CN103191040B - Night cream and preparation method thereof - Google Patents
Night cream and preparation method thereof Download PDFInfo
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- CN103191040B CN103191040B CN201310129305.8A CN201310129305A CN103191040B CN 103191040 B CN103191040 B CN 103191040B CN 201310129305 A CN201310129305 A CN 201310129305A CN 103191040 B CN103191040 B CN 103191040B
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Abstract
The invention provides night cream containing lavender essential oil, white oil, glycerin, silicone oil, an amino acid moisturizing agent, isopropyl palmitate, a mixture of caprylic triglyceride and capric triglyceride, monostearin, triethanolamine, mixed alcohol, bisabolol, allantoin, vitamin E, sep-305, arbutin, propyl ester, methyl ester, EDTA-2Na, an emulsifying agent, a thickener, a preservative and water. The night cream provided by the invention has the good functions of whitening, repairing, preventing acnes, calming nerves and promoting sleep.
Description
Technical field
The present invention relates to daily skincare product technical field, be specifically related to a kind of late frost and preparation method thereof.
Background technology
Late frost, referred to for night, to the skin-protection product that daytime, impaired skin carried out conditioning at night, maintenance.In general late frost, active component content is higher, and quality is also more moist.
Current late frost only plays some and moistens and whitening functions, but current many people are by acne and bad puzzlement of sleep, need a pre-anti-acne, repair skin and can play calm the nerves, the product of whitening function.
Summary of the invention
The invention solves late frost of the prior art only can play and moisten whitening function and the technical problem of anti-acne, the hypnotic of cannot calming the nerves in advance.
The invention provides a kind of late frost, in described late frost, contain following component:
Herba Lysimachiae foenum-graeci quintessence oil 0.2-1wt%;
White oil 2-6wt%;
Glycerol 4-7wt%;
Silicone oil 2-5wt%;
Amino acid humectant 1.5-2wt%;
Isopropyl palmitate 2.3-2.7wt%;
The mixture 2.5-3.5wt% of Trivent OCG and tricaprin;
Monoglyceride 1-2wt%;
Triethanolamine 0.15-0.2wt%;
Mixed alcohol 1-2wt%;
Bisabolol 0.3-0.6wt%;
Allantoin 0.2-0.3wt%;
Vitamin E 0.2-0.3wt%;
sep-305 0.5-1.5wt％；
Arbutin 1-4wt%;
Propyl ester 0.05-0.15wt%;
Methyl ester 0.1-0.2wt%;
EDTA-2Na 0.05-0.15wt％；
Emulsifying agent 2-3wt%;
Thickening agent 0.1-0.2wt%;
Antiseptic 0.1-0.2wt%;
Water 60-70wt%.
As a further improvement on the present invention, the squalane that also contains 2-6wt% in described late frost.
As a further improvement on the present invention, the Vc phosphate ester sodium that also contains 0.1-0.3wt% in described late frost.
As a further improvement on the present invention, the hyaluronate sodium that also contains 0.05-0.15wt% in described late frost.
As a further improvement on the present invention, described emulsifying agent is polyhydroxyalkanoate derivant.
As a further improvement on the present invention, described thickening agent is carbomer.
As a further improvement on the present invention, described antiseptic is IS45.
As a further improvement on the present invention, consisting of of described late frost:
Herba Lysimachiae foenum-graeci quintessence oil 0.6wt%;
White oil 4.5wt%;
Glycerol 6wt%;
Silicone oil 3wt%;
Amino acid humectant 2wt%;
Isopropyl palmitate 2.5wt%;
The mixture 3wt% of Trivent OCG and tricaprin;
Vc phosphate ester sodium 0.2wt%;
Monoglyceride 1.5wt%;
Triethanolamine 0.15wt%;
Mixed alcohol 1.5wt%;
Bisabolol 0.5wt%;
Hyaluronate sodium 0.1wt%;
Allantoin 0.25wt%;
Vitamin E 0.25wt%;
Sep-305 1wt％；
Arbutin 2.8wt%;
Propyl ester 0.1wt%;
Methyl ester 0.15wt%;
EDTA-2Na 0.1wt％；
Polyhydroxyalkanoate derivant 2.5wt%;
Carbomer 0.15wt%;
IS 45 0.15wt％；
Water 64wt%.
The present invention also provides the preparation method of described late frost, comprise in proportion by the oil phase component in late frost, water component difference mix homogeneously, then oil phase component is mixed with water component, and add emulsifying agent to carry out emulsifying, add again thickening agent, finally add Herba Lysimachiae foenum-graeci quintessence oil, antiseptic, triethanolamine and sep305, mix homogeneously; Wherein, described oil phase component comprises mixture, monoglyceride, mixed alcohol, bisabolol, vitamin E, arbutin, propyl ester and the methyl ester of white oil, silicone oil, isopropyl palmitate, Trivent OCG and tricaprin, and water component comprises glycerol, amino acid humectant, allantoin, EDTA-2Na and water.
As a further improvement on the present invention,, described oil phase component also comprises squalane and Vc phosphate ester sodium, described water component also comprises hyaluronate sodium.
Late frost provided by the invention and preparation method thereof, the various whitening night cream in compared to existing technology, have the following advantages:
1, in late frost provided by the invention, contain Herba Lysimachiae foenum-graeci quintessence oil, can play cleaning skin, control oil content, pre-anti-acne, the effect of the hypnotic of calming the nerves.
2, in late frost provided by the invention, contain arbutin composition, can play and accelerate melanic decomposition and excretion, thereby reduce Skin pigmentation, dispelling stain and freckle also have the effect of sterilization, antiinflammatory simultaneously.
3, in late frost provided by the invention, by the kind of various active components and content are suitably selected, make to adopt the late frost that the present invention forms can play pre-anti-acne, repair the effect of skin and whitening, reach the effect of whitening reparation, pre-anti-acne, the hypnotic of calming the nerves.
4, the preparation method technique of late frost provided by the invention is simple, easy operating.
The specific embodiment
The invention provides a kind of late frost, in described late frost, contain following component:
Herba Lysimachiae foenum-graeci quintessence oil 0.2-1wt%;
White oil 2-6wt%;
Glycerol 4-7wt%;
Silicone oil 2-5wt%;
Amino acid humectant 1.5-2wt%;
Isopropyl palmitate 2.3-2.7wt%;
The mixture 2.5-3.5wt% of Trivent OCG and tricaprin;
Monoglyceride 1-2wt%;
Triethanolamine 0.15-0.2wt%;
Mixed alcohol 1-2wt%;
Bisabolol 0.3-0.6wt%;
Allantoin 0.2-0.3wt%;
Vitamin E 0.2-0.3wt%;
sep-305 0.5-1.5wt％；
Arbutin 1-4wt%;
Propyl ester 0.05-0.15wt%;
Methyl ester 0.1-0.2wt%;
EDTA-2Na 0.05-0.15wt％；
Emulsifying agent 2-3wt%;
Thickening agent 0.1-0.2wt%;
Antiseptic 0.1-0.2wt%;
Water 60-70wt%.
In late frost provided by the invention, by the kind of various active components and content are suitably selected, make to adopt the late frost that the present invention forms can play pre-anti-acne, repair the effect of skin and whitening, reach the effect of whitening reparation, pre-anti-acne, the hypnotic of calming the nerves.
Particularly, inventor finds, in late frost of the present invention, adopts Herba Lysimachiae foenum-graeci quintessence oil, can play cleaning skin, control oil content, pre-anti-acne, the effect of the hypnotic of calming the nerves.Under preferable case, described Herba Lysimachiae foenum-graeci quintessence oil adopts pure natural without the pure quintessence oil adding, and by lavandula angustifolia, is directly refined and obtains, and must not contain the materials such as Camphora.
In addition, in the present invention, bisabolol preferably adopts oil-soluble bisabolol, and it can be dispersed in oil phase, is convenient to the dispersed of follow-up and other components.Wherein, sep-305 is polyacrylamide and polyethyleneglycol diacrylate.In the present invention, mixed alcohol refers to the mixture of 16 natural fatty alcohols (abbreviation hexadecanol) and 18 natural fatty alcohols (abbreviation octadecanol), and its mass ratio is 3: 7.In addition, in the present invention, in the mixture of Trivent OCG and tricaprin, the mass ratio of Trivent OCG and tricaprin is 56.3: 43.4.
In late frost provided by the invention, contain arbutin composition, can play and accelerate melanic decomposition and excretion, thereby reduce Skin pigmentation, dispelling stain and freckle also have the effect of sterilization, antiinflammatory simultaneously.
As a kind of preferred implementation of the present invention, in described late frost, also contain squalane.Inventor's discovery, squalane can be strengthened maintenance epidermis, effectively forms natural protecting film, helps the balance between skin and sebum.Meanwhile, squalane is a kind of lipid that approaches the most human body sebum, and affinity is strong, can combine together with mankind itself's sebum film, at skin surface, forms the natural barrier of one deck.In addition, squalane can also suppress the peroxidating of skin lipid, can effectively infiltrate through skin, and promotes the propagation of skin base cell, and to delay skin aging, improving and eliminating chloasma all has obvious physiologic effect.Finally, squalane also can make skin pore open, and promotes blood microcirculation, promotes the metabolism of cell, helps to repair damaged cell.More preferably in situation, the gross mass of described late frost of take is benchmark, and wherein the content of squalane is 2-6wt%, but is not limited to this.
As another kind of preferred implementation of the present invention, in described late frost, also contain Vc phosphate ester sodium, it has anti-radical action, can suppress lipids peroxidating and aging, thereby reaches antidotal effect; Promote recovery and the generation of skin elasticity albumen and collagen protein simultaneously, make skin maintenance, the vigor of renewing one's youth.More preferably in situation, the gross mass of described late frost of take is benchmark, and wherein the content of Vc phosphate ester sodium is 0.1-0.3wt%, but is not limited to this.
In addition, as a kind of preferred implementation of the present invention, in described late frost, also can contain the hyaluronic acid of 0.05-0.15wt%.Hyaluronic acid is the bio-molecules extensively existing in skin and other tissue, has fabulous moisture-keeping function, is called in the world desirable nature moisturizing factor (Natural MolsturlZlng Factor, NMF).It is the best material of used for cosmetic performance of keeping humidity that current occurring in nature is found.
In the present invention, described emulsifying agent is the various emulsifying agents that those skilled in the art commonly use, and is convenient to oil-based system in late frost and mixes with the even of aqueous phase system.For example, described emulsifying agent can adopt various common surfactants, preferably adopts polyhydroxyalkanoate derivant, but is not limited to this.
Acting as of described thickening agent is conventionally known to one of skill in the art, for regulation system viscosity to OK range.In the present invention, described thickening agent can adopt carbomer, but is not limited to this.
Described antiseptic is various antiseptic common in prior art, for example, can be IS45.IS45 is a kind of preservative blends, is the mixture of propylene glycol, two imidazolidinyl urea, methyl hydroxybenzoate and propylparaben.
As a kind of preferred forms of the present invention, the consisting of of described late frost:
Herba Lysimachiae foenum-graeci quintessence oil 0.6wt%;
White oil 4.5wt%;
Glycerol 6wt%;
Silicone oil 3wt%;
Amino acid humectant 2wt%;
Isopropyl palmitate 2.5wt%;
The mixture 3wt% of Trivent OCG and tricaprin;
Vc phosphate ester sodium 0.2wt%;
Monoglyceride 1.5wt%;
Triethanolamine 0.15wt%;
Mixed alcohol 1.5wt%;
Bisabolol 0.5wt%
Hyaluronate sodium 0.1wt%;
Allantoin 0.25wt%;
Vitamin E 0.25wt%;
Sep-305 1wt％；
Arbutin 2.8wt%;
Propyl ester 0.1wt%;
Methyl ester 0.15wt%;
EDTA-2Na 0.1wt％；
Polyhydroxyalkanoate derivant 2.5wt%;
Carbomer 0.15wt%;
IS 45 0.15wt％；
Water 64wt%.
The present invention also provides the preparation method of described late frost, comprise in proportion by the oil phase component in late frost, water component difference mix homogeneously, then oil phase component is mixed with water component, and add emulsifying agent to carry out emulsifying, add again thickening agent, finally add Herba Lysimachiae foenum-graeci quintessence oil, antiseptic, triethanolamine and sep305, mix homogeneously.The preparation method technique of late frost provided by the invention is simple, easy operating.
Wherein, described oil phase component comprises mixture, monoglyceride, mixed alcohol, bisabolol, vitamin E, arbutin, propyl ester and the methyl ester of white oil, silicone oil, isopropyl palmitate, Trivent OCG and tricaprin, and water component comprises glycerol, amino acid humectant, allantoin, EDTA-2Na and water.
Under preferable case, described oil phase component also comprises squalane and Vc phosphate ester sodium, and described water component also comprises hyaluronate sodium.
Wherein, when oil phase component, water component are mixed respectively, it carries out respectively in corresponding oil phase pot, water pot.For each component energy mix homogeneously in guarantee system, it all can carry out under heating condition, for example, can at 75-80 ℃, be incubated 10min, is convenient to the dispersed and sterilizing of each component.
Under preferable case, then when oil phase component is mixed with water component, first by the water suction emulsifying pot of 3/4 volume, and open stirring at low speed, simultaneously by oil phase component suction emulsifying pot, and add emulsifying agent, the more remaining 1/4 volume water of suction; Stop stirring, open homogenizer, homogenizing 5-10min, opens middling speed again and stirs after finishing, insulation 15min; After being cooled to 65 ℃, add thickening agent, continue homogenizing 2-5min, add Herba Lysimachiae foenum-graeci quintessence oil, antiseptic, triethanolamine and sep305 while continuing to be cooled to 45 ℃, after mix homogeneously, at 38 ℃, sampling detects OK, obtains late frost provided by the invention.
Late frost provided by the invention, multiple natural effective composition is effectively combined, it is very easy to use, directly this late frost is evenly spread upon on the face at night after cleaning skin, has reduced night because use loaded down with trivial details step and the time of multiple cosmetics skin protection.
In order to make technical problem solved by the invention, technical scheme and beneficial effect clearer, below in conjunction with specific embodiment, the present invention is further elaborated.Should be appreciated that specific embodiment described herein, only in order to explain the present invention, is not intended to limit the present invention.Embodiment is that in comparative example, the raw material that adopts is all commercially available, and the present invention is not particularly limited.
Embodiment 1
(1) raw material forms (quality percentage composition): water-64%, white oil-4.5%, Herba Lysimachiae foenum-graeci quintessence oil-0.6%, glycerol-6%, silicone oil-3%, squalane-3%, amino acid humectant-2%, isopropyl palmitate-2.5%, mixture-3% of Trivent OCG and tricaprin, Vc phosphate ester sodium-0.2%, monoglyceride-1.5%, triethanolamine-0.15%, mixed alcohol-1.5%, polyhydroxyalkanoate derivant-2.5%, bisabolol-0.5%, sodium hyaluronate-0.1%, allantoin-0.25%, carbomer-0.15%, vitamin e-0.25%, sep-305-1%, arbutin-2.8%, propyl ester-0.1%, methyl ester-0.15%, EDTA-2Na-0.1%, IS45-0.15%.
(2) according to said ratio, first white oil, silicone oil, isopropyl palmitate, Trivent OCG are mixed with mixture, monoglyceride, mixed alcohol, bisabolol, vitamin E, arbutin, propyl ester and the methyl ester of tricaprin, and be incubated 10min at 75-80 ℃, obtain oil phase component.Again glycerol, amino acid humectant, allantoin, EDTA-2Na and water are mixed, and be incubated 10min at 75-80 ℃, obtain water component.Then, first by the water component suction emulsifying pot of 3/4 volume, and open stirring at low speed, simultaneously by oil phase component suction emulsifying pot, and add emulsifying agent, the more remaining 1/4 volume water of suction; Stop stirring, open homogenizer, homogenizing 5-10min, opens middling speed again and stirs after finishing, insulation 15min; After being cooled to 65 ℃, add thickening agent, continue homogenizing 2-5min, add Herba Lysimachiae foenum-graeci quintessence oil, antiseptic, triethanolamine and sep305 while continuing to be cooled to 45 ℃, after mix homogeneously, at 38 ℃, sampling detects OK, obtains the late frost of the present embodiment, is designated as S10.
Embodiment 2-7
According to the step identical with embodiment 1, prepare late frost S20-S70, difference, in step (1), raw material forms as shown in table 1.
Table 1
Comparative example 1
The late frost DS10 for preparing this comparative example according to the step identical with embodiment 1, difference, in step (1), raw material consists of (quality percentage composition): water-64%, white oil-4.5%, glycerol-6%, silicone oil-3.5%, squalane-3.1%, amino acid humectant-2%, isopropyl palmitate-2.5%, mixture-3% of Trivent OCG and tricaprin, Vc phosphate ester sodium-0.2%, monoglyceride-1.5%, triethanolamine-0.15%, mixed alcohol-1.5%, polyhydroxyalkanoate derivant-2.5%, bisabolol-0.5%, sodium hyaluronate-0.1%, allantoin-0.25, carbomer-0.15%, vitamin e-0.25, sep-305-1%, arbutin-2.8%, propyl ester-0.1%, methyl ester-0.15%, EDTA-2Na-0.1%, IS 45-0.15%.
Comparative example 2
The late frost DS20 for preparing this comparative example according to the step identical with embodiment 1, difference, in step (1), raw material consists of (quality percentage composition): water-64%, white oil-5%, Herba Lysimachiae foenum-graeci quintessence oil-0.6%, glycerol-6%, silicone oil-4%, squalane-4.3%, amino acid humectant-2%, isopropyl palmitate-2.5%, mixture-3% of Trivent OCG and tricaprin, Vc phosphate ester sodium-0.2%, monoglyceride-1.5%, triethanolamine-0.15%, mixed alcohol-1.5%, polyhydroxyalkanoate derivant-2.5%, bisabolol-0.5%, sodium hyaluronate-0.1%, allantoin-0.25, carbomer-0.15%, vitamin e-0.25, sep-305-1%, propyl ester-0.1%, methyl ester-0.15%, EDTA-2Na-0.1%, IS45-0.15%.
Performance test:
Adopt various late frost sample S10-S70 and DS10-DS20, offering 100 user tests, after cleaning skin, directly this late frost is evenly spread upon on the face at night, record the experiment efficiently individual quantity of hypnotic, whitening and speckle dispelling, pre-anti-acne effect.Test result is as shown in table 2.
Table 2
| Late frost sample | Hypnotic | Whitening and speckle dispelling | Pre-anti-acne |
| S10 | 87 | 80 | 88 |
| S20 | 92 | 93 | 97 |
| S30 | 85 | 84 | 85 |
| S40 | 86 | 83 | 87 |
| S50 | 83 | 88 | 89 |
| S60 | 82 | 85 | 88 |
| S70 | 87 | 80 | 83 |
| DS10 | 12 | 80 | 31 |
| DS20 | 89 | 28 | 90 |
From the test result of upper table 2, can find out, adopt late frost sample S10-S70 that method provided by the invention prepares to there is the effect of good whitening reparation, pre-anti-acne and the hypnotic of calming the nerves, obviously be better than the late frost sample DS10-DS20 of comparative example.
In addition, from the test result of embodiment 1-4 and embodiment 5-7, relatively can find out, while containing squalane, Vc phosphate ester sodium and hyaluronate sodium in late frost provided by the invention, its effect is better.
Above embodiment is only the preferred embodiment of the present invention, it should be pointed out that to those skilled in the art, and under the premise without departing from the principles of the invention, some improvement of having done, also should be considered as protection scope of the present invention.
Claims (7)
1. a late frost, is characterized in that, contains following component in described late frost:
Wherein:
Described emulsifying agent is polyhydroxyalkanoate derivant, and described thickening agent is carbomer;
Described antiseptic is IS45.
2. late frost according to claim 1, is characterized in that, also contains the squalane of 2-6wt% in described late frost.
3. late frost according to claim 1, is characterized in that, also contains the Vc phosphate ester sodium of 0.1-0.3wt% in described late frost.
4. late frost according to claim 1, is characterized in that, also contains the hyaluronate sodium of 0.05-0.15wt% in described late frost.
5. late frost according to claim 1, is characterized in that, the consisting of of described late frost:
6. the preparation method of late frost claimed in claim 1, it is characterized in that, comprise in proportion by the oil phase component in late frost, water component difference mix homogeneously, then oil phase component is mixed with water component, and add emulsifying agent to carry out emulsifying, add again thickening agent, finally add Herba Lysimachiae foenum-graeci quintessence oil, antiseptic, triethanolamine and sep305, mix homogeneously; Wherein, described oil phase component comprises mixture, monoglyceride, mixed alcohol, bisabolol, vitamin E, arbutin, propyl ester and the methyl ester of white oil, silicone oil, isopropyl palmitate, Trivent OCG and tricaprin, and water component comprises glycerol, amino acid humectant, allantoin, EDTA-2Na and water.
7. preparation method according to claim 6, is characterized in that, described oil phase component also comprises squalane and Vc phosphate ester sodium, and described water component also comprises hyaluronate sodium.
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| CN201310129305.8A CN103191040B (en) | 2013-04-15 | 2013-04-15 | Night cream and preparation method thereof |
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| CN201310129305.8A CN103191040B (en) | 2013-04-15 | 2013-04-15 | Night cream and preparation method thereof |
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Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104055712A (en) * | 2014-07-08 | 2014-09-24 | 广州千百度化妆品有限公司 | Cosmetic composition for preventing acne and preparation method thereof |
| CN104940222B (en) * | 2015-01-21 | 2018-10-19 | 长沙达瑞奇实业有限公司 | Prevent and treat the preparation method of the creme of hyperplastic scar |
| CN106619178A (en) * | 2016-11-26 | 2017-05-10 | 无锡市汉方八珍科技有限公司 | Cream used for whitening and preparation method thereof |
| CN107595744A (en) * | 2017-09-30 | 2018-01-19 | 广州凯淇化妆品有限公司 | A kind of folium artemisiae argyi conditioning essential oil dew and preparation method thereof |
| CN107822908B (en) * | 2017-11-13 | 2021-02-26 | 前海会喜科技(深圳)有限公司 | Fruit and vegetable essence facial massage cream and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102872224A (en) * | 2011-09-19 | 2013-01-16 | 徐柔云 | Externally-applied sleeping cream |
| CN103027867A (en) * | 2011-09-30 | 2013-04-10 | 天津市中科健新材料技术有限公司 | Finishing liquor applied on wet tissue and available for after-sun makeup removal and repair |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102872224A (en) * | 2011-09-19 | 2013-01-16 | 徐柔云 | Externally-applied sleeping cream |
| CN103027867A (en) * | 2011-09-30 | 2013-04-10 | 天津市中科健新材料技术有限公司 | Finishing liquor applied on wet tissue and available for after-sun makeup removal and repair |
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Effective date of registration: 20170125 Address after: No. two road 518000 Guangdong city of Shenzhen province Futian District Xiangmi Lake Street Han City Shop No. 2 Han Sheng Garden 7 semi basement 02 Patentee after: Shi Biman Science and Technology Ltd. of Shenzhen Address before: 518000 Guangdong city of Shenzhen province Futian District Fu Road Royal Tsui 25B-A Patentee before: Zhu Jianjiu |