CN104173230A - Cosmetic composition and preparation method thereof - Google Patents

Cosmetic composition and preparation method thereof Download PDF

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Publication number
CN104173230A
CN104173230A CN201410370969.8A CN201410370969A CN104173230A CN 104173230 A CN104173230 A CN 104173230A CN 201410370969 A CN201410370969 A CN 201410370969A CN 104173230 A CN104173230 A CN 104173230A
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China
Prior art keywords
extracting solution
cosmetic composition
mixing
agent
radix
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不公告发明人
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Guangzhou Danqi Daily Chemical Co Ltd
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Guangzhou Danqi Daily Chemical Co Ltd
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Priority to CN201410370969.8A priority Critical patent/CN104173230A/en
Publication of CN104173230A publication Critical patent/CN104173230A/en
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Abstract

The invention discloses a cosmetic composition and a preparation method thereof. The cosmetic composition comprises the following components in parts by weight: 2-20 parts of plant extracting solution, 3-11 parts of wetting agent, 0.2-0.4 part of thickening agent, 0.1-0.5 part of emulsifier, 0.1-2 parts of silica, 0.03-0.07 part of potassium hydroxide, 0.055-0.88 part of pH regulator, 0.8-4 parts of preservative and 60-90 parts of water, wherein the plant extracting solution comprises a rosa multiflora extracting solution and a rheum palmatum extracting solution; and the preservative comprises a rhizoma nardostachyos extracting solution. According to the invention, the mixed solution of the rosa multiflora extracting solution and the rheum palmatum extracting solution is applied to the cosmetic composition, so that the intensity of blood vessels is effectively enhanced and red blood silk of skin is prevented.

Description

A kind of cosmetic composition and preparation method thereof
Technical field
The present invention relates to cosmetic field, particularly relate to a kind of cosmetic composition that prevents red blood streak and preparation method thereof.
Background technology
Cosmetics are to smear, spray or other similar methods, impose on any position of human body surface (skin, fingernail, lip, the ripe film in oral cavity etc.), with the product that reaches clean, eliminates bad smell, skin protection, beauty treatment and modification object.
Telangiectasis claims again red blood streak, is the telangiectasis that is distributed in two cheeks.The initial stage of skin sensitivity face red, itch, swollen, can clearly see the red blood streak of a rule in skin outside.The reason producing, the one, local life-time service corticoid medicine, causes telangiectasis, causes thinning of skin, atrophy etc.; The 2nd, inhabitation extremely frigid zones or be subject to cold injury, causes blood circulation to be obstructed, and blood vessel wall is retarded by silt and is made face present a rule red blood streak; The 3rd, change after skin through beauty treatment, due to long-term top rake matter, make the skin corium not being protected be exposed to outside, accept due to the irradiation of intense UV rays; The 4th, the general many horny layer of sensitive skin are thin, and their sunlight to external world, medicinal herbs, cosmetics, temperature (cold and hot) etc. are all more responsive, and pine when tight while causing not tip blood vessel, presents congestion state repeatedly, causes the roundabout expansion of blood vessel, forms red blood streak.
Along with the development of cosmetics industry, natural plants series products due to use safety, action temperature and, the advantage such as successful welcome.Be generally to obtain by corresponding processing the plant extract that contains effective ingredient, and add in cosmetics.
At present, the DeGrain of cosmetics prevention skin red blood streak on the market, and very easily cause allergic phenomena.Therefore, select which kind of plant, and by the effect that reaches prevention skin red blood streak in cosmetics that is applied to of its safety, be problem demanding prompt solution.
Summary of the invention
Based on this, the object of the present invention is to provide a kind of cosmetic composition.
Concrete technical scheme is as follows:
A kind of cosmetic composition, by weight, comprises following component:
Wherein, above-mentioned wetting agent comprises Flos Rosae Multiflorae extracting solution and sorrel extracting solution, and antiseptic comprises Radix Et Rhizoma Nardostachyos extracting solution.
In an embodiment, described plant extraction liquid is that weight part ratio is (1~10): the Flos Rosae Multiflorae extracting solution of (1~10) and the mixing of sorrel extracting solution therein.
In an embodiment, the weight part ratio of described Flos Rosae Multiflorae extracting solution and sorrel extracting solution is (5~8): (5~10) therein.
In an embodiment, described wetting agent is that weight part ratio is (0.1~1): the trehalose of (2~10), the mixing of glycerol therein.
In an embodiment, described thickening agent is that weight part ratio is (0.1~0.2): the transparent HANSHENGJIAO of (0.1~0.2) and the mixing of carbomer therein.
In an embodiment, described emulsifying agent is fine jade wax stearyl Fructus Canarii albi oils and fats/sorbitol Fructus Canarii albi oils and fats therein.
In an embodiment, described pH adjusting agent is that mass parts ratio is (0.005~0.08): the sodium hydroxide of (0.05~0.8) and the mixing of water therein.
In an embodiment, described antiseptic is that weight part ratio is (0.3~1): the mixing of the sodium benzoate/potassium sorbate of (0.5~3) and Radix Et Rhizoma Nardostachyos extracting solution therein.
In an embodiment, the weight portion of described Radix Et Rhizoma Nardostachyos extracting solution is 1~2 part therein.
Flos Rosae Multiflorae extracting solution of the present invention, sorrel extracting solution and Radix Et Rhizoma Nardostachyos extracting solution can be by conventional alcohol extracting method preparations, preferably following extracting method: it is in 50% ethanol that dry plant (Radix Et Rhizoma Nardostachyos, sorrel, Flos Rosae Multiflorae) is joined to mass ratio, under backflow and dipping, extract 1~3h, extract 1~3 time; Subsequently, extracting solution is filtered with filter cloth, obtain filtrate.Mix the filtrate of 1~3 time and be concentrated into dry plant (Radix Et Rhizoma Nardostachyos, sorrel, Flos Rosae Multiflorae) extracting solution.
The preparation method of above-mentioned cosmetic composition, comprises the following steps:
(1) first use the glycerol in wetting agent scattered thickening agent, add emulsifying pot, then add wetting agent, skinfeel regulator, the emulsifying agent of plant extraction liquid, remainder, be heated to 75~85 DEG C, insulated and stirred 10~20 minutes, stir speed (S.S.) is 20~40rpm, then homogenizing 2~5 minutes, stir speed (S.S.) is 2000~4000rpm, cools, and obtains A phase;
(2) by complete pH adjusting agent mixed dissolution, obtain B phase;
(3) A of step (1) is cooled to 65~70 DEG C mutually, adds the B phase in step (2), stir, continue cooling;
(4) when the temperature in step (3) near 40~45 DEG C, add antiseptic, stir, cosmetic composition.
Flos Rosae Multiflorae is Rosaceae gul, has another name called Flos rosae multiflorae, Flos Nelumbinis Flos Rosae Multiflorae etc.The mutation of Flos Rosae Multiflorae is a lot, originates in various places, is born in wilderness, roadside, is distributed widely in China North China, East China, Central China, south China and southwest.Its leaf, root, stem, fruit and spend all can people's medicine, the present invention mainly uses its dry flower.Flos Rosae Multiflorae extract is proliferation activity to vascular endothelial cell, can strengthen the intensity of blood vessel, can prevent skin red blood streak.
Sorrel is polygonaceae plant, has another name called certain herbaceous plants with big flowers leaf Radix Et Rhizoma Rhei, Beijing University's Huang, pearl Mo Sa etc., is distributed in the provinces and regions such as Gansu, Sichuan, Qinghai, northwestern Yunnan Province and Eastern Tibet.Root and rhizome can be used as medicine, and autumn, winter excavate when stem and leaf is withered, remove residual stem and radicula, scrape off rough bark, and valve cutting or section, dry or dry for subsequent use.Its equal plant Rheum officinale is similar with composition to the performance of sorrel with Rheum tanguticum, between them, also often uses mutually.But about medicinal research and the application of sorrel are greater than the latter two, what the present invention adopted is their dry root and rhizomes.Sorrel extract, to the good proliferation function of vascular endothelial cell, can solidify blood capillary, thereby reduces the generation of red blood streak.
The Silicon stone adding in cosmetic composition of the present invention is that skinfeel regulator can make people be combined and improve skin condition with physiology from psychology, increases moisture of skin; The effect of pH adjusting agent is that cosmetic composition of the present invention is had the good acid-base value of skin effect.
Radix Et Rhizoma Nardostachyos is the dry root and rhizome of Valerianaceae plant Radix Et Rhizoma Nardostachyos, the lid area if be mainly distributed in Songpan, Nanping of Sichuan Abazangzuqiangzu Autonomous Prefecture, and oil mountain area, the river in Mianyang.Its equal plant jatamansi is similar to Radix Et Rhizoma Nardostachyos performance, and both can use mutually.Gather rhizome season in spring and autumn, taking autumn as good, dry.The present invention adopts its dry rhizome.Radix Et Rhizoma Nardostachyos extracting solution has the antibiotic property of wide spectrum, uses in the present invention as antiseptic.But antibacterial is killed in the prevention that act as of antiseptic, and protection product is avoided microbial contamination, extends the product shelf phase; Prevent that consumer's use is subject to the product of microbial contamination and causes possible infection, guarantees safety.
The following composition title that the application occurs is the title of INCI (International Nomenclaure Cosmetic Ingredient, i.e. international cosmetic raw material name) defined: fine jade wax stearyl Fructus Canarii albi oils and fats/sorbitol Fructus Canarii albi oils and fats and sodium benzoate/potassium sorbate.
Advantage of the present invention is as follows:
Compared with prior art, cosmetic composition of the present invention can strengthen blood vessel intensity, prevention skin red blood streak; Separately, in the present invention, use natural botanical extraction liquid to use as antiseptic, and reached good effect.
Detailed description of the invention
Below in conjunction with specific embodiment, present techniques scheme is described further.
Embodiment 1
The preparation of plant extraction liquid
It is in 50% ethanol that dry Flos Rosae Multiflorae is joined to mass ratio, reflux and dipping under extract 2.5h, extract 3 times; Subsequently, extracting solution is filtered with filter cloth, obtain filtrate.Mix the filtrate of 3 times and be concentrated into dry Flos Rosae Multiflorae extracting solution.
It is in 50% ethanol that dry sorrel is joined to mass ratio, reflux and dipping under extract 2h, extract 3 times; Subsequently, extracting solution is filtered with filter cloth, obtain filtrate.Mix the filtrate of 3 times and be concentrated into dry sorrel extracting solution.
It is in 50% ethanol that dry plant Radix Et Rhizoma Nardostachyos is joined to mass ratio, reflux and dipping under extract 1.5h, extract 2 times; Subsequently, extracting solution is filtered with filter cloth, obtain filtrate.Mix the filtrate of 2 times and be concentrated into dry Radix Et Rhizoma Nardostachyos extracting solution.
Embodiment 2
The preparation of cosmetic composition
One, the formula of cosmetic composition
The cosmetic combinations composition formula of experimental example 1~3 and comparative example 1~3 is in table 1.
Table 1
The cosmetic combinations composition formula of experimental example 4~6 and comparative example 4~6 is in table 2.
Table 2
The cosmetic combinations composition formula of experimental example 7~12 is in table 3.
Table 3
The cosmetic combinations composition formula of experimental example 13~18 is in table 4.
Table 4
Two, the preparation of cosmetic composition
The cosmetic composition of above-mentioned experimental example 1-18 and comparative example 1-6 makes by following preparation method:
(1) first use the glycerol in wetting agent scattered thickening agent, add emulsifying pot, then add wetting agent, skinfeel regulator, the emulsifying agent of plant extraction liquid, remainder, be heated to 80 DEG C, insulated and stirred 15 minutes, stir speed (S.S.) is 30rpm, then homogenizing 3 minutes, stir speed (S.S.) is 3000rpm, cools, and obtains A phase;
(2) by complete pH adjusting agent mixed dissolution, obtain B phase;
(3) A of step (1) is cooled to 70 DEG C mutually, adds the B phase in step (2), stir, continue cooling;
(4) when the temperature in step (3) near 40 DEG C, add antiseptic, stir, cosmetic composition.
Embodiment 3
Effect experiment
The cosmetic composition that experimental example 1~12 in above-mentioned table 1 and table 2 and comparative example 1~6 are made, try out 30 days continuously through 100 personnel of 20~55 years old respectively, the prevention red blood streak effect of prepared cosmetic composition in above-mentioned each experimental example is evaluated in relative analysis.Wherein, described effect is the improvement situation that pruritus, redness, red blood streak and skin are thin etc., the results are shown in Table 5.
Table 5
The cosmetic composition of above-mentioned experimental example 1-12 and comparative example 1-6 is not all found zest and allergic phenomena in process on probation.
As known from Table 5: in experimental example, each cosmetic composition is that the improvement degree that pruritus, redness, red blood streak and skin are thin etc. is obviously high than the improvement degree of each product in matched group; And the weight portion of Flos Rosae Multiflorae extracting solution and sorrel extracting solution is larger, improvement degree is higher; The weight portion of Flos Rosae Multiflorae extracting solution is 5~8, the weight portion of sorrel extracting solution is 5~10 o'clock, and the cost performance of cosmetic composition is the highest.
Embodiment 4
Anti-corrosive properties test
The protective system efficiency evaluation method that this experiment is recommended with reference to U.S.'s cosmetics, toilet articles and essence association (CTFA), the anticorrosion single challenge experiment of classical 28 days by a definite date of recommending with CTFA.
1. challenge microorganism: antibacterial and mycete
2. mode and the quantity of inoculation
(1) mode of inoculation: adopt combined inoculation.Because natural microorganism has mixed raw feature of living together, so the situation of the realistic pollution of combined inoculation.
(2) quantity of inoculation: each strain is inoculated in suitable culture medium, cultivates in 37 DEG C (antibacterials) and 28 DEG C of (mycete) incubators.Antibacterial culturing 48 hours, mycotic culture, after 72 hours, is selected typical bacterium colony and in the fluid medium of sterilizing, is made certain density antibacterial and mycete mixing suspension, is placed in refrigerator cold-storage for subsequent use.Antibacterial: every gram of suspension bacteria containing amount is 1 × 10 6cFU/g or CFU/ml; Mycete is that every gram of suspension bacteria containing amount is 1 × 10 5cFU/g or CFU/ml.
3. Microbial Challenge experiment
Take each 100 grams of experimental example 13~18 cosmetic samples, add in the container of sterilizing, add mixed cell and mould bacteria suspension, fully mix.Every gram of sample is 1 × 10 containing amount of bacteria 6cFU/g or CFU/ml; Be 1 × 10 containing mycete amount 5cFU/g or CFU/ml.Then be placed at 28 DEG C.Connecing 0,7,14,21,28 day sample analysis of bacterium: accurately take 10 grams of samples, be added in the conical flask that contains glass pellet and 90ml sterile saline, fully concussion mixes, and this suspension is 1:10 diluent, and then dilutes successively by 1:10 with normal saline.At 37 DEG C, antibacterial, cultivate 48 hours; At 28 DEG C, mycete, cultivate 72 hours, by bacteria containing amount in dull and stereotyped tilt-pour process counting sample.
4. evaluation methodology
In 28 days samples, contain antibacterial or mycete at 10CFU/g~100CFU/g (CFU/ml), but the protective system that shows this sample has the stronger effect of killing to microorganism, test by challenge, below within the 7th day, dropping to 1000CFU/g (CFU/m1), be considered as passing through, other is considered as not passing through.
5. experimental result
Inoculation 0,7,14,2l and 28 days sampling detects, the anticorrosion test result of experimental example 13~18 cosmetic combinations matter sample is in table 6.
Table 6
As known from Table 6: in experimental example, each cosmetic composition has certain antiseptic effect; The weight portion of Radix Et Rhizoma Nardostachyos extracting solution is larger, and antiseptic effect is more obvious; Show that Radix Et Rhizoma Nardostachyos extracting solution has good antisepsis.In the time that the weight portion of Radix Et Rhizoma Nardostachyos extracting solution is 1~2, the antisepsis of Radix Et Rhizoma Nardostachyos extracting solution is better, and cost performance is the highest.
The above embodiment has only expressed several embodiment of the present invention, and it describes comparatively concrete and detailed, but can not therefore be interpreted as the restriction to the scope of the claims of the present invention.It should be pointed out that for the person of ordinary skill of the art, without departing from the inventive concept of the premise, can also make some distortion and improvement, these all belong to protection scope of the present invention.Therefore, the protection domain of patent of the present invention should be as the criterion with claims.

Claims (10)

1. a cosmetic composition, is characterized in that, by weight, comprises following component:
Wherein, described plant extraction liquid is the mixing of Flos Rosae Multiflorae extracting solution and sorrel extracting solution, and antiseptic comprises Radix Et Rhizoma Nardostachyos extracting solution.
2. cosmetic composition according to claim 1, is characterized in that, described plant extraction liquid is that weight part ratio is (1~10): the Flos Rosae Multiflorae extracting solution of (1~10) and the mixing of sorrel extracting solution.
3. cosmetic composition according to claim 2, is characterized in that, the weight part ratio of described Flos Rosae Multiflorae extracting solution and sorrel extracting solution is (5~8): (5~10).
4. according to cosmetic composition described in claim 1-3 any one, it is characterized in that described wetting agent is that weight part ratio is (0.1~1): the trehalose of (2~10), the mixing of glycerol.
5. according to cosmetic composition described in claim 1-3 any one, it is characterized in that, described thickening agent is that weight part ratio is (0.1~0.2): the transparent HANSHENGJIAO of (0.1~0.2) and the mixing of carbomer.
6. according to cosmetic composition described in claim 1-3 any one, it is characterized in that, described emulsifying agent is fine jade wax stearyl Fructus Canarii albi oils and fats/sorbitol Fructus Canarii albi oils and fats.
7. according to cosmetic composition described in claim 1-3 any one, it is characterized in that, described pH adjusting agent is that mass parts ratio is (0.005~0.08): the sodium hydroxide of (0.05~0.8) and the mixing of water.
8. according to cosmetic composition described in claim 1-3 any one, it is characterized in that, described antiseptic is that weight part ratio is (0.3~1): the mixing of the sodium benzoate/potassium sorbate of (0.5~3) and Radix Et Rhizoma Nardostachyos extracting solution.
9. cosmetic composition according to claim 7, is characterized in that, the weight portion of described Radix Et Rhizoma Nardostachyos extracting solution is 1~2 part.
10. a preparation method for cosmetic composition described in claim 1-8 any one, is characterized in that, comprises the following steps:
(1) first use the glycerol in wetting agent scattered thickening agent, add emulsifying pot, then add wetting agent, skinfeel regulator, the emulsifying agent of plant extraction liquid, remainder, be heated to 75~85 DEG C, insulated and stirred 10~20 minutes, stir speed (S.S.) is 20~40rpm, then homogenizing 2~5 minutes, stir speed (S.S.) is 2000~4000rpm, cools, and obtains A phase;
(2) by complete pH adjusting agent mixed dissolution, obtain B phase;
(3) A of step (1) is cooled to 65~70 DEG C mutually, adds the B phase in step (2), stir, continue cooling;
(4) when the temperature in step (3) near 40~45 DEG C, add antiseptic, stir, cosmetic composition.
CN201410370969.8A 2014-07-30 2014-07-30 Cosmetic composition and preparation method thereof Pending CN104173230A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105267084A (en) * 2015-09-23 2016-01-27 嘉兴市蝶柔化妆品有限公司 Moisturizer
CN114344213A (en) * 2021-12-31 2022-04-15 青海省中医院 Skin care product containing plant extract, composition, preparation method and application thereof

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1485024A (en) * 2002-09-28 2004-03-31 戚海波 Bee honey and its use in beautifying cosmetics
CN102573787A (en) * 2009-08-14 2012-07-11 株式会社爱茉莉太平洋 Composition containing a natural extract
CN103565673A (en) * 2013-10-30 2014-02-12 广州品赫化妆品有限公司 Emollient lotion for moisturizing skin and controlling oil and preparation method of emollient lotion

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1485024A (en) * 2002-09-28 2004-03-31 戚海波 Bee honey and its use in beautifying cosmetics
CN102573787A (en) * 2009-08-14 2012-07-11 株式会社爱茉莉太平洋 Composition containing a natural extract
CN103565673A (en) * 2013-10-30 2014-02-12 广州品赫化妆品有限公司 Emollient lotion for moisturizing skin and controlling oil and preparation method of emollient lotion

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105267084A (en) * 2015-09-23 2016-01-27 嘉兴市蝶柔化妆品有限公司 Moisturizer
CN114344213A (en) * 2021-12-31 2022-04-15 青海省中医院 Skin care product containing plant extract, composition, preparation method and application thereof
CN114344213B (en) * 2021-12-31 2024-05-07 青海省中医院 Skin care product and composition containing plant extracts, and preparation method and application thereof

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Application publication date: 20141203