Summary of the invention
The objective of the invention is to overcome the deficiencies in the prior art, a kind of combination various plants composition is provided, collection is isolated, and whitens, the triple effect of preserving moisture unification, skin care, moisturizing comprehensively, adjust the colour of skin, keep skin health, strengthen elastic skin whitening lotion of skin and preparation method thereof.
Purpose of the present invention is achieved by following technical proposals
A kind of skin whitening lotion, the quality sum of each component is 100 mass parts, is made up of following component:
The quality sum of each component of the present invention is 100 mass parts, and each components contents is preferably as follows:
Described component A is acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, mainly be used as the cosmetics thickening agent, be used in a Hair and the skin-protection product, wiping can form thin film and have adhesion on skin, hold moisture provides the moistening effect of persistence to skin, allow dermal sensation such as silkiness softness, for example the commodity ULRVEZ-21 of the sharp biochemical industry company limited in sky, Beijing.
Described B component is the copolymer of PEG and PPG, UCON Fluids is the Polyethylene Glycol propylene glycol, liquid with midium-viscosity can make emollient cream, water-activated eye make-up remover, hidroschesis reveal and moist suitable cunning of deodorizer, simultaneously can bring a series of additional effects, for example: can make the rapid humidifying of color make-up, in use can produce heat rapidly, perhaps control the viscosity of shampoo, for example PEG/PPG-17/6 copolymer 75-H 450.
Described component C is the mixture of ammonium acrylate/acrylamide copolymer, polyisobutylene and polysorbas20, belongs to hydration expansion drop (HSD) polymer of a new generation, has improved electrolytical resistance and stronger emulsification function is arranged.The thickener/emulsifier of wieldy liquid state, for example France's match commodity Sepiplus of BIC Corp 265.
Described component D is the ring-type dimethyl siloxane, it has the compatibility of height with many components in all kinds of cosmetics, reduce greasy feeling in the prescription, make cosolvency, solid powder dispersant, gentle light, smooth tender, be used for light cream frost, emulsion, cleansing milk, astringent, color make-up, shampoo water.Make hair increase gloss, significantly improve cardability, noresidue deposition, for example the commodity DC345 of Dow corning company.
Described component E is dimethicone/ring penta dimethyl-silicon oleogel, form by the polydimethylsiloxane of mass percent 45.0~50.0wt%, ring penta siloxanes of 36.0~42.0wt% and the GRANSIL GCM-5 of 12.0~16.0wt%, be that the spongy dimethyl siloxane crosslinked spherical powder that will have oily swelling character is scattered in dimethicone and ring penta dimethicone is prepared from, can be applicable to the color make-up prescription as face's fat absorption agent, reach inferior light, smoothly with the appearance of not having oil.It shows similar smooth silica flour, can give the unusual silk of skin sliding skin sense, can add essence or directly uses as the skin protection finished product, or composite with other active matters, as vitamin, antibacterial, cholesterol or sunscreen etc., for example poly-commodity Gransil DMCM-5 of trade Co., Ltd of Guangzhou connection.
Described component F is lock hydromagnetic stone, can close with the epsilon-amino Suan Guan Neng Ji Knot in the cutin, bring into play powerful hydration and reach long-acting moisture-keeping function, even the water flushing is flush away easily, just as Magnetitum firmly is incorporated into skin surface, its another group is then brought into play powerful hydration, prevent that moisture content scatters and disappears, and, dynamically keep the water balance of skin, for example the lock hydromagnetic stone of Switzerland Pan Defa company from the external environment suction.
Described component G is the three kind of plant extracts of scutellariae,radix, Glycyrrhiza glabra L. root and Fructus Jujubae fruit, be prepared according to following step: at first with quality such as scutellariae,radix, Glycyrrhiza glabra L. root and Fructus Jujubae fruit put in the reactor, add sterile deionized water to the submergence material, soak and remove impurity after 1-3 hour, add the sterile deionized water that material gross mass 8-10 doubly measures again, heat boil 2-4 hour after, discharging is also filtered, and obtains plant extract.
Described component H is a Tricholoma matsutake (lto et lmai) Singer extract, be prepared according to following step: at first Tricholoma matsutake (lto et lmai) Singer is put in the reactor, add sterile deionized water to the submergence Tricholoma matsutake (lto et lmai) Singer, soak and remove impurity after 1-3 hour, add the sterile deionized water that Tricholoma matsutake (lto et lmai) Singer gross mass 8-10 doubly measures again, heat boil 2-4 hour after, discharging is also filtered, and obtains Tricholoma matsutake (lto et lmai) Singer extract.
Described component I is bisabolol, ginger-root extract, aspect the skin that the reduction product stimulates, reparation has inflammation damnification effect preferably being arranged, is used in the sunscreen product, can reduce the injury of ultraviolet to skin effectively; Be used in the product for resolving poxes, can alleviate the acne of skin; In the flush away product, skin there is certain tack, sustainable performance effect, the commodity SymRelief of place of production Germany Symrise (fragrant quick relaxing) for example, oil-soluble is pale yellow to light brown liquid.
Described component J be the methyl isothiazolone (with) iodine propilolic alcohol butyl mephenesin Carbamate, i.e. the Microcare MTI of ACTI-ch em company, it is dissolved in the water preparation system fully, does not need to use the solubilizing agent solubilising, non-volatile formaldehyde is fine to the mycete antiseptic effect.
Described essence is selected food stage essence W1005238.
A kind of method for preparing the skin whitening lotion of the present invention, carry out according to following step:
(1) deionized water is put into the vacuum emulsification still, add triethanolamine, hyaluronate sodium, sodium metabisulfite, methyl propanediol, endecatylene acyl group phenylalanine, component F, essence, citric acid again, after being uniformly dispersed, extracting vacuum is warming up to 80-90 ℃ simultaneously to 5-10Pa;
(2) component A, B component, hydrolecithin, hydrogenated polydecene, plant sterol isostearate, Ascorbyl Tetraisopalmitate, component C, component D, polydimethylsiloxane, component E, component J are put into the oil phase still, be warming up to 80-90 ℃;
(3) oil phase component after step (2) preparation is sucked in the vacuum emulsification still, and keep 5-10Pa;
(4) the vacuum emulsification temperature in the kettle is cooled to 40-45 ℃, adds component G, component H, component I, and keep 5-10Pa;
When (5) treating that mixture temperature is reduced to 36-38 ℃ naturally in the emulsion reactor, discharging is also filtered, and promptly gets skin whitening lotion of the present invention.
In the described step (1), be warming up to 80-85 ℃.
In the described step (1), extracting vacuum is to 5-10Pa.
In the described step (2), be warming up to 80-85 ℃.
In described step (3) and (4), pressure maintains 5-8Pa.
Compared with prior art, technical scheme of the present invention is concentrated the elite of several plant composition, and collection is isolated, and whitens, the triple effect of preserving moisture unification, skin care, the colour of skin is adjusted in moisturizing comprehensively, keep skin health, strengthen skin elasticity, make skin present natural gloss again, can isolate the infringement to skin such as extraneous in the daytime various dirts and radiation simultaneously.Except that the above-mentioned component of having made description, also have:
1. Ascorbyl Tetraisopalmitate, oil-soluble VC as a kind of uniqueness, can suppress intracellular tyrosine enzyme and melanin generates. antioxidation, remove free radical, reduce cell and DNA damage that UV brings, prevent greasy peroxidating and skin aging, have outstanding heat and oxidation stability, can recover cytoactive.
2. undecanoyl phenylalanine; as a kind of melanin inhibitor; can promote skin to be converted into normal chromogenesis; prevent that melanin from forming; warp is to the Asia tuerculoderma; every day is with 2 times; through 3 months, measure glossiness before using and with the back, effect shows very good; can remedy the single deficiency of traditional whitening agent action pathway; effect more obviously with lasting, has multiple whitening function simultaneously, and skin is whitened at many levels; antagonism produces melanic a plurality of links, can suppress melanin comprehensively and generate.
3. Tricholoma matsutake (lto et lmai) Singer extract, use as the whitening anti-wrinkling concentrating agents,, established melanin is converted into the light black element directly at the melanin effect that has generated, the melanin generation that suppresses new of comparing needs a physiological period, the fast and safety of whitening and speckle dispelling speed.
The specific embodiment
Further specify technical scheme of the present invention below in conjunction with specific embodiment.
In an embodiment of the present invention, component A is acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, adopts the commodity ULRVEZ-21 of the sharp biochemical industry company limited in sky, Beijing.B component is the copolymer of PEG and PPG, adopts PEG/PPG-17/6 copolymer 75H-450.Component C is the mixture of ammonium acrylate/acrylamide copolymer, polyisobutylene and polysorbas20, adopts the France match commodity Sepiplus of BIC Corp 265.Component D is the ring-type dimethyl siloxane, adopts the commodity DC345 of Dow corning company.Component E is dimethicone/ring penta dimethyl-silicon oleogel, adopts the poly-commodity Gransil DMCM-5 of trade Co., Ltd of Guangzhou connection.Component F is the lock hydromagnetic stone of Switzerland Pan Defa company.Component G is the three kind of plant extracts of scutellariae,radix, Glycyrrhiza glabra L. root and Fructus Jujubae fruit, be prepared according to following step: at first with quality such as scutellariae,radix, Glycyrrhiza glabra L. root and Fructus Jujubae fruit put in the reactor, add sterile deionized water to the submergence material, soak and remove impurity after 1-3 hour, add the sterile deionized water that material gross mass 8-10 doubly measures again, heat boil 2-4 hour after, discharging is also filtered, and obtains plant extract.Component H is a Tricholoma matsutake (lto et lmai) Singer extract, be prepared according to following step: at first Tricholoma matsutake (lto et lmai) Singer is put in the reactor, add sterile deionized water to the submergence Tricholoma matsutake (lto et lmai) Singer, soak and remove impurity after 1-3 hour, add the sterile deionized water that Tricholoma matsutake (lto et lmai) Singer gross mass 8-10 doubly measures again, heat boil 2-4 hour after, discharging is also filtered, and obtains Tricholoma matsutake (lto et lmai) Singer extract.Component I is bisabolol, ginger-root extract, adopts the commodity SymRelief (fragrant quick relaxing) of place of production Germany Symrise, and oil-soluble is pale yellow to light brown liquid.Component J is the Microcare MTI of ACTI-chem company.The quality sum of each component is 100kg.
Embodiment 1
(1) deionized water (promptly the quality that deducts behind all the other constituent masses with 100kg takes by weighing) is put into the vacuum emulsification still, add triethanolamine 0.025kg, hyaluronate sodium 0.2kg, sodium metabisulfite 0.5kg, methyl propanediol 2kg, endecatylene acyl group phenylalanine 0.08kg, component F 6kg, essence 0.05kg, citric acid 0.05kg again, after being uniformly dispersed, extracting vacuum is warming up to 80 ℃ simultaneously to 5Pa;
(2) component A 0.3kg, B component 1kg, hydrolecithin 0.5kg, hydrogenated polydecene 4kg, plant sterol isostearate 0.1kg, Ascorbyl Tetraisopalmitate 1kg, component C 1kg, component D 1kg, polydimethylsiloxane 1kg, component E 1.5kg, component J 0.05kg are put into the oil phase still, be warming up to 80 ℃;
(3) oil phase component after step (2) preparation is sucked in the vacuum emulsification still, and keep 5Pa;
(4) the vacuum emulsification temperature in the kettle is cooled to 45 ℃, adds component G 3kg, component H 0.2kg, component I 1kg, and keep 5Pa;
When (5) treating that mixture temperature is reduced to 38 ℃ naturally in the emulsion reactor, discharging is also filtered, and promptly gets skin whitening lotion sample 1 of the present invention.
Embodiment 2
(1) deionized water (promptly the quality that deducts behind all the other constituent masses with 100kg takes by weighing) is put into the vacuum emulsification still, add triethanolamine 0.4kg, hyaluronate sodium 0.005kg, sodium metabisulfite 0.2kg, methyl propanediol 5kg, endecatylene acyl group phenylalanine 0.03kg, component F 2kg, essence 0.1kg, citric acid 0.01kg again, after being uniformly dispersed, extracting vacuum is warming up to 90 ℃ simultaneously to 8Pa;
(2) component A 0.1kg, B component 0.5kg, hydrolecithin 1.5kg, hydrogenated polydecene 1kg, plant sterol isostearate 0.5kg, Ascorbyl Tetraisopalmitate 4kg, component C 3kg, component D 3kg, polydimethylsiloxane 3kg, component E 0.5kg, component J 0.1kg are put into the oil phase still, be warming up to 90 ℃;
(3) oil phase component after step (2) preparation is sucked in the vacuum emulsification still, and keep 8Pa;
(4) the vacuum emulsification temperature in the kettle is cooled to 40 ℃, adds component G 0.5kg, component H 1kg, component I 0.1kg, and keep 8Pa;
When (5) treating that mixture temperature is reduced to 36 ℃ naturally in the emulsion reactor, discharging is also filtered, and promptly gets skin whitening lotion sample 2 of the present invention.
Embodiment 3
(1) deionized water (promptly the quality that deducts behind all the other constituent masses with 100kg takes by weighing) is put into the vacuum emulsification still, add triethanolamine 0.3kg, hyaluronate sodium 0.015kg, sodium metabisulfite 0.3kg, methyl propanediol 4kg, endecatylene acyl group phenylalanine 0.06kg, component F 4kg, essence 0.08kg, citric acid 0.02kg again, after being uniformly dispersed, extracting vacuum is warming up to 85 ℃ simultaneously to 10Pa;
(2) component A 0.2kg, B component 0.8kg, hydrolecithin 1kg, hydrogenated polydecene 3kg, plant sterol isostearate 0.3kg, Ascorbyl Tetraisopalmitate 2kg, component C 2kg, component D 2kg, polydimethylsiloxane 2kg, component E 1kg, component J 0.08kg are put into the oil phase still, be warming up to 85 ℃;
(3) oil phase component after step (2) preparation is sucked in the vacuum emulsification still, and keep 10Pa;
(4) the vacuum emulsification temperature in the kettle is cooled to 42 ℃, adds component G 2kg, component H 0.5kg, component I 0.8kg, and keep 10Pa;
When (5) treating that mixture temperature is reduced to 38 ℃ naturally in the emulsion reactor, discharging is also filtered, and promptly gets skin whitening lotion sample 3 of the present invention.
Embodiment 4
(1) deionized water (promptly the quality that deducts behind all the other constituent masses with 100kg takes by weighing) is put into the vacuum emulsification still, add triethanolamine 0.3kg, hyaluronate sodium 0.01kg, sodium metabisulfite 0.4kg, methyl propanediol 4kg, endecatylene acyl group phenylalanine 0.06kg, component F 4kg, essence 0.08kg, citric acid 0.02kg again, after being uniformly dispersed, extracting vacuum is warming up to 90 ℃ simultaneously to 10Pa;
(2) component A 0.2kg, B component 0.8kg, hydrolecithin 1kg, hydrogenated polydecene 3kg, plant sterol isostearate 0.3kg, Ascorbyl Tetraisopalmitate 3kg, component C 2kg, component D 2kg, polydimethylsiloxane 2kg, component E 1kg, component J 0.08kg are put into the oil phase still, be warming up to 90 ℃;
(3) oil phase component after step (2) preparation is sucked in the vacuum emulsification still, and keep 5Pa;
(4) the vacuum emulsification temperature in the kettle is cooled to 40 ℃, adds component G 2kg, component H 0.5kg, component I 0.8kg, and keep 5Pa;
When (5) treating that mixture temperature is reduced to 36 ℃ naturally in the emulsion reactor, discharging is also filtered, and promptly gets skin whitening lotion sample 4 of the present invention.
Embodiment 5
(1) deionized water (promptly the quality that deducts behind all the other constituent masses with 100kg takes by weighing) is put into the vacuum emulsification still, add triethanolamine 0.35kg, hyaluronate sodium 0.2kg, sodium metabisulfite 0.4kg, methyl propanediol 4kg, endecatylene acyl group phenylalanine 0.06kg, component F 4kg, essence 0.07kg, citric acid 0.02kg again, after being uniformly dispersed, extracting vacuum is warming up to 80 ℃ simultaneously to 5Pa;
(2) component A 0.3kg, B component 0.8kg, hydrolecithin 1.2kg, hydrogenated polydecene 3kg, plant sterol isostearate 0.4kg, Ascorbyl Tetraisopalmitate 3kg, component C 1.5kg, component D 1.5kg, polydimethylsiloxane 2.5kg, component E 1kg, component J 0.08kg are put into the oil phase still, be warming up to 80 ℃;
(3) oil phase component after step (2) preparation is sucked in the vacuum emulsification still, and keep 5Pa;
(4) the vacuum emulsification temperature in the kettle is cooled to 45 ℃, adds component G 2kg, component H 0.5kg, component I 0.5kg, and keep 5Pa;
When (5) treating that mixture temperature is reduced to 38 ℃ naturally in the emulsion reactor, discharging is also filtered, and promptly gets skin whitening lotion sample 5 of the present invention.
Embodiment 6
(1) deionized water (promptly the quality that deducts behind all the other constituent masses with 100kg takes by weighing) is put into the vacuum emulsification still, add triethanolamine 0.3kg, hyaluronate sodium 0.008kg, sodium metabisulfite 0.5kg, methyl propanediol 3kg, endecatylene acyl group phenylalanine 0.07kg, component F 5kg, essence 0.05kg, citric acid 0.02kg again, after being uniformly dispersed, extracting vacuum is warming up to 82 ℃ simultaneously to 8Pa;
(2) component A 0.3kg, B component 0.8kg, hydrolecithin 1.5kg, hydrogenated polydecene 3kg, plant sterol isostearate 0.5kg, Ascorbyl Tetraisopalmitate 2kg, component C 2kg, component D 2kg, polydimethylsiloxane 2kg, component E 1.5kg, component J 0.6kg are put into the oil phase still, be warming up to 82 ℃;
(3) oil phase component after step (2) preparation is sucked in the vacuum emulsification still, and keep 8Pa;
(4) the vacuum emulsification temperature in the kettle is cooled to 42 ℃, adds component G 2.5kg, component H 1kg, component I 0.3kg, and keep 8Pa;
When (5) treating that mixture temperature is reduced to 36 ℃ naturally in the emulsion reactor, discharging is also filtered, and promptly gets skin whitening lotion sample 6 of the present invention.
Embodiment 7
(1) deionized water (promptly the quality that deducts behind all the other constituent masses with 100kg takes by weighing) is put into the vacuum emulsification still, add triethanolamine 0.025kg, hyaluronate sodium 0.01kg, sodium metabisulfite 0.4kg, methyl propanediol 5kg, endecatylene acyl group phenylalanine 0.05kg, component F 5kg, essence 0.08kg, citric acid 0.02kg again, after being uniformly dispersed, extracting vacuum is warming up to 85 ℃ simultaneously to 10Pa;
(2) component A 0.2kg, B component 0.8kg, hydrolecithin 1kg, hydrogenated polydecene 3kg, plant sterol isostearate 0.3kg, Ascorbyl Tetraisopalmitate 2.5kg, component C 2kg, component D 3kg, polydimethylsiloxane 1kg, component E 0.5kg, component J 0.1kg are put into the oil phase still, be warming up to 85 ℃;
(3) oil phase component after step (2) preparation is sucked in the vacuum emulsification still, and keep 10Pa;
(4) the vacuum emulsification temperature in the kettle is cooled to 42 ℃, adds component G 1kg, component H 0.5kg, component I 0.8kg, and keep 10Pa;
When (5) treating that mixture temperature is reduced to 38 ℃ naturally in the emulsion reactor, discharging is also filtered, and promptly gets skin whitening lotion sample 7 of the present invention.
Investigate the whiten action effect of sample 1-7 of skin of the present invention, the personnel that choose 50 all ages and classes use, and life cycle is fortnight, and 99% user is good to above-mentioned sample performance, and effectively skin protection and whitening of sample comprehensively solves skin problem.
More than the present invention has been done exemplary description; should be noted that; under the situation that does not break away from core of the present invention, the replacement that is equal to that any simple distortion, modification or other those skilled in the art can not spend creative work all falls into protection scope of the present invention.