embodiment of the present invention, and it describes comparatively concrete and detailed, but can not therefore be interpreted as the restriction to the scope of the claims of the present invention.It should be pointed out that for the person of ordinary skill of the art, without departing from the inventive concept of the premise, can also make some distortion and improvement, these all belong to protection scope of the present invention.Therefore, the protection domain of patent of the present invention should be as the criterion with claims.
Claims (9)
1. a cosmetic composition, is characterized in that, by weight, comprises following component:
Wherein, described wetting agent comprises Rhizoma Alpiniae Officinarum extracting solution and Herba Agrimoniae extracting solution, and antiseptic comprises Artemisia dracunculus extracting solution.
2. cosmetic composition according to claim 1, it is characterized in that, described wetting agent is that weight part ratio is (0.1～1): (2～10): (1～10): the mixing of the trehalose of (1～10), glycerol, Rhizoma Alpiniae Officinarum extracting solution and Herba Agrimoniae extracting solution.
3. cosmetic composition according to claim 2, is characterized in that, the weight part ratio of described Rhizoma Alpiniae Officinarum extracting solution and Herba Agrimoniae extracting solution is (5～8): (5～10).
4. according to cosmetic composition described in claim 1-3 any one, it is characterized in that, described thickening agent is that weight part ratio is (0.1～0.2): the transparent HANSHENGJIAO of (0.1～0.2) and the mixing of carbomer.
5. according to cosmetic composition described in claim 1-3 any one, it is characterized in that, described emulsifying agent is fine jade wax stearyl Fructus Canarii albi oils and fats/sorbitol Fructus Canarii albi oils and fats.
6. according to cosmetic composition described in claim 1-3 any one, it is characterized in that, described pH adjusting agent is that mass parts ratio is (0.005～0.08): the sodium hydroxide of (0.05～0.8) and the mixing of water.
7. according to cosmetic composition described in claim 1-3 any one, it is characterized in that, described antiseptic is that weight part ratio is (0.3～1): the mixing of the sodium benzoate/potassium sorbate of (0.5～3) and Artemisia dracunculus extracting solution.
8. cosmetic composition according to claim 7, is characterized in that, the weight portion of described Artemisia dracunculus extracting solution is 1～2 part.
9. a preparation method for cosmetic composition described in claim 1-8 any one, is characterized in that, comprises the following steps:
(1) first use the glycerol in wetting agent scattered thickening agent, add emulsifying pot, then add remaining wetting agent, skinfeel regulator, emulsifying agent, be heated to 75～85 ℃, insulated and stirred 10～20 minutes, stir speed (S.S.) is 20～40rpm, then homogenizing is 2～5 minutes, stir speed (S.S.) is 2000～4000rpm, cools, and obtains A phase;
(2) pH adjusting agent mixed dissolution is complete, obtain B phase;
(3) A of step (1) is cooled to 65～70 ℃ mutually, adds the B phase in step (2), stir, continue cooling;
(4) temperature in step (3) is near 40～45 ℃, adds antiseptic, stir, cosmetic composition.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104434628A (en) * | 2014-11-11 | 2015-03-25 | 广东幸美化妆品股份有限公司 | Moisture cream membrane capable of continuously moisturizing for 48 hours, and preparation method of moisture cream membrane |
| CN104523481A (en) * | 2014-12-10 | 2015-04-22 | 常州诺瑞格纳米科技有限公司 | Skin rejuvenation and itching relieving skin care product |
| CN106580777A (en) * | 2016-12-12 | 2017-04-26 | 广州环亚化妆品科技有限公司 | Natural Chinese herbal medicine antibiosis composition, and preparation method and application thereof |
| CN111304281A (en) * | 2020-03-31 | 2020-06-19 | 广州立白企业集团有限公司 | Evaluation method of corrosion resistance |
| CN114025740A (en) * | 2019-05-07 | 2022-02-08 | 皮埃尔·法布尔皮肤化妆品公司 | Agrimonia pilosa extract as anti-fouling agent |
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| CN103565673A (en) * | 2013-10-30 | 2014-02-12 | 广州品赫化妆品有限公司 | Emollient lotion for moisturizing skin and controlling oil and preparation method of emollient lotion |
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2014
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Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103565673A (en) * | 2013-10-30 | 2014-02-12 | 广州品赫化妆品有限公司 | Emollient lotion for moisturizing skin and controlling oil and preparation method of emollient lotion |
Non-Patent Citations (2)
| Title |
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| 王建新: "《化妆品植物原料大全》", 30 June 2012, article "高良姜", pages: 112-113,394-395 * |
| 王建新: "《化妆品植物原料手册》", 30 June 2009, article "《仙鹤草》", pages: 301-303 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104434628A (en) * | 2014-11-11 | 2015-03-25 | 广东幸美化妆品股份有限公司 | Moisture cream membrane capable of continuously moisturizing for 48 hours, and preparation method of moisture cream membrane |
| CN104523481A (en) * | 2014-12-10 | 2015-04-22 | 常州诺瑞格纳米科技有限公司 | Skin rejuvenation and itching relieving skin care product |
| CN106580777A (en) * | 2016-12-12 | 2017-04-26 | 广州环亚化妆品科技有限公司 | Natural Chinese herbal medicine antibiosis composition, and preparation method and application thereof |
| CN114025740A (en) * | 2019-05-07 | 2022-02-08 | 皮埃尔·法布尔皮肤化妆品公司 | Agrimonia pilosa extract as anti-fouling agent |
| CN111304281A (en) * | 2020-03-31 | 2020-06-19 | 广州立白企业集团有限公司 | Evaluation method of corrosion resistance |
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