CN107412016A - A kind of compound essential oil with whitening effect and preparation method thereof - Google Patents
A kind of compound essential oil with whitening effect and preparation method thereof Download PDFInfo
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
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- A61K36/06—Fungi, e.g. yeasts
- A61K36/07—Basidiomycota, e.g. Cryptococcus
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
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- A61K36/185—Magnoliopsida (dicotyledons)
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/65—Paeoniaceae (Peony family), e.g. Chinese peony
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- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/75—Rutaceae (Rue family)
- A61K36/752—Citrus, e.g. lime, orange or lemon
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- C11B9/00—Essential oils; Perfumes
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- A61K2236/30—Extraction of the material
- A61K2236/37—Extraction at elevated pressure or temperature, e.g. pressurized solvent extraction [PSE], supercritical carbon dioxide extraction or subcritical water extraction
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Abstract
The invention discloses a kind of compound essential oil with whitening effect and preparation method thereof.The active component of the described compound essential oil with whitening effect is prepared by the raw material of following parts by weight：1 100 parts of lemon peel, 1 10 parts of ganoderma lucidum, 1 10 parts of the bighead atractylodes rhizome, 1 10 parts of Chinese herbaceous peony, 1 10 parts of radix glycyrrhizae, 1 10 parts of the flower bud of lily magnolia.Start with from the function of the regulation of qi and blood, conditioning the five internal organs, enhance metabolism, improve body immunity, nourishing blood and liver, make qi and blood abundant, appearance is ruddy, so as to whitening spot-removing, may also suppress dark sore, delay skin aging.
Description
Technical field
The invention belongs to cosmetic field, is specifically related to a kind of compound essential oil with whitening effect and its preparation
Method.
Background technology
Everybody has a love of beauty, and pale soft skin is pursuing a goal for most of women.But with the age
Increase, most women were crossed after 25 years old, and the metabolic function of body slows down, and melanin can not be mediated normally, easily in cutin
Layer deposition forms spot, causes skin obscure, and serious can also form chloasma, blackspot and color spot；On the other hand, the modern life
Anxiety, irregularities of working and resting, it is led to that itself resistance declines, endocrinopathy, makes interior free yl activate, increase melanin is different
Often secretion, aggravates skin aging, and the colour of skin is intensely dark.Therefore, the cosmetics with whitening effect are the indispensable use of women
Product.
Plants essential oil be extraction the distinctive aromatic substance of plant, be taken from herbal flower, leaf, root, bark, fruit,
What seed, resin etc. were extract to distill, in a manner of squeezing.Because essential oil-fumigation volatility is high, and molecule is small, it is easy to by people
Body absorbs, and can permeate people's intracorporeal organ rapidly, unnecessary composition is excreted, whole process only needs a few minutes, and plants
The fragrance of thing in itself, the secretion of pituitary gland is also directly stimulated, ferment and hormone secretion etc., function in balanced body, plays U.S.
Hold the effect of skin care.
Chinese patent ZL 200710303707.X disclose a kind of compound essential oil of whitening and skin-protecting, and it is mainly by lemon extract
Oil, frankincense essential oil, refined jasmine oil, flores aurantii essential oil, carrot seed essential oil, grape-kernel oil are mixed according to certain ratio, are had
Good whitening, moisturizing, the effect of skin care.Chinese patent ZL 201410495895.0 discloses a kind of multiple-effect whitening and softening skin and answered
Square essential oil and preparation method, mainly contain flores aurantii essential oil, Rosa Damascana, Geranium Essential, lemon, sweet orange oil, chamomile essence
The compositions such as oil, there is the effect of Eradicates Huangs gas, even skin tone, whitening, tender skin.
From the foregoing, have great importance using essential oil, especially compound essential oil in terms of whitening spot-removing.However,
The compound essential oil that prior art provides all is according to demand to make different folk prescription essential oils together according to certain ratio compounding
, according to the method described above there is the problems such as fragrance is not pure enough, easy discoloration is rotten, effect is bad in obtained compound essential oil.Base
In this, the invention provides a kind of whitening compound essential oil unlike the prior art, contains lemon, bighead atractylodes rhizome isoreactivity composition, tool
There is good whitening spot-removing effect.
The content of the invention
Based on this, the invention provides a kind of compound essential oil with whitening effect.
Concrete technical scheme is as follows：
A kind of compound essential oil with whitening effect, its active component are prepared by the raw material of following parts by weight：Lemon
Skin 1-100 parts, ganoderma lucidum 1-10 parts, bighead atractylodes rhizome 1-10 parts, Chinese herbaceous peony 1-10 parts, radix glycyrrhizae 1-10 parts, flower bud of lily magnolia 1-10 parts.
In wherein some embodiments, the described compound essential oil with whitening spot-removing, its active component is by following weight
The raw material of part is prepared：Lemon peel 10-50 parts, ganoderma lucidum 2-4 parts, bighead atractylodes rhizome 6-8 parts, Chinese herbaceous peony 2-4 parts, radix glycyrrhizae 2-4 parts, flower bud of lily magnolia 6-
8 parts.
In wherein some embodiments, the described compound essential oil with whitening spot-removing can also add base oil, described
Base oil can be selected from hydrocarbon ils, Acrawax, vegetable and animals oils, silicone oil and its mixture.
In a preferred embodiment of the invention, the hydrocarbon ils is White Mineral Oil, vaseline, C15-19 alkane, the hydrogenation poly- last of the ten Heavenly stems
Alkene, isohexadecane, Parleam, paraffin, Permethyl 99A, saualane, ceresine, vaccenic acid it is one or more kinds of
Mixing.
In a preferred embodiment of the invention, the Acrawax is caprylic/capric triglyceride, myristic acid
Isopropyl ester, isononyl isononanoate, ethylhexyl palmitate, glycol distearate, glycerine three（Thylhexoic acid）Ester, cetanol
Ethylhexoate, diisopropyl sebacate, Dermol 105, three different nonyl essences, carbonic acid dioctyl ester, C12-15 alcohol benzoic ethers,
One or more kinds of mixing of propylene glycol carbonate, isopropyl isostearate.
In a preferred embodiment of the invention, the vegetable and animals oils are lanolin, fat of Oromaius norvaehollandeae, horse fat, hippophae rhamnoides fruit oil, ginger
Root oil, soybean oil, safflower seed oil, sun flower seed oil, olive oil, evening primrose oil, rose hip oil, avocado oil, jojoba oil, grape
Seed is oily, white pond flower seed oil, Butyrospermum parkii fruit fatty oil, cocoa seed fat, Queensland nut seed oil, camellia seed oil, palm oil, palm kernel
Oil, dog rose fruit oil, wheat-germ oil, one kind in Sweet Almond Oil or their mixing.
In a preferred embodiment of the invention, the silicone oil is ring five dimethyl silicone polymer, trimethyl silicane alkoxy
The poly- trimethicone of esters of silicon acis, dimethyl silicone polymer, methyl, dimethiconol, phenyl trimethicone,
Cetyl dimethicone, octyl group polymethyl siloxane, the one or more kinds of of stearyl dimethione mix
Close.
Present invention also offers the preparation method of the above-mentioned compound essential oil with whitening spot-removing.
Concrete technical scheme is as follows：
A kind of preparation method of the above-mentioned compound essential oil with whitening spot-removing, comprises the following steps：
（1）Parts by weight as described in claim 1 or 2, by lemon peel, ganoderma lucidum, the bighead atractylodes rhizome, Chinese herbaceous peony, radix glycyrrhizae, the flower bud of lily magnolia remove hard stalk and
Impurity, mixing, dry, pulverize, and cross 10-50 mesh sieve, obtain crushed mixture；Farina is added into crushed mixture
With the mixture of glutinous rice starch, it is well mixed, then freezes 1 ~ 24 hour, obtains freezing；
（2）Freezing is sent into Bulking tank, sealed, takes out negative pressure, steam valve heating is opened, swelling temperature is risen to 90 ~ 95
DEG C, kept for 5-10 minutes；Pressure release, cooling water is opened, be cooled to 70 ~ 80 DEG C, dried；Room temperature is cooled to, recovers normal pressure, is obtained swollen
Change mixture；
（3）Expanded mixture is put into supercritical extraction reactor, CO260 ~ 120min of supercritical extract, obtain Chinese medicine compound prescription essence
Oil.
In wherein some embodiments, step（1）The addition of the mixture of the farina and glutinous rice starch is
The 10%-20% of crushed mixture weight, the weight ratio of the farina and glutinous rice starch are（1-10):(1-10).
In wherein some embodiments, step（1）Described cryogenic temperature is -15 DEG C ~ 0 DEG C.
In wherein some embodiments, step（2）Described negative pressure is -0.01 ~ -0.05MPa.
In wherein some embodiments, step（3）Described supercritical extract pressure is 50 ~ 60MPa, extraction temperature 50
~65℃。
Compound essential oil with whitening spot-removing of the present invention and preparation method thereof is with advantages below and beneficial effect：
The compound essential oil with whitening spot-removing of the present invention is largely to test and study acquisition through inventor, selected lemon
Skin, ganoderma lucidum, the bighead atractylodes rhizome, Chinese herbaceous peony, radix glycyrrhizae, the flower bud of lily magnolia carry out compatibility according to specific ratio, and show that its optimum formula forms.Wherein lemon
Lemon skin is main ingredient, and the bighead atractylodes rhizome, Chinese herbaceous peony are ministerial drug, and ganoderma lucidum, radix glycyrrhizae, the flower bud of lily magnolia are adjuvant, is entered from the function of the regulation of qi and blood, conditioning the five internal organs
Hand, enhance metabolism, improve body immunity, nourishing blood and liver, make qi and blood abundant, appearance is ruddy, so as to whitening spot-removing, may be used also
Suppress dark sore, delay skin aging.Using in the case of modern extraction process, can simultaneously significantly more efficient Collection utilization its
Volatile ingredient, and because essential oil is all made up of small-molecule substance, it has high osmosis on skin.Therefore institute of the present invention
Disclosed compound essential oil has good whitening effect.
The preparation method of the compound essential oil with whitening spot-removing of the present invention is successively using cryogenic freezing, specific starch swelling
Processing, supercritical extract acquisition active ingredient, the efficiency high of this kind of method effective component extracting, the compound essential oil being prepared
Effect is good, and technique is simple to operation, is adapted to large-scale production.
Embodiment
With reference to specific embodiment to compound essential oil with whitening spot-removing of the present invention and its preparation method and application
It is for a more detailed description, but the implementation of the present invention is not limited to this.For especially not dated technological parameter or condition, can join
More solito technology is carried out.
Part material involved by compound essential oil of the present invention with whitening spot-removing is described as follows：
Lemon peel, Chinese medicine, the pericarp of the ripening fruits of rutaceae lemon.Lemon peel mildly bitter flavor, warm-natured, returns spleen, stomach,
Cure mainly promoting the circulation of qi and stomach, analgesic.Rich in limonene, citral isoreactivity composition in lemon peel, it is beneficial to whitening, convergence, equilibrium oil
The Oily symptoms such as fat secretion, treatment whelk.
Ganoderma lucidum, Chinese medicine, the fructification of On Polyporaceae ganoderma lucidum.Ganoderma lucidum is mild-natured, sweet, enters kidney, liver, the heart, lung channel, tool
There are invigorating qi for tranquilization, relieving cough and asthma, the effect of promoting longevity.《Sheng Nong's herbal classic》Described in：Ganoderma lucidum, strengthening the essence gas, hard muscles and bones, good face
Color.
The bighead atractylodes rhizome, Chinese medicine, the root of the feverfew bighead atractylodes rhizome.Bighead atractylodes rhizome bitter, sweet, warm-natured, returns spleen, stomach, strengthening the spleen and replenishing qi, eliminating dampness
Li Shui, hidroschesis, it is antiabortive the effect of.《Haigoushen》Claim:" interarea light is pleased, nti-freckle of preserving youthful looks.”
Chinese herbaceous peony, Chinese medicine, the root of Paeoniaceae plant peony.Chinese herbaceous peony bitter, is slightly cold, Return liver, the spleen channel, can blood-nourishing hold back the moon, soft liver is stopped
Bitterly, suppressing liver-YANG.《Elementary Medicine》Three plain soups recorded, " each 5 grams of the root of herbaceous peony, the bighead atractylodes rhizome, PORIA ALBA, 3 grams of radix glycyrrhizae, decocting, warmly take ",
The effect of with invigorating qi and benefiting blood, whitening and moistening skin.
Radix glycyrrhizae, Chinese medicine, the root and root-like stock of glycyrrhizic legume.Radix glycyrrhizae property is sweet, puts down, the thoughts of returning home, spleen, lung, stomach, can benefit
Gas bowl spares, relieving spasm to stop pain, moistens the lung and relieve the cough, purging intense heat and detonicating, coordinating the drug actions of a prescription.
The flower bud of lily magnolia, Chinese medicine, the bud of the Magnoliacea plant flower bud of lily magnolia.The flower bud of lily magnolia is pungent, warm, attaches to the lung and stomach meridians, and light fragrance, that is, sends out
Dispersing wind and cold, it is apt to clearing the nasal passage again, suppresses inflammatory swelling.
Embodiment 1
A kind of compound essential oil with whitening effect, its preparation comprise the following steps：
（1）Weigh lemon peel 1kg, ganoderma lucidum 10kg, bighead atractylodes rhizome 1kg, Chinese herbaceous peony 10kg, radix glycyrrhizae 1kg, flower bud of lily magnolia 10kg, remove hard stalk and miscellaneous
Matter, mixing, dry, pulverize, and cross 50 mesh sieve, obtain crushed mixture；Farina and glutinous is added into crushed mixture
The mixture of rice starch, the addition of the mixture of the farina and glutinous rice starch are the 10% of crushed mixture weight,
The weight ratio of the farina and glutinous rice starch is 1：10;It is well mixed, then freeze 1 hour, obtain at a temperature of 0 DEG C
Obtain freezing；
（2）Freezing is sent into Bulking tank, sealed, negative pressure is taken out to -0.05MPa, opens steam valve heating, make swelling temperature
90 DEG C are risen to, is kept for 10 minutes；Pressure release, cooling water is opened, be cooled to 70 DEG C, dried；Room temperature is cooled to, recovers normal pressure, is obtained
Expanded mixture；
（3）Expanded mixture is put into supercritical extraction reactor, extracting pressure 60MPa, extraction temperature is 50 DEG C, CO2It is super to face
Boundary extracts 120min, obtains Chinese medicine compound prescription essential oil.
Embodiment 2
A kind of compound essential oil with whitening effect, its preparation comprise the following steps：
（1）Weigh lemon peel 100kg, ganoderma lucidum 1kg, bighead atractylodes rhizome 10kg, Chinese herbaceous peony 1kg, radix glycyrrhizae 10kg, flower bud of lily magnolia 1kg, remove hard stalk and miscellaneous
Matter, mixing, dry, pulverize, and cross 50 mesh sieve, obtain crushed mixture；Farina and glutinous is added into crushed mixture
The mixture of rice starch, the addition of the mixture of the farina and glutinous rice starch are the 10% of crushed mixture weight,
The weight ratio of the farina and glutinous rice starch is 10：1;Well mixed, then freezing 24 is small at a temperature of -15 DEG C
When, obtain freezing；
（2）Freezing is sent into Bulking tank, sealed, negative pressure is taken out to -0.01MPa, opens steam valve heating, make swelling temperature
95 DEG C are risen to, is kept for 5 minutes；Pressure release, cooling water is opened, be cooled to 80 DEG C, dried；Room temperature is cooled to, recovers normal pressure, is obtained swollen
Change mixture；
（3）Expanded mixture is put into supercritical extraction reactor, extracting pressure 50MPa, extraction temperature is 65 DEG C, CO2It is super to face
Boundary extracts 60min, obtains Chinese medicine compound prescription essential oil.
Embodiment 3
A kind of compound essential oil with whitening effect, its preparation comprise the following steps：
（1）Lemon peel 10kg, ganoderma lucidum 4kg, bighead atractylodes rhizome 6kg, Chinese herbaceous peony 4kg, radix glycyrrhizae 2kg, flower bud of lily magnolia 8kg are weighed, removes hard stalk and impurity,
Mixing, dry, pulverize, and cross 10 mesh sieve, obtain crushed mixture；Farina is added into crushed mixture and glutinous rice forms sediment
The mixture of powder, the addition of the mixture of the farina and glutinous rice starch is the 15% of crushed mixture weight, described
The weight ratio of farina and glutinous rice starch is 1：1;It is well mixed, then freeze 12 hours, obtain at a temperature of -10 DEG C
Freezing；
（2）Freezing is sent into Bulking tank, sealed, negative pressure is taken out to -0.03MPa, opens steam valve heating, make swelling temperature
92 DEG C are risen to, is kept for 8 minutes；Pressure release, cooling water is opened, be cooled to 75 DEG C, dried；Room temperature is cooled to, recovers normal pressure, is obtained swollen
Change mixture；
（3）Expanded mixture is put into supercritical extraction reactor, extracting pressure 55MPa, extraction temperature is 55 DEG C, CO2It is super to face
Boundary extracts 90min, obtains Chinese medicine compound prescription essential oil.
Embodiment 4
A kind of compound essential oil with whitening effect, its preparation comprise the following steps：
（1）Lemon peel 50kg, ganoderma lucidum 2kg, bighead atractylodes rhizome 8kg, Chinese herbaceous peony 2kg, radix glycyrrhizae 4kg, flower bud of lily magnolia 6kg are weighed, removes hard stalk and impurity,
Mixing, dry, pulverize, and cross 50 mesh sieve, obtain crushed mixture；Farina is added into crushed mixture and glutinous rice forms sediment
The mixture of powder, the addition of the mixture of the farina and glutinous rice starch is the 15% of crushed mixture weight, described
The weight ratio of farina and glutinous rice starch is 1：1;It is well mixed, then freeze 12 hours, obtain at a temperature of -10 DEG C
Freezing；
（2）Freezing is sent into Bulking tank, sealed, negative pressure is taken out to -0.03MPa, opens steam valve heating, make swelling temperature
92 DEG C are risen to, is kept for 8 minutes；Pressure release, cooling water is opened, be cooled to 75 DEG C, dried；Room temperature is cooled to, recovers normal pressure, is obtained swollen
Change mixture；
（3）Expanded mixture is put into supercritical extraction reactor, extracting pressure 55MPa, extraction temperature is 55 DEG C, CO2It is super to face
Boundary extracts 90min, obtains Chinese medicine compound prescription essential oil.
Embodiment 5
A kind of compound essential oil with whitening effect, include each component of following mass percent：Obtained by embodiment 1
Chinese medicine compound prescription essential oil 0.1%, Parleam 40%, tocopherol acetate 1%, diisopropyl sebacate 5%, more than Sweet Almond Oil
Amount.
Embodiment 6
A kind of compound essential oil with whitening effect, include each component of following mass percent：Obtained by embodiment 2
Chinese medicine compound prescription essential oil 1%, White Mineral Oil 50%, tocopherol acetate 1%, olive oil surplus.
Embodiment 7
A kind of compound essential oil with whitening effect, include each component of following mass percent：Obtained by embodiment 3
Chinese medicine compound prescription essential oil 5%, carbonic acid dioctyl ester 50%, tocopherol acetate 1%, Queensland nut seed oil surplus.
Embodiment 8
A kind of compound essential oil with whitening effect, include each component of following mass percent：Obtained by embodiment 4
Chinese medicine compound prescription essential oil 10%, octyl group polymethyl siloxane 5%, tocopherol acetate 1%, grape-kernel oil surplus.
Comparative example 1
A kind of compound essential oil with whitening effect, include each component of following mass percent：Compound essential oil 5%, carbonic acid
Dioctyl ester 50%, tocopherol acetate 1%, Queensland nut seed oil surplus；Described compound essential oil and the essence obtained by embodiment 3
The difference of oil is not add lemon peel, and other preparation conditions and method are same as Example 3.
Comparative example 2
A kind of compound essential oil with whitening effect, include each component of following mass percent：Compound essential oil 5%, carbonic acid
Dioctyl ester 50%, tocopherol acetate 1%, Queensland nut seed oil surplus；Described compound essential oil and the essence obtained by embodiment 3
The difference of oil is not add the bighead atractylodes rhizome, Chinese herbaceous peony, and other preparation conditions and method are same as Example 3.
Comparative example 3
A kind of compound essential oil with whitening effect, include each component of following mass percent：Compound essential oil 5%, carbonic acid
Dioctyl ester 50%, tocopherol acetate 1%, Queensland nut seed oil surplus；Described compound essential oil and the essence obtained by embodiment 3
The difference of oil is not add ganoderma lucidum, radix glycyrrhizae, the flower bud of lily magnolia, and other preparation conditions and method are same as Example 3.
Comparative example 4
A kind of compound essential oil with whitening effect, include each component of following mass percent：Compound essential oil 5%, carbonic acid
Dioctyl ester 50%, tocopherol acetate 1%, Queensland nut seed oil surplus；Described compound essential oil and the essence obtained by embodiment 3
The difference of oil is not add ganoderma lucidum, the bighead atractylodes rhizome, and other preparation conditions and method are same as Example 3.
Embodiment 9
Effect test and appraisal are carried out to the compound essential oil with whitening spot-removing obtained by embodiment 5-8 and comparative example 1-5, wherein contrasting
Example 5 is the commercially available essential oil for declaring to have whitening effect.Specific method of testing is as follows：Each experimental group chooses 10 aspirations
Person, age 35-55 year, there is that skin is obscure, color spot phenomenon；Application method：After face cleaning, take in right amount in the centre of the palm, pressed after rubbing heat with the hands
Rub skin of face, 1 evening 1 time, continuous on probation 12 weeks, mug.Evaluation method：Contrast the 0th day and the 12nd week photo and inquire
The use feeling of volunteer, wherein facial skin become that pale, glossy, color spot significantly reduces to be effective；Facial skin is obscure
Improved, color spot mitigate be effective；Facial skin do not have to improve to be invalid.Specific test result such as table 1.It is on probation 12 weeks
Trier is paid a return visit afterwards, without there is allergic phenomenon, shows that the Chinese medicine compound prescription essential oil is safe and non-toxic.
The test recording table of table 1
From the result of table 1：
Embodiment 5-8 contrasted with comparative example 5 it is visible, the present invention obtained by the compound essential oil with whitening spot-removing with well
Whitening effect.
Embodiment 7 and comparative example 1-4 contrasts are visible, and lemon peel of the invention, ganoderma lucidum, the bighead atractylodes rhizome, Chinese herbaceous peony, radix glycyrrhizae, the flower bud of lily magnolia close
Used time whitening spot-removing is better, and each traditional Chinese medicine ingredients after specific ratio compatibility according to playing the role of Synergistic.
Stability test
Method of testing：Respectively by above-described embodiment 1-8 and comparative example 5 it is obtained/compound essential oil bought places
Placed 3 months under conditions of 45 DEG C, -15 DEG C, room temperature, seen whether the abnormal conditions such as precipitation, discoloration, spoiled.Survey
Test result is shown in Table 2.
The stability test record sheet of table 2
| 1 month | 2 months | 3 months | |
| Embodiment 1 | It is qualified | It is qualified | It is qualified |
| Embodiment 2 | It is qualified | It is qualified | It is qualified |
| Embodiment 3 | It is qualified | It is qualified | It is qualified |
| Embodiment 4 | It is qualified | It is qualified | It is qualified |
| Embodiment 5 | It is qualified | It is qualified | It is qualified |
| Embodiment 6 | It is qualified | It is qualified | It is qualified |
| Embodiment 7 | It is qualified | It is qualified | It is qualified |
| Embodiment 8 | It is qualified | It is qualified | It is qualified |
| Comparative example 5 | It is qualified | It is unqualified | It is unqualified |
As seen from Table 2, the compound essential oil stability obtained by the embodiment of the present invention is more preferably.
Each technical characteristic of embodiment described above can be combined arbitrarily, to make description succinct, not to above-mentioned reality
Apply all possible combination of each technical characteristic in example to be all described, as long as however, the combination of these technical characteristics is not deposited
In contradiction, the scope that this specification is recorded all is considered to be.
Embodiment described above only expresses the several embodiments of the present invention, and its description is more specific and detailed, but simultaneously
Can not therefore it be construed as limiting the scope of the patent.It should be pointed out that come for one of ordinary skill in the art
Say, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to present invention protection model
Enclose.Therefore, the protection domain of patent of the present invention should be determined by the appended claims.
Claims (8)
- A kind of 1. compound essential oil with whitening effect, it is characterised in that the compound essence with whitening effect The active component of oil is prepared by the raw material of following parts by weight：Lemon peel 1-100 parts, ganoderma lucidum 1-10 parts, bighead atractylodes rhizome 1-10 parts, Chinese herbaceous peony Medicine 1-10 parts, radix glycyrrhizae 1-10 parts, flower bud of lily magnolia 1-10 parts.
- 2. the compound essential oil according to claim 1 with whitening effect, it is characterised in that described to be dispelled with whitening The active component of the compound essential oil of spot effect is prepared by the raw material of following parts by weight：Lemon peel 10-50 parts, ganoderma lucidum 2-4 parts, Bighead atractylodes rhizome 6-8 parts, Chinese herbaceous peony 2-4 parts, radix glycyrrhizae 2-4 parts, flower bud of lily magnolia 6-8 parts.
- 3. the compound essential oil according to claim 1 or 2 with whitening effect, it is characterised in that described has The compound essential oil of whitening spot-removing is additionally added base oil, and the base oil is selected from hydrocarbon ils, Acrawax, vegetable and animals oils, silicone oil And its mixture.
- 4. a kind of preparation method of the compound essential oil with whitening spot-removing described in any one of claim 1 or 2, its feature exist In comprising the following steps：（1）Parts by weight as described in claim 1 or 2, by lemon peel, ganoderma lucidum, the bighead atractylodes rhizome, Chinese herbaceous peony, radix glycyrrhizae, the flower bud of lily magnolia remove hard stalk and Impurity, mixing, dry, pulverize, and cross 10-50 mesh sieve, obtain crushed mixture；Farina is added into crushed mixture With the mixture of glutinous rice starch, it is well mixed, then freezes 1 ~ 24 hour, obtains freezing；（2）Freezing is sent into Bulking tank, sealed, takes out negative pressure, steam valve heating is opened, swelling temperature is risen to 90 ~ 95 DEG C, kept for 5-10 minutes；Pressure release, cooling water is opened, be cooled to 70 ~ 80 DEG C, dried；Room temperature is cooled to, recovers normal pressure, is obtained swollen Change mixture；（3）Expanded mixture is put into supercritical extraction reactor, CO260 ~ 120min of supercritical extract, obtain Chinese medicine compound prescription essential oil.
- 5. the preparation method of the compound essential oil according to claim 4 with whitening spot-removing, it is characterised in that step（1） The addition of the mixture of the farina and glutinous rice starch be crushed mixture weight 10%-20%, the potato The weight ratio of starch and glutinous rice starch is（1-10):(1-10).
- 6. the preparation method of the compound essential oil according to claim 4 with whitening spot-removing, it is characterised in that step（1） Described cryogenic temperature is -15 DEG C ~ 0 DEG C.
- 7. the preparation method of the compound essential oil according to claim 4 with whitening spot-removing, it is characterised in that step（2） Described negative pressure is -0.01 ~ -0.05MPa.
- 8. the preparation method of the compound essential oil according to claim 4 with whitening spot-removing, it is characterised in that step（3） Described supercritical extract pressure is 50 ~ 60MPa, and extraction temperature is 50 ~ 65 DEG C.
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