CN109966183A - A kind of moisturizing remediation composition and its preparation method and application - Google Patents

A kind of moisturizing remediation composition and its preparation method and application Download PDF

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CN109966183A
CN109966183A CN201910365190.XA CN201910365190A CN109966183A CN 109966183 A CN109966183 A CN 109966183A CN 201910365190 A CN201910365190 A CN 201910365190A CN 109966183 A CN109966183 A CN 109966183A
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parts
oil
fruit
composition
palm fibre
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CN109966183B (en
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吴新星
卢桂田
高合意
曾飒
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Guangdong Essence Biotechnology Co Ltd
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Guangdong Essence Biotechnology Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/63Steroids; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/68Sphingolipids, e.g. ceramides, cerebrosides, gangliosides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/70Biological properties of the composition as a whole
    • A61K2800/72Hypo-allergenic

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Public Health (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
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  • Dermatology (AREA)
  • Gerontology & Geriatric Medicine (AREA)
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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a kind of moisturizing remediation composition and its preparation method and application, the composition includes following component in parts by weight: 30-50 parts of Queensland nut seed oil, 1-10 parts of highland barley embryo bud oils, 0.1-8 parts of phytosterols oletates, 0.1-8 parts of great Hua cocoa seeds of trees rouge, 0.1-8 parts of ceramides -2.Rationally, various ingredients are synergistic for moisture-keeping composition formula of the invention, can effectively repair skin barrier, and performance of keeping humidity is prominent, and mild non-stimulated, good using skin sense, assimilation effect is good, have the function of the moisturizing of water profit, repair skin barrier.

Description

A kind of moisturizing remediation composition and its preparation method and application
Technical field
The present invention relates to daily use chemicals technical field, a kind of moisturizing remediation composition and its preparation method and application is related generally to.
Background technique
Moisture is the first element of skin beauty, and whether Skin Cell is full plump, and whether skin quality is fine and smooth tender, and the colour of skin is It is no glittering and translucent, the number of moisture content in skin both depended on.Water loss rate is to influence in skin in moisture content most Important factor.Normal skin has common by sebum film, cuticula keratin, lipid, corium mucopolysaccharide, mucopolysaccharide etc. The barrier function of composition can effectively inhibit water loss.But with the increase at age, the sebum secretion of skin is reduced, in addition The external worlds such as, computer radiation dry with the exacerbation of environmental pollution, the pressure of social cChange, the temperature inversion of seasonal migration and air-conditioning Infringement, keratoderma surface sebum film is gradually thinning, and the natural moisturizing factor of skin, hyaluronic acid are invaded reduction, Bu Nengyou The passage of effect control moisture, causes skin corium water content constantly to decline, dry skin, wrinkle, dim mute, loose, aging wait many Skin problem is haunted in advance.Moisture in female skin was largely lost since 20 years old, and sebum film is thinning, in addition extraneous infringement, The natural renewal speed for carrying water fugacity does not catch up with the requirement of skin moisture-keeping, and collagen elasticated net is caused to be broken, and metabolism is slack-off, respectively Kind skin problem will come one after another, and moisturizing movement is not in place, and skin finally will sink into irreversible desert state.Any season The perfect transformation of middle realization can be consoled and be moistened to section, age, skin quality, skin problem all in water.The barrier function of skin is repaired, The loss for reducing moisture is the basis of all skin cares, and whitening, sun-proof, oil-control, anti-acne, anti-aging etc. are all the bases in water profit skin It is completed on plinth.
CN105213226A discloses a kind of cosmetic composition and preparation method thereof containing macadimia nut oil, and Australia is hard Fruit oil accounts for 0.01-15 part of cosmetic composition total weight, is first mutually to be separately heated to oily after being completely dissolved with water phase, then incite somebody to action Water phase is added slowly in oily phase and quickly stirs, and is prepared after cooling to room temperature.Invention preparation contains Australia The cosmetic composition of macadamia nut oil has moistening effect;And the cosmetic composition prepared can slow down Australia in composition The oxidation rate of macadamia nut oil to extend the shelf-life of cosmetic composition, but the moistening effect of the composition is unobvious, and is inhaled Yield and use skin sense are poor.
The multiple-effect that CN105411865A discloses a kind of grease containing various plants moistens micro emulsion essence, consisting of: octanoic acid/ Triglyceride DDD, dimethyl silicone polymer, olive oil, A Gan tree oil, macadimia nut oil, wheat-germ oil, coconut oil, cream wood Fruit oil, grape seed oil, avocado oil, jojoba oil, Tower rape oil, white pond flower seed oil, tocopherol acetate, phytosterol/ Octyl dodecanol lauroyl glutamate ester, purified water, hydrolecithin, glycerol, EDTA-2NA, 1.3- propylene glycol, Natrulon H-10 The micro emulsion essence of the grease containing various plants is made under high-pressure homogeneous effect in -2 oleate of oleate and polyglycereol.Micro emulsion essence Magnificent formulation stable, use feeling do not stick clearly greasy, are easily absorbed by the skin.But the invention is without moistening effect, and complicated components, prepares work Skill is cumbersome.
Therefore it provides a kind of moisture-keeping composition with brilliant moistening effect, has great importance in cosmetic field And vast market prospect.
Summary of the invention
The present invention provides a kind of moisturizing remediation compositions and its preparation method and application, and the moisture-keeping composition includes Australia Continent nut seed oil, highland barley embryo bud oil, phytosterols oletate, great Hua cocoa seeds of trees rouge and the collaboration of ceramide -2, five kind component Synergy has moisturizing and nourishing, the effect of mild skin care.
In a first aspect, the present invention provides a kind of moisture-keeping composition, the composition includes following component in parts by weight:
Entire leaf Queensland nut seed oil, also known as macadimia nut oil, are derived from entire leaf Queensland nut core, are yellow oily liquid Body, slightly grease fragrance can mix with most plants essential oil, be it is relatively rare in a low temperature of not variable muddiness pure plant Object grease.Entire leaf Queensland nut seed oil forms nutrient essential to grease protective layer rich in skin, and the calm skin of energy is repaired Skin caused by environment is sensitive, tans severely and blows wound, protect cell membrane and moisten, moisturizing, and ductility is good, and skin can be made soft And it is vibrant.
Great Hua cocoa chocolate tree is also known as simple and unsophisticated A Su fruit tree, is a kind of fruit tree for being grown in Amazon River basin, and protection rain The environmental-friendly plant of woods.Great Hua cocoa chocolate tree is grown on branch as cocoa tree species, and fruit is maximum in cocoa species , the oil extracted from their seed shows peculiar property after filtering and purification in cosmetics industry.Great Hua Cocoa seeds of trees rouge is a kind of by being saturated the triglyceride uniformly formed with unsaturated fatty acid, and it is lower molten that this has product Point is quickly rendered into a kind of lotion of softness when in contact with the skin.Simple and unsophisticated A Su fruit oil has high water absorption ability, about sheep The 240% of hair rouge, and certain sterols with animal and plant source, these characteristics enable product very stable in lotion. Simple and unsophisticated A Su fruit oil has a kind of pleasant and soft sense of touch as a kind of emollient, to skin, in dry and impaired skin There are natural moisture retention and elasticity on skin.
Green is that one of Qinghai-Tibet staple crops have long plantation history.Qinghai-Tibet day and night temperature is big, day Strong according to radiation, unique growth conditions makes green naked trophic function composition rich in.Green plumule is the by-product of green powder processed Product, unsaturated fatty acid content is abundant in green plumule, and the content of linoleic acid plus linolenic acid is higher than phase in wheat-germ oil Answer the content of fatty acid.In addition to this, green embryo oil middle vitamin E, vitamin D and cupreol also rich in;Its Middle VE is a kind of important health factor, has strong anti-oxidation, eliminates free radical, adjusts because radical damage causes body function The ability of energy sexual maladjustment.
Ceramide is a kind of lipid being naturally present in skin, forms the barrier of one layer of waterproof in skin surface. They not only assist in skin and lock moisture, moreover it is possible to promote skin barrier self-regeneration and regulation Skin Cell.Newborn baby's Skin often wraps up in the same substance of coating of wax matter, and this substance is called vernix caseosa, is mainly made of ceramide, can prevent skin Skin water loss.In skin ceramide secretion can reduce with age, and then cause have dry skin, wrinkle and Some scytitis.
Phytosterol is to obtain from corn and soybean by physical purification, has the spies such as nutritive value is high, physiological activity is strong Point.Phytosterol has very high permeability to skin, can keep skin surface moisture content, promotes skin metabolism, inhibits Scytitis, can anti-sun erythema, skin aging, the effect of there are also hair tonics, hair care.It can be used as emulsifier, the life for cream It produces, has the characteristics that use feeling good (auxiliary malleability good, smooth do not glue), durability is good, is unlikely to deteriorate.In addition phytosterol has antioxygen The property changed can maintain the softness of cell and wet, and have mild permeability to skin, be able to maintain skin moisture, and can be with Promote skin metabolism, repairs skin barrier.
Moisture-keeping composition provided by the invention measures skin selection according to preserving moisture and protecting skin theory, with a definite target in view, not only has moisturizing The effect of nourishing, also has and skin is promoted newly to create metabolism, anti-aging, anti-inflammatory and other effects, the proportion that each component is mentioned in the present invention Lower common cooperation, can achieve synergistic purpose.
The Queensland nut seed oil be 30-50 parts, such as can be 30 parts, 33 parts, 35 parts, 37 parts, 39 parts, 41 parts, 42.6 parts, 43 parts, 45 parts, 47 parts, 49 parts or 50 parts.
The highland barley embryo bud oil is 1-10 parts, such as can be 1 part, 2 parts, 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts, 9 parts Or 10 parts.
The phytosterol grease is 0.1-8 parts, such as can be 0.1 part, 0.2 part, 0.3 part, 0.5 part, 1 part, 3 parts, 5 Part, 7 parts or 8 parts.
The great Hua cocoa seeds of trees rouge is 0.1-8 parts, such as can be 0.1 part, 0.2 part, 0.3 part, 0.5 part, 1 part, 3 Part, 5 parts, 7 parts or 8 parts.
The ceramide -2 is 0.1-8 parts, such as can be 0.1 part, 0.2 part, 0.3 part, 0.5 part, 1 part, 3 parts, 5 Part, 7 parts or 8 parts.
Preferably, the composition includes following component in parts by weight:
Preferably, the composition includes following component in parts by weight:
Preferably, the composition further includes base-material.
Preferably, the base-material includes jojoba seed oil, olive oil, dog rose fruit oil, evening primrose oil, fertility Phenol, Wild soybean oil, Asian puccoon root extract, essence, bisabolol, wooden Shandong star fruit palm fibre seed rouge, Butyrospermum parkii fatty oil, cooked food Etard palm fibre The auspicious palmitic acid fruit oil of fruit oil, hair and ethylhexyl salicylate.
Preferably, the base-material includes following component in parts by weight: 8-15 parts of jojoba seed oil, 20-40 parts of oil Olive fruit oil, 2-5 parts of dog rose fruit oil, 3-5 parts of evening primrose oil, 0.3-1 parts of tocopherol and Wild soybean oil, 0.3-1 The Asian puccoon root extract of part, 0.05-1 parts of essence, 0.3-1 parts of bisabolol, 0.01-1 parts of the wooden Shandong star fruit palm fibre seed rouge, 0.01-1 parts of Butyrospermum parkii fatty oil, 0.01-1 parts of cooked food Etard palm fibre fruit oil, the auspicious palmitic acid fruit oil of 0.05-1 parts of hair and 0.05-1 The ethylhexyl salicylate of part.
The jojoba seed oil is 8-15 parts, such as can be 8 parts, 10 parts, 11 parts, 12 parts, 13 parts, 14 parts or 15 parts.
The olive oil be 20-40 parts, such as can be 20 parts, 22.27 parts, 26.36 parts, 30 parts, 30.87 parts, 31.76 parts, 35.67 parts or 40 parts.
The dog rose fruit oil is 2-5 parts, such as can be 2 parts, 3 parts, 4 parts or 5 parts.
The evening primrose oil is 3-5 parts, such as can be 3 parts, 4 parts or 5 parts.
The tocopherol and Wild soybean oil are 0.3-1 parts, such as can be 0.3 part, 0.5 part, 0.7 part, 0.9 part or 1 part, The proportion of the tocopherol and Wild soybean oil does not influence the effect of moisture-keeping composition, and sum of the two is 0.3-1 parts.
The Asian puccoon root extract is 0.3-1 parts, such as can be 0.3 part, 0.5 part, 0.7 part or 1 part.
The essence is 0.05-1 parts, such as can be 0.05 part, 0.1 part, 0.3 part, 0.5 part, 0.7 part or 1 part.
The bisabolol is 0.3-1 parts, such as can be 0.3 part, 0.5 part, 0.7 part or 1 part.
The wood Shandong star fruit palm fibre seed rouge is 0.01-1 parts, such as can be 0.01 part, 0.1 part, 0.3 part, 0.5 part or 1 part.
The Butyrospermum parkii fatty oil is 0.01-1 parts, such as can be 0.01 part, 0.1 part, 0.3 part, 0.5 part or 1 part.
The cooked food Etard palm fibre fruit oil is 0.01-1 parts, such as can be 0.01 part, 0.1 part, 0.3 part, 0.5 part or 1 part.
The auspicious palmitic acid fruit oil of hair be 0.05-1 parts, such as can be 0.05 part, 0.15 part, 0.35 part, 0.4 part, 0.6 part, 0.8 part or 1 part.
The ethylhexyl salicylate, which is 0.05-1 parts, for example can be 0.05 part, 0.1 part, 0.3 part, 0.5 part or 1 part.
Preferably, composition score by weight includes following component: 30-50 parts of Queensland nut seed oil, and 1-10 parts Highland barley embryo bud oil, 0.1-8 parts of phytosterols oletate, 0.1-8 parts of great Hua cocoa seeds of trees rouge, 0.1-8 parts of neural acyl The jojoba seed oil of amine -2,8-15 part, 20-40 parts of olive oil, 2-5 parts of dog rose fruit oil, 3-5 parts of oenothera biennis Oil, 0.3-1 parts of tocopherol and Wild soybean oil, 0.3-1 parts of Asian puccoon root extract, 0.05-1 parts of essence, 0.3-1 parts red Bisabol, 0.01-1 parts of the wooden Shandong star fruit palm fibre seed rouge, 0.01-1 parts of Butyrospermum parkii fatty oil, 0.01-1 parts of cooked food Etard palm fibre fruit Oil, the auspicious palmitic acid fruit oil of 0.05-1 parts of hair and 0.05-1 parts of ethylhexyl salicylate.
Preferably, the base-material includes following component in parts by weight:: 10 parts of jojoba seed oil, 30 parts of olive Fruit oil, 3 parts of dog rose fruit oil, 4 parts of evening primrose oil, 0.5 part of tocopherol and Wild soybean oil, 0.5 part of alkanet mention Take object, 0.05 part of essence, 0.5 part of bisabolol, 0.3 part of the wooden Shandong star fruit palm fibre seed rouge, 0.3 part of Butyrospermum parkii fatty oil, 0.3 part of cooked food Etard palm fibre fruit oil, the auspicious palmitic acid fruit oil of 0.5 part of hair and 0.05 part of ethylhexyl salicylate.
Preferably, the composition includes following component in parts by weight: 42 parts of Queensland nut seed oil, 5 parts of highland barley Embryo oil, 1 part of phytosterols oletate, 1 part of great Hua cocoa seeds of trees rouge, the Jojoba seed of 1 part of ceramide -2,10 part Oil, 30 parts of olive oil, 3 parts of dog rose fruit oil, 4 parts of evening primrose oil, 0.5 part of tocopherol and Wild soybean oil, 0.5 part of Asian puccoon root extract, 0.05 part of essence, 0.5 part of bisabolol, 0.3 part of the wooden Shandong star fruit palm fibre seed rouge, 0.3 part Butyrospermum parkii fatty oil, 0.3 part of cooked food Etard palm fibre fruit oil, the auspicious palmitic acid fruit oil of 0.5 part of hair and 0.05 part of salicylic acid ethyl hexyl Ester.
Second aspect, the present invention provide a kind of method for preparing moisturizing remediation composition as described in relation to the first aspect, feature It is, includes the following steps:
It weighs corresponding component respectively according to formula ratio, is heated to 60-80 DEG C after mixing, with turning for 100-2000rpm/min Fast homogeneous stirring, mixing time 3-10min after being sufficiently mixed, are filtered, and encapsulation seals to get the moisture-keeping composition.
The temperature be 60-80 DEG C, such as can be 60 DEG C, 62 DEG C, 65 DEG C, 67 DEG C, 70 DEG C, 72 DEG C, 75 DEG C, 78 DEG C or 80℃。
The revolving speed be 100-2000rpm/min, such as can be 100rpm/min, 200rpm/min, 300rpm/min, 400rpm/min、500rpm/min、600rpm/min、700rpm/min、800rpm/min、900rpm/min、1000rpm/ min、1100rpm/min、1200rpm/min、1300rpm/min、1400rpm/min、1500rpm/min、1600rpm/min、 1700rpm/min, 1800rpm/min, 1900rpm/min or 2000rpm/min.
The time is 3-10min, such as can be 3min, 4min, 5min, 6min, 7min or 10min.
The preparation method simple possible of the composition, it is easily prepared.
Preferably, the highland barley embryo bud oil the preparation method comprises the following steps: take barley germ crush, drying, pass through supercritical CO2Stream Body method is extracted, extracting pressure 30-50MPa, and extraction temperature is 30-50 DEG C, separating pressure 5-15MPa, separation temperature 40-60 DEG C, extraction time 1-2h, gained highland barley embryo bud oil crude product is further purified by molecular distillation technique, distillation pressure 3-10Pa, It 130-150 DEG C of vapo(u)rizing temperature, collects heavy constituent and obtains required highland barley embryo bud oil.
The extracting pressure is 30-50MPa, such as can be 30MPa, 35MPa, 40MPa, 45MPa or 50MPa.
The extraction temperature is 30-50 DEG C, such as can be 30 DEG C, 32 DEG C, 35 DEG C, 40 DEG C, 45 DEG C or 50 DEG C.
The separating pressure be 5-15MPa, such as can be 5MPa, 6MPa, 7MPa, 8MPa, 9MPa, 10MPa, 11MPa, 12MPa, 13MPa, 14MPa or 15MPa.
The separation temperature is 40-60 DEG C, such as can be 40 DEG C, 45 DEG C, 50 DEG C, 55 DEG C or 60 DEG C.
The extraction time is 1-2h, such as can be 1h, 1.2h, 1.5h, 1.8h or 2h.
The distillation pressure is 3-10Pa, such as can be 3Pa, 4Pa, 5Pa, 6Pa, 7Pa, 8Pa, 9Pa or 10Pa.
The vapo(u)rizing temperature is 130-150 DEG C, such as can be 130 DEG C, 135 DEG C, 140 DEG C, 145 DEG C or 150 DEG C.
The method prepares highland barley embryo bud oil, first passes through supercritical CO2Fluids extraction, recovery rate is high, resulting blueness Highland barley embryo oil contain have more than 75% unsaturated fatty acid, comprising 10% oleic acid, 65% linoleic acid and 1% linolenic acid, With vitamin E abundant and cupreol.Its Linoleic acid, linolenic acid, vitamin E and cupreol, which all have, repairs skin screen The effect of barrier, but oleic acid but has blocking pore, moreover it is possible to the permeability for increasing epidermis destroys the barrier function of skin, causes Stimulation.Consolidate method and resulting highland barley embryo bud oil be further purified by molecular distillation technique, separate oleic acid therein at Point, highland barley embryo bud oil obtained has the effect of repairing skin barrier and moisturizing well.
The third aspect, the present invention provides one kind, and moisture-keeping composition is used to prepare with moisture-keeping function as described in relation to the first aspect The application of cosmetics.
Preferably, the cosmetics include any one in facial cleanser, essential oils, face cream or moisturizer or at least two Combination, such as can be the combination of facial cleanser and essential oils, the group of the combination of face cream and moisturizer or essential oils and moisturizer It closes, preferably essential oils.
Compared with prior art, beneficial effects of the present invention:
(1) rationally, various ingredients are synergistic, can effectively repair skin screen for moisture-keeping composition formula provided by the invention Barrier, performance of keeping humidity is prominent, and mild non-stimulated, good using skin sense, assimilation effect is good, has the function of the moisturizing of water profit, conditioning skin.
(2) preparation method provided by the invention is succinctly efficient, easy to spread, environmentally friendly.
Specific embodiment
Further to illustrate technological means and its effect adopted by the present invention, below in conjunction with preferred implementation of the invention Example to further illustrate the technical scheme of the present invention, but the present invention is not limited in scope of embodiments.
Embodiment 1
The parts by weight of five kinds of components in moisture-keeping composition are as follows:
The group of base-material is divided into 10 parts of jojoba seed oil, and 30 parts of olive oil, 3 parts of dog rose fruit is oily, 4 parts Evening primrose oil, 0.5 part of tocopherol and Wild soybean oil, 0.5 part of Asian puccoon root extract, 0.05 part of essence, 0.5 part red does not have Medicine alcohol, 0.3 part of the wooden Shandong star fruit palm fibre seed rouge, 0.3 part of Butyrospermum parkii fatty oil, 0.3 part of cooked food Etard palm fibre fruit oil, 0.5 part The auspicious palmitic acid fruit oil of hair and 0.05 part of ethylhexyl salicylate.
It is as follows with the method that said components prepare essential oils: to weigh corresponding component respectively according to formula ratio, heated after mixing It to 70 DEG C, is stirred 3-10 minutes with the equidirectional homogeneous of 100rpm/min, after being sufficiently mixed, is filtered, encapsulation seals to get described Essential oils;
Wherein, the highland barley embryo bud oil the preparation method comprises the following steps: take barley germ crush, drying, pass through supercritical CO2Fluid Method is extracted, extracting pressure 40MPa, extraction temperature be 40 DEG C, separating pressure 10MPa, 50 DEG C of separation temperature, extraction time 1.5h, gained highland barley embryo bud oil crude product are further purified by molecular distillation technique, distillation pressure 6Pa, and 140 DEG C of vapo(u)rizing temperature, It collects heavy constituent and obtains required highland barley embryo bud oil.
Embodiment 2
The parts by weight of five kinds of components in moisture-keeping composition are as follows:
The group of base-material is divided into 8 parts of jojoba seed oil, and 20 parts of olive oil, 2 parts of dog rose fruit is oily, 3 parts Evening primrose oil, 0.3 part of tocopherol and Wild soybean oil, 0.4 part of Asian puccoon root extract, 0.05 part of essence, 0.3 part red does not have Medicine alcohol, 0.01 part of the wooden Shandong star fruit palm fibre seed rouge, 0.01 part of Butyrospermum parkii fatty oil, 0.01 part of cooked food Etard palm fibre fruit oil, 0.05 The auspicious palmitic acid fruit oil of hair and 0.05 part of ethylhexyl salicylate of part;
The preparation method is the same as that of Example 1.
Embodiment 3
The parts by weight of five kinds of components in moisture-keeping composition are as follows:
The group of base-material is divided into 15 parts of jojoba seed oil, and 40 parts of olive oil, 5 parts of dog rose fruit is oily, 5 parts Evening primrose oil, 1 part of tocopherol and Wild soybean oil, 1 part of Asian puccoon root extract, 1 part of essence, 1 part of bisabolol, 1 part The wooden Shandong star fruit palm fibre seed rouge, 1 part of Butyrospermum parkii fatty oil, 1 part of cooked food Etard palm fibre fruit oil, the auspicious palmitic acid fruit oil of 1 part of hair and 1 part Ethylhexyl salicylate;
The preparation method is the same as that of Example 1.
Embodiment 4
The parts by weight of five kinds of components in moisture-keeping composition are as follows:
The group of base-material is divided into 9 parts of jojoba seed oil, and 36 parts of olive oil, 3 parts of dog rose fruit is oily, 4 parts Evening primrose oil, 0.7 part of tocopherol and Wild soybean oil, 0.5 part of Asian puccoon root extract, 0.3 part of essence, 0.5 part red does not have Medicine alcohol, 0.3 part of the wooden Shandong star fruit palm fibre seed rouge, 0.5 part of Butyrospermum parkii fatty oil, 0.5 part of cooked food Etard palm fibre fruit oil, 0.5 part The auspicious palmitic acid fruit oil of hair and 0.5 part of ethylhexyl salicylate;
The preparation method is the same as that of Example 1.
Embodiment 5
The parts by weight of five kinds of components in moisture-keeping composition are as follows:
The group of base-material is divided into 13 parts of jojoba seed oil, and 38 parts of olive oil, 4 parts of dog rose fruit is oily, 4 parts Evening primrose oil, 0.7 part of tocopherol and Wild soybean oil, 0.7 part of Asian puccoon root extract, 0.3 part of essence, 0.7 part red does not have Medicine alcohol, 0.7 part of the wooden Shandong star fruit palm fibre seed rouge, 0.3 part of Butyrospermum parkii fatty oil, 0.7 part of cooked food Etard palm fibre fruit oil, 0.5 part The auspicious palmitic acid fruit oil of hair and 0.7 part of ethylhexyl salicylate;
The preparation method is the same as that of Example 1.
Comparative example 1
Compared with Example 1, other than only adding base-material, other conditions are same as Example 1.
Comparative example 2
Buy the tender skin essential oils of the village Zhi Xiu gloss (caprylic/capric triglyceride, three monooctyl ester of carbonic acid, tocopherol (vitamin E), essence, sunflower seed oil, pentaerythritol tetra (di-tert-butyl hydroxy hydrocinnamate), camellia seed oil, apricot kernel oil, egg Fruit seed oil, Queensland nut seed oil, jojoba seed oil, Fructus Coriandri sativi oil, corn oil, rice chaff oil, dog rose fruit oil, the sub- seed of dark green tea bit of a bridle Oil, pepper extract).
Comparative example 3
It is (wood-nut seed oil, European India sunflower oil, rosemary leaf oil, thin that purchase Clarins naturally reconciles body care oil Lotus leaf oil).
Comparative example 4
Purchase Sisley black rose treasure dotes on nourishing essence oil (saualane, European Lee's seed extract, False flax seed oil, fertility Phenol (vitamin E), caprylic/capric triglyceride, rose extract, jojoba seed oil, the lobate extract of powder ball fan algae, white orchid leaf Oil, Pelargonium sunflower oil, Tujue's rose caul-fat, avocado oil unsaponifiable matter, oil with hydrogenated soybean).
Comparative example 5
Compared with Example 1, other than not adding macadimia nut oil, other conditions are same as Example 1.
Comparative example 6
Compared with Example 1, other than not adding highland barley embryo bud oil, other conditions are same as Example 1.
Comparative example 7
Compared with Example 1, other than not adding ceramide -2, other conditions are same as Example 1.
Comparative example 8
Compared with Example 1, other than not adding phytosterols oletate, other conditions are same as Example 1.
Comparative example 9
Compared with Example 1, other than not adding big cocoa seeds of trees rouge, other conditions are same as Example 1.
Sensory testing
9 subjects are selected, to the fragrance of the sample of embodiment and comparative example, appearance, brightness, absorbability, oil sense, residual 9 sense, fever sense, irritation, overall hobby indexs are evaluated, and evaluation criterion is shown in Table 1, and test result is shown in Table 2.
Table 1
Table 2
Contrast test on probation is carried out to each sample by 9 subjects, as seen from table:
1, the essential oils of embodiment 1 and the base-material of comparative example 1 compare, under three fragrance, appearance, brightness appearance index have Drop, absorbability, fever sense two indices are unchanged, and residual sense, irritation, overall preference degree have promotion;
2, Clarins naturally reconciles the residual after body care oil, essential oils, Sisley nourishing essence oil and base-material use Sense is close, and the residual sense below after the use of Shu Uemera essential oils;
3, it is similar and bright naturally to reconcile body care oil to the overall preference degree of essential oils with Clarins by 9 subjects It is powerful and influential to be higher than base-material;
4, the essential oils of embodiment 1-5 all have good fragrance, appearance, brightness and trap, lower oil sense, stimulation Property and heat generation, overall preference degree are higher.Compared to comparative example 5, lack Queensland nut seed oil, the appearance of product, brightness, absorption Property is poor;Compared to comparative example 6, lack highland barley embryo bud oil, the absorbability of product is poor, and product residue sense is serious;Compared to comparative example 7, lack phytosterols oletate, product brightness, absorbability are poor, residual sense weight, and skin sense is partially greasy;Compared to comparative example 8, lack Few great Hua cocoa seeds of trees rouge, product appearance is relatively poor, and product fever sense and irritation are stronger;Compared to comparative example 9, lack Ceramide -2, product absorbability is poor, residual sense weight, and product fever is felt, irritation is more serious.Comprehensive totality preference degree, Embodiment 1-5 will be substantially better than comparative example 5-9.
Moisture content test
Instrument: skin moisture content tester (German C&K, Corneometer CM825)
Principle: the probe of skin moisture content analyzer is that the principle based on capacitor measures.The dielectric constant of water is 81, the dielectric constant of other substances is usually less than 7, and water is the maximum substance of dielectric constant on skin.When moisture content becomes When change, the capacitance of skin also changes, therefore can be by measuring skin pricktest capacitance, the water content on analyzing skin surface.It measures Value is a relative value.Unit indicates that test result is as shown in table 3 with C.U. (Corneometer Units).
Subject: selection subject chooses the subject that forearm skin quality is stemness, is included in moisture value less than 45;
Test position: it is surveyed in forearm
Product dosage: 2mg/cm2
Table 3
As shown in Table 3, the moisture-keeping efficacy that the essential oils of embodiment 1-5 preparation compare base-material greatly promotes, wherein embodiment 1 Moistening effect it is best, be significantly better than that the sample of comparative example 1-9.Moistening effect is substantially better than commercially available three sections competing product essence, Five kinds of components are indispensable, and any component is lacked in comparative example 5-9 can all be substantially reduced moistening effect, influence moisturizing reparation The synergy of composition.
Percutaneous water loss test
Instrument: skin surface water loss tester (German C&K, Tewameter TM300)
Principle: the test probe of skin surface water loss tester uses the cylinder of the both ends open of special designing Cavity vehicle probe forms metastable test subenvironment in skin surface, close by two groups of temperature-humidity sensor measurements Epidermis (about in 1cm) gives as security gradient by the vapor in different two o'clocks that cuticula moisture loss is formed, and directly measures and steams through epidermis The amount of moisture of hair measures skin surface water loss situation with this.Unit is g/hm2, test result is as shown in table 4.
Subject: selection subject chooses the subject that forearm skin quality is stemness, is included in moisture value less than 45;
Test position: it is surveyed in forearm
Product dosage: 2mg/cm2
Table 4
Sample Before use One week Two weeks 4 weeks
Embodiment 1 23.15 22.83 21.63 18.36
Embodiment 2 25.18 25.12 23.58 20.74
Embodiment 3 23.66 23.27 22.46 19.35
Embodiment 4 24.75 24.58 23.15 19.93
Embodiment 5 22.83 22.68 21.36 18.42
Comparative example 1 25.47 25.45 25.32 24.82
Comparative example 2 24.62 24.55 23.88 22.15
Comparative example 3 25.48 25.34 25.06 23.28
Comparative example 4 26.73 26.52 26.17 24.47
Comparative example 5 25.48 25.62 25.44 24.15
Comparative example 6 25.17 25.15 24.96 24.33
Comparative example 7 26.22 26.26 25.78 24.52
Comparative example 8 24.82 24.96 24.38 23.68
Comparative example 9 25.63 25.56 25.07 24.27
Percutaneous water loss amount, moisture loss is fewer, shows that skin barrier function is better.As shown in Table 4, in test period In 4 weeks, after the essential oils that subject is prepared using embodiment 1-5, when the percutaneous water loss amount of test zone is used with sample Between gradually lower, show that it can effectively improve the barrier function of skin, and its effect will be significantly better than the comparison for containing only base-material Example 1.The barrier repair function for comparing base-material greatly promotes, and wherein the barrier repairing effect of embodiment 1 is best, uses sample 4 weeks Afterwards, being lost through transepidermal water for subject improves 20.69%.Moistening effect is substantially better than commercially available three sections competing product essence, and five kinds Component is indispensable, and any component is lacked in comparative example 5-9 all can be substantially reduced its barrier repair function, influences moisturizing and repairs The synergy of compound composition.
In conclusion moisture-keeping composition provided by the invention is theoretical according to oil-control skin care, skin selection is measured, with a definite target in view, respectively Component cooperates jointly under the proportion that the present invention mentions, and can achieve synergistic purpose.
The Applicant declares that the present invention is explained by the above embodiments method detailed of the invention, but the present invention not office Be limited to above-mentioned method detailed, that is, do not mean that the invention must rely on the above detailed methods to implement.Technical field Technical staff it will be clearly understood that any improvement in the present invention, equivalence replacement and auxiliary element to each raw material of product of the present invention Addition, selection of concrete mode etc., all of which fall within the scope of protection and disclosure of the present invention.

Claims (10)

1. a kind of moisturizing remediation composition, which is characterized in that the composition includes following component in parts by weight:
2. composition according to claim 1, which is characterized in that the composition includes following component in parts by weight:
3. composition according to claim 1 or 2, which is characterized in that the composition includes such as the following group in parts by weight Point:
4. composition according to any one of claim 1-3, which is characterized in that the composition further includes base-material;
Preferably, the base-material includes jojoba seed oil, olive oil, dog rose fruit oil, evening primrose oil, tocopherol, open country Soybean oil, Asian puccoon root extract, essence, bisabolol, the wooden Shandong star fruit palm fibre seed rouge, Butyrospermum parkii fatty oil, cooked food Etard palm fibre fruit oil, The auspicious palmitic acid fruit oil of hair and ethylhexyl salicylate.
5. composition according to claim 4, which is characterized in that the base-material includes following component: 8- in parts by weight 15 parts of jojoba seed oil, 20-40 parts of olive oil, 2-5 parts of dog rose fruit oil, 3-5 parts of evening primrose oil, 0.3- 1 part of tocopherol and Wild soybean oil, 0.3-1 parts of Asian puccoon root extract, 0.05-1 parts of essence, 0.3-1 parts of bisabolol, 0.01-1 parts of the wooden Shandong star fruit palm fibre seed rouge, 0.01-1 parts of Butyrospermum parkii fatty oil, 0.01-1 parts of cooked food Etard palm fibre fruit oil, The auspicious palmitic acid fruit oil of 0.05-1 parts of hair and 0.05-1 parts of ethylhexyl salicylate.
6. combination according to claim 4 or 5, which is characterized in that composition score by weight includes following component: 30-50 parts of Queensland nut seed oil, 1-10 parts of highland barley embryo bud oil, 0.1-8 parts of phytosterols oletate, 0.1-8 parts big Flower cocoa seeds of trees rouge, the jojoba seed oil of 0.1-8 parts of ceramide -2,8-15 part, 20-40 parts of olive oil, 2-5 parts Dog rose fruit oil, 3-5 part of evening primrose oil, 0.3-1 part of tocopherol and Wild soybean is oily, 0.3-1 parts of alkanet extraction Object, 0.05-1 parts of essence, 0.3-1 parts of bisabolol, 0.01-1 parts of the wooden Shandong star fruit palm fibre seed rouge, 0.01-1 parts of butter fruit Resinon, 0.01-1 parts of cooked food Etard palm fibre fruit oil, the auspicious palmitic acid fruit oil of 0.05-1 parts of hair and 0.05-1 parts of salicylic acid ethyl hexyl Ester.
7. the composition according to any one of claim 4-6, which is characterized in that the base-material includes such as in parts by weight Lower component: 10 parts of jojoba seed oil, 30 parts of olive oil, 3 parts of dog rose fruit oil, 4 parts of evening primrose oil, 0.5 Tocopherol and the Wild soybean oil of part, 0.5 part of Asian puccoon root extract, 0.05 part of essence, 0.5 part of bisabolol, 0.3 part The wooden Shandong star fruit palm fibre seed rouge, 0.3 part of Butyrospermum parkii fatty oil, 0.3 part of cooked food Etard palm fibre fruit oil, the auspicious palmitic acid fruit oil of 0.5 part of hair and 0.05 part of ethylhexyl salicylate.
8. the composition according to any one of claim 4-7, which is characterized in that the composition includes in parts by weight Following component: 42 parts of Queensland nut seed oil, 5 parts of highland barley embryo bud oil, 1 part of phytosterols oletate, 1 part of great Hua cocoa Seeds of trees rouge, the jojoba seed oil of 1 part of ceramide -2,10 part, 30 parts of olive oil, 3 parts of dog rose fruit oil, 4 The evening primrose oil of part, 0.5 part of tocopherol and Wild soybean oil, 0.5 part of Asian puccoon root extract, 0.05 part of essence, 0.5 part Bisabolol, 0.3 part of the wooden Shandong star fruit palm fibre seed rouge, 0.3 part of Butyrospermum parkii fatty oil, 0.3 part of cooked food Etard palm fibre fruit oil, 0.5 The auspicious palmitic acid fruit oil of hair and 0.05 part of ethylhexyl salicylate of part.
9. the preparation method of moisturizing remediation composition according to claim 1 to 8, which is characterized in that including such as Lower step:
It weighs corresponding component respectively according to formula ratio, is heated to 60-80 DEG C after mixing, it is equal with the revolving speed of 100-2000rpm/min Matter stirring, mixing time 3-10min after being sufficiently mixed, are filtered, and encapsulation seals to get the moisture-keeping composition;
Preferably, the highland barley embryo bud oil the preparation method comprises the following steps: take barley germ crush, drying, pass through supercritical CO2Flow process It being extracted, extracting pressure 30-50MPa, extraction temperature is 30-50 DEG C, separating pressure 5-15MPa, 40-60 DEG C of separation temperature, Extraction time 1-2h, gained highland barley embryo bud oil crude product are further purified by molecular distillation technique, distillation pressure 3-10Pa, distillation It 130-150 DEG C of temperature, collects heavy constituent and obtains required highland barley embryo bud oil.
10. the application that a kind of composition as described in any one of claim 1-8 is used to prepare the cosmetics with moisture-keeping function;
Preferably, the cosmetics include in facial cleanser, essential oils, face cream or moisturizer any one or at least two group It closes, preferably essential oils.
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CN111110596A (en) * 2020-02-18 2020-05-08 广州栋方生物科技股份有限公司 Sebum membrane bionic composition and preparation method thereof
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CN115444773A (en) * 2022-08-23 2022-12-09 陕西畅想制药有限公司 Anti-inflammatory repairing composition containing glycol salicylate, preparation method and application
CN115501160A (en) * 2022-09-23 2022-12-23 广州千蕊生物科技有限公司 Long-acting moisturizing repairing lip balm and preparation method thereof
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CN110200858A (en) * 2019-07-09 2019-09-06 许富明 A kind of bath oil and preparation method thereof
CN110840778A (en) * 2019-12-13 2020-02-28 广州诗妃生物科技有限公司 Emulsion type mask liquid and preparation method thereof
CN111110596A (en) * 2020-02-18 2020-05-08 广州栋方生物科技股份有限公司 Sebum membrane bionic composition and preparation method thereof
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CN115501160A (en) * 2022-09-23 2022-12-23 广州千蕊生物科技有限公司 Long-acting moisturizing repairing lip balm and preparation method thereof
CN115501160B (en) * 2022-09-23 2024-03-19 广州千蕊生物科技有限公司 Long-acting moisturizing and repairing lip balm and preparation method thereof
CN115721581A (en) * 2022-11-23 2023-03-03 深圳市仙迪化妆品股份有限公司 Antioxidant composition and skin-moistening essence oil prepared from same

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