CN103565673A - Emollient lotion for moisturizing skin and controlling oil and preparation method of emollient lotion - Google Patents
Emollient lotion for moisturizing skin and controlling oil and preparation method of emollient lotion Download PDFInfo
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- CN103565673A CN103565673A CN201310523721.6A CN201310523721A CN103565673A CN 103565673 A CN103565673 A CN 103565673A CN 201310523721 A CN201310523721 A CN 201310523721A CN 103565673 A CN103565673 A CN 103565673A
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Abstract
The invention discloses an emollient lotion for moisturizing skin and controlling oil. The emollient lotion is prepared from the following components in percentage by mass: 0.1-5% of hydrogenated phosphatidylcholine, 0.1-5% of phytosterol, 0.001-1% of ceramide, 0.1-5% of silica, 2-20% of humectant, 2-20% of grease, 0.1-1% of thickening agent, 0.5-5% of emulsifying agent, 0.1-0.6% of preservative and the balance of distilled water. The emollient lotion has efficient moisture retention and can be used for enhancing the protection mechanism of the skin, promoting the metabolism of cell membranes of the skin and achieving the aims of improving dry skin as well as relieving and repairing the skin.
Description
Technical field
The present invention relates to cosmetic field, be specifically related to a kind of milky lotion for skin moisture-keeping control oil and preparation method thereof.
Background technology
Skin has barrier function; and in daily life, skin barrier often can sustain damage, as: hot water; solvent; mechanical damages etc., although human body can self be repaired barrier, with advancing age; the time of repairing is more and more longer; like this will cutaneous normal function, usually to skin, bring hydropenia dry, the relevant issues such as allergic stimulated.Milky lotion is the white class cosmetics of a kind of liquid state, has good skin moistening effect, also has damping effect, and the emulsion of early stage milky lotion is oil-in-water emulsion, is one of cosmetics conventional in daily life.Traditional milky lotion adopts potash soap to make emulsifying agent more, but meeting retrogradation in depositing process is difficult for pouring out from bottle.
The maintenance of skin barrier is mainly synthetic skin lipid composition, that is: cholesterol, ceramide and phospholipid etc. is a large amount of synthetic, and this lipoids of external can be accelerated skin barrier structure.The impact that external lipid builds lipid barrier, phospholipid, cholesterol, several lipid of ceramide have facilitation to the recovery of skin barrier function.Phospholipid is extensively distributed in animal and plant body, is the important composition composition of biological cell, and it plays very important effect to the infiltration of metabolism and film.Yet, because the main component of natural phospholipid is unsaturated fatty acid, so resistance to oxidation is not also unstable to heat, be difficult to be applied in cosmetics.
Summary of the invention
For overcoming the defect of prior art, be of the present inventionly to provide a kind of milky lotion for skin moisture-keeping control oil, there is efficient moisture retention, the protection function of strengthening skin, promotes the metabolism of Skin Cell film, reaches the effect that improves xerosis cutis and releive maintenance.
Another object of the present invention is to provide a kind of preparation method of the milky lotion for skin moisture-keeping control oil, by the method, obtain a kind of effect milky lotion that can improve xerosis cutis and the maintenance skin of releiving.
The technical solution adopted in the present invention is as follows for achieving the above object:
For a milky lotion for skin moisture-keeping control oil, it contains following component by percentage to the quality:
Hydrolecithin: 0.1-5%,
Plant sterol: 0.1%-5%,
Ceramide 0.001%-1%,
Silicon stone: 0.1-5%,
Wetting agent: 2-20%,
Oils and fats: 2-20%,
Thickening agent: 0.1-1%,
Emulsifying agent: 0.5-5%,
Antiseptic: 0.1-0.6%,
Surplus is distilled water.
As a kind of preferred scheme of the present invention, it contains following component by percentage to the quality:
Hydrolecithin: 2-4%,
Plant sterol: 2%-4%,
Ceramide: 0.1%-0.5%,
Silicon stone: 2-4%,
Wetting agent: 5-10%,
Oils and fats: 5-10%,
Thickening agent: 0.5-1%,
Emulsifying agent: 2-4%,
Antiseptic: 0.2-0.4%,
Surplus is distilled water.
Although phospholipid is the important composition composition of biological cell, it plays very important effect to the infiltration of metabolism and film.Yet, because the main component of natural phospholipid is unsaturated fatty acid, so resistance to oxidation is not also unstable to heat, be difficult to be applied directly in cosmetics.Inventor finds through research; the hydrolecithin extracting from Semen sojae atricolor is a kind of naturally occurring emulsifying agent with anti-inflammatory effect, and can effectively reduce the stimulation to skin, has efficient moisture retention; the protection function of strengthening skin, can promote the metabolism of Skin Cell film.Plant sterol is as Skin Cell promoter, Wound-healing agent and moisture retention in the present invention; and there is good resistance to oxidation; can rebuild sebum protection and repair skin barrier; and there is very high permeability; can keep skin surface moisture content; promote skin metabolism, suppress scytitis, can anti-day erythema, skin aging.Ceramide has good barrier function in the present invention, and has bonding and moisture-keeping function.Plant sterol is combined with hydrolecithin, ceramide and Silicon stone, has excellent moisturizing control oil effect.
The Silicon stone adopting in the present invention is hydrophilic hollow silica, mean diameter 2.0-4.0 μ m, and average oil absorption is 130-170ml/100g.In above-mentioned formula, Silicon stone has effective absorption oils and fats, keeps the function of the dry and comfortable non-greasy of skin.
Wetting agent described in such scheme is that one or more of glycerol, propylene glycol, butanediol, Polyethylene Glycol or glycerin polyether apoplexy due to endogenous wind are with arbitrarily than mixing.
The thickening agent polymer that thickening agent of the present invention is all produced purchased from U.S. Lubrizol Corp., preferably Carbopol
?980 polymer, Carbopol
?981 polymer, Pemulen
?tR-1 polymer, Pemulen
?tR-2 polymer, Carbopol
?one or more in ETD 2020 polymer are with arbitrarily than mixing.
In such scheme, described oils and fats is a kind of in Vegetable oil lipoprotein, synthetic ester oil, Dormant oils, silicone oil.Preferred oils and fats of the present invention is Vegetable oil lipoprotein.
In the present invention, institute's employing emulsifying agent is selected from one or more mixing in C20-22 alkyl phosphate, C20-22 alcohol or cetearyl glucoside or cetearyl alcohol.
In such scheme, described antiseptic is a kind of in methyl hydroxybenzoate, phenoxyethanol, two imidazolidinyl urea.
In such scheme, described milky lotion is yellow semi-transparent viscous emulsion, and viscosity is 10000-30000mPa.s.
The preparation method of milky lotion of the present invention, the steps include: thickening agent to add in the water pot that distilled water is housed, and homogenous disperse is even, is warmed up to 80-85 ℃, adds wetting agent and hydrolecithin, is incubated standby after stirring; Then oils and fats and emulsifying agent are added to oil phase pot, stir and be warming up to 80-85 ℃, then by oil phase suction water, homogenizer homogenizing, insulation, stirs and is cooled to 30-45 ℃, adds respectively pH value regulator and antiseptic, and adjusting pH value is 6.0-7.0.
In above-mentioned preparation method, preferred, the speed of described homogenizer is 3000rpm, and homogenizing time is 5-15 minute.
Compared to existing technology, beneficial effect of the present invention is:
1. milky lotion of the present invention can effectively reduce stimulation, reduces the potential stimulus of other surfactants, and the antiphlogistic effects that strengthens oil-soluble active matter;
2. milky lotion of the present invention has efficient moisture retention, and the protection function of strengthening skin, promotes the metabolism of Skin Cell film;
3. milky lotion of the present invention has good affinity to horny layer, and efficient soft effect, is improved effect to dry skin;
4. milky lotion of the present invention has good infiltration moisture retention, can promote the absorption of skin to effective ingredient, improves the utilization of effective ingredient, and permanent moisturizing;
5. milky lotion of the present invention can promote wound healing, makes muscle hypertrophy, strengthens blood capillary circulation.
Below in conjunction with concrete embodiment, the present invention is described in further detail.
The specific embodiment
The thickening agent polymer that the thickening agent adopting in the present invention is all produced purchased from U.S. Lubrizol Corp., preferably Carbopol
?980 polymer, Carbopol
?981 polymer, Pemulen
?tR-1 polymer, Pemulen
?tR-2 polymer, Carbopol
?one or more in ETD 2020 polymer are with arbitrarily than mixing; The hydrolecithin adopting, plant sterol, ceramide all adopt the conventional method of this area to purify and obtain or obtain by purchase.
Below specific embodiments of the invention.
Embodiment 1
For a milky lotion for skin moisture-keeping control oil, it contains following component by percentage to the quality:
Hydrolecithin: 5%,
Plant sterol: 5%,
Ceramide: 0.001%,
Silicon stone: 0.1%,
Glycerol: 2%,
Vegetable oil lipoprotein: 20%,
Carbopol
?980 polymer: 0.1%,
Emulsifying agent: 5%,
Phenoxyethanol: 0.1%,
Surplus is distilled water; And be prepared from by the following method:
Thickening agent is added in the water pot that distilled water is housed, and homogenous disperse is even, is warmed up to 80-85 ℃, adds wetting agent and hydrolecithin, is incubated standby after stirring; Then oils and fats and emulsifying agent are added to oil phase pot, stir and be warming up to 80-85 ℃, then by oil phase suction water, homogenizer homogenizing, insulation, stirs and is cooled to 30-45 ℃, adds respectively pH value regulator and antiseptic, and regulating pH value is 6.7.
The product obtaining for yellow semi-transparent viscous emulsion, viscosity is 10089mPa.s.
Embodiment 2
For a milky lotion for skin moisture-keeping control oil, it contains following component by percentage to the quality:
Hydrolecithin: 0.1%,
Plant sterol:: 0.1%,
Ceramide: 1%,
Silicon stone: 5%,
Polyethylene Glycol: 20%,
Vegetable oil lipoprotein: 2%,
Pemulen
?tR-1 polymer: 1%,
Emulsifying agent: 5%,
Two imidazolidinyl urea: 0.1%,
Surplus is distilled water; And be prepared from by the following method:
Thickening agent is added in the water pot that distilled water is housed, and homogenous disperse is even, is warmed up to 80-85 ℃, adds wetting agent and hydrolecithin, is incubated standby after stirring; Then oils and fats and emulsifying agent are added to oil phase pot, stir and be warming up to 80-85 ℃, then by oil phase suction water, homogenizer homogenizing, insulation, stirs and is cooled to 30-45 ℃, adds respectively pH value regulator and antiseptic, regulates pH value to be: 6.1
The product obtaining for yellow semi-transparent viscous emulsion, viscosity is 12760mPa.s.
Embodiment 3
For a milky lotion for skin moisture-keeping control oil, it contains following component by percentage to the quality:
Hydrolecithin: 2%,
Plant sterol: 4%,
Ceramide: 0.5%,
Silicon stone: 2%,
Glycerin polyether class: 10%,
Dormant oils: 10%,
Carbopol
?eTD 2020 polymer: 0.5%,
Emulsifying agent: 2%,
Methyl hydroxybenzoate: 0.5%,
Surplus is distilled water; And be prepared from by the following method:
Thickening agent is added in the water pot that distilled water is housed, and homogenous disperse is even, is warmed up to 85 ℃, adds wetting agent and hydrolecithin, is incubated standby after stirring; Then oils and fats and emulsifying agent are added to oil phase pot, stir and be warming up to 80 ℃, then by oil phase suction water, homogenizer homogenizing, insulation, stirs and is cooled to 35 ℃, adds respectively pH value regulator and antiseptic, and regulating pH value is 6.9.
The product obtaining for yellow semi-transparent viscous emulsion, viscosity is 21091mPa.s.
Embodiment 4
For a milky lotion for skin moisture-keeping control oil, it contains following component by percentage to the quality:
Hydrolecithin: 0.1%,
Plant sterol: 5%,
Ceramide: 1%,
Silicon stone: 5%,
Polyethylene Glycol: 2%
Vegetable oil lipoprotein: 20%,
Carbopol
?eTD 2020 polymer: 0.1%,
Emulsifying agent: 5%,
Methyl hydroxybenzoate: 0.1%,
Surplus is distilled water; And be prepared from by the following method:
By Carbopol
?eTD 2020 polymer add in the water pot that distilled water is housed, and homogenous disperse is even, is warmed up to 80-85 ℃, add ceramide and hydrolecithin, are incubated standby after stirring; Then Vegetable oil lipoprotein and emulsifying agent are added to oil phase pot, stir and be warming up to 80-85 ℃, then by oil phase suction water, homogenizer homogenizing, insulation, stirs and is cooled to 30-45 ℃, adds respectively pH value regulator and methyl hydroxybenzoate, regulates pH value to be: 6.3.
The product obtaining for yellow semi-transparent viscous emulsion, viscosity is 18469mPa.s.
Embodiment 5
For a milky lotion for skin moisture-keeping control oil, it contains following component by percentage to the quality:
Hydrolecithin: 5%,
Plant sterol: 0.1%,
Ceramide: 0.2%,
Silicon stone: 0.1%,
Polyethylene Glycol: 20%,
Vegetable oil lipoprotein: 2%,
Carbopol
?eTD 2020 polymer: 1%,
Emulsifying agent: 0.5%,
Methyl hydroxybenzoate: 0.6%,
Surplus is distilled water; And be prepared from by the following method:
By Carbopol
?eTD 2020 polymer add in the water pot that distilled water is housed, and homogenous disperse is even, is warmed up to 80-85 ℃, add ceramide and hydrolecithin, are incubated standby after stirring; Then Vegetable oil lipoprotein and emulsifying agent are added to oil phase pot, stir and be warming up to 80-85 ℃, then by oil phase suction water, homogenizer homogenizing, insulation, stirs and is cooled to 30-45 ℃, adds respectively pH value regulator and methyl hydroxybenzoate, regulates pH value to be: 6.3.
The product obtaining for yellow semi-transparent viscous emulsion, viscosity is 27405mPa.s.
Embodiment 6
For a milky lotion for skin moisture-keeping control oil, it contains following component by percentage to the quality:
Hydrolecithin: 2%,
Plant sterol: 2%,
Ceramide: 0.1%,
Silicon stone: 2%,
Polyethylene Glycol: 10%, Vegetable oil lipoprotein: 10%,
Carbopol
?eTD 2020 polymer: 0.5%,
Emulsifying agent: 2%,
Methyl hydroxybenzoate: 0.5%,
Surplus is distilled water; And be prepared from by the following method:
By Carbopol
?eTD 2020 polymer add in the water pot that distilled water is housed, and homogenous disperse is even, is warmed up to 80-85 ℃, add ceramide and hydrolecithin, are incubated standby after stirring; Then Vegetable oil lipoprotein and emulsifying agent are added to oil phase pot, stir and be warming up to 80-85 ℃, then by oil phase suction water, homogenizer homogenizing, insulation, stirs and is cooled to 30-45 ℃, adds respectively pH value regulator and methyl hydroxybenzoate, regulates pH value to be: 6.5.
The product obtaining for yellow semi-transparent viscous emulsion, viscosity is 29613mPa.s.
Compositions of the present invention meets the indices in the national < < cosmetics health standard 2007 > > that promulgate, this product is not containing any noxious substance, by the said goods directly by outer spray or the mode of smearing between 20-40 year, have the women of different skin problem on probation, user is total up to 100 people, time operating period is 14-28 days, can obviously improve the dry, low and deep of skin; Product of the present invention easily absorbs, moisture preserving time is long, has the oily effect of obvious control.
Above-mentioned embodiment is only the preferred embodiment of the present invention; can not limit the scope of protection of the invention with this, the variation of any unsubstantiality that those skilled in the art does on basis of the present invention and replacement all belong to the present invention's scope required for protection.
Claims (9)
1. for a milky lotion for skin moisture-keeping control oil, it is characterized in that, it contains following component by percentage to the quality:
Hydrolecithin: 0.1-5%,
Plant sterol: 0.1%-5%,
Ceramide: 0.001%-1%,
Silicon stone: 0.1-5%,
Wetting agent: 2-20%,
Oils and fats: 2-20%,
Thickening agent: 0.1-1%,
Emulsifying agent: 0.5-5%,
Antiseptic: 0.1-0.6%,
Surplus is distilled water.
2. milky lotion according to claim 1, is characterized in that, it contains following component by percentage to the quality:
Hydrolecithin: 2-4%,
Plant sterol: 2%-4%,
Ceramide: 0.1%-0.5%,
Silicon stone: 2-4%,
Wetting agent: 5-10%,
Oils and fats: 5-10%,
Thickening agent: 0.5-1%,
Emulsifying agent: 2-4%,
Antiseptic: 0.2-0.4%,
Surplus is distilled water.
3. milky lotion according to claim 1 and 2, is characterized in that, described Silicon stone is hydrophilic hollow silica, mean diameter 2.0-4.0 μ m, and average oil absorption is 130-170ml/100g
Milky lotion according to claim 1 and 2, is characterized in that, described wetting agent comprise glycerol, propylene glycol, butanediol, Polyethylene Glycol, glycerin polyether apoplexy due to endogenous wind one or more with arbitrarily than mixing.
4. milky lotion according to claim 1 and 2, is characterized in that, described thickening agent is Carbopol
?980 polymer, Carbopol
?981 polymer, Pemulen
?tR-1 polymer emulsifier, Pemulen
?tR-2 polymer emulsifier, Carbopol
?one or more in ETD 2020 polymer are with arbitrarily than mixing.
5. milky lotion according to claim 1 and 2, is characterized in that, described oils and fats is a kind of in Vegetable oil lipoprotein, synthetic ester oil, Dormant oils, silicone oil.
6. milky lotion according to claim 1 and 2, is characterized in that, described antiseptic is a kind of in methyl hydroxybenzoate, phenoxyethanol, two imidazolidinyl urea.
7. milky lotion according to claim 1 and 2, is characterized in that, described milky lotion is yellow semi-transparent viscous emulsion, and viscosity is 10000-30000mPa.s.
8. a preparation method for milky lotion as claimed in claim 1, is characterized in that, the steps include: thickening agent to add in the water pot that distilled water is housed, homogenous disperse is even, be warmed up to 80-85 ℃, add wetting agent and hydrolecithin, after stirring, be incubated standby; Then oils and fats and emulsifying agent are added to oil phase pot, stir and be warming up to 80-85 ℃, then by oil phase suction water, homogenizer homogenizing, insulation, stirs and is cooled to 30-45 ℃, adds respectively pH value regulator and antiseptic, regulates pH value to be: 6.0-7.0.
9. preparation method according to claim 9, is characterized in that, the speed of homogenizer is 3000rpm, and homogenizing time is 5-15 minute.
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