CN110840778A - Emulsion type mask liquid and preparation method thereof - Google Patents
Emulsion type mask liquid and preparation method thereof Download PDFInfo
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- CN110840778A CN110840778A CN201911283036.4A CN201911283036A CN110840778A CN 110840778 A CN110840778 A CN 110840778A CN 201911283036 A CN201911283036 A CN 201911283036A CN 110840778 A CN110840778 A CN 110840778A
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/68—Sphingolipids, e.g. ceramides, cerebrosides, gangliosides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
The invention relates to a facial mask liquid and a preparation method thereof, and particularly discloses an emulsion type facial mask liquid and a preparation method thereof, aiming at solving the technical problems of relatively weak moisturizing and skin-moistening durability and poor mildness of the existing facial mask. The emulsion type mask liquid comprises the following raw materials: trehalose, glycerol, jojoba oil, olive oil and ceramide 3 mixture, phytosterol oleate, caprylic/capric triglyceride, and sodium hyaluronate. The preparation method comprises the following steps: mixing, stirring and heating water, trehalose, glycerol, acrylate/C10-30 alkanol acrylate cross-linked polymer, hydroxyethyl cellulose and sodium hyaluronate to obtain solution a; mixing jojoba oil, olive oil and ceramide 3 mixture, phytosterol oleate and caprylic/capric triglyceride, stirring and heating to obtain solution b; adding b into a, adding triethanolamine, stirring and homogenizing; adding antiseptic and antibacterial agent and essence, and stirring. The obtained facial mask liquid is added with less emulsifier, and has better mildness.
Description
Technical Field
The invention relates to a facial mask liquid and a preparation method thereof, in particular to an emulsion type facial mask liquid and a preparation method thereof.
Background
Facial masks, one category of skin care products. The most basic and important purpose is to make up the still insufficient cleaning work of makeup removal and face washing, and other maintenance functions such as water replenishing and moisturizing, whitening, anti-aging, grease balancing and the like are realized by matching with other essential components on the basis. Mainly comprises a facial mask patch, facial cream and the like.
Among them, the mask has become one of the mainstream product categories of skin care and beauty care products due to its advantages of convenience and high efficiency. However, most of the facial masks sold in the market are aqueous solution. Due to the characteristics of the formula of the aqueous solution type facial mask, oil-soluble skin moistening and caring components cannot be added in the formula, so that the lasting performance of moisturizing and caring is relatively weak. The dosage forms with better moistening and lasting performances are mostly cream-shaped facial mask products in smearing dosage forms, and the convenience is relatively lower.
A large amount of emulsifier is added to a general emulsion formula to stabilize the formula system; and too much emulsifier can easily cause the emulsification of skin lipid layers and destroy the skin lipid barrier function, thereby easily causing skin irritation and allergy. The facial mask made of the emulsion system has poor mildness.
Disclosure of Invention
The invention aims to provide an emulsion type facial mask liquid, which can be added with various lipophilic skin care components and has better effects of moistening and maintaining skin compared with the common water-based facial mask liquid.
In order to realize the purpose of the invention, the following technical scheme is provided:
an emulsion type mask liquid comprises the following raw materials in percentage by mass: 1 to 3 percent of trehalose, 1 to 15 percent of glycerol, 0.01 to 1 percent of acrylic acid (ester)/C10 to 30 alkanol acrylate cross-linked polymer, 0.01 to 1 percent of hydroxyethyl cellulose, 0.01 to 10 percent of jojoba oil, 0.01 to 5 percent of the mixture of olive oil and ceramide 3, 0.01 to 5 percent of phytosterol oleate, 0.01 to 10 percent of caprylic/capric triglyceride, 0.01 to 1 percent of triethanolamine, 0.001 to 1 percent of sodium hyaluronate, 0.1 to 1 percent of antiseptic bacteriostatic agent, 0.001 to 0.5 percent of essence, and the balance of water.
The emulsion type mask liquid comprises the following raw materials in percentage by mass: 2 to 3 percent of trehalose, 5 to 12 percent of glycerol, 0.1 to 0.8 percent of acrylic acid (ester)/C10 to 30 alkanol acrylate cross-linked polymer, 0.1 to 1 percent of hydroxyethyl cellulose, 0.5 to 6 percent of jojoba oil, 0.5 to 3 percent of the mixture of olive oil and ceramide 3, 1 to 5 percent of phytosterol oleate, 1 to 8 percent of caprylic/capric triglyceride, 0.2 to 1 percent of triethanolamine, 0.1 to 0.9 percent of sodium hyaluronate, 0.1 to 0.5 percent of antiseptic bacteriostatic agent, 0.001 to 0.5 percent of essence, and the balance of water.
The emulsion type mask liquid comprises the following raw materials in percentage by mass: 2 to 3 percent of trehalose, 5 to 8 percent of glycerol, 0.5 to 0.8 percent of acrylic acid (ester)/C10 to 30 alkanol acrylate cross-linked polymer, 0.2 to 0.5 percent of hydroxyethyl cellulose, 1 to 3 percent of jojoba oil, 1 to 3 percent of mixture of olive oil and ceramide 3, 2 to 5 percent of phytosterol oleate, 1 to 3 percent of caprylic/capric triglyceride, 0.2 to 0.8 percent of triethanolamine, 0.1 to 0.5 percent of sodium hyaluronate, 0.1 to 0.5 percent of antiseptic bacteriostatic agent, 0.001 to 0.5 percent of essence and the balance of water.
The invention also provides a preparation method of the emulsion type facial mask liquid, which comprises the following steps:
(1) weighing water, trehalose, glycerol, acrylic acid (acrylate)/C10-30 alkanol acrylate cross-linked polymer, hydroxyethyl cellulose and sodium hyaluronate according to the formula ratio, mixing, stirring and heating to 85-95 ℃, keeping the temperature, and cooling to 40-45 ℃ to obtain a solution a;
(2) weighing jojoba oil, olive oil and ceramide 3 mixture, phytosterol oleate and caprylic/capric triglyceride, mixing, stirring and heating to obtain solution b;
(3) adding the solution b into the solution a, adding the triethanol, stirring, and homogenizing for 10-15 min;
(4) adding antiseptic and bacteriostatic agent and essence, and stirring to obtain emulsion type facial mask liquid.
Further, the constant temperature time in the step (1) is 20-25 min.
Further, the heating temperature in the step (2) is 40-45 ℃.
Compared with the prior art, the invention has the beneficial effects that:
1. the emulsion type facial mask liquid disclosed by the invention can effectively improve the barrier function of skin and maintain the health state of skin by adding the mixture of trehalose, glycerol, jojoba oil, olive (OLEAEUROPAEA) fruit oil and ceramide 3, phytosterol oleate, caprylic/capric triglyceride and sodium hyaluronate, and can achieve the effects of moisturizing, nourishing and repairing skin.
2. The emulsion type facial mask liquid can be added with various lipophilic skin care components, and has better effects of moistening and maintaining skin compared with the common water-based facial mask liquid.
3. The preparation method is simple and suitable for quantitative production, and compared with a common emulsion type product, the prepared emulsion type facial mask liquid is added with less emulsifier and has better mildness.
Detailed Description
The technical solution of the present invention will be described in further detail with reference to the following embodiments, but the present invention is not limited thereto.
Examples 1 to 4 are raw material ratios (by mass percent) of the emulsion type facial mask liquid, which are shown in the following table:
example 5
The preparation method of the emulsion type facial mask liquid in the embodiment 1 comprises the following steps:
(1) weighing water, trehalose, glycerol, acrylic acid (acrylate)/C10-30 alkanol acrylate cross-linked polymer, hydroxyethyl cellulose and sodium hyaluronate according to the formula, mixing, stirring and heating to 85 ℃, keeping the temperature for 20min, and cooling to 40 ℃ to obtain a solution a;
(2) weighing jojoba oil, olive oil and ceramide 3 mixture, phytosterol oleate and caprylic/capric triglyceride, mixing, stirring and heating to 45 ℃ to obtain solution b;
(3) adding the solution b into the solution a, adding the triethanol, stirring, and then starting homogenizing for 10 min;
(4) adding antiseptic and bacteriostatic agent and essence, and stirring to obtain emulsion type facial mask liquid.
Example 6
The emulsion-type facial mask solution of example 2 was prepared in the same manner as in example 5.
Example 7
The preparation method of the emulsion type facial mask liquid of the embodiment 3 comprises the following steps:
(1) weighing water, trehalose, glycerol, acrylic acid (acrylate)/C10-30 alkanol acrylate cross-linked polymer, hydroxyethyl cellulose and sodium hyaluronate according to the formula, mixing, stirring and heating to 95 ℃, keeping the temperature for 25min, and cooling to 45 ℃ to obtain a solution a;
(2) weighing jojoba oil, olive oil and ceramide 3 mixture, phytosterol oleate and caprylic/capric triglyceride, mixing, stirring and heating to 40 ℃ to obtain solution b;
(3) adding the solution b into the solution a, adding the triethanol, stirring, and then starting homogenizing for 15 min;
(4) adding antiseptic and bacteriostatic agent and essence, and stirring to obtain emulsion type facial mask liquid.
Example 8
The preparation method of the emulsion type facial mask liquid of the embodiment 4 comprises the following steps:
(1) weighing water, trehalose, glycerol, acrylic acid (acrylate)/C10-30 alkanol acrylate cross-linked polymer, hydroxyethyl cellulose and sodium hyaluronate according to the formula, mixing, stirring and heating to 85-95 ℃, keeping the temperature for 2-25 min, and cooling to 40-45 ℃ to obtain a solution a;
(2) weighing jojoba oil, olive oil and ceramide 3 mixture, phytosterol oleate and caprylic/capric triglyceride, mixing, stirring and heating to 40-45 ℃ to obtain solution b;
(3) adding the solution b into the solution a, adding the triethanol, stirring, and homogenizing for 10-15 min;
(4) adding antiseptic and bacteriostatic agent and essence, and stirring to obtain emulsion type facial mask liquid.
In order to test the technical effects of the embodiments of the invention, a test is performed with reference to the evaluation guideline for cosmetic moisturizing efficacy (QB/T4256-2011), namely, after the facial mask is used by a volunteer in a single time in a constant temperature and humidity environment, the moisturizing effect of the facial mask within 30 minutes is non-invasively evaluated by using an instrument. During the test, the test face masks and the blank control were randomly distributed on the inner sides of the left and right forearm of the subject. The product is used for a single time, and the application time is 30 minutes. The stratum corneum moisture content was measured on the product application zone and the placebo zone using a skin moisture tester (Corneometer) before and after 5, 15, 20, and 30 minutes of product application, respectively. Each face film sample had 24 ginseng samples and the test was completed.
The short-term moisturizing and skin moistening after the use has obvious difference. Five (one commercially available mask, masks from examples 1-4) samples all showed an increase in skin moisture when tested 20 minutes after use. However, the moisturizing effect is significantly different between the facial masks. (group A is a commercially available mask, group B is the mask of example 1, group C is the mask of example 2, group D is the mask of example 3, group F is the mask of example 4). The detailed results are shown in table 1.
TABLE 1 moisturizing and skin moisturizing Effect test results of commercially available masks and masks of examples 1-4
As can be seen from the above results, the increase in skin moisture content of the commercially available mask gradually decreased with time, whereas the skin moisture of the B, C, D, F samples was sequentially increased by about 3 to 10 points when tested 5 minutes after the mask used in examples 1 to 4; the skin moisture content of the B, C, D, F samples increased by 7-15 points 15 minutes after use; after 30 minutes, the skin moisture of the B, C, D, F samples was steadily at 3-10 points relative to the commercial mask (5 points down).
The pH value of the masks of examples 1-4 were tested and the heat and cold resistance was tested for 48 hours with reference to QB/T2872-2017. As can be seen from table 2, the stability of the present invention is good and the pH of the mask of example 4 is closer to the skin (about 5.8), i.e., the pH of the mask with the addition of 1% jojoba oil, 3% olive oil and ceramide 3 mixture, 2% phytosterol oleate, 8% caprylic/capric triglyceride, etc. (example 4) is the best.
TABLE 2
The above embodiments are preferred embodiments of the present invention, but the present invention is not limited to the above embodiments, and any other changes, modifications, substitutions, combinations, and simplifications which do not depart from the spirit and principle of the present invention should be construed as equivalents thereof, and all such changes, modifications, substitutions, combinations, and simplifications are intended to be included in the scope of the present invention.
Claims (6)
1. The emulsion type mask liquid is characterized by comprising the following raw materials in percentage by mass: 1-3% of trehalose, 1-15% of glycerol, 0.01-1% of acrylate/C10-30 alkanol acrylate cross-linked polymer, 0.01-1% of hydroxyethyl cellulose, 0.01-10% of jojoba oil, 0.01-5% of a mixture of olive oil and ceramide 3, 0.01-5% of phytosterol oleate, 0.01-10% of caprylic/capric triglyceride, 0.01-1% of triethanolamine, 0.001-1% of sodium hyaluronate, 0.1-1% of a preservative bacteriostatic agent, 0.001-0.5% of essence and the balance of water.
2. The emulsion type mask liquid according to claim 1, which is characterized by comprising the following raw materials in percentage by mass: 2 to 3 percent of trehalose, 5 to 12 percent of glycerol, 0.1 to 0.8 percent of acrylate/C10 to 30 alkanol acrylate cross-linked polymer, 0.1 to 1 percent of hydroxyethyl cellulose, 0.5 to 6 percent of jojoba oil, 0.5 to 3 percent of the mixture of olive oil and ceramide 3, 1 to 5 percent of phytosterol oleate, 1 to 8 percent of caprylic/capric triglyceride, 0.2 to 1 percent of triethanolamine, 0.1 to 0.9 percent of sodium hyaluronate, 0.1 to 0.5 percent of antiseptic bacteriostatic agent, 0.001 to 0.5 percent of essence, and the balance of water.
3. An emulsion type mask liquid according to claim 1 or 2, which is characterized by comprising the following raw materials in percentage by mass: 2 to 3 percent of trehalose, 5 to 8 percent of glycerol, 0.5 to 0.8 percent of acrylate/C10 to 30 alkanol acrylate cross-linked polymer, 0.2 to 0.5 percent of hydroxyethyl cellulose, 1 to 3 percent of jojoba oil, 1 to 3 percent of the mixture of olive oil and ceramide 3, 2 to 5 percent of phytosterol oleate, 1 to 3 percent of caprylic/capric triglyceride, 0.2 to 0.8 percent of triethanolamine, 0.1 to 0.5 percent of sodium hyaluronate, 0.1 to 0.5 percent of antiseptic bacteriostatic agent, 0.001 to 0.5 percent of essence, and the balance of water.
4. A method of preparing an emulsion-type facial mask fluid according to any of claims 1-3, comprising the steps of:
(1) weighing water, trehalose, glycerol, acrylate/C10-30 alkanol acrylate cross-linked polymer, hydroxyethyl cellulose and sodium hyaluronate according to the formula, mixing, stirring and heating to 85-95 ℃, keeping the temperature constant, and cooling to 40-45 ℃ to obtain a solution a;
(2) weighing jojoba oil, olive oil and ceramide 3 mixture, phytosterol oleate and caprylic/capric triglyceride, mixing, stirring and heating to obtain solution b;
(3) adding the solution b into the solution a, adding the triethanol, stirring, and homogenizing for 10-15 min;
(4) adding antiseptic and bacteriostatic agent and essence, and stirring to obtain emulsion type facial mask liquid.
5. The preparation method of an emulsion-type mask liquid according to claim 4, wherein the constant temperature in the step (1) is 20-25 min.
6. An emulsion type facial solution preparation method according to claim 4, wherein the heating temperature in the step (2) is 40-45 ℃.
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| CN201911283036.4A CN110840778A (en) | 2019-12-13 | 2019-12-13 | Emulsion type mask liquid and preparation method thereof |
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| CN201911283036.4A CN110840778A (en) | 2019-12-13 | 2019-12-13 | Emulsion type mask liquid and preparation method thereof |
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| CN110840778A true CN110840778A (en) | 2020-02-28 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113244141A (en) * | 2021-05-14 | 2021-08-13 | 广州市悦色荷堂生物科技有限公司 | Essence cream for repairing skin barrier function and preparation method thereof |
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| CN106344490A (en) * | 2016-11-05 | 2017-01-25 | 诺斯贝尔化妆品股份有限公司 | Soft skin-friendly superfine essence facial mask |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113244141A (en) * | 2021-05-14 | 2021-08-13 | 广州市悦色荷堂生物科技有限公司 | Essence cream for repairing skin barrier function and preparation method thereof |
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Application publication date: 20200228 |