CN104825377A - Formula and preparation method of water seepage emulsion - Google Patents

Formula and preparation method of water seepage emulsion Download PDF

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Publication number
CN104825377A
CN104825377A CN201510198842.7A CN201510198842A CN104825377A CN 104825377 A CN104825377 A CN 104825377A CN 201510198842 A CN201510198842 A CN 201510198842A CN 104825377 A CN104825377 A CN 104825377A
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China
Prior art keywords
formula
oil
caprylic
polydimethylsiloxane
emulsion
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Pending
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CN201510198842.7A
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Chinese (zh)
Inventor
琚建伟
刘勇
段毅鹏
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Shanghai Tong Yan Industrial Co Ltd
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Shanghai Tong Yan Industrial Co Ltd
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Priority to CN201510198842.7A priority Critical patent/CN104825377A/en
Publication of CN104825377A publication Critical patent/CN104825377A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a formula of a water seepage emulsion. The water seepage emulsion is composed of the following raw materials by weight: 1-15% of glycerin, 1-10% of butylene glycol, 1-10% of betaine, 1-5% of olive oil, 1-5% of jojoba oil, 1-5% of polydimethylsiloxane, 1-5% of caprylic/capric triglyceride, 0.01-1% silk protein glue, 0.5-5% of a snail extracted liquid, 0.01-0.5% of hyaluronic acid, and the balance water. The water seepage emulsion provided by the invention has the advantages that: 1. the product has very strong stringiness, can have obvious drawing effect and generating a lot of water drops simultaneously by taking a small amount of the emulsion to flap on hands or on the face; and 2. the product contains multiple moisturizing ingredients, and can achieve excellent moisturizing effect by release of the water drops produced by flapping.

Description

A kind of go out the formula and preparation method thereof of aqueous emulsion
Technical field
The present invention relates to a kind of formula of cosmetics, be specially a kind of go out the formula of aqueous emulsion, and the preparation method of this emulsion, belongs to daily use chemicals technical field.
Background technology
Along with the development of technology, various cosmetics emerge in an endless stream, and moisturizing class cosmetics are one of them, because it can be given skin moisturizing oil film, supplement the nutrient that lacks of skin, keep the softness of skin and elasticity and deeply welcomed by the people.Natural moisture preserving system in human body skin is primarily of water, lipid, nature moisturizing factor composition, and wherein lipid is apolar substance, can flow at intraor extracellular and iuntercellular by limiting moisture.At cell by basal layer in horny layer atomization, the content of lipid increases gradually, distribution also there occurs change, in granular layer, lipid aggregation is in lamellated granule, when Granulosa cells is converted into corneocyte, these lipids are discharged and are filled in intercellular substance, define the barrier preventing loss of moist.When a variety of causes causes lipid to lack, its water barrier action weakens, and the moisture run off through epidermis will increase, and causes xerosis cutis desquamation.Therefore the mechanism of action of moisture-keeping cosmetics generally shows: the oil film protective layer one, forming one deck closure at skin surface, reduces or stops moisture to evaporate from skin surface, making lower layers of skin diffuse to cuticular moisture and the further hydration of horny layer; Two, absorbing moisture from the external world makes skin keep moistening.But the moisturizing materials contained in these moisture-keeping cosmetics only rests on skin surface, keratodermatitis provides deep layer nourishing to skin can not be penetrated into, fundamentally do not solve skin and lack water problem, life-time service also can make skin become responsive, is unfavorable for skin health.
Summary of the invention
The object of the invention is in order to provide a kind of go out the formula of aqueous emulsion, to solve the problems referred to above of prior art.
Another object of the present invention be in order to provide this go out the preparation method of aqueous emulsion.
Object of the present invention realizes by following technical scheme:
Go out a formula for aqueous emulsion, be made up of the raw material of following weight percent meter:
1 ~ 15% glycerol, 1 ~ 10% butanediol, 1 ~ 10% betanin, 1 ~ 5% olive oil, 1 ~ 5% Jojoba oil, 1 ~ 5% polydimethylsiloxane, 1 ~ 5% caprylic/capric triglyceride, 0.01 ~ 1% silk gum albumen, 0.5 ~ 5% snail extract, 0.01 ~ 0.5% hyaluronic acid, add water to 100%.
Preferably, a kind of go out the formula of aqueous emulsion, be made up of the raw material of following weight percent meter:
8 ~ 12% glycerol, 4 ~ 6% butanediols, 4 ~ 6% betanins, 3 ~ 5% olive oil, 3 ~ 5% Jojoba oils, 1 ~ 3% polydimethylsiloxane, 1 ~ 3% caprylic/capric triglyceride, 0.1 ~ 1% silk gum albumen, 2 ~ 5% snail extracts, 0.01 ~ 0.1% hyaluronic acid, add water to 100%.
More typical proportioning is: 10% glycerol, 5% butanediol, 5% betanin, 5% olive oil, 3% Jojoba oil, 2% polydimethylsiloxane, 2% caprylic/capric triglyceride, 0.5% silk gum albumen, 3% snail extract, 0.1% hyaluronic acid, add water to 100%.
Above-mentioned go out the preparation method of aqueous emulsion, comprise the following steps:
1) each raw material is weighed by formula;
2) by olive oil, Jojoba oil, polydimethylsiloxane, caprylic/capric triglyceride mix and blend be heated to 70 DEG C ~ 85 DEG C and obtain oil mixture; Glycerol, butanediol, betanin and deionized water mix homogeneously are heated to 80 DEG C ~ 85 DEG C and obtain aqueous mixture;
3) aqueous mixture is added oil mixture high speed emulsifying homogeneous 5 to 10 minutes, continue to stir cooling;
4) emulsifying mixt is cooled to 40-45 DEG C, then adds snail extract, silk gum albumen, hyaluronic acid mix homogeneously; Continue stirring discharging in 10 to 20 minutes and obtain finished product.
In this product, glycerol, butanediol, betanin, hyaluronic acid are wetting agent, and olive oil, Jojoba oil, polydimethylsiloxane, caprylic/capric triglyceride are for moistening oils and fats, and silk gum albumen and snail extract produce wire drawing outlet effect.
Beneficial effect of the present invention is:
1, this product has very strong stringiness, take a morsel on hand or face pat, obvious wire-drawing effect can be had, produce a large amount of globule simultaneously;
2, this product contains multiple moisturizing ingredient, being discharged into skin, having fabulous moistening effect by patting the globule produced.
Detailed description of the invention
Technical characterstic of the present invention is set forth further below in conjunction with specific embodiment.
The embodiment of the present invention is prepared in accordance with the following methods:
1) each raw material is weighed by formula;
2) by olive oil, Jojoba oil, polydimethylsiloxane, caprylic/capric triglyceride mix and blend be heated to 70 DEG C ~ 85 DEG C and obtain oil mixture; Glycerol, butanediol, betanin and deionized water mix homogeneously are heated to 80 DEG C ~ 85 DEG C and obtain aqueous mixture;
3) aqueous mixture is added oil mixture high speed emulsifying homogeneous 5 to 10 minutes, continue to stir cooling;
4) emulsifying mixt is cooled to 40-45 DEG C, then adds snail extract, silk gum albumen, hyaluronic acid mix homogeneously; Continue stirring discharging in 10 to 20 minutes and obtain finished product.
The formula of embodiment 1-embodiment 6 is as follows:
Embodiment 1:
1% glycerol, 9% butanediol, 1% betanin, 5% olive oil, 5% Jojoba oil, 1% polydimethylsiloxane, 1% caprylic/capric triglyceride, 1% silk gum albumen, 0.5% snail extract, 0.05% hyaluronic acid, add water to 100%.
Embodiment 2:
15% glycerol, 1% butanediol, 1% betanin, 5% olive oil, 1% Jojoba oil, 5% polydimethylsiloxane, 5% caprylic/capric triglyceride, 0.01% silk gum albumen, 5% snail extract, 0.05% hyaluronic acid, add water to 100%.
Embodiment 3:
7% glycerol, 3% butanediol, 7% betanin, 2% olive oil, 2% Jojoba oil, 5% polydimethylsiloxane, 4% caprylic/capric triglyceride, 0.01% silk gum albumen, 1% snail extract, 0.1% hyaluronic acid, add water to 100%.
: embodiment 4:
8% glycerol, 4% butanediol, 4% betanin, 3% olive oil, 3% Jojoba oil, 1% polydimethylsiloxane, 1% caprylic/capric triglyceride, 0.1% silk gum albumen, 2% snail extract, 0.01% hyaluronic acid, add water to 100%.
Embodiment 5:
10% glycerol, 5% butanediol, 5% betanin, 5% olive oil, 3% Jojoba oil, 2% polydimethylsiloxane, 2% caprylic/capric triglyceride, 0.5% silk gum albumen, 3% snail extract, 0.1% hyaluronic acid, add water to 100%.
Embodiment 6:
12% glycerol, 6% butanediol, 6% betanin, 5% olive oil, 5% Jojoba oil, 3% polydimethylsiloxane, 3% caprylic/capric triglyceride, 1% silk gum albumen, 5% snail extract, 0.01% hyaluronic acid, add water to 100%.
Moisturizing is tested:
Extensively solicit volunteer on probation totally 50 examples, wherein male 20, women 30; The oldest 42 years old, minimum 15 years old, about 24 years old mean age.50 triers use of the present invention go out the aqueous emulsion indices of after 30 days, moisturizing being correlated with to improve the result of degree self evaluation as follows:
Increase skin moisture-keeping: have the trier of 56.1% (man) and 60% (female) have moderate to improve and obviously improve respectively;
Reduce pachylosis: have the trier of 67.5% (man) and 52.2% (female) have moderate to improve and obviously improve respectively;
Increase skin emolliency: have the trier of 51.5% (man) and 78.5% (female) have moderate to improve and obviously improve respectively;
Increase skin to moisten: have respectively 67.5% (man) and 70.5% trier have moderate to improve and obvious improvement;
As can be seen from the result of the self assessment of trier, this product is moistened to increasing skin, reduce pachylosis, is increased skin emolliency and increase the skin improvement of moistening in various degree.
Moisture-keeping efficacy is tested: moisture flow vector (TEWL) measures
Skin water loss amount (TEWL) (German Tewameter TM210), what TEWL embodied is skin barrier function, and TEWL is less, and skin barrier function is better.The numerical value of skin moisture loss TEWL to assessment skin beauty water skin moisture loss TEWL is lower.TEWL unit ghm -2.
Test group be experimenter position smear embodiment 5 go out aqueous emulsion.Take out aqueous emulsion 0.1 gram and be applied to experimenter's arm skin (about 1 square centimeter), before using and after use 30,60,90 and 120min, measure the moisture of skin windage of skin.Reference group is smeared for experimenter position and is dissolved aqueous emulsion with reference to product.After recipient site smears sample 30min, the percentage of water loss of test recipe test group is starkly lower than reference group; In test period 120min, the percentage of water loss of test group always lower than reference group, and is negative value always; Test group, compared with reference group, have instant lock water effect, and it is good to continue lock outlet capacity.
On probation by 50 people of different skin quality, without the situation of any zest and skin allergy.
In addition, other embodiments of the invention have also all carried out above-mentioned test, and achieve and the data of embodiment 5 with trend, and because length limit, the present invention will not enumerate.Above-mentioned test demonstrates compositions moistening effect of the present invention and is better than other formulation products of prior art.

Claims (4)

1. go out a formula for aqueous emulsion, it is characterized in that: be made up of the raw material of following weight percent meter:
1 ~ 15% glycerol, 1 ~ 10% butanediol, 1 ~ 10% betanin, 1 ~ 5% olive oil, 1 ~ 5% Jojoba oil, 1 ~ 5% polydimethylsiloxane, 1 ~ 5% caprylic/capric triglyceride, 0.01 ~ 1% silk gum albumen, 0.5 ~ 5% snail extract, 0.01 ~ 0.5% hyaluronic acid, add water to 100%.
2. according to claim 1 a kind of go out the formula of aqueous emulsion, it is characterized in that: be made up of the raw material of following weight percent meter:
8 ~ 12% glycerol, 4 ~ 6% butanediols, 4 ~ 6% betanins, 3 ~ 5% olive oil, 3 ~ 5% Jojoba oils, 1 ~ 3% polydimethylsiloxane, 1 ~ 3% caprylic/capric triglyceride, 0.1 ~ 1% silk gum albumen, 2 ~ 5% snail extracts, 0.01 ~ 0.1% hyaluronic acid, add water to 100%.
3. according to claim 1 a kind of go out the formula of aqueous emulsion, it is characterized in that: be made up of the raw material of following weight percent meter: 10% glycerol, 5% butanediol, 5% betanin, 5% olive oil, 3% Jojoba oil, 2% polydimethylsiloxane, 2% caprylic/capric triglyceride, 0.5% silk gum albumen, 3% snail extract, 0.1% hyaluronic acid, add water to 100%.
4. claim 1-3 one of any described in go out the preparation method of aqueous emulsion, it is characterized in that: comprise the following steps:
1) each raw material is weighed by formula;
2) by olive oil, Jojoba oil, polydimethylsiloxane, caprylic/capric triglyceride mix and blend be heated to 70 DEG C ~ 85 DEG C and obtain oil mixture; Glycerol, butanediol, betanin and deionized water mix homogeneously are heated to 80 DEG C ~ 85 DEG C and obtain aqueous mixture;
3) aqueous mixture is added oil mixture high speed emulsifying homogeneous 5 to 10 minutes, continue to stir cooling;
4) emulsifying mixt is cooled to 40-45 DEG C, then adds snail extract, silk gum albumen, hyaluronic acid mix homogeneously; Continue stirring discharging in 10 to 20 minutes and obtain finished product.
CN201510198842.7A 2015-04-22 2015-04-22 Formula and preparation method of water seepage emulsion Pending CN104825377A (en)

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Application Number Priority Date Filing Date Title
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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107320427A (en) * 2017-07-13 2017-11-07 韦卓林 A kind of preparation method of olive oil elite
CN107802585A (en) * 2017-12-14 2018-03-16 佛山市万良商贸有限公司 A kind of silk gum condensation and preparation method thereof
CN107998019A (en) * 2017-12-14 2018-05-08 佛山市万良商贸有限公司 A kind of silk gum lotion and preparation method thereof
CN110840778A (en) * 2019-12-13 2020-02-28 广州诗妃生物科技有限公司 Emulsion type mask liquid and preparation method thereof
CN112603847A (en) * 2021-01-11 2021-04-06 上海菩兰实业有限公司 Novel silk skin cream and preparation method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102058511A (en) * 2010-12-28 2011-05-18 海南京润珍珠生物技术股份有限公司 Water outlet cream added with pearl hydrolysate liposome
CN103800247A (en) * 2014-02-27 2014-05-21 上海海洋大学 Agar crude polysaccharide cream and preparation method thereof
CN104188817A (en) * 2014-08-28 2014-12-10 广州芭薇化妆品有限公司 Water cream with wrinkle-removing effect and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102058511A (en) * 2010-12-28 2011-05-18 海南京润珍珠生物技术股份有限公司 Water outlet cream added with pearl hydrolysate liposome
CN103800247A (en) * 2014-02-27 2014-05-21 上海海洋大学 Agar crude polysaccharide cream and preparation method thereof
CN104188817A (en) * 2014-08-28 2014-12-10 广州芭薇化妆品有限公司 Water cream with wrinkle-removing effect and preparation method thereof

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107320427A (en) * 2017-07-13 2017-11-07 韦卓林 A kind of preparation method of olive oil elite
CN107802585A (en) * 2017-12-14 2018-03-16 佛山市万良商贸有限公司 A kind of silk gum condensation and preparation method thereof
CN107998019A (en) * 2017-12-14 2018-05-08 佛山市万良商贸有限公司 A kind of silk gum lotion and preparation method thereof
CN110840778A (en) * 2019-12-13 2020-02-28 广州诗妃生物科技有限公司 Emulsion type mask liquid and preparation method thereof
CN112603847A (en) * 2021-01-11 2021-04-06 上海菩兰实业有限公司 Novel silk skin cream and preparation method thereof

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Application publication date: 20150812

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