CN104127349A - Cosmetic composition and preparation method thereof - Google Patents
Cosmetic composition and preparation method thereof Download PDFInfo
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- CN104127349A CN104127349A CN201410371001.7A CN201410371001A CN104127349A CN 104127349 A CN104127349 A CN 104127349A CN 201410371001 A CN201410371001 A CN 201410371001A CN 104127349 A CN104127349 A CN 104127349A
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Abstract
A disclosed cosmetic composition comprises the following compositions in parts by weight: 2-20 parts of a plant extraction liquid, 3-11 parts of a moisture-retaining agent, 0.2-0.4 part of a thickening agent, 0.1-0.5 part of an emulsifier, 0.1-2 parts of quartz stone, 0.03-0.07 part of potassium hydroxide, 0.055-0.88 part of a pH conditioner, 0.8-4 parts of an antiseptic, and 60-90 parts of water. The plant extraction liquid comprises a polyghace seche extraction liquid and a radix glycyrrhiza extraction liquid, and the antiseptic comprises an artemisia carvifolia extraction liquid. According to the cosmetic composition, a mixed solution of the polyghace seche extraction liquid and the radix glycyrrhiza extraction liquid is applied to cosmetic compositions, skin activity is effectively improved and skin is whitened.
Description
Technical field
The present invention relates to cosmetic field, particularly relate to a kind of cosmetic composition with white-skinned face function and preparation method thereof.
Background technology
Cosmetics are to smear, spray or other similar methods, impose on any position of human body surface (skin, fingernail, lip, the ripe film in oral cavity etc.), with the product that reaches clean, eliminates bad smell, skin protection, beauty treatment and modification object.
Because the pollution of heredity, endocrine, ultraviolet, sunlight, free radical, environment etc. reason makes skin, easily produce the phenomenon that some row such as low and deep, yellowish, freckle, black speck affects skin appearance, the while has also more been increased the weight of cutaneous activity the bad performance of above-mentioned skin.How to allow skin activity improves, skin whitening is an important topic.
Along with the development of cosmetics industry, natural plants series products due to use safety, action temperature and, the advantage such as successful welcome.Be generally to obtain by corresponding processing the plant extract that contains effective ingredient, and add in cosmetics.
At present, cosmetics whitening effect is on the market not obvious, and very easily causes allergic phenomena.Therefore, select which kind of plant, and by the effect that reaches whitening in cosmetics that is applied to of its safety, be problem demanding prompt solution.
Summary of the invention
Based on this, the object of the present invention is to provide a kind of cosmetic composition.
Concrete technical scheme is as follows:
A cosmetic composition, by weight, comprises following component:
Wherein, above-mentioned wetting agent comprises Rhizoma Polygonati Odorati extracting solution and Radix Glycyrrhizae extract, and antiseptic comprises Herba Artemisiae Annuae extracting solution.
In an embodiment, described plant extraction liquid is that weight part ratio is (1～10): the Rhizoma Polygonati Odorati extracting solution of (1～10) and the mixing of Radix Glycyrrhizae extract therein.
In an embodiment, the weight part ratio of described Rhizoma Polygonati Odorati extracting solution and Radix Glycyrrhizae extract is (5～8): (5～10) therein.
In an embodiment, described wetting agent is that weight part ratio is (0.1～1): the trehalose of (2～10), the mixing of glycerol therein.
In an embodiment, described thickening agent is that weight part ratio is (0.1～0.2): the transparent HANSHENGJIAO of (0.1～0.2) and the mixing of carbomer therein.
In an embodiment, described emulsifying agent is fine jade wax stearyl Fructus Canarii albi oils and fats/sorbitol Fructus Canarii albi oils and fats therein.
In an embodiment, described pH adjusting agent is that mass parts ratio is (0.005～0.08): the sodium hydroxide of (0.05～0.8) and the mixing of water therein.
In an embodiment, described antiseptic is that weight part ratio is (0.3～1): the mixing of the sodium benzoate/potassium sorbate of (0.5～3) and Herba Artemisiae Annuae extracting solution therein.
In an embodiment, the weight portion of described Herba Artemisiae Annuae extracting solution is 1～2 part therein.
Rhizoma Polygonati Odorati extracting solution of the present invention, Radix Glycyrrhizae extract and Herba Artemisiae Annuae extracting solution can be prepared by conventional alcohol extracting method, preferred following extracting method: it is in 50% ethanol that dry plant (Herba Artemisiae Annuae, Radix Glycyrrhizae, Rhizoma Polygonati Odorati) is joined to mass ratio, under backflow and dipping, extract 1～3h, extract 1～3 time; Subsequently, with filter cloth, extracting solution is filtered, obtain filtrate.Mix the filtrate of 1～3 time and be concentrated into dry plant (Herba Artemisiae Annuae, Radix Glycyrrhizae, Rhizoma Polygonati Odorati) extracting solution.
The preparation method of above-mentioned cosmetic composition, comprises the following steps:
(1) first use the glycerol in wetting agent scattered thickening agent, add emulsifying pot, then the wetting agent, skinfeel regulator, the emulsifying agent that add plant extraction liquid, remainder, be heated to 75～85 ℃, insulated and stirred 10～20 minutes, stir speed (S.S.) is 20～40rpm, then homogenizing is 2～5 minutes, stir speed (S.S.) is 2000～4000rpm, cools, and obtains A phase;
(2) pH adjusting agent mixed dissolution is complete, obtain B phase;
(3) A of step (1) is cooled to 65～70 ℃ mutually, adds the B phase in step (2), stir, continue cooling;
(4) temperature in step (3) is near 40～45 ℃, adds antiseptic, stir, cosmetic composition.
Rhizoma Polygonati Odorati is Liliaceae Polygonatum plant Rhizoma Polygonati Odorati dry rhizome.There is growth or the plantation of certified products Rhizoma Polygonati Odorati China northeast, North China, northwest, East China, each provinces and regions, Central China, main product in Hunan, the province such as Guangdong, Henan, Jiangsu, Zhejiang.Originate in northeast person and claim " closing Rhizoma Polygonati Odorati ", originate in Jiangsu person and claim " eastern Rhizoma Polygonati Odorati ", originate in Anhui person and claim " southern Rhizoma Polygonati Odorati ", originate in Hunan person and claim " Polygonatum Modoratum (Mill.) Druce ", the Rhizoma Polygonati Odorati of wherein especially producing with Hunan (Polygonatum Modoratum (Mill.) Druce) is the most famous.Rhizoma Polygonati Odorati extracting solution has good facilitation to the activity of fibrous bud cell, and the propagation of B-16 melanocyte is had to inhibition, the also generation of check melanin simultaneously; Be that Rhizoma Polygonati Odorati extracting solution can improve skin activity, suppress skin darkening, there is the effect of whitening.
Radix Glycyrrhizae is the ground such as the root of glycyrrhizic legume, the main product Inner Mongol, Shanxi, Gansu and Xinjiang.Radix Glycyrrhizae root and rhizome can be excavated in spring, Qiu Erji, removes fibrous root, dries.Radix Glycyrrhizae extract is to myocyte's proliferation function, have facilitation to the facilitation of vascular endothelial cell proliferation, Action Specification Radix Glycyrrhizae extract such as inhibition that NO is generated at the aspects such as activity that improve skin; Meanwhile, Radix Glycyrrhizae extract has inhibitory action to melanocyte propagation, and these can show that Radix Glycyrrhizae extract is improved the effect of skin activity, skin whitening.
The Silicon stone adding in cosmetic composition of the present invention is that skinfeel regulator can make people be combined and improve skin condition with physiology from psychology, increases moisture of skin; The effect of pH adjusting agent is that cosmetic composition of the present invention is had the good acid-base value of skin effect.
Herba Artemisiae Annuae has another name called careless Artemisia, is feverfew, is distributed widely in the ground such as Liaoning, Hebei, Shandong, Shanxi, Shaanxi, Jiangsu, Anhui, Jiangxi, Hubei, Zhejiang, Fujian, Guangdong, is the very large a kind of wormwood of output.Herba Artemisiae Annuae extracting solution has the antibiotic property of wide spectrum, uses in the present invention as antiseptic.But antibacterial is killed in the prevention that act as of antiseptic, and protection product is avoided microbial contamination, extends the product shelf phase; Prevent that consumer's use is subject to the product of microbial contamination and causes possible infection, guarantees safety.
The following composition title that the application occurs is the title of INCI (International Nomenclaure Cosmetic Ingredient, i.e. international cosmetic raw material name) defined: fine jade wax stearyl Fructus Canarii albi oils and fats/sorbitol Fructus Canarii albi oils and fats and sodium benzoate/potassium sorbate.
Advantage of the present invention is as follows:
Compared with prior art, cosmetic composition of the present invention can improve skin activity, skin whitening; Separately, in the present invention, use natural botanical extraction liquid to use as antiseptic, and reached good effect.
The specific embodiment
Below in conjunction with specific embodiment, present techniques scheme is described further.
Embodiment 1
The preparation of plant extraction liquid
It is in 50% ethanol that dry Rhizoma Polygonati Odorati is joined to mass ratio, reflux and dipping under extract 1.5h, extract 3 times; Subsequently, with filter cloth, extracting solution is filtered, obtain filtrate.Mix the filtrate of 3 times and be concentrated into dry Rhizoma Polygonati Odorati extracting solution.
It is in 50% ethanol that dry Radix Glycyrrhizae is joined to mass ratio, reflux and dipping under extract 2h, extract 2 times; Subsequently, with filter cloth, extracting solution is filtered, obtain filtrate.Mix the filtrate of 2 times and be concentrated into dry Radix Glycyrrhizae extract.
It is in 50% ethanol that dry plant Herba Artemisiae Annuae is joined to mass ratio, reflux and dipping under extract 2h, extract 2 times; Subsequently, with filter cloth, extracting solution is filtered, obtain filtrate.Mix the filtrate of 2 times and be concentrated into dry Herba Artemisiae Annuae extracting solution.
Embodiment 2
The preparation of cosmetic composition
One, the formula of cosmetic composition
The cosmetic combinations composition formula of experimental example 1～3 and comparative example 1～3 is in Table 1.
Table 1
The cosmetic combinations composition formula of experimental example 4～6 and comparative example 4～6 is in Table 2.
Table 2
The cosmetic combinations composition formula of experimental example 7～12 is in Table 3.
Table 3
The cosmetic combinations composition formula of experimental example 13～18 is in Table 4.
Table 4
Two, the preparation of cosmetic composition
The cosmetic composition of above-mentioned experimental example 1-18 and comparative example 1-6 makes by following preparation method:
(1) first use the glycerol in wetting agent scattered thickening agent, add emulsifying pot, then the wetting agent, skinfeel regulator, the emulsifying agent that add plant extraction liquid, remainder, be heated to 80 ℃, insulated and stirred 15 minutes, stir speed (S.S.) is 30rpm, then homogenizing is 3 minutes, stir speed (S.S.) is 3000rpm, cools, and obtains A phase;
(2) pH adjusting agent mixed dissolution is complete, obtain B phase;
(3) A of step (1) is cooled to 70 ℃ mutually, adds the B phase in step (2), stir, continue cooling;
(4) temperature in step (3) is near 40 ℃, adds antiseptic, stir, cosmetic composition.
Embodiment 3
Effect experiment
The cosmetic composition that experimental example 1～12 in above-mentioned table 1 and table 2 and comparative example 1～6 are made, through 100 personnel of 20～55 years old 30 days on probation continuously, the whitening effect of prepared cosmetic composition in above-mentioned each experimental example was evaluated in relative analysis respectively.Wherein, described effect is that skin is yellowish, low and deep, the improvement situation of black speck, freckle etc., the results are shown in Table 5.
Table 5
The cosmetic composition of above-mentioned experimental example 1-12 and comparative example 1-6 is not all found zest and allergic phenomena in process on probation.
As known from Table 5: in experimental example, each cosmetic composition is that skin is yellowish, low and deep, the improvement degree of black speck, freckle etc. is obviously high than the improvement degree of each product in matched group; And the weight portion of Rhizoma Polygonati Odorati extracting solution and Radix Glycyrrhizae extract is larger, improvement degree is higher; The weight portion of Rhizoma Polygonati Odorati extracting solution is 5～8, the weight portion of Radix Glycyrrhizae extract is 5～10 o'clock, and the cost performance of cosmetic composition is the highest.
Embodiment 4
Anti-corrosive properties test
The protective system efficiency evaluation method that this experiment is recommended with reference to U.S.'s cosmetics, toilet articles and essence association (CTFA), the anticorrosion single challenge experiment of classical 28 days by a definite date of recommending with CTFA.
1. challenge microorganism: antibacterial and mycete
2. mode and the quantity inoculated
(1) mode of inoculation: adopt combined inoculation.Because natural microorganism has mixed raw feature of living together, so the situation of the realistic pollution of combined inoculation.
(2) quantity of inoculation: each strain is inoculated in suitable culture medium, cultivates in 37 ℃ (antibacterials) and 28 ℃ of (mycete) incubators.Antibacterial culturing 48 hours, mycotic culture, after 72 hours, is selected typical bacterium colony and in the fluid medium of sterilizing, is made certain density antibacterial and mycete mixing suspension, is placed in refrigerator cold-storage standby.Antibacterial: every gram of suspension bacteria containing amount is 1 * 10
6cFU/g or CFU/ml; Mycete is that every gram of suspension bacteria containing amount is 1 * 10
5cFU/g or CFU/ml.
3. Microbial Challenge experiment
Take each 100 grams of experimental example 13～18 cosmetic samples, add in the container of sterilizing, add mixed cell and mould bacteria suspension, fully mix.Every gram of sample is 1 * 10 containing amount of bacteria
6cFU/g or CFU/ml; Containing mycete amount, be 1 * 10
5cFU/g or CFU/ml.Then be placed at 28 ℃.Connecing 0,7,14,21,28 day sample analysis of bacterium: accurately take 10 grams of samples, be added in the conical flask that contains glass pellet and 90ml sterile saline, fully concussion mixes, and this suspension is 1:10 diluent, and then dilutes successively by 1:10 with normal saline.At 37 ℃, antibacterial, cultivate 48 hours; At 28 ℃, mycete, cultivate 72 hours, by bacteria containing amount in dull and stereotyped tilt-pour process counting sample.
4. evaluation methodology
In 28 days samples, contain antibacterial or mycete at 10CFU/g～100CFU/g (CFU/ml), but the protective system that shows this sample has the stronger effect of killing to microorganism, by challenge, test, at the 7th day, drop to below 1000CFU/g (CFU/m1), be considered as by, other is considered as not passing through.
5. experimental result
Inoculation 0,7,14,2l and 28 days sampling detects, the anticorrosion test result of experimental example 13～18 cosmetic combinations matter sample is in Table 6.
Table 6
As known from Table 6: in experimental example, each cosmetic composition has certain antiseptic effect; The weight portion of Herba Artemisiae Annuae extracting solution is larger, and antiseptic effect is more obvious; Show that Herba Artemisiae Annuae extracting solution has good antisepsis.When the weight portion of Herba Artemisiae Annuae extracting solution is 1～2, the antisepsis of Herba Artemisiae Annuae extracting solution is better, and cost performance is the highest.
The above embodiment has only expressed several embodiment of the present invention, and it describes comparatively concrete and detailed, but can not therefore be interpreted as the restriction to the scope of the claims of the present invention.It should be pointed out that for the person of ordinary skill of the art, without departing from the inventive concept of the premise, can also make some distortion and improvement, these all belong to protection scope of the present invention.Therefore, the protection domain of patent of the present invention should be as the criterion with claims.
Claims (10)
1. a cosmetic composition, is characterized in that, by weight, comprises following component:
Wherein, described plant extraction liquid is the mixing of Rhizoma Polygonati Odorati extracting solution and Radix Glycyrrhizae extract, and antiseptic comprises Herba Artemisiae Annuae extracting solution.
2. cosmetic composition according to claim 1, is characterized in that, described plant extraction liquid is that weight part ratio is (1～10): the Rhizoma Polygonati Odorati extracting solution of (1～10) and the mixing of Radix Glycyrrhizae extract.
3. cosmetic composition according to claim 2, is characterized in that, the weight part ratio of described Rhizoma Polygonati Odorati extracting solution and Radix Glycyrrhizae extract is (5～8): (5～10).
4. according to cosmetic composition described in claim 1-3 any one, it is characterized in that described wetting agent is that weight part ratio is (0.1～1): the trehalose of (2～10), the mixing of glycerol.
5. according to cosmetic composition described in claim 1-3 any one, it is characterized in that, described thickening agent is that weight part ratio is (0.1～0.2): the transparent HANSHENGJIAO of (0.1～0.2) and the mixing of carbomer.
6. according to cosmetic composition described in claim 1-3 any one, it is characterized in that, described emulsifying agent is fine jade wax stearyl Fructus Canarii albi oils and fats/sorbitol Fructus Canarii albi oils and fats.
7. according to cosmetic composition described in claim 1-3 any one, it is characterized in that, described pH adjusting agent is that mass parts ratio is (0.005～0.08): the sodium hydroxide of (0.05～0.8) and the mixing of water.
8. according to cosmetic composition described in claim 1-3 any one, it is characterized in that, described antiseptic is that weight part ratio is (0.3～1): the mixing of the sodium benzoate/potassium sorbate of (0.5～3) and Herba Artemisiae Annuae extracting solution.
9. cosmetic composition according to claim 7, is characterized in that, the weight portion of described Herba Artemisiae Annuae extracting solution is 1～2 part.
10. a preparation method for cosmetic composition described in claim 1-8 any one, is characterized in that, comprises the following steps:
(1) first use the glycerol in wetting agent scattered thickening agent, add emulsifying pot, then the wetting agent, skinfeel regulator, the emulsifying agent that add plant extraction liquid, remainder, be heated to 75～85 ℃, insulated and stirred 10～20 minutes, stir speed (S.S.) is 20～40rpm, then homogenizing is 2～5 minutes, stir speed (S.S.) is 2000～4000rpm, cools, and obtains A phase;
(2) pH adjusting agent mixed dissolution is complete, obtain B phase;
(3) A of step (1) is cooled to 65～70 ℃ mutually, adds the B phase in step (2), stir, continue cooling;
(4) temperature in step (3) is near 40～45 ℃, adds antiseptic, stir, cosmetic composition.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108685821A (en) * | 2018-08-10 | 2018-10-23 | 广东卓明仕生物科技有限公司 | It is a kind of to have effects that enhance the Chinese medicine composition and its preparation method and application of skin tolerance |
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| CN108685821A (en) * | 2018-08-10 | 2018-10-23 | 广东卓明仕生物科技有限公司 | It is a kind of to have effects that enhance the Chinese medicine composition and its preparation method and application of skin tolerance |
| CN108685821B (en) * | 2018-08-10 | 2021-04-02 | 广东卓明仕生物科技有限公司 | Traditional Chinese medicine composition with effect of enhancing skin tolerance and preparation method and application thereof |
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