CN109966183B - Moisturizing and repairing composition and preparation method and application thereof - Google Patents
Moisturizing and repairing composition and preparation method and application thereof Download PDFInfo
- Publication number
- CN109966183B CN109966183B CN201910365190.XA CN201910365190A CN109966183B CN 109966183 B CN109966183 B CN 109966183B CN 201910365190 A CN201910365190 A CN 201910365190A CN 109966183 B CN109966183 B CN 109966183B
- Authority
- CN
- China
- Prior art keywords
- parts
- oil
- moisturizing
- fruit oil
- fruit
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/68—Sphingolipids, e.g. ceramides, cerebrosides, gangliosides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
Abstract
The invention discloses a moisturizing and repairing composition, a preparation method and an application thereof, wherein the composition comprises the following components in parts by weight: 30-50 parts of macadamia nut seed oil, 1-10 parts of highland barley germ oil, 0.1-8 parts of phytosterol oleate, 0.1-8 parts of cocoa resin of dahua cocoa and 0.1-8 parts of ceramide-2. The moisturizing composition disclosed by the invention is reasonable in formula, multiple components are synergistic, the skin barrier can be effectively repaired, the moisturizing performance is outstanding, the moisturizing composition is mild and non-irritant, the skin feeling is good, the absorption effect is good, and the moisturizing composition has the effects of moisturizing and repairing the skin barrier.
Description
Technical Field
The invention relates to the technical field of daily chemicals, and mainly relates to a moisturizing and repairing composition as well as a preparation method and application thereof.
Background
Moisture is the first factor of beautiful skin, and whether skin cells are plump and full, whether skin is smooth and tender, and whether skin color is crystal clear or not all depend on the moisture content in skin. The rate of water loss is the most important factor in affecting the moisture content of the skin. Normal skin has barrier function composed of sebum membrane, horny layer keratin, lipid, mucopolysaccharide in dermis, mucopolysaccharide, etc., and can effectively inhibit water loss. However, with the aging, the sebum secretion of the skin is reduced, and with the aggravation of environmental pollution, the pressure of social transition, the temperature change of seasonal transition, dry air conditioner, computer radiation and other external invasion, the sebum membrane on the surface of the horny layer of the skin becomes gradually thinner, the natural moisturizing factor and hyaluronic acid of the skin are reduced, the water content of the dermis layer is continuously reduced, and various skin problems such as dry skin, wrinkles, dullness, looseness, aging and the like can not be effectively controlled. The moisture in the female skin is greatly lost from the age of 20, the sebum membrane is thinned, and the external invasion is added, the renewal speed of natural water-carrying factors cannot meet the requirement of skin moisture retention, so that the collagen elastic net is broken, the metabolism is slowed, various skin problems can be followed, the water replenishing action is not in place, and the skin finally falls into an irreversible desert state. Perfect disintegration can be achieved in water soothing and moisturizing for any season, age, skin problem. The skin-care product has the functions of repairing the barrier function of the skin and reducing the loss of moisture, and is the basis of all skin care, and whitening, sun protection, oil control, acne resistance, aging resistance and the like are completed on the basis of moistening the skin.
CN105213226A discloses a cosmetic composition containing macadamia nut oil and a preparation method thereof, wherein the macadamia nut oil accounts for 0.01-15 parts of the total weight of the cosmetic composition, and the cosmetic composition is prepared by respectively heating an oil phase and a water phase until the oil phase and the water phase are completely dissolved, slowly adding the water phase into the oil phase, rapidly stirring, cooling to room temperature and then cooling. The cosmetic composition containing the macadamia nut oil prepared by the invention has moisturizing effect; and the prepared cosmetic composition can slow down the oxidation speed of the macadamia nut oil in the composition, thereby prolonging the shelf life of the cosmetic composition, but the moisturizing effect of the composition is not obvious, and the absorption rate and the use skin feel of the composition are poor.
CN105411865A discloses a multi-effect moisturizing microemulsion essence containing multiple vegetable oils, which comprises the following components: caprylic/capric triglyceride, polydimethylsiloxane, olive oil, argania oil, macadamia nut oil, wheat germ oil, coconut oil, shea butter, grape seed oil, avocado oil, jojoba oil, canola oil, meadowfoam seed oil, tocopheryl acetate, phytosterol/octyldodecanol lauroyl glutamate, purified water, hydrogenated lecithin, glycerol, EDTA-2NA, 1, 3-propanediol, polyglycerol-10 oleate and polyglycerol-2 oleate, and the microemulsion essence containing various vegetable oils and fats is prepared under the action of high-pressure homogenization. The microemulsion essence has stable formula, refreshing feeling, no stickiness, and easy absorption by skin. However, the invention has no moisturizing effect, and has complex components and complex preparation process.
Therefore, the moisturizing composition with excellent moisturizing effect is provided, and has important significance and wide market prospect in the field of cosmetics.
Disclosure of Invention
The invention provides a moisturizing and repairing composition and a preparation method and application thereof, the moisturizing composition comprises macadamia nut seed oil, highland barley germ oil, phytosterol oleate, cocoa butter of dahua and ceramide-2, the five components are synergistic, and the moisturizing and repairing composition has the effects of moisturizing, nourishing and protecting skin.
In a first aspect, the invention provides a moisturizing composition, which comprises the following components in parts by weight:
the macadamia nut oil is a yellow oily liquid which has a slightly oil fragrant smell, can be dissolved with most of plant essential oil, and is a pure plant oil which is difficult to obtain and is not easy to be turbid at a low temperature. The macadimia fuliginea nut seed oil is rich in nutrients necessary for forming a grease protective layer on skin, can calm skin, repair skin sensitivity, sunburn and blow wound caused by environment, protect cell membrane, moisten and preserve moisture, has good ductility, and can make skin soft and active.
The hydrangea macrophylla is also called a gupuacu fruit tree, is a fruit tree growing in amazon river basin, and is also an environment-friendly plant for protecting rainforests. The cocoa mass grows on branches like the species theobroma cacao, the fruit of which is the largest among the species theobroma, and the oils extracted from their seeds, after filtration and refining, show exceptional properties in the cosmetic industry. Cocoa butter of the dahua tree is a triglyceride consisting of saturated and unsaturated fatty acids uniformly, which results in a product with a lower melting point that quickly appears as a soft paste when in contact with the skin. The cupuasu fruit oil has a high water absorption capacity, about 240% of lanolin, and certain sterols of animal and vegetable origin, which make the product very stable in emulsion. The oil of cupuasu fruit, as an emollient, has a pleasant and soft feel to the skin and a natural moisturization and elasticity on dry and damaged skin.
The green plants are one of the main crops in the Qinghai-Tibet plateau and have a long planting history. The day and night temperature difference of the Qinghai-Tibet plateau is large, the sunlight radiation is strong, and the unique growth conditions ensure that the Qinghai-naked plants contain rich nutritional functional components. The green plant germ is a byproduct of green plant milling, the content of unsaturated fatty acid in the green plant germ is rich, and the content of linoleic acid and linolenic acid is higher than that of corresponding fatty acid in wheat germ oil. Besides, the oil of the green plant germ is rich in vitamin E, vitamin D and beta-sitosterol; wherein VE is an important health-care functional factor and has the capabilities of resisting oxidation, eliminating free radicals and regulating functional disorder of the organism caused by free radical damage.
Ceramide is a lipid naturally present in the skin, forming a water-resistant barrier at the skin surface. They not only help the skin to retain moisture, but also promote self-repair of the skin barrier and regulate skin cells. The skin of newborn babies is often covered with a waxy substance called vernix, which is mainly composed of ceramide and prevents the loss of water from the skin. The secretion of ceramides in the skin decreases with age, causing skin dryness, wrinkles and some skin inflammations.
The phytosterol is obtained by physical purification from corn and soybean, and has the characteristics of high nutritive value, strong physiological activity and the like. The phytosterol has high permeability to skin, can maintain skin surface moisture, promote skin metabolism, inhibit skin inflammation, prevent sunburn and erythema, prevent skin aging, and promote hair growth and caring hair. Can be used as emulsifier for cream production, and has the advantages of good use feeling (good auxiliary spreading property, smoothness, non-stick), good durability, and no deterioration. In addition, the phytosterol has oxidation resistance, can maintain the softness and the moisture of cells, has mild permeability to the skin, can keep the moisture of the skin, and can promote the metabolism of the skin and repair the skin barrier.
The moisturizing composition provided by the invention is prepared from the skin materials according to a moisturizing and skin-care theory, has a targeting effect, not only has the effects of moisturizing and nourishing, but also has the effects of promoting the metabolism of skin, resisting aging, diminishing inflammation and the like, and all components are matched together in the proportion provided by the invention, so that the purpose of synergy can be achieved.
The macadamia nut seed oil is 30-50 parts, such as 30 parts, 33 parts, 35 parts, 37 parts, 39 parts, 41 parts, 42.6 parts, 43 parts, 45 parts, 47 parts, 49 parts or 50 parts.
The highland barley germ oil is 1-10 parts, for example, 1 part, 2 parts, 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts, 9 parts or 10 parts.
The phytosterol oleate is 0.1-8 parts, and can be, for example, 0.1 part, 0.2 part, 0.3 part, 0.5 part, 1 part, 3 parts, 5 parts, 7 parts or 8 parts.
The above-mentioned cacao seed resin is 0.1-8 portions, for example, 0.1 portion, 0.2 portion, 0.3 portion, 0.5 portion, 1 portion, 3 portions, 5 portions, 7 portions or 8 portions.
The ceramide-2 is 0.1 to 8 parts, and may be, for example, 0.1 part, 0.2 part, 0.3 part, 0.5 part, 1 part, 3 parts, 5 parts, 7 parts or 8 parts.
Preferably, the composition comprises the following components in parts by weight:
preferably, the composition comprises the following components in parts by weight:
preferably, the composition further comprises a binder.
Preferably, the base comprises jojoba oil, olive oil, rosa canina oil, evening primrose oil, tocopherol, wild soybean oil, alkanna tinctoria extract, perfume, bisabolol, mugwort palm seed fat, shea butter oil, vegetable egyptian palm oil, maurel oil and ethylhexyl salicylate.
Preferably, the base material comprises the following components in parts by weight: 8-15 parts of jojoba seed oil, 20-40 parts of olive fruit oil, 2-5 parts of rosa canina fruit oil, 3-5 parts of evening primrose oil, 0.3-1 part of tocopherol and wild soybean oil, 0.3-1 part of radix lithospermi extract, 0.05-1 part of essence, 0.3-1 part of bisabolol, 0.01-1 part of murraya asteroides palm seed fat, 0.01-1 part of shea butter oil, 0.01-1 part of vegetable elaeagnus conferta fruit oil, 0.05-1 part of maurel fruit oil and 0.05-1 part of ethylhexyl salicylate.
The jojoba seed oil is 8-15 parts, for example, 8 parts, 10 parts, 11 parts, 12 parts, 13 parts, 14 parts or 15 parts.
The olive fruit oil is 20-40 parts, such as 20 parts, 22.27 parts, 26.36 parts, 30 parts, 30.87 parts, 31.76 parts, 35.67 parts or 40 parts.
The Rosa canina fruit oil is 2-5 parts, such as 2 parts, 3 parts, 4 parts or 5 parts.
The evening primrose oil is 3-5 parts, for example, 3 parts, 4 parts or 5 parts.
The tocopherol and the wild soybean oil are 0.3-1 part, for example, 0.3 part, 0.5 part, 0.7 part, 0.9 part or 1 part, the proportion of the tocopherol and the wild soybean oil does not influence the effect of the moisturizing composition, and the sum of the tocopherol and the wild soybean oil is 0.3-1 part.
The amount of the radix Arnebiae extract is 0.3-1 parts, such as 0.3 parts, 0.5 parts, 0.7 parts or 1 part.
The essence is 0.05-1 part, for example, 0.05 part, 0.1 part, 0.3 part, 0.5 part, 0.7 part or 1 part.
The bisabolol is 0.3 to 1 part, and may be, for example, 0.3 part, 0.5 part, 0.7 part or 1 part.
The content of the malus micromalus seed fat is 0.01-1 part, such as 0.01 part, 0.1 part, 0.3 part, 0.5 part or 1 part.
The shea butter oil is 0.01-1 part, and can be 0.01 part, 0.1 part, 0.3 part, 0.5 part or 1 part, for example.
The vegetable Evola nervosa fruit oil is 0.01-1 part, such as 0.01 part, 0.1 part, 0.3 part, 0.5 part or 1 part.
The amount of the Daphnia lansium fruit oil is 0.05-1 part, and may be, for example, 0.05 part, 0.15 part, 0.35 part, 0.4 part, 0.6 part, 0.8 part or 1 part.
The ethylhexyl salicylate may be, for example, 0.05 part, 0.1 part, 0.3 part, 0.5 part or 1 part to 0.05 part to 1 part.
Preferably, the composition comprises the following components in parts by weight: 30-50 parts of macadamia nut seed oil, 1-10 parts of highland barley germ oil, 0.1-8 parts of phytosterol oleate, 0.1-8 parts of cocoa butter of dahua, 0.1-8 parts of ceramide-2, 8-15 parts of jojoba seed oil, 20-40 parts of olive fruit oil, 2-5 parts of rosa canina fruit oil, 3-5 parts of evening primrose oil, 0.3-1 part of tocopherol and wild soybean oil, 0.3-1 part of radix lithospermi extract, 0.05-1 part of essence, 0.3-1 part of bisabolol, 0.01-1 part of muruscus aluta seed fat, 0.01-1 part of shea butter, 0.01-1 part of vegetable egyptian palm fruit oil, 0.05-1 part of ruizhi palm fruit oil and 0.05-1 part of ethylhexyl salicylate.
Preferably, the base material comprises the following components in parts by weight: : 10 parts of jojoba seed oil, 30 parts of olive fruit oil, 3 parts of rosa canina fruit oil, 4 parts of evening primrose oil, 0.5 part of tocopherol and wild soybean oil, 0.5 part of radix lithospermi extract, 0.05 part of essence, 0.5 part of bisabolol, 0.3 part of mugwort palm seed fat, 0.3 part of shea butter resin oil, 0.3 part of vegetable egyptian palm fruit oil, 0.5 part of palmityl palm fruit oil and 0.05 part of ethylhexyl salicylate.
Preferably, the composition comprises the following components in parts by weight: 42 parts of macadamia nut seed oil, 5 parts of highland barley germ oil, 1 part of phytosterol oleate, 1 part of cocoa butter of dahua, 1 part of ceramide-2, 10 parts of jojoba seed oil, 30 parts of olive fruit oil, 3 parts of rosa canina fruit oil, 4 parts of evening primrose oil, 0.5 parts of tocopherol and wild soybean oil, 0.5 parts of radix lithospermi extract, 0.05 parts of essence, 0.5 parts of bisabolol, 0.3 parts of mugwort palm seed fat, 0.3 parts of shea butter, 0.3 parts of vegetable eggplanta fruit oil, 0.5 parts of palm fruit oil and 0.05 parts of ethylhexyl salicylate.
In a second aspect, the present invention provides a method for preparing the moisturizing repair composition according to the first aspect, comprising the steps of:
weighing the corresponding components according to the formula ratio, mixing, heating to 60-80 ℃, homogenizing and stirring at the rotating speed of 100-2000rpm/min for 3-10min, fully mixing, filtering, packaging and sealing to obtain the moisturizing composition.
The temperature is 60-80 deg.C, such as 60 deg.C, 62 deg.C, 65 deg.C, 67 deg.C, 70 deg.C, 72 deg.C, 75 deg.C, 78 deg.C or 80 deg.C.
The rotation speed is 100-2000rpm/min, and may be, for example, 100rpm/min, 200rpm/min, 300rpm/min, 400rpm/min, 500rpm/min, 600rpm/min, 700rpm/min, 800rpm/min, 900rpm/min, 1000rpm/min, 1100rpm/min, 1200rpm/min, 1300rpm/min, 1400rpm/min, 1500rpm/min, 1600rpm/min, 1700rpm/min, 1800rpm/min, 1900rpm/min or 2000 rpm/min.
The time is 3-10min, for example, 3min, 4min, 5min, 6min, 7min or 10 min.
The preparation method of the composition is simple and feasible, and is easy to prepare.
Preferably, the preparation method of the highland barley germ oil comprises the following steps: pulverizing fructus Avenae Nudae embryo, oven drying, and passing through supercritical CO2Extracting by a fluid method, wherein the extraction pressure is 30-50MPa, the extraction temperature is 30-50 ℃, the separation pressure is 5-15MPa, the separation temperature is 40-60 ℃, the extraction time is 1-2h, further purifying the obtained highland barley embryo oil crude product by a molecular distillation technology, the distillation pressure is 3-10Pa, the distillation temperature is 130-150 ℃, and collecting heavy components to obtain the required highland barley embryo oil.
The extraction pressure is 30 to 50MPa, and may be, for example, 30MPa, 35MPa, 40MPa, 45MPa or 50 MPa.
The extraction temperature is 30-50 deg.C, such as 30 deg.C, 32 deg.C, 35 deg.C, 40 deg.C, 45 deg.C or 50 deg.C.
The separation pressure is 5 to 15MPa, and may be, for example, 5MPa, 6MPa, 7MPa, 8MPa, 9MPa, 10MPa, 11MPa, 12MPa, 13MPa, 14MPa or 15 MPa.
The separation temperature is 40-60 deg.C, such as 40 deg.C, 45 deg.C, 50 deg.C, 55 deg.C or 60 deg.C.
The extraction time is 1-2h, for example 1h, 1.2h, 1.5h, 1.8h or 2 h.
The distillation pressure is 3 to 10Pa, and may be, for example, 3Pa, 4Pa, 5Pa, 6Pa, 7Pa, 8Pa, 9Pa or 10 Pa.
The distillation temperature is 130-150 ℃, and can be 130 ℃, 135 ℃, 140 ℃, 145 ℃ or 150 ℃.
The method for preparing the highland barley germ oil comprises the steps of firstly passing through supercritical CO2The fluid extraction method has high extraction rate, and the obtained highland barley germ oil contains more than 75% of unsaturated fatty acid, 10% of oleic acid, 65% of linoleic acid and 1% of linolenic acid, and abundant vitamin E and beta-sitosterol. The linoleic acid, the linolenic acid, the vitamin E and the beta-sitosterol have the effect of repairing skin barriers, but the oleic acid blocks pores, can increase the permeability of epidermis, destroys the barrier function of skin and causes stimulation. The highland barley embryo oil obtained by the method is further purified by a molecular distillation technology, oleic acid components in the highland barley embryo oil are separated, and the prepared highland barley embryo oil has good effects of repairing skin barriers and moisturizing.
In a third aspect, the present invention provides the use of a moisturizing composition as described in the first aspect for the preparation of a cosmetic product having a moisturizing effect.
Preferably, the cosmetic comprises any one or combination of at least two of facial cleanser, essential oil, cream or moisturizing milk, for example, the combination of facial cleanser and essential oil, the combination of facial cream and moisturizing milk or the combination of essential oil and moisturizing milk, preferably the essential oil.
Compared with the prior art, the invention has the beneficial effects that:
(1) the moisturizing composition provided by the invention is reasonable in formula, multiple components are synergistic, the skin barrier can be effectively repaired, the moisturizing performance is outstanding, the moisturizing composition is mild and non-irritant, the skin feeling is good, the absorption effect is good, and the moisturizing composition has the effects of moisturizing and conditioning the skin.
(2) The preparation method provided by the invention is simple and efficient, easy to popularize and environment-friendly.
Detailed Description
To further illustrate the technical means and effects of the present invention, the following further describes the technical solution of the present invention with reference to the preferred embodiments of the present invention, but the present invention is not limited to the scope of the embodiments.
Example 1
The moisture-keeping composition comprises the following five components in parts by weight:
the components of the base material are 10 parts of jojoba seed oil, 30 parts of olive fruit oil, 3 parts of rosa canina fruit oil, 4 parts of evening primrose oil, 0.5 part of tocopherol and wild soybean oil, 0.5 part of radix lithospermi extract, 0.05 part of essence, 0.5 part of bisabolol, 0.3 part of mugwort palm seed fat, 0.3 part of shea butter, 0.3 part of vegetable egyptian palm fruit oil, 0.5 part of sorrel fruit oil and 0.05 part of ethylhexyl salicylate.
The method for preparing the essential oil by using the components comprises the following steps: weighing the corresponding components according to the formula ratio, mixing, heating to 70 ℃, homogenizing and stirring for 3-10 minutes in the same direction at 100rpm/min, fully mixing, filtering, packaging and sealing to obtain the essential oil;
the preparation method of the highland barley germ oil comprises the following steps: pulverizing fructus Avenae Nudae embryo, oven drying, and passing through supercritical CO2Extracting by a fluid method, wherein the extraction pressure is 40MPa, the extraction temperature is 40 ℃, the separation pressure is 10MPa, the separation temperature is 50 ℃, the extraction time is 1.5h, further purifying the obtained highland barley embryo oil crude product by a molecular distillation technology, the distillation pressure is 6Pa, the distillation temperature is 140 ℃, and collecting heavy components to obtain the required highland barley embryo oil.
Example 2
The moisture-keeping composition comprises the following five components in parts by weight:
the components of the base material are 8 parts of jojoba seed oil, 20 parts of olive fruit oil, 2 parts of rosa canina fruit oil, 3 parts of evening primrose oil, 0.3 part of tocopherol and wild soybean oil, 0.4 part of radix lithospermi extract, 0.05 part of essence, 0.3 part of bisabolol, 0.01 part of mugwort palm seed fat, 0.01 part of shea butter, 0.01 part of vegetable egyptian palm fruit oil, 0.05 part of sorrel fruit oil and 0.05 part of ethylhexyl salicylate;
the preparation method is the same as example 1.
Example 3
The moisture-keeping composition comprises the following five components in parts by weight:
the components of the base material are 15 parts of jojoba seed oil, 40 parts of olive fruit oil, 5 parts of rosa canina fruit oil, 5 parts of evening primrose oil, 1 part of tocopherol and wild soybean oil, 1 part of radix Arnebiae extract, 1 part of essence, 1 part of bisabolol, 1 part of mugwort palm seed fat, 1 part of shea butter, 1 part of vegetable elaeagnus mollis fruit oil, 1 part of palmetto fruit oil and 1 part of ethylhexyl salicylate;
the preparation method is the same as example 1.
Example 4
The moisture-keeping composition comprises the following five components in parts by weight:
the components of the base material are 9 parts of jojoba seed oil, 36 parts of olive fruit oil, 3 parts of rosa canina fruit oil, 4 parts of evening primrose oil, 0.7 part of tocopherol and wild soybean oil, 0.5 part of radix lithospermi extract, 0.3 part of essence, 0.5 part of bisabolol, 0.3 part of mugwort palm seed fat, 0.5 part of shea butter, 0.5 part of vegetable egyptian palm fruit oil, 0.5 part of sorrel fruit oil and 0.5 part of ethylhexyl salicylate;
the preparation method is the same as example 1.
Example 5
The moisture-keeping composition comprises the following five components in parts by weight:
the components of the base material are 13 parts of jojoba seed oil, 38 parts of olive fruit oil, 4 parts of rosa canina fruit oil, 4 parts of evening primrose oil, 0.7 part of tocopherol and wild soybean oil, 0.7 part of radix lithospermi extract, 0.3 part of essence, 0.7 part of bisabolol, 0.7 part of mugwort palm seed fat, 0.3 part of shea butter, 0.7 part of vegetable egyptian palm fruit oil, 0.5 part of sorrel fruit oil and 0.7 part of ethylhexyl salicylate;
the preparation method is the same as example 1.
Comparative example 1
The conditions were the same as in example 1 except that only the binder was added, compared to example 1.
Comparative example 2
Shouwu village skin rejuvenation essential oils (caprylic/capric triglyceride, trioctyl carbonate, tocopherol (vitamin E), essence, sunflower seed oil, pentaerythritol tetrakis (bis-tert-butyl hydroxyhydrocinnamic acid) ester, camellia seed oil, almond oil, eggnoguo seed oil, macadamia nut oil, jojoba seed oil, coriander fruit oil, corn oil, rice bran oil, rosa canina fruit oil, ribes nigrum seed oil, capsicum extract) were purchased.
Comparative example 3
The natural harmonizing body care oil (European hazel seed oil, European geranium oil, rosemary leaf oil and peppermint leaf oil) of charming poem is purchased.
Comparative example 4
The nourishing essence oil (squalane, European plum seed extract, camelina sativa seed oil, tocopherol (vitamin E), caprylic/capric triglyceride, rose extract, jojoba seed oil, leaf extract of Padina pavonica, white orchid leaf oil, Pelargonium graveolens sunflower oil, Rosa damascena flower oil, avocado oil unsaponifiable matter, hydrogenated soybean oil) is purchased from Hicissi black rose.
Comparative example 5
The conditions were the same as in example 1 except that no macadamia nut oil was added, compared to example 1.
Comparative example 6
Compared with example 1, the method is the same as example 1 except that highland barley germ oil is not added.
Comparative example 7
The conditions were the same as in example 1 except that ceramide-2 was not added, compared with example 1.
Comparative example 8
The procedure of example 1 was repeated except that phytosterol oleate was not added, as compared with example 1.
Comparative example 9
The conditions were the same as in example 1 except that no macrocarpable resin was added as compared with example 1.
Sensory testing
9 subjects were selected and evaluated for 9 indexes of fragrance, appearance, brightness, absorbency, oily feeling, residual feeling, heat sensation, irritation, and general preference of the samples of examples and comparative examples, with the evaluation criteria shown in Table 1 and the test results shown in Table 2.
TABLE 1
TABLE 2
The test comparison test is carried out on each sample by 9 subjects, and the following results are shown in the table:
1. compared with the base material of the comparative example 1, the essential oil of the example 1 has the advantages that three appearance indexes of fragrance, appearance and brightness are reduced, two indexes of absorptivity and heating feeling are unchanged, and the residual feeling, irritation and overall preference are improved;
2. the residues of the natural harmony poem blended body care oil, the essential oil, the shizuri nourishing essential oil and the base material after use are close to each other and are lower than the residues of the essence oil after use;
3. the overall preference of 9 subjects to essential oil was similar to the natural blend body care oil of the charm poem and was significantly higher than the base;
4. the essential oils of examples 1-5 all had good aroma, appearance, brightness and absorbency, low oily feel, irritation and heat build-up, and high overall preference. Compared with the comparative example 5, the product has poor appearance, brightness and absorption in the absence of the macadimia nut seed oil; compared with the comparative example 6, the highland barley germ oil is lacked, the product has poor absorptivity, and the product has serious residual feeling; compared with the comparative example 7, the product lacks phytosterol oleate, and has poor brightness and absorption, heavy residual feeling and greasy skin feeling; compared with the comparative example 8, the product lacks the cocoa butter of the dahua, the appearance of the product is relatively poor, and the product has stronger heat sensation and irritation; compared with comparative example 9, the product lacks ceramide-2, the product has poor absorptivity, heavy residual feeling and more serious heating and irritation. Overall preference, examples 1-5 are significantly better than comparative examples 5-9.
Moisture content test
The instrument comprises the following steps: skin moisture content tester (Germany C & K, Corneometer CM825)
The principle is as follows: the probe of the skin moisture content measuring instrument is based on the principle of capacitance to measure. Water has a dielectric constant of 81, other substances generally have a dielectric constant of less than 7, and water is the substance with the highest dielectric constant on the skin. When the moisture content changes, the capacitance of the skin also changes, so the moisture content on the skin surface can be analyzed by measuring the capacitance of the skin. The measured value is a relative value. The Units are represented by C.U. (Corneometer Units) and the test results are shown in table 3.
Subject: selecting a subject, selecting a subject with dry forearm skin, and enabling the inclusion moisture value to be less than 45;
testing parts: inner side of forearm
The product dosage is as follows: 2mg/cm2
TABLE 3
As can be seen from table 3, the moisturizing effects of the essential oils prepared in examples 1 to 5 are greatly improved compared to the base material, wherein the moisturizing effect of example 1 is the best, and is significantly better than that of the samples of comparative examples 1 to 9. The moisturizing effect is obviously superior to that of the essence of the three competitive products sold in the market, one of the five components is not available, and the lack of any one of the components in comparative examples 5-9 can obviously reduce the moisturizing effect and influence the synergistic effect of the moisturizing repair composition.
Transdermal water loss test
The instrument comprises the following steps: skin surface moisture loss tester (Germany C & K, Tewameter TM300)
The principle is as follows: a test probe of a skin surface moisture loss tester forms a relatively stable test small environment on the skin surface by using a specially designed cylindrical cavity vehicle probe with two open ends, measures the water vapor pressure gradient at two different points formed by the moisture loss of the horny layer near the epidermis (within about 1 cm) through two groups of temperature and humidity sensors, and directly measures the water content evaporated by the epidermis so as to measure the moisture loss condition on the skin surface. The unit is g/h.m2The test results are shown in Table 4.
Subject: selecting a subject, selecting a subject with dry forearm skin, and enabling the inclusion moisture value to be less than 45;
testing parts: inner side of forearm
The product dosage is as follows: 2mg/cm2
TABLE 4
| Sample (I) | Before use | One week | Two weeks | 4 weeks |
| Example 1 | 23.15 | 22.83 | 21.63 | 18.36 |
| Example 2 | 25.18 | 25.12 | 23.58 | 20.74 |
| Example 3 | 23.66 | 23.27 | 22.46 | 19.35 |
| Example 4 | 24.75 | 24.58 | 23.15 | 19.93 |
| Example 5 | 22.83 | 22.68 | 21.36 | 18.42 |
| Comparative example 1 | 25.47 | 25.45 | 25.32 | 24.82 |
| Comparative example 2 | 24.62 | 24.55 | 23.88 | 22.15 |
| Comparative example 3 | 25.48 | 25.34 | 25.06 | 23.28 |
| Comparative example 4 | 26.73 | 26.52 | 26.17 | 24.47 |
| Comparative example 5 | 25.48 | 25.62 | 25.44 | 24.15 |
| Comparative example 6 | 25.17 | 25.15 | 24.96 | 24.33 |
| Comparative example 7 | 26.22 | 26.26 | 25.78 | 24.52 |
| Comparative example 8 | 24.82 | 24.96 | 24.38 | 23.68 |
| Comparative example 9 | 25.63 | 25.56 | 25.07 | 24.27 |
The less moisture is lost through the skin, indicating better skin barrier function. As can be seen from Table 4, the amount of transdermal water loss in the test area after the subjects used the essential oils prepared in examples 1 to 5 was gradually reduced with the time of use of the samples within 4 weeks of the test period, indicating that it was effective in improving the barrier function of the skin and the effect was significantly better than that of comparative example 1 containing only the base material. The barrier repair function was greatly improved compared to the base material, with the best barrier repair of example 1, and the transepidermal water loss of subjects was improved by 20.69% after 4 weeks using the samples. The moisturizing effect is obviously superior to that of the essence of the three competitive products sold in the market, one of the five components is not available, and the lack of any one of the components in comparative examples 5-9 can obviously reduce the barrier repair function of the composition and influence the synergy of the moisturizing repair composition.
In conclusion, the moisturizing composition provided by the invention is based on the theory of oil control and skin care, the materials are selected for skin measurement, and the components are matched together according to the proportion mentioned in the invention, so that the purpose of synergy can be achieved.
The applicant states that the present invention is illustrated in detail by the above examples, but the present invention is not limited to the above detailed methods, i.e. it is not meant that the present invention must rely on the above detailed methods for its implementation. It should be understood by those skilled in the art that any modification of the present invention, equivalent substitutions of the raw materials of the product of the present invention, addition of auxiliary components, selection of specific modes, etc., are within the scope and disclosure of the present invention.
Claims (10)
1. The moisturizing and repairing composition is characterized by comprising the following components in parts by weight:
and a base stock;
the base material comprises the following components in parts by weight: 8-15 parts of jojoba seed oil, 20-40 parts of olive fruit oil, 2-5 parts of rosa canina fruit oil, 3-5 parts of evening primrose oil, 0.3-1 part of tocopherol and wild soybean oil, 0.3-1 part of radix lithospermi extract, 0.05-1 part of essence, 0.3-1 part of bisabolol, 0.01-1 part of murraya asteroides palm seed fat, 0.01-1 part of shea butter oil, 0.01-1 part of vegetable elaeagnus conferta fruit oil, 0.05-1 part of maurel fruit oil and 0.05-1 part of ethylhexyl salicylate.
2. The composition according to claim 1, wherein the composition comprises the following components in parts by weight:
and a base stock;
the base material comprises the following components in parts by weight: 8-15 parts of jojoba seed oil, 20-40 parts of olive fruit oil, 2-5 parts of rosa canina fruit oil, 3-5 parts of evening primrose oil, 0.3-1 part of tocopherol and wild soybean oil, 0.3-1 part of radix lithospermi extract, 0.05-1 part of essence, 0.3-1 part of bisabolol, 0.01-1 part of murraya asteroides palm seed fat, 0.01-1 part of shea butter oil, 0.01-1 part of vegetable elaeagnus conferta fruit oil, 0.05-1 part of maurel fruit oil and 0.05-1 part of ethylhexyl salicylate.
3. The composition according to claim 2, wherein the composition comprises the following components in parts by weight:
and a base stock;
the base material comprises the following components in parts by weight: 8-15 parts of jojoba seed oil, 20-40 parts of olive fruit oil, 2-5 parts of rosa canina fruit oil, 3-5 parts of evening primrose oil, 0.3-1 part of tocopherol and wild soybean oil, 0.3-1 part of radix lithospermi extract, 0.05-1 part of essence, 0.3-1 part of bisabolol, 0.01-1 part of murraya asteroides palm seed fat, 0.01-1 part of shea butter oil, 0.01-1 part of vegetable elaeagnus conferta fruit oil, 0.05-1 part of maurel fruit oil and 0.05-1 part of ethylhexyl salicylate.
4. The composition as claimed in claim 1, wherein the base material comprises the following components in parts by weight: 10 parts of jojoba seed oil, 30 parts of olive fruit oil, 3 parts of rosa canina fruit oil, 4 parts of evening primrose oil, 0.5 part of tocopherol and wild soybean oil, 0.5 part of radix lithospermi extract, 0.05 part of essence, 0.5 part of bisabolol, 0.3 part of mugwort palm seed fat, 0.3 part of shea butter resin oil, 0.3 part of vegetable egyptian palm fruit oil, 0.5 part of palmityl palm fruit oil and 0.05 part of ethylhexyl salicylate.
5. The composition according to claim 3, wherein the composition comprises the following components in parts by weight: 42 parts of macadamia nut seed oil, 5 parts of highland barley germ oil, 1 part of phytosterol oleate, 1 part of cocoa butter of dahua, 1 part of ceramide-2, 10 parts of jojoba seed oil, 30 parts of olive fruit oil, 3 parts of rosa canina fruit oil, 4 parts of evening primrose oil, 0.5 parts of tocopherol and wild soybean oil, 0.5 parts of radix lithospermi extract, 0.05 parts of essence, 0.5 parts of bisabolol, 0.3 parts of mugwort palm seed fat, 0.3 parts of shea butter, 0.3 parts of vegetable eggplanta fruit oil, 0.5 parts of palm fruit oil and 0.05 parts of ethylhexyl salicylate.
6. A method of preparing a moisturizing repair composition according to any of claims 1-5 comprising the steps of:
weighing the corresponding components according to the formula ratio, mixing, heating to 60-80 ℃, homogenizing and stirring at the rotating speed of 100-2000rpm/min for 3-10min, fully mixing, filtering, packaging and sealing to obtain the moisturizing composition.
7. The preparation method of claim 6, wherein the method for preparing the highland barley germ oil comprises: pulverizing fructus Avenae Nudae embryo, oven drying, and passing through supercritical CO2Extracting by a fluid method, wherein the extraction pressure is 30-50MPa, the extraction temperature is 30-50 ℃, the separation pressure is 5-15MPa, the separation temperature is 40-60 ℃, the extraction time is 1-2h, further purifying the obtained highland barley embryo oil crude product by a molecular distillation technology, the distillation pressure is 3-10Pa, the distillation temperature is 130-150 ℃, and collecting heavy components to obtain the required highland barley embryo oil.
8. Use of a composition according to any one of claims 1 to 5 for the preparation of a cosmetic product with moisturizing effect.
9. The use according to claim 8, wherein the cosmetic comprises any one of facial cleanser, essential oil, cream or moisturizing milk or a combination of at least two of them.
10. Use according to claim 9, characterized in that the cosmetic product is a serum.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910365190.XA CN109966183B (en) | 2019-04-30 | 2019-04-30 | Moisturizing and repairing composition and preparation method and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910365190.XA CN109966183B (en) | 2019-04-30 | 2019-04-30 | Moisturizing and repairing composition and preparation method and application thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109966183A CN109966183A (en) | 2019-07-05 |
| CN109966183B true CN109966183B (en) | 2021-12-07 |
Family
ID=67087476
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910365190.XA Active CN109966183B (en) | 2019-04-30 | 2019-04-30 | Moisturizing and repairing composition and preparation method and application thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109966183B (en) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110200858A (en) * | 2019-07-09 | 2019-09-06 | 许富明 | A kind of bath oil and preparation method thereof |
| CN110840778A (en) * | 2019-12-13 | 2020-02-28 | 广州诗妃生物科技有限公司 | Emulsion type mask liquid and preparation method thereof |
| CN111110596A (en) * | 2020-02-18 | 2020-05-08 | 广州栋方生物科技股份有限公司 | Sebum membrane bionic composition and preparation method thereof |
| CN111388394B (en) * | 2020-04-22 | 2022-07-05 | 广州栋方生物科技股份有限公司 | Biphase freeze-dried powder solvent and preparation method and application thereof |
| CN115444773B (en) * | 2022-08-23 | 2023-09-05 | 陕西畅想制药有限公司 | Anti-inflammatory repair composition containing glycol salicylate, and preparation method and application thereof |
| CN115501160B (en) * | 2022-09-23 | 2024-03-19 | 广州千蕊生物科技有限公司 | Long-acting moisturizing and repairing lip balm and preparation method thereof |
| CN115721581A (en) * | 2022-11-23 | 2023-03-03 | 深圳市仙迪化妆品股份有限公司 | Antioxidant composition and skin-moistening essence oil prepared from same |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107536733A (en) * | 2016-06-27 | 2018-01-05 | 李启初 | A kind of crocodile maintenance oil and preparation method thereof |
| CN108245463A (en) * | 2016-12-28 | 2018-07-06 | 西藏天麦力健康品有限公司 | A kind of preparation method of composition and moisturizing face cream with moisture-keeping efficacy |
| CN106943537B (en) * | 2017-02-28 | 2021-01-26 | 上海清轩生物科技有限公司 | Antibacterial composition and moisturizing repair composition containing camellia seed oil |
| CN108578324A (en) * | 2018-07-02 | 2018-09-28 | 上海新高姿化妆品有限公司 | A kind of skin cream and preparation method thereof with long-acting moisture-keeping efficacy |
| CN109431964A (en) * | 2018-12-29 | 2019-03-08 | 吕飞 | Assign maintenance essence cream living and preparation method thereof in flesh source |
| CN109481338A (en) * | 2019-01-04 | 2019-03-19 | 上海彤颜实业有限公司 | Moisturizing maintenance composition and preparation method comprising ceramide and phytosterol |
-
2019
- 2019-04-30 CN CN201910365190.XA patent/CN109966183B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN109966183A (en) | 2019-07-05 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN109966183B (en) | Moisturizing and repairing composition and preparation method and application thereof | |
| CN107007492B (en) | A kind of makeup remover and preparation method thereof | |
| CN113244151B (en) | Soothing repair cream and preparation method thereof | |
| CN109602668A (en) | A kind of anti-aging anti-wrinkle composition and its application | |
| CN106109308A (en) | facial cleaning cream | |
| CN102406581A (en) | Skin protecting composite with function of tightening skin | |
| CN105505635B (en) | A kind of skin cleansing composition and preparation method thereof containing lotus active constituent | |
| CN108743474A (en) | A kind of ointment shape baby's diaper ointment and preparation method thereof | |
| CN103462835B (en) | A kind of skincare lotion and preparation method thereof | |
| CN106511216A (en) | Moisturizing cosmetic composition and application thereof | |
| US20100323040A1 (en) | Cosmetic composition for topical use comprising wasabi | |
| CN108567641A (en) | The tender factor of vegetation water and the skin care compositions for including the tender factor of vegetation water | |
| CN109381356A (en) | A kind of sleep late frost and preparation method thereof | |
| CN109394608A (en) | A kind of skin maintenance essence cream and preparation method thereof | |
| CN111658566A (en) | Deep moisturizing and face repairing nourishing cream and preparation method thereof | |
| CN110051569A (en) | A kind of chest enlarge conditioning essential oils and preparation method thereof containing fennel oil | |
| CN111481475A (en) | Edible lipstick capable of improving female hormone and preparation method thereof | |
| JP6622015B2 (en) | External preparation for skin or cosmetics | |
| CN114028277A (en) | Skin-soothing cream with effects of relieving and repairing sensitive skin | |
| KR20080096132A (en) | A cosmetic composition containing extracts of suaeda asparagoides for wrinkle reduction | |
| KR20160091798A (en) | Shampoo composition | |
| CN116549323A (en) | Acne-removing skin-care cleansing cream based on oiled acne muscles and preparation method thereof | |
| CN107412016A (en) | A kind of compound essential oil with whitening effect and preparation method thereof | |
| CN105687031A (en) | Total-effect multifunctional moisturizing cream and preparation method thereof | |
| CN110882204A (en) | Camellia repair honey and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |