CN102406578B - Silky bright-color smoothing toner composition - Google Patents

Silky bright-color smoothing toner composition Download PDF

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CN102406578B
CN102406578B CN 201110297683 CN201110297683A CN102406578B CN 102406578 B CN102406578 B CN 102406578B CN 201110297683 CN201110297683 CN 201110297683 CN 201110297683 A CN201110297683 A CN 201110297683A CN 102406578 B CN102406578 B CN 102406578B
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skin
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composition
smoothing toner
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CN102406578A (en
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姚国英
何丹
张丽华
沈伟良
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Ou Shi Overflows Biological Co Ltd
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沈志荣
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Abstract

The invention belongs to a smoothing toner composition capable of improving skin color and a preparation method thereof. A silky bright-color smoothing toner composition comprises the following components in mass percentage: (a) 0.01-20% of moisturizer; (b) 0.01-20% of moisturizing grease; (c) 0.01-10% of surfactant; (d) 0.01-10% of thickening polymer; (e) 0.01-10% of skin conditioner; and (f) 0.01-90% of deionized water. The composition has the advantages of deeply nourishing, regularizing skin, improving skin color, regulating yellowness state and enabling skin to become moist and tenderly white.

Description

A kind of toner/smoothing toner compositions
Technical field
The invention belongs to a kind of toner/smoothing toner composition and method of making the same of Titanium Dioxide.
Background technology
Because modern people's rhythm of life is fast, and be subjected to various environmental effects, the frequent drying of skin, intensely dark pool.For this situation, we have prepared this toner/smoothing toner compositions that consumer is liked, and deep layer is nourished, the conditioning skin, improves the colour of skin, adjusts dark yellow state, make skin moist tender white.
Chinese invention patent application (application number: 200910010837.3 applyings date: 2009-03-24) disclose a kind of skincare humectant.It is made of according to the following number of weight ratio following component: the skin protection base material: natural dimethylamino proline acid: glycerol: Mel: shea butter: vitamin E=80-120: 5-12: 1-3: 10-20: 1-3: 2-4.This invention contains shea butter, glycerol, Mel isoreactivity nourishing moisturizing composition, can help rapidly to moisten dry skin, makes the skin exquisiteness soft and smooth.
Chinese invention patent application (application number: 200710150410.4 applyings date: 2007-11-26) disclose a kind of cosmetic humectant that contains xylitol, it is comprised of the raw material of following portions by weight: 2-10 part wetting agent, 0.1-2 part oils and fats, emulsifying agent 5-15 part, 60~80 parts, water.The cosmetic humectant of this invention can more deeply be diffused into the skin depths, is combined with deep water, keeps the moist of skin.
Summary of the invention
In order to solve the problem in the frequent drying of people's skin, intensely dark pool, an object of the present invention is to provide a kind of bright color toner/smoothing toner compositions of profit, said composition can deep layer nourish, nurse one's health skin, improves the colour of skin, adjusts dark yellow state, makes skin moist tender white.Another one purpose of the present invention is to provide the preparation method that a kind of above-mentioned silk moistens bright color toner/smoothing toner compositions.
In order to realize above-mentioned first purpose, the present invention has adopted following technical scheme:
A kind of bright color toner/smoothing toner compositions of profit, described compositions comprises following component by mass percentage:
(a) 0.01% to 20% wetting agent;
(b) 0.01% to 20% skin moistening oils and fats;
(c) 0.01% to 10% surfactant;
(d) 0.01% to 10% thickening polymer;
(e) 0.01% to 10% skin conditioning agent; With
(f) 10% to 90% deionized water.
As preferably, described compositions comprises following component by mass percentage:
(a) 1% to 20% wetting agent;
(b) 0.01% to 15% skin moistening oils and fats;
(c) 0.01% to 8% surfactant;
(d) 0.01% to 8% thickening polymer;
(e) 0.01% to 8% skin conditioning agent; With
(f) 10% to 90% deionized water.
As preferred again, described compositions comprises following component by mass percentage:
(a) 2% to 20% wetting agent;
(b) 0.01% to 10% skin moistening oils and fats;
(c) 0.01% to 6% surfactant;
(d) 0.01% to 6% thickening polymer;
(e) 0.01% to 6% skin conditioning agent; With
(f) 10% to 90% deionized water.
As preferably, above-mentioned wetting agent is selected propylene glycol, sorbitol, butanediol, 1, one or more in 2-hexanediol, caprylyl glycol, dipropylene glycol, glycerol, diglycerol, pentanediol, Polyethylene Glycol, and what be preferred for this compositions is butanediol or glycerol; Described skin moistening oils and fats is selected one or more in polydimethylsiloxane, glycerol three (thylhexoic acid) ester and squalane.
As preferably, above-mentioned surfactant is selected hydrolecithin.
As preferably, above-mentioned thickening polymer is selected one or more in the synthetic high molecular polymer of carboxylic acid polyalcohol, cross-linked polyacrylate polymer, cellulose ethers, natural high molecular polymer; Preferably cellulose ethers and crosslinked acrylate polymer are more preferably by by CTFA called after hydroxyethyl-cellulose and acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer.
As preferably, above-mentioned skin conditioning agent is selected from one or more in hydrolyzed pearl, hyaluronate sodium, Herba Saussureae Involueratae extract, root of Paeonia suffruticosa Ardr. extract, bermuda lily flower extract.
As preferably, above-mentioned said composition has also comprised one or more in pH adjusting agent, food coloring, antiseptic, essence and solvent.
The present composition also can comprise various other compositions.The function of the concrete composition of compositions of the present invention and effect will be described in more detail below.
Wetting agent
In the present invention by weight approximately 0.01% to 20% wetting agent be polyhydric alcohol, compositions described herein preferably comprises by weight of the composition approximately 1% to 20%, the wetting agent of 2%-20% more preferably, example comprises propylene glycol, sorbitol, butanediol, 1,2-hexanediol, caprylyl glycol, dipropylene glycol, glycerol, diglycerol, pentanediol, Polyethylene Glycol, and their mixture, what be preferred for this compositions is butanediol and glycerol.
The skin moistening oils and fats
Skin moistening oils and fats in the present composition can pin moisture, prevents excessive volatilization, makes skin keep the tender gloss of water.
Skin moistening oils and fats polydimethylsiloxane in the present composition, its by weight of the composition approximately 0.01% to 20%, preferably be about 0.01% to 15%, more preferably from about 0.01% to 10%.It is nontoxic, to skin and mucosa nonirritant, but irritant to eyes.It is generally accepted it is safe.Have good chemical stability, antistatic behaviour and breathability can freely be breathed skin.
Skin moistening oils and fats glycerol three (thylhexoic acid) ester in the present composition, its by weight of the composition approximately 0.01% to 20%, preferably be about 0.01% to 15%, more preferably from about 0.01% to 10%.It is a kind of triglycerin esters, derives from glycerol and fatty acid, is a kind of lightweight oils and fats, but antistatic is skin softening agent and conditioner.
Skin moistening oils and fats squalane in the present composition, its by weight of the composition approximately 0.01% to 20%, preferably be about 0.01% to 15%, more preferably from about 0.01% to 10%.It has the cosmetic properties of natural squalane, is a kind of colourless, tasteless, nontoxic high-purity liquid clothes hook linear paraffin, can give cosmetics fabulous and noble feel, moistens non-greasy, and moisturizing is lubricated, and penetration is strong, and good stability.
Surfactant
Surfactant in the present composition is hydrolecithin, is a kind of natural green emulsifying agent, and its main chemical compositions is lecithin, PHOSPHATIDYL ETHANOLAMINE and phosphatidylinositols.Total institute is known, and phospholipid is distributed in animal and plant body widely, is one of important component part of biological cell.It is to metabolism, and membrane permeation plays very important effect.
Phospholipid is the material with interfacial activity that consists of the lipophilic group that is combined into by the fatty acid of two long-chains and glycerol and the hydrophilic group that contains simultaneously phosphoric acid, amido.Thereby it has good emulsifying dispersivity, wettability, stability and viscosity adjustment performance.Hydrolecithin in the present invention is to obtain by the hydrogenation to phospholipid of natural soybean, has overcome natural phospholipid not resistance to oxidation and thermal instability, has been widely used in each industrial circle of cosmetics and pharmaceuticals.Its feature also has lasting performance of keeping humidity, promotes the subcutaneous absorption of skin, reduces other surfactants to the zest of skin.
Thickening agent
In some embodiments, compositions of the present invention can also comprise one or more thickening agents, and described compositions comprises by weight of the composition approximately 0.01% to 10%, preferably is about 0.01% to 8%, more preferably from about 0.01% to 6% thickening agent.
The non-limiting kind of thickening agent comprises and is selected from following material: carboxylic acid polyalcohol (as Carbopol 980), cross-linked polyacrylate polymer, synthetic high molecular polymer (as cellulose ethers), natural high molecular polymer (as natural gum), preferably cellulose ethers and crosslinked acrylate polymer, more preferably press CTFA called after hydroxyethyl-cellulose and acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer.
Skin conditioning agent
The various skin conditioner that the present composition adds is Herba Saussureae Involueratae extract, root of Paeonia suffruticosa Ardr. extract, bermuda lily flower extract.
The content of the Herba Saussureae Involueratae extract that the present composition adds is preferably approximately 0.01% to 8% by weight of the composition, more preferably from about 0.01% to 6%, the active quantities of the Herba Saussureae Involueratae extract of the present composition is preferred approximately 0.001% to 8% by weight of the composition, and more preferably from about 0.001% to 6%.
The Herba Saussureae Involueratae extract that the present composition adds contains the fragrant glycoside of cloud, xuelianlactone, alkaloid, volatile oil, polysaccharide.Has antiinflammatory, antibiotic and analgesic activity.Promote the permeability of sebum, improve microcirculation, keep skin elasticity.
The content of the root of Paeonia suffruticosa Ardr. extract that the present composition adds is preferably approximately 0.01% to 8% by weight of the composition, more preferably from about 0.01% to 6%, the active quantities of the Herba Saussureae Involueratae extract of the present composition is preferred approximately 0.001% to 8% by weight of the composition, and more preferably from about 0.001% to 6%.
The root of Paeonia suffruticosa Ardr. extract of the present composition, be rich in aminoacid, mineral, multivitamin and zinc, the selenium and other trace elements of needed by human body, have the powerful effect of releiving, can reduce the activity of melanin enzyme in the skin keratin cell, thereby help to suppress to produce melanin; Has antibiotic, antiinflammation; The lymph circulation of chafe makes skin more glossy, improves skin quality, after continuing to use, can allow skin slowly say goodbye to obscure and coarse, and skin is beautiful, the water profit.
The content of the bermuda lily flower extract that the present composition adds is preferably approximately 0.01% to 8% by weight of the composition, more preferably from about 0.01% to 6%, the active quantities of the Herba Saussureae Involueratae extract of the present composition is preferred approximately 0.001% to 8% by weight of the composition, and more preferably from about 0.001% to 6%.
The bermuda lily flower extract of the present composition, except containing starch, protein, fat, carotene, vitamin, trace element, also contain some special nutritional labelings, as multiple alkaloids such as colchicine, have very strong moisture-retaining capacity, regulate skin moisture.
The hydrolyzed pearl of the present composition, the weighing scale that its content is pressed the present composition approximately 0.01% to 10%, preferably be about 0.01% to 8%, be more preferably 0.01% to 6%, the weighing scale that its active matter content is pressed the present composition approximately 0.001% to 10%, preferred approximately 0.001% to 8%, more preferably from about 0.001% to 6%.
The hydrolyzed pearl of the present composition is that the enzymolysis process by Margarita powder obtains, and contains a large amount of calcium ions and pearl protein, has the elimination oxygen-derived free radicals, anti-aging effects, and light speckle makes the beautiful gloss of skin.
The hyaluronate sodium of the present composition is the glutinous sugar of a kind of bionical thing, and molecular weight is greater than 1,000,000, and the hyaluronic acid sodium content of the present composition is by invention composition weight meter approximately 0.01% to 10%, and is preferred approximately 0.01% to 5%, is more preferably 0.01% to 3%.
Contain 10% to 20% moisture in the normal human skin horny layer, it prevents skin aging, prevents that the various stimulations of external environment from having significant role skin care.With advancing age or environmental evolution, moisture can drop to below 10%, and skin can be dry, produces wrinkle.The hyaluronate sodium of the present composition can be alleviated this problem, and its theoretical water retention value reaches 1000ml/g, is the key component of water conservation in human body skin, and not only moistening effect is good, and without greasy feeling and stop up pore etc. shortcoming.Can also eliminate oxygen-derived free radicals, repair the skin of damage after shining.
As preferred again, described compositions is made of following component by mass percentage:
Composition % by weight
Glycerol 5.0~20.0
Butanediol 2.0~10.0
Propylene glycol 0~6.0
Hydrolecithin 0~5.0
Polydimethylsiloxane 2.0~10.0
Glycerol three (thylhexoic acid) ester 0~6.0
Squalane 0~4.0
Deionized water 40~80
Hydroxyethyl-cellulose 0~1.2
Hyaluronate sodium 0~1.0
Acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer 0~1.0
Triethanolamine 0~1.0
Potassium hydroxide (10%) 0~3.0
Herba Saussureae Involueratae extract 0~2.0
The root of Paeonia suffruticosa Ardr. extract 0~3.0
The bermuda lily flower extract 0~4.0
Hydrolyzed pearl 0~3.0
Essence 0~0.5
Antiseptic 0~0.8
Solvent 0~0.5
Pigment 0~0.5
It is not 0 that above-mentioned Herba Saussureae Involueratae extract, root of Paeonia suffruticosa Ardr. extract, bermuda lily flower extract and hydrolyzed pearl have a kind of composition at least.
In order to realize second above-mentioned purpose, the present invention has adopted following technical scheme:
A kind of preparation method for preparing the above-mentioned bright color toner/smoothing toner compositions of silk profit, the method comprises the following steps:
1) butanediol, glycerol, hydrolecithin mix, and are heated to 78 ℃ of left and right, and dissolve complete forms phase 1;
2) with polydimethylsiloxane, glycerol three (thylhexoic acid) ester, squalane, be heated to 78 ℃, stir, join in phase 1 low speed homogenizing 5 minutes;
3) with in the mixture more than the water suction, high speed homogenization 10-15 minute, then add hydroxyethyl-cellulose, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, hyaluronate sodium, high speed homogenization 10-15 minute;
4) be cooled to 50 ℃, add triethanolamine, Herba Saussureae Involueratae extract, root of Paeonia suffruticosa Ardr. extract, bermuda lily flower extract, hydrolyzed pearl, essence, pigment, solvent and antiseptic, middling speed homogenizing 8-10 minute, rear discharging stirs;
5) storage → inspection of semifinished product → fill → product inspection → warehouse-in.
The present invention is owing to having adopted above-mentioned technical scheme, and product can keep the skin wet to skin after use, and the effective ingredient Titanium Dioxide in plant extract promotes the glossy degree of skin.
The specific embodiment
Preparation process of the present invention is the state of comparison homogeneous that each composition is mixed to, and step is:
1. butanediol, glycerol, hydrolecithin mix, and are heated to 78 ℃ of left and right, and dissolve complete forms phase 1;
2. with polydimethylsiloxane, glycerol three (thylhexoic acid) ester, squalane, be heated to 78 ℃, stir, join in phase 1 low speed homogenizing 5 minutes;
3. with in the mixture more than the water suction, high speed homogenization 10-15 minute, then add hydroxyethyl-cellulose, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, hyaluronate sodium, high speed homogenization 10-15 minute;
4. be cooled to 50 ℃, add triethanolamine, Herba Saussureae Involueratae extract, root of Paeonia suffruticosa Ardr. extract, bermuda lily flower extract, hydrolyzed pearl, essence, pigment, solvent and antiseptic, middling speed homogenizing 8-10 minute, rear discharging stirs;
5. storage → the inspection of semifinished product → fill → product inspection → warehouse-in.
Specific embodiment:
Figure DEST_PATH_IMAGE001
* 1. acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, derive from Lubrizol
* 2. acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, derive from Lubrizol
Mutually 1 put into container and mix, be heated to 78 ℃, stirring and dissolving is complete; Phase 2 is added phase 1, stir, add phase 3, stirring, homogenizing are with its mixing.Then add phase 4, stirring, homogenizing, mix homogeneously; Add again mutually 5 to 50 ℃, stir, homogenizing, mix homogeneously, discharging.
Method of testing:
In order to test moisturizing of the present invention and to improve colour of skin effect, carried out investigation experiment on probation:
1, respondent: each department ordinary consumer 50 people, 40 parts of the trial state feedback forms of regaining at last;
2, control time: on October 10th, 1 2008 on August 10th, 2008;
3, use product: No. 1 product is the product for preparing according to formula of the present invention; No. 2 products are the rival factory similar products;
4, method of testing: after tester face cleaning, respectively No. 1 product and No. 2 products are coated on the cheek of two of left and right, observe and experience result of use;
5, the test form is as follows:
The use of No. 1 product of table 1 (60 days) feedback conclusive table
Figure 995617DEST_PATH_IMAGE002
No. 2 products of table 2 use (60 days) feedback conclusive table
Figure DEST_PATH_IMAGE003
No. 1 product of table 3 and No. 2 products improve the contrast statistical table of the colour of skin
Figure 813531DEST_PATH_IMAGE004
The statistical table of table 4 tester recommended products model
Proposed model No. 1 No. 2
The recommendation number 32 8
Percentage ratio 80% 20%
6, feedback conclusion:
The tester all represents, the moisture-retaining capacity of No. 1 product and nourish effect and all be better than product No. 2, and No. 1 product conditioning property is good, and after often using, the colour of skin is improved obviously, and is moist tender white; And there is not the people that allergic phenomena is arranged in the questionnaire that reclaims.
As shown in Table 5, No. 1 product of people's recommendation of 80% only has No. 2 products of people's recommendation of 20%.

Claims (1)

1. toner/smoothing toner compositions is characterized in that described toner/smoothing toner compositions is made of following component by mass percentage:
Phase 1:
Glycerol 10% propylene glycol 3%
Butanediol 8% hydrolecithin 2.5%;
Phase 2:
Polydimethylsiloxane 5% squalane 2%;
Phase 3:
Deionized water 42.5%;
Phase 4:
Hydroxyethyl-cellulose 0.6% Carbopol 1,342 0.5%
Hyaluronate sodium 0.5% deionized water 20%;
Phase 5:
Triethanolamine 0.5% essence 0.25%
Herba Saussureae Involueratae extract 1% antiseptic 0.4%
Bermuda lily flower extract 2% solvent 0.25%
Hydrolyzed pearl 1%;
The preparation method of above-mentioned toner/smoothing toner compositions is as follows:
Mutually 1 put into container and mix, be heated to 78 ℃, stirring and dissolving is complete; Phase 2 is added phase 1, stir, add phase 3, stirring, homogenizing are with its mixing; Then add phase 4, stirring, homogenizing, mix homogeneously; Add again mutually 5 to 50 ℃, stir, homogenizing, mix homogeneously, discharging.
CN 201110297683 2011-09-27 2011-09-27 Silky bright-color smoothing toner composition Active CN102406578B (en)

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CN201310157438.6A Division CN103222945B (en) 2011-09-27 2011-09-27 Preparation method for skin softening water composition containing nature plant extract and hydrolyzed pearl

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CN105055238A (en) * 2015-08-13 2015-11-18 刘汉科 Neroli hydrolat lotion and preparation method thereof
CN105055240A (en) * 2015-08-13 2015-11-18 刘汉科 Witchazel hydrosol lotion and preparation method thereof
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CN107519083A (en) * 2017-08-28 2017-12-29 李冉冉 Toner containing natural plant extracts
CN109512734B (en) * 2017-11-24 2021-04-16 北京东方淼森生物科技有限公司 External plant extract and cosmetic with skin elasticity and gloss recovery effects and preparation method thereof
CN109044946A (en) * 2018-09-27 2018-12-21 张言聚 A kind of whitening and moisturizing facial mask liquid and its preparation process
CN109953938A (en) * 2019-04-10 2019-07-02 华子昂 Skin regulates and controls water and preparation method thereof
CN113520974A (en) * 2021-06-25 2021-10-22 温州文恪美容科技有限公司 Skin-moistening anti-wrinkle composition and preparation method and application thereof

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CN101697954A (en) * 2009-10-19 2010-04-28 海南京润珍珠生物技术股份有限公司 Anti-wrinkle emulsion with pearl hydrolyzate liposome
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