CN101695470B - Composite for cosmetics, cosmetic product containing same and preparation method thereof - Google Patents
Composite for cosmetics, cosmetic product containing same and preparation method thereof Download PDFInfo
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- CN101695470B CN101695470B CN2009100709765A CN200910070976A CN101695470B CN 101695470 B CN101695470 B CN 101695470B CN 2009100709765 A CN2009100709765 A CN 2009100709765A CN 200910070976 A CN200910070976 A CN 200910070976A CN 101695470 B CN101695470 B CN 101695470B
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Abstract
The invention provides a composite for cosmetics, a cosmetic product containing the same and a preparation method thereof. The composite for cosmetics comprises phellodendron essential oil, wild chrysanthemum flower essential oil, chamomile essential oil and fresh milk, wherein composite essential oil is formed by the phellodendron essential oil, the wild chrysanthemum flower essential oil and the chamomile essential oil; the weight ratio of the composite essential oil to the fresh milk is 0.2-0.8 to 5-20; the weight ratio of the phellodendron essential oil to the wild chrysanthemum flower essential oil to the chamomile essential oil is 1:1.5-2.5:2.5-3.5. The composite can be used as an addition phase for manufacturing cosmetic products, particularly skin care products and cleaning products so that the products have the efficacy of antianaphylaxis, antiphlogosis, eczema elimination, and the like.
Description
Technical field
The invention relates to a kind of cosmetic composition, contain cosmetics of said composition and preparation method thereof, particularly about a kind of Cortex Phellodendri quintessence oil, Flos Chrysanthemi Indici quintessence oil and the compound essential Oil of three kinds of quintessence oil preparations of Flos Matricariae chamomillae quintessence oil and compositions of fresh milk of containing, and said composition is used to prepare cosmetics particularly skin care item and cleaning series products, make it to have antiallergic, effects such as antiinflammatory, elimination eczema.
Background technology
The broad definition of cosmetics is meant to smear, to spray or other similar approach, impose on human body surface (as epidermis, hair, fingernail, lip etc.), play cleaning, maintain, beautify or eliminate the product of bad smell effect, this series products can have abirritation to using the position.From application point, cosmetics mainly comprise several big classes such as skin type, hair care category, hair washing class, cleaning class, beauty treatment class.Along with growth in the living standard, consumer also has more demand to the effect of all kinds of cosmetics, develops and produce the R﹠D direction that the cosmetics with various nutrition or protection effect have become cosmetic industry.For reaching such effect, various nutrition, health care composition are managed to add in the cosmetics, for example all kinds of plant extract compositions, bioactie agent, quintessence oil etc., and then indicate that product has for example effects such as whitening and speckle dispelling, defying age, anti-dermatitis, skin nutrition or hair.
Eczema (eczema) is superficial dermis and the epidermitis that is caused by multiple inside and outside factor, has syringe needle to arrive pimple, the papulovesicle of foxtail millet grain size on the erythema of the being everlasting basis, phlysis is arranged, permelting answer print, indefinite border Chu when serious.In the periphery of infringement, pruritus is heavier, and Chang Yin scratches and makes erythra form rotten to the corn face, and has serosity to ooze out and form a scab.The tradition traditional Chinese medical science is thought: dermatosis mostly is the exopathogen invasion greatly, blood is dry to be mingled with stasis of blood poison, thereby takes the method for heat clearing away, removing heat from blood mostly, reuses the thing of bitter cold, initial stage is effective, but often can not go this, and the life-time service impairment of the spleen, cause dermatosis to transfer chronic delay to and show effect repeatedly, dysfunction of spleen and stomach, the stomach abdominal distention and pain, dampness day is heavy, secondary infection.Western medicine is thought: dermatosis mainly is pathogenic microorganism (antibacterial, virus, fungus) invasion, cause the body's immunity disorder, damage skin basement membrane then, cause the sings and symptoms of a series of skin damage, use the hormone anti symptom treatment mostly, fast, easily recurrence proves effective.
At present existing literature research has been reported the cosmetic composition of eliminating and/or treating dermatosis functions such as eczema about having, for example, CN1947776A (2007-04-18) has reported a kind of Chinese medicine medicine for external use and cosmetics for the treatment of infant eczema and dermatitis, cosmetics wherein be select for use have heat-clearing and toxic substances removing, Chinese herbal medicine paeonol of antiinflammatory, antiallergic, removing dampness to relieve itching, Bulbus Allii, Ramulus et Folium Bauhiniae Faberi, Cortex Moutan, Radix Arnebiae (Radix Lithospermi), Herba Hedyotidis Diffusae, Cortex Dictamni, Flos Caryophylli etc. be made; JP2003342184 (2003-12-03) has reported a kind of cosmetic composition that contains hyaluronidase activity inhibitor, can be used for preventing dermatitis such as skin aging and prevention eczema, pruritus, said composition is made by Fructus Vitis viniferae leaves, Pericarpium Zanthoxyli, Herba Astragali Melilotoidis (Herba Astragali Sinici) and hyaluronidase activity inhibitor etc.; KR20070079596 (2007-08-07) reported a kind of be used for the treatment of dermatosiss such as eczema, allergic dermatitis and have brighten, the cosmetic composition of the anti-ageing function of waiting for a long time, said composition comprises extract of Flos Carthami and aloetic extract, sulfur, Colophonium, Cortex Phellodendri etc.; JP2006321758 (2006-11-30) has reported a kind of dermopathic cosmetics such as eczema, dermatitis and skin allergy that can be used for treating, these cosmetics are mainly by the extract of scutellariae,radix and Cortex Phellodendri, or scutellariae,radix extract and G1ycyrrhiza glabra, or Cortex Phellodendri extract and G1ycyrrhiza glabra, or the three forms.
In addition, there are some documents to study respectively in the prior art and reported that Flos Chrysanthemi Indici has effects such as heat-clearing and toxic substances removing, detumescence, Flos Matricariae chamomillae has effects such as antiallergic, anti-inflammatory, antipruritic, antibiotic, soft skin, Cortex Phellodendri have heat clearing and damp drying, pathogenic fire purging remove steam, detoxifcation treats effects such as skin ulcer.In addition, also there is lot of documents to put down in writing fresh milk (sweet milk) to have profit skin, the lung that nourishes heart, separates pyretic toxicity, delaying decrepitude of skin, makes skin keep effects such as smooth pliable is delicate.But Shang Weijian is applied to these combinations of substances the technology report of cosmetics.
Summary of the invention
One object of the present invention is to provide a kind of cosmetic composition, and said composition comprises the quintessence oil and the fresh milk of Cortex Phellodendri, Flos Chrysanthemi Indici and Flos Matricariae chamomillae, can be used for the production of cosmetics.
Another object of the present invention is to provide a kind of cosmetics, these cosmetics comprise Cortex Phellodendri quintessence oil, Flos Chrysanthemi Indici quintessence oil and Flos Matricariae chamomillae quintessence oil and fresh milk, have antiinflammatory, anti-allergic effects, can effectively prevent and/or eliminate eczema.
Another object of the present invention is to provide a kind of method for preparing described cosmetics, by rational production technology, the described compositions of Cortex Phellodendri quintessence oil, Flos Chrysanthemi Indici quintessence oil and Flos Matricariae chamomillae quintessence oil and fresh milk that comprises is used for the production of cosmetics, preparing stable in properties, and have good antiinflammatory, antiallergic, prevention and/or eliminate the cosmetics of effects such as eczema.
On the one hand, the invention provides a kind of cosmetic composition, said composition comprises: Cortex Phellodendri quintessence oil, Flos Chrysanthemi Indici quintessence oil and Flos Matricariae chamomillae quintessence oil, and fresh milk.
Quintessence oil is flower, leaf, stem, root or the fruit from plant, refines the volatile flavor of extraction by steam distillation, squeezing and pressing method, cold-maceration or solvent extraction method.Cortex Phellodendri quintessence oil among the present invention, Flos Chrysanthemi Indici quintessence oil, Flos Matricariae chamomillae quintessence oil extract from Cortex Phellodendri, Flos Chrysanthemi Indici, Flos Matricariae chamomillae respectively and obtain.These quintessence oils can be commercially available respectively, also can extract preparation voluntarily according to the method for prior art.Each quintessence oil among the present invention should meet the correlated quality standard-required.
According to specific embodiments of the present invention, used Flos Chrysanthemi Indici quintessence oil is to utilize the inflorescence of perennial perennial root herbaceous plant Flos Chrysanthemi Indici to be raw material among the present invention, make extractum with the perfume solvent extraction, obtain the brownish red oily liquids through the ethanol dewaxing again, its main component has Flos Chrysanthemi Indici lactone, camphene Eucarvone, Camphora, absinthol etc. more than 40 kinds, has pure Flos Chrysanthemi Indici fragrance.Used Flos Matricariae chamomillae quintessence oil is the blue liquid from the flower process vapor distillation acquisition of annual herb plant Matricaria, its main component is Chamomile azulene, sesquiterpenoid and sad button ester, other composition also contains 5,7, the 4-trihydroxyflavone, the methyl ether of umbelliferone and fatty acid, Flos Matricariae chamomillae quintessence oil have the characteristic perfume of bitter medicinal herbs fragrance.Used Cortex Phellodendri quintessence oil can be to utilize solvent extraction method to extract from the bark of rutaceae Cortex Phellodendri or phellodendron bark to obtain, and contains alkaloids such as berberine, jateorhizine, phellodendrine, and other contains obacunone, obakulactone etc.; According to a specific embodiments of the present invention, described Cortex Phellodendri quintessence oil can be to add the pastel of 1～1.5 weight portion Oleum sesami furnishing by Cortex Phellodendri powder (be purchased the medical material Cortex Phellodendri and pulverize the powder that obtains) 1 weight portion; Also can be Cortex Phellodendri (tincture), for example will grind to form smalls available from the Cortex Phellodendri in medical material shop, with 40%～60% ethanol, 6～10 times of volumes, 80～90 ℃ of reflux, extract, twice, each about 1.5～2.5 hours, make the Cortex Phellodendri preserved material, be referred to as the Cortex Phellodendri quintessence oil.
Though existing document has been reported heat-clearing and toxic substances removing, the detumescence effect of Flos Chrysanthemi Indici respectively in the prior art, the antiallergic of Flos Matricariae chamomillae, anti-inflammatory, antipruritic, antibiotic, soft skin effect, the heat clearing and damp drying of Cortex Phellodendri, pathogenic fire purging remove steams, detoxifies and treat the skin ulcer effect, also there is document to put down in writing the profit skin of fresh milk, separates effects such as pyretic toxicity, but technology record or instruction can be with Cortex Phellodendri, Flos Chrysanthemi Indici, Flos Matricariae chamomillae (or its extract) applied in any combination, more not about three's the quintessence oil and the technology of fresh milk applied in any combination are enlightened.
Among the present invention, according to Cortex Phellodendri quintessence oil, Flos Chrysanthemi Indici quintessence oil, the different characteristics character of Flos Matricariae chamomillae quintessence oil, Cortex Phellodendri quintessence oil, Flos Chrysanthemi Indici quintessence oil and Flos Matricariae chamomillae quintessence oil are formed compound essential Oil, and further make up with fresh milk, a kind of cosmetic composition is provided, can be used as the interpolation phase, be applied to the production of cosmetics.
Select the quintessence oil of Cortex Phellodendri, Flos Chrysanthemi Indici, this three kind of plant of Flos Matricariae chamomillae among the present invention for use and do not select its conventional Chinese medicine extract for use, mainly be to consider that compositions of the present invention is the production that is used for cosmetics, and conventional Chinese medicine extract has the offending abnormal smells from the patient of Chinese medicine, joins in the cosmetics and will bring bad abnormal smells from the patient to cosmetics.
The derived essential oil complexity in the apolegamy of compound essential Oil, needs to consider the interaction each other of several special quintessence oils that wherein, the consumption of each quintessence oil is one of key factor.According to preferred specific embodiments of the present invention, the weight ratio of Cortex Phellodendri quintessence oil, Flos Chrysanthemi Indici quintessence oil and Flos Matricariae chamomillae quintessence oil is 1: 1.5～2.5: 2.5～3.5 in the described compound essential Oil, more preferably 1: 2: 3 (except that specifying, ratio described in the present invention and content are part by weight and content).
Usage ratio between described compound essential Oil and the fresh milk also is one of the factor that need consider of the present invention.According to specific embodiments of the present invention, in the cosmetic composition of the present invention, the compound essential Oil that described Cortex Phellodendri quintessence oil, Flos Chrysanthemi Indici quintessence oil and Flos Matricariae chamomillae quintessence oil are formed and the weight ratio of fresh milk are 0.2～0.8: 5～20, and more preferably scope 0.5: 5～20.
The quintessence oil of the Cortex Phellodendri that the present invention selects for use, Flos Chrysanthemi Indici, this three kind of plant of Flos Matricariae chamomillae has natural fragrance respectively, and after the present invention selects these three kinds of quintessence oil combinations for use, abnormal smells from the patient fragrance, and further make up with fresh milk, can not bring offending abnormal smells from the patient yet, add to can play in the cosmetics and compose fragrant effect, thereby can reduce the consumption of cosmetic essence, or do not add essence, produce no fragrant cosmetics.And, after the present invention uses Cortex Phellodendri, Flos Chrysanthemi Indici, the combination of Flos Matricariae chamomillae quintessence oil, and further with the fresh milk combination, can not have side effects to skin, non-stimulated, be suitable for being added to cosmetics for example in the skin care item, particularly juvenile product.The combination of three kinds of quintessence oils that the present invention selects for use, and further make up with fresh milk, compositions is added cosmetics such as cream frost or emulsion to particularly in the skin care item, by controlling rational addition and proper technical conditions, can the structure of product not damaged, stability to cosmetics can not brought adverse influence, can not cause problems such as variable color, layering.
Described cosmetic composition of the present invention, it has effects such as good antiallergic, antiinflammatory, prevention and/or elimination eczema, and effect is much larger than the independent effect sum of using of Cortex Phellodendri quintessence oil, Flos Chrysanthemi Indici quintessence oil and Flos Matricariae chamomillae quintessence oil.Related Experimental Study shows, the cosmetic composition that contains compound essential Oil and fresh milk of the present invention, and its secretory volume that can reduce IL-1 α reduces the activity of Protein kinase C to 100pg/mL, the inhibition degree of Protein kinase C is reached more than 98%.Compositions of the present invention is added in the cosmetics, can make preparation-obtained cosmetics when possessing the effect of conventional cosmetics, it is suitable and have good antiallergic, antiinflammatory, prevention and/or eliminate effects such as eczema also to have fragrance.
That is, on the other hand, the present invention also provides the application of described cosmetic composition in the preparation cosmetics, when specifically using, is that described cosmetic composition is applied in the production of cosmetics mutually as adding.For example, in a specific embodiment of the present invention, be that cosmetic composition of the present invention is added in skin care item and cleaning series products such as cleansing milk, the bath foam etc., preparation-obtained skin care item and cleaning series products are except that having conventional skin protection, cleaning efficacy, and also the elimination for eczema has obvious effects.
Whether can need the factor of consideration a lot of for a kind of new material or compositions as adding the production that is applied to cosmetics mutually.For example, except that considering to add the influence of abnormal smells from the patient to cosmetics of phase, also need consider to add relative cosmetics product structure and whether can damage, whether can bring adverse effect, whether can cause the problems such as variable color, layering of paste, emulsion form cosmetics the stability of cosmetics.The consumption that adds in cosmetics is one of the factor that at first will control, according to specific embodiments of the present invention, preferably controlling described cosmetic composition and be with the amount of fresh milk wherein is that the amount that cosmetic material is formed gross weight 5%～20% is added in the cosmetics; In other words, preferably controlling described cosmetic composition is to be that the amount that cosmetic material is formed gross weight 0.2%～0.8% is added in the cosmetics with the amount of compound essential Oil wherein.
On the other hand, the present invention also provides a kind of cosmetics, and the raw material of these cosmetics comprises cosmetic composition of the present invention in forming.
According to specific embodiments of the present invention, in the cosmetics of the present invention, the content of the fresh milk in the described cosmetic composition in the raw material of these cosmetics is formed is 5%～20%.
Cosmetics of the present invention can be skin type, cleaning class etc., are preferably skin type or cleaning class oil-in-water type or expansion type product, and described skin type is skin lotion (frost or honey) etc. for example, and described cleaning class is handwashing liquid, facial milk cleanser or bath oil etc. for example.In dissimilar cosmetics, the addition that contains the cosmetic composition of compound essential Oil and fresh milk of the present invention can be different, for example, in the skin type product, can be that the amount that cosmetic material is formed gross weight 5%～20% is added with the amount of fresh milk wherein; In the cleaning series products, can be that the amount that cosmetic material is formed gross weight 5%～8% is added with the amount of fresh milk wherein.
Among the present invention, described cosmetic composition adds in the described cosmetics mutually to add.According to specific embodiments of the present invention, the interpolation of cosmetics of the present invention is except comprising the described compositions that is made into by compound essential Oil and fresh milk, under also further comprising in the field commonly used other for example add mutually Moisture factor hyaluronate sodium etc., other kinds of adding phases are selected and consumption for a person skilled in the art can be according to the knowledge of prior art and definite easily.
In the cosmetics of the present invention, except described interpolation mutually, during forming, its raw material also comprises conventional oil phase and water.For example, in emulsified make-up of the present invention, generally include emulsifying agent, excipient (thickening) agent, also can add basic material and necessary additive that cosmetics contain usually, emollient (for example vegetable oil, white oil, animal oil and derivant thereof etc.), wetting agent (for example glycerol, propylene glycol, 1 for example, 3-butanediol etc.), essence, deionized water, antioxidant, antiseptic etc., also can add some nutritional labelings.The application of these concrete compositions and consumption can be selected according to the concrete kind (skin type, cleaning class etc.) of described cosmetics, perhaps add according to convention amount, and this is easy to grasp for a person skilled in the art.
For example, the possible prescription of an emulsified make-up of the present invention (skin moistening honey or cream, cleansing milk etc.) is:
Fresh milk: 5%～20%
Compound essential Oil 0.2%～0.8%
(master) emulsifying agent: 0.5%～5.0%
Coemulsifier: 0.5%～10%
Emollient: 5%～40%
Excipient thickening agent: 0.1%～10%
Wetting agent: 5%～30%
Nutritional labeling: optionally, formula ratio
Functional components: optionally, formula ratio
Antiseptic: convention amount (hygienic standards for cosmetics regulation)
Antioxidant: convention amount
Deionized water: add to 100%.
More specifically, the representative formula of an emulsified make-up of the present invention can be:
Fresh milk (through preservative treatment): 5%～20%
Compound essential Oil 0.3%～0.8% (wherein Flos Chrysanthemi Indici quintessence oil 0.1%～0.4%, Flos Matricariae chamomillae quintessence oil 0.15%～0.6%, Cortex Phellodendri quintessence oil 0.05%～0.2%)
Octadecanol: 1%～4%
White oil: 1.5%～4.5%
Emulgade?PL68/50：2％～4％
Isopropyl palmitate: 4%～8%
Dimethicone: 2%～5%
Methyl hydroxybenzoate: 0.02%～0.1%
Glycerol: 10%～18%
Sodium lauryl sulphate: 0.3%～0.8%
Propylene glycol: 5%～10%
Hyaluronate sodium: 0.01%～0.1%
IPBC-1：0.01％
Bronopol: 0.02%
Deionized water: surplus.
As the indefiniteness example, the basic components of all kinds of cosmetics can also be:
1, skin type (for example skin moistening honey)
Fresh milk: 5%～20%
Compound essential Oil 0.3%～0.8% (wherein Flos Chrysanthemi Indici quintessence oil 0.1%～0.4%, Flos Matricariae chamomillae quintessence oil 0.15%～0.6%, Cortex Phellodendri quintessence oil 0.05%～0.2%)
Emollient: 5%～40%
Wetting agent (glycerin/propylene glycol/1,3 butanediol): 6%～13%
Primary emulsion (anion/anion+anion/anion+nonionic/nonionic+nonionic/nonionic): 0.5%～3.0%
Coemulsifier (monostearate monoglyceride): 2%～4%
Excipient thickening agent (octadecanol, or octadecanol+hydroxyethyl-cellulose): 3%～5%
Antioxidant: 0.01%～0.5%
Antiseptic: 0.03%～0.5%
Deionized water: to 100.
2, cleaning class (for example cleansing milk)
Fresh milk: 5%～20%
Compound essential Oil 0.3%～0.8% (wherein Flos Chrysanthemi Indici quintessence oil 0.1%～0.4%, Flos Matricariae chamomillae quintessence oil 0.15%～0.6%, Cortex Phellodendri quintessence oil 0.05%～0.2%)
Emollient: 5%～40%
Skin detergents: 0.1%～5%
Wetting agent (glycerin/propylene glycol/1,3 butylene glycol): 5%～30%
Antiseptic: 0.03%～0.5%
Primary emulsion (anion/anion+anion/anion+nonionic/nonionic+nonionic/nonionic): 0.5%～3%
Coemulsifier: 0.5%～5%
Excipient thickening agent (octadecanol+hydroxyethyl-cellulose): 0.5%～5%
Antioxidant: 0.01%～0.5%
Water: to 100%.
On the other hand, the present invention also provides a kind of method for preparing described cosmetics, and the raw material of described cosmetics is formed and comprised oil phase, water and interpolation mutually, and this method comprises:
Make the oil phase and the water of cosmetic material carry out preliminary emulsifying earlier, the temperature of adjusting this emulsification system adds fresh milk when being lower than 60 ℃, after stirring, backheat to 75～90 ℃ insulated and stirred 5～15 minutes, be cooled to 48～60 ℃ then, add quintessence oil (add phase as other are arranged in prescription, in this step, add other and add phase), system is through stirring, and further the cooling back requires complete operation according to prescription.
The method according to this invention, be the forfeiture of avoiding active component in the fresh milk and the Over emulsfication phenomenon of fresh milk, in the oil-in-water type production, fresh milk should be added to as interpolation after oil phase and the preliminary emulsifying of water mixed system, the temperature that should control emulsification system when adding fresh milk simultaneously can not be too high, should make reactor keep maximum vacuum after fresh milk adds, start quick stirring homogenizing (for example 1～2 minute), make and add phased soln fully and can carry out the later stage operation when not having bubble.The step of specifically not mentioning in the method for the present invention for example oil phase and the preliminary emulsifying of water, the operation after the system cooling behind the adding quintessence oil etc. all can be carried out according to the routine operation in affiliated field.
In sum, the invention provides a kind of abnormal smells from the patient fragrance, have certain antiinflammatory, antiallergic, prevention and/or eliminate the cosmetic composition of effects such as eczema, utilize its cosmetics that prepare effectively to eliminate eczema to a certain extent by its active component, and can be used for preventing the eczema problem that causes by exopathogenic factor by antiallergic, antiinflammatory etc., help making the skin state of getting well.The present invention is by reasonable proportioning, and the control proper production process, and its outward appearance of cosmetic product, the inherent quality produced are maintained a long-term stability, and makes us being easy to accepting.
The specific embodiment
Below describe the beneficial effect of implementation process of the present invention and generation in detail by specific embodiment, be intended to help the reader to understand essence of the present invention and characteristics better, but not as qualification to this case practical range.
In following scheme description of the present invention and the prescription, used Flos Chrysanthemi Indici quintessence oil and Flos Matricariae chamomillae quintessence oil are commercially available.Wherein, described Flos Chrysanthemi Indici quintessence oil is to utilize the inflorescence of perennial perennial root herbaceous plant Flos Chrysanthemi Indici to be raw material, make extractum with the perfume solvent extraction, obtain the brownish red oily liquids through the ethanol dewaxing again, its main component has Flos Chrysanthemi Indici lactone, camphene Eucarvone, Camphora, absinthol etc., has pure Flos Chrysanthemi Indici fragrance, 20 ℃ 0.9782～0.9942 of proportion, 20 ℃ 1.5057～1.5087 of refraction index; Described Flos Matricariae chamomillae quintessence oil is the blue liquid from the flower process vapor distillation acquisition of annual herb plant Matricaria; its main component is Chamomile azulene, sesquiterpenoid and sad button ester; organoleptic feature: the characteristic perfume of bitter medicinal herbs fragrance; 20 ℃ 0.913～0.953 of proportion, acid number (after the acetylation) 66～155.Following scheme of the present invention describe and prescription in, the Cortex Phellodendri quintessence oil use 50% ethanol, 8 times of volumes, 85 ℃ of reflux, extract, twice, about 2 hours at every turn, the Cortex Phellodendri preserved material that makes for after the Cortex Phellodendri available from the medical material shop grinds to form fine powder (containing berberine 1.6%); The inventor also uses 1 part of Cortex Phellodendri powder (containing berberine 1.6%) to add in the cosmetics as Cortex Phellodendri quintessence oil of the present invention with 1.2 parts of furnishing pasty states of Oleum sesami in research process of the present invention, the cosmetics that obtain of producing, with add above-mentioned through alcohol reflux to the cosmetics of Cortex Phellodendri quintessence oil compare, have the effect of the suitable substantially antiallergic of effect, antiinflammatory and elimination eczema.In following scheme description of the present invention and the prescription, used each raw material meets correlated quality standard-required (for example fresh milk should meet the requirement of GB6914).
The production of embodiment 1, child's skin moistening honey
1, prescription (each component all by weight percentage)
| Material name | Percentage ratio |
| Add phase | |
| Fresh milk | 8 |
| The Herba Dendranthematis indici caul-fat | 0.10 |
| Flos Matricariae chamomillae oil | 0.15 |
| Cortex Phellodendri oil | 0.05 |
| Hyaluronate sodium | 0.03 |
| IPBC-1 | 0.01 |
| Bronopol | 0.02 |
| Oil phase | |
| Octadecanol | 3 |
| The monostearate monoglyceride | 4 |
| Polydimethylsiloxane | 3 |
| Glycerol | 5 |
| Propylene glycol | 5 |
| Methyl hydroxybenzoate | 0.06 |
| Water | |
| Aliphatic acid polyethenoxy ether 20 | 0.3 |
| Sodium lauryl sulphate | 0.8 |
| Deionized water | To 100 |
2, production technology
Take by weighing each component according to said ratio, and oil phase and water are melted in operation respectively routinely, treat oil, the biphase fusion temperature of water mixes in reactor when reaching 85 ℃ of left and right sides respectively carries out preliminary emulsifying, again temperature is reduced to rapidly about 55 ℃, add the fresh milk in adding mutually, after stirring, backheat to 75～90 ℃ insulated and stirred 5～15 minutes is so that the fresh milk sterilization, and then be cooled to 48～60 the degree, add other compositions that add phase, reactor keeps maximum vacuum, started quick stirring and homogenizing 1～2 minute, with guarantee to add phased soln fully and no bubble is control criterion, about starting refrigeration system fast cooling to 40 simultaneously and spending, qualifiedly get final product discharging.
Skin moistening honey through above-mentioned explained hereafter, abnormal smells from the patient fragrance is pleasant, no essence, non-stimulated composition, through long-term shelf storage test (following 3 years of room temperature) and heat-resisting repeatedly (40 ± 1 ℃, recovered room temperatures in 24 hours after, mastic is normal, not muddy), cold-resistant (15 ± 1 ℃, recovered room temperatures in 24 hours after, system is normal, do not have muddy water outlet phenomenon) destructive testing, the every sense index of product, physical and chemical index, sanitary index all meet corresponding national standards.
The production of embodiment 2, child's skin moistening honey
Prescription (each component is all by weight percentage):
| Material name | Percentage ratio |
| Add phase | |
| Fresh milk | 18 |
| The Herba Dendranthematis indici caul-fat | 0.15 |
| Flos Matricariae chamomillae oil | 0.35 |
| Cortex Phellodendri oil | 0.1 |
| Hyaluronate sodium | 0.08 |
| IPBC-1 | 0.01 |
| Bronopol | 0.02 |
| Oil phase | |
| Octadecanol | 5 |
| The monostearate monoglyceride | 2 |
| Polydimethylsiloxane | 1 |
| Glycerol | 6 |
| Propylene glycol | 2 |
| Methyl hydroxybenzoate | 0.05 |
| Water | |
| Aliphatic acid polyethenoxy ether 20 | 1.0 |
| Sodium lauryl sulphate | 0.1 |
| Deionized water | To 100 |
The production technology of present embodiment is substantially with embodiment 1, and the every sense index of the product that obtains, physical and chemical index, sanitary index all meet corresponding national standards.
The production of embodiment 3, senior child's frost
Prescription (each component all by weight percentage)
| Material name | Percentage ratio |
| Add phase | |
| Fresh milk | 15 |
| The Herba Dendranthematis indici caul-fat | 0.25 |
| Flos Matricariae chamomillae oil | 0.4 |
| Cortex Phellodendri oil | 0.15 |
| Hyaluronate sodium | 0.02 |
| IPBC-1 | 0.01 |
| Bronopol | 0.02 |
| Oil phase | |
| Octadecanol | 1 |
| White oil | 4.5 |
| Emulgade?PL68/50 | 3 |
| Isopropyl palmitate | 6 |
| Dimethicone DC200 | 2 |
| Methyl hydroxybenzoate | 0.06 |
| Water | |
| Glycerol | 10 |
| Sodium lauryl sulphate | 0.3 |
| Propylene glycol | 8 |
| Deionized water | To 100 |
The production technology of present embodiment is substantially with embodiment 1, and the every sense index of the product that obtains, physical and chemical index, sanitary index all meet corresponding national standards.
The production of embodiment 4, senior child's frost
Prescription (each component all by weight percentage)
| Material name | Percentage ratio |
| Add phase | |
| Fresh milk | 5 |
| The Herba Dendranthematis indici caul-fat | 0.25 |
| Flos Matricariae chamomillae oil | 0.25 |
| Cortex Phellodendri oil | 0.1 |
| Hyaluronate sodium | 0.1 |
| IPBC-1 | 0.01 |
| Bronopol | 0.02 |
| Oil phase | |
| Octadecanol | 4 |
| White oil | 1.5 |
| Emulgade?PL68/50 | 4 |
| Isopropyl palmitate | 4 |
| Dimethicone DC200 | 5 |
| Methyl hydroxybenzoate | 0.05 |
| Water | |
| Glycerol | 15 |
| Sodium lauryl sulphate | 0.8 |
| Propylene glycol | 5 |
| Deionized water | To 100 |
The production technology of present embodiment is substantially with embodiment 1, and the every sense index of the product that obtains, physical and chemical index, sanitary index all meet corresponding national standards.
The production of embodiment 5, senior child's frost
Prescription (each component all by weight percentage)
| Material name | Percentage ratio |
| Add phase | |
| Fresh milk | 15 |
| The Herba Dendranthematis indici caul-fat | 0.2 |
| Flos Matricariae chamomillae oil | 0.3 |
| Cortex Phellodendri oil | 0.1 |
| Hyaluronate sodium | 0.02 |
| IPBC-1 | 0.01 |
| Bronopol | 0.02 |
| Oil phase | |
| Octadecanol | 1 |
| White oil | 4.5 |
| Emulgade?PL68/50 | 3 |
| Isopropyl palmitate | 6 |
| Dimethicone DC200 | 2 |
| Methyl hydroxybenzoate | 0.02 |
| Water | |
| Glycerol | 12 |
| Sodium lauryl sulphate | 0.5 |
| Propylene glycol | 8 |
| Deionized water | To 100 |
The production technology of present embodiment is substantially with embodiment 1, the product odour fragrance that obtains, the pleasant aroma, product is through long-term shelf storage test and heat-resisting repeatedly, cold-resistant destructive testing, and every sense index, physical and chemical index, sanitary index all meet corresponding national standards.
The production of embodiment 6, cleansing milk
Prescription (each component all by weight percentage)
| Material name | Percentage ratio |
| Add phase | |
| Fresh milk | 8 |
| The Herba Dendranthematis indici caul-fat | 0.25 |
| Flos Matricariae chamomillae oil | 0.4 |
| Cortex Phellodendri oil | 0.15 |
| Hyaluronate sodium | 0.05 |
| IPBC-1 | 0.01 |
| Bronopol | 0.02 |
| Oil phase | |
| Octadecanol | 1 |
| The monostearate monoglyceride | 2 |
| White oil | 8 |
| Isopropyl palmitate | 16 |
| Methyl hydroxybenzoate | 0.1 |
| Water | |
| Glycerol | 8 |
| Propylene glycol | 8 |
| Sodium lauryl sulphate | 0.5 |
| Aliphatic acid polyethenoxy ether 20 | 1.0 |
| EDTA-4Na | 0.05 |
| Deionized water | To 100 |
The production technology of present embodiment is substantially with embodiment 1, and the every sense index of the product that obtains, physical and chemical index, sanitary index all meet corresponding national standards.
The production of embodiment 7, cleansing milk
Prescription (each component all by weight percentage)
| Material name | Percentage ratio |
| Add phase | |
| Fresh milk | 5 |
| The Herba Dendranthematis indici caul-fat | 0.2 |
| Flos Matricariae chamomillae oil | 0.25 |
| Cortex Phellodendri oil | 0.08 |
| Hyaluronate sodium | 0.1 |
| IPBC-1 | 0.01 |
| Bronopol | 0.02 |
| Oil phase | |
| Octadecanol | 0.3 |
| The monostearate monoglyceride | 4 |
| White oil | 15 |
| Isopropyl palmitate | 8 |
| Methyl hydroxybenzoate | 0.02 |
| Water | |
| Glycerol | 15 |
| Propylene glycol | 5 |
| Sodium lauryl sulphate | 1.2 |
| Aliphatic acid polyethenoxy ether 20 | 0.3 |
| EDTA-4Na | 0.1 |
| Deionized water | To 100 |
The production technology of present embodiment is substantially with embodiment 1, and the every sense index of the product that obtains, physical and chemical index, sanitary index all meet corresponding national standards.
The result of use experiment:
Among the present invention, to produce the senior child's frost (Yu Mei clear height level child frost) that obtains according to embodiment 5 is example, and (prescription of this contrast sample is compared with embodiment 5 to adopt the contrast sample, be that water with equivalent has substituted compound essential Oil and the fresh milk in embodiment 5 prescriptions, other batchings and consumption are substantially with embodiment 5, in the production technology except that the step of not adding fresh milk and compound essential Oil substantially with embodiment 5), carry out the actual use of crowd tracking test, to investigate the antiinflammatory of having added the cosmetics of described fresh milk and compound essential Oil compositions of the present invention, antiallergic, eliminate the result of use of eczema.In this experiment, choose 300 volunteers, at 0.5～12 years old age, eczema is in various degree arranged respectively, the volunteer is divided into two groups (test group and matched groups) at random, every group 150 people, test group is coated with Yu Mei clear height level child frost of the present invention, and matched group is coated with the contrast sample, consumption adopts in right amount according to the eczema area, be coated with usefulness every day after with the clear water cleaning skin, each 1 time sooner or later, follow the tracks of the statistics operating position.Test and after 30 days eczema is improved Evaluation on effect outcome record such as following table.
As can be seen from the above table, consumer is to using behind senior child's frost of the present invention for the improvement situation of eczema, and satisfaction rate can reach more than 85%; And consumer only reaches 10% to using the contrast sample for the improvement situation satisfaction rate of eczema.
In addition, the inventor has also carried out the use tracking test at the child's frost sample that adds Flos Chrysanthemi Indici quintessence oil, Flos Matricariae chamomillae quintessence oil, Cortex Phellodendri quintessence oil or fresh milk respectively separately as Comparative Examples of the present invention in research process, the result shows that consumer all is lower than 20% to using these four kinds of comparative sample for the effect satisfaction rate that improves of eczema.
Claims (7)
1. cosmetic composition, said composition comprises: Cortex Phellodendri quintessence oil, Flos Chrysanthemi Indici quintessence oil and Flos Matricariae chamomillae quintessence oil, and fresh milk;
Wherein, described Cortex Phellodendri quintessence oil, Flos Chrysanthemi Indici quintessence oil and Flos Matricariae chamomillae quintessence oil are formed compound essential Oil, and the weight ratio of this compound essential Oil and fresh milk is 0.2～0.8: 5～20;
The weight ratio of described Cortex Phellodendri quintessence oil, Flos Chrysanthemi Indici quintessence oil and Flos Matricariae chamomillae quintessence oil is 1: 1.5～2.5: 2.5～3.5.
2. cosmetic composition according to claim 1, wherein, the weight ratio of described compound essential Oil and fresh milk is 0.5: 5～20.
3. cosmetic composition according to claim 1, wherein, the weight ratio of described Cortex Phellodendri quintessence oil, Flos Chrysanthemi Indici quintessence oil and Flos Matricariae chamomillae quintessence oil is 1: 2: 3.
4. the application of each described cosmetic composition of claim 1～3 in the preparation cosmetics.
5. application according to claim 4, wherein, described cosmetic composition is to be that the amount that cosmetic material is formed gross weight 5%～20% is added in the cosmetics with the amount of fresh milk wherein.
6. cosmetics comprise each described cosmetic composition of claim 1～3 in the raw material composition of these cosmetics; Wherein, the content of the fresh milk in the described cosmetic composition in the raw material of these cosmetics is formed is 5%～20%.
7. cosmetics according to claim 6, these cosmetics are skin care item or cleaning series products.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009100709765A CN101695470B (en) | 2009-10-27 | 2009-10-27 | Composite for cosmetics, cosmetic product containing same and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009100709765A CN101695470B (en) | 2009-10-27 | 2009-10-27 | Composite for cosmetics, cosmetic product containing same and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101695470A CN101695470A (en) | 2010-04-21 |
| CN101695470B true CN101695470B (en) | 2011-08-10 |
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| CN102614101B (en) * | 2012-04-25 | 2013-07-03 | 天津郁美净集团有限公司 | Cosmetic composition containing amur corktree bark extract and preparation method and application thereof |
| CN105816342A (en) * | 2015-01-09 | 2016-08-03 | 捷通国际有限公司 | Composition containing obacunone and method for using obacunone in skin whitening |
| CN106539716A (en) * | 2017-01-23 | 2017-03-29 | 钟苏 | A kind of antiallergic repairs quintessence oil |
| CN114146031A (en) * | 2020-09-08 | 2022-03-08 | 上海文峰美发美容有限公司 | Acne-removing composition and preparation method thereof |
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