CN109044946A - A kind of whitening and moisturizing facial mask liquid and its preparation process - Google Patents
A kind of whitening and moisturizing facial mask liquid and its preparation process Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/676—Ascorbic acid, i.e. vitamin C
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- A61K8/678—Tocopherol, i.e. vitamin E
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- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
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- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
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- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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Abstract
The invention discloses a kind of whitening and moisturizing facial mask liquid and its preparation processes, be prepared from the following raw materials: deionized water, glycerol, 1,3-PD, glycerin monostearate, polyacrylic acid, cetanol palmitate, SIMMONDSIA CHINENSIS SEED OIL, carboxymethyl chitosan, algal polysaccharides, hyaluronic acid, deep-sea fish skin collagen, Chinese herbal medicine extract, yeast dextran, hydrolysis avenin, aloe zymophyte powder, tocopherol acetate, Symwhite-337, hydrolecithin, carbomer receive, vitamin, Phenoxyethanol, triethanolamine and essence.Whitening and moisturizing facial mask liquid of the invention gives full play to moisturizing, whitening, water lock triple function, and is conducive to the advantages that user absorbs.
Description
Technical field
The present invention relates to cosmetic technical fields, and in particular to a kind of whitening and moisturizing facial mask liquid and its preparation process.
Background technique
Facial mask is a classification in skin care item, and its most basic and most important purpose is to make up makeup removing and wash one's face still
Right insufficient cleaning cooperates other essential ingredients to realize other maintenance functions, such as replenishing water and preserving moisture, beauty on this basis
White, anti-aging, Sage Extract etc..
The principle of facial mask is to be temporarily isolating extraneous air and pollution using the of short duration time for being covered on face, improve flesh
Skin temperature, the pore expansion of skin, promotes sweat gland secretion and metabolism, increase the oxygen content of skin, is conducive to skin row
Except the product of epidermal cell metabolism and the oil substances of accumulation, the moisture in facial mask penetrates into the cuticula of epidermis, skin
Become soft, skin is naturally bright flexible.Currently, most of facial mask is made of the non-woven fabrics for being soaked with facial mask liquid, the function of facial mask
Effect is determined by facial mask liquid substantially.
Chinese patent application CN201710072919. discloses a kind of germ juice skin whitening, moisturizing essence facial mask liquid, be by
The raw material composition of following parts by weight: 42-50 parts of germ juice, 9-12 parts of gadol extract, gathers 8-15 parts of fragrant citrus fruit extracting solution
6-8 parts of vinyl alcohol, 9-11 parts of 1,3-BDO, 10-15 parts of glycerol, 8-10 parts of honeysuckle, 5-9 parts of lemon, 4-7 parts of lavender,
3-8 parts of Hydrolyzed Collagen, 10-12 parts of hyaluronic acid, 5-10 parts of methylcellulose, 4-6 parts of dispersing agent, 3-7 parts of preservative.It should
Though patent has effects that whitening and moisturizing, its application has limitation, it is difficult to rise on shriveling water shortage, gloomy unglazed skin
To preferable therapeutic effect.
And Chinese patent application CN201310667039.4 disclose a kind of mask liquid for whitening hydrating mask paste and its
Preparation method and application, the facial mask liquid contain following whitening and moisturizing component, other components, triethanolamine and preservative and perfume (or spice)
Essence, whitening and moisturizing component include oxidoreducing enzyme, niacinamide, dipotassium glycyrrhizinate, Sodium Hyaluronate, white pond lily flower extract,
PEG/PPG-70/30 gives birth to phenolic ether, Flos Mume extract.The present invention can provide facial antiallergic moist for a long time, absorb fastly, after being finished
Half h can obviously see it is white, and for 24 hours continue whitening.The patent has preferable whitening effect, but it is short of in terms of moisturizing effect
Point, it is difficult to play the effect that whitening is mutually cooperateed with moisturizing.
Based on this, it is necessary to a kind of whitening and moisturizing facial mask liquid and its preparation process are provided, to solve to exist in the prior art
The problem of.
Summary of the invention
In order to solve the problems in the existing technology, the present invention provides a kind of whitening and moisturizing facial mask liquid and its preparation works
Skill gives full play to moisturizing, whitening, water lock triple function, and is conducive to the advantages that user absorbs.
It is of the existing technology in order to solve the problems, such as, it adopts the following technical scheme that
A kind of whitening and moisturizing facial mask liquid, is prepared from the following raw materials in parts by weight: 50-60 parts of deionized water, glycerol 2-5
Part, 2-5 parts of 1,3- propylene glycol, 4-8 parts of glycerin monostearate, 3-7 parts of polyacrylic acid, 2-6 parts of cetanol palmitate, lotus lotus
Bar 1-4 parts of oil, 1-3 parts of carboxymethyl chitosan, 0.5-1.5 parts of algal polysaccharides, 0.3-0.7 parts of hyaluronic acid, deep-sea fish skin collagen
0.6-1.2 parts of albumen, 0.8-1.6 parts of Chinese herbal medicine extract, 0.4-0.8 parts of yeast dextran, hydrolysis avenin 0.5-1 parts,
0.4-0.8 parts of aloe zymophyte powder, 0.2-0.4 parts of tocopherol acetate, 0.3-0.6 parts of Symwhite-337, hydrogenation lecithin
0.1-0.3 parts of rouge, carbomer receive 0.2-0.4 parts, 0.1-0.3 parts of vitamin, 0.3-0.6 parts of Phenoxyethanol, triethanolamine 0.1-
0.5 part and essence 0.1-0.3 parts.
Wherein, the Chinese herbal medicine extract is the mixture of Herba Saussureae Involueratae extract, licorice and Rhizoma Atractylodis Macrocephalae root extract,
The weight ratio of the Herba Saussureae Involueratae extract, licorice and Rhizoma Atractylodis Macrocephalae root extract is (0.5-10): (0.5-10): (0.5-
10)。
Wherein, the Herba Saussureae Involueratae extract the preparation method is as follows: lanatechead saussurea herb with flower is cleaned up with drinking water, it is dry after powder
It is broken into coarse grain, 5 times 70% of lanatechead saussurea herb with flower of ethyl alcohol is added and carries out alcohol extracting, alcohol extracting 2 times, each 2h, merges alcohol extract, is concentrated into opposite
Density is 1.25 medicinal extract, lets cool, medicinal extract is put into rail mounted film drier, is dried, and after dry, is ground into fine powder,
And it sieves with 100 mesh sieve to get Herba Saussureae Involueratae extract.
The licorice the preparation method comprises the following steps: extracting liquorice, is extracted using 80%v/v alcohol reflux, extracting solution recycling
It after ethyl alcohol, then with AB-8 macroreticular resin carries out absorption passivation, and is eluted using 90%v/v ethyl alcohol, collect ethanol eluate,
Ethyl alcohol is recycled, concentration is dry to get licorice.
The Rhizoma Atractylodis Macrocephalae root extract the preparation method comprises the following steps: by coarse grain is ground into after the drinking water cleaning, drying of Rhizoma Atractylodis Macrocephalae root, add
Enter 8 times of purified waters of Rhizoma Atractylodis Macrocephalae root, decoct 2 times, decoct 2h every time, merge decoction liquor, being concentrated into relative density is 1.15 medicinal extract, is put
It is cold, 95%v/v ethyl alcohol is added and carries out alcohol precipitation, final alcohol precipitation degree is 70, it stands more than for 24 hours, extracts supernatant, be concentrated,
Being concentrated into relative density is 1.30, and medicinal extract is put into rail mounted film drier, is dried, and after dry, is ground into fine powder, and
It sieves with 100 mesh sieve to get Rhizoma Atractylodis Macrocephalae root extract.
Preferably, it is prepared from the following raw materials in parts by weight: 55 parts of deionized water, 3.5 parts of glycerol, 1,3- the third two
3.5 parts of alcohol, 6 parts of glycerin monostearate, 5 parts of polyacrylic acid, 4 parts of cetanol palmitate, 2.5 parts of SIMMONDSIA CHINENSIS SEED OIL, methylol
2 parts of chitosan, 1 part of algal polysaccharides, 0.5 part of hyaluronic acid, 0.8 part of deep-sea fish skin collagen, 1.2 parts of Chinese herbal medicine extract,
0.6 part of yeast dextran, hydrolysis 0.7 part of avenin, 0.6 part of aloe zymophyte powder, 0.3 part of tocopherol acetate, phenethyl
0.5 part of resorcinol, 0.2 part of hydrolecithin, carbomer receive 0.3 part, 0.2 part of EDETATE SODIUM, 0.4 part of Phenoxyethanol, three second
0.3 part and 0.2 part of essence of hydramine.
Preferably, the weight ratio of the Herba Saussureae Involueratae extract, licorice and Rhizoma Atractylodis Macrocephalae root extract is (3-
7): (3-7): (3-7).
Preferably, the hyaluronic acid is macromolecular Sodium Hyaluronate, middle numerator sodium hyaluronate and small molecule
The mixture of Sodium Hyaluronate, and its weight ratio is 1:1:2.
Preferably, the aloe zymophyte powder is made of the substance of following parts by weight: 60-80 parts of aloe, hydrolysis
5-10 parts of royal jelly, 3-6 parts of peptone, 0.3-0.7 parts of phosphoric acid hydrogen dimethylamino potassium, 0.5-1.5 parts of epsom salt；
The aloe zymophyte powder is sufficiently beaten the preparation method comprises the following steps: dry aloe is mixed with water 1:10-15 in mass ratio,
As basic liquid, hydrolysis royal jelly, peptone, phosphoric acid hydrogen dimethylamino potassium and the seven water sulfuric acid of above-mentioned parts by weight are added into basal liquid
Magnesium sterilizes after mixing well, and microbe inoculation leavening, is kept for 25-35 DEG C of temperature, ferments after 48-54h, high-temperature sterilization is cold
It is lyophilized dry to get aloe zymophyte powder.
Preferably, the microbe leaven presses matter by Bacillus acidi lactici, bacillus licheniformis, Corynebacterium glutamicum
Amount mixes gained than 3:2:1.
Preferably, the vitamin is vitamin B, vitamin C and vitamin E, and weight ratio is 1:2:5.
Deep-sea fish skin collagen: it is a large amount of to include skin for the fish collagen at the deep-sea from Pacific waters
The collagen of demand has extraordinary compatibility to be able to maintain skin moisture easily by percutaneous absorption, and has with water
The formation for preventing melanocyte in skin, to have the function that whitening.
Chinese herbal medicine extract is mixed by Herba Saussureae Involueratae extract, licorice and Rhizoma Atractylodis Macrocephalae root extract, three kinds of extractions
Object has significant moisturizing, highlights, white-skinned face function, meanwhile, three has preferable synergistic function, improves the beauty of facial mask liquid
White moisturizing performance.
Yeast dextran: being a kind of and the high complex carbohydrate of skin similarity, because it has uniqueness for skin
Compatibility and compatibility, moisture can tie up the ability in skin by yeast dextran, have and adjust moisturizing, continue moisturizing, reduce thorn
The abilities such as sharp, while it can enhance skin elasticity, and keep skin tender pale, improve the conjunction of collagen and elastic fibers element
At supply various kinds of cell growth factor, to have the function that skin whitening.
Hydrolyze avenin: the albumen of the protein containing a large amount of small-molecular-weight and macromolecule in hydrolysis avenin
Matter, wherein the protein of small-molecular-weight is easy to permeate, and is conducive to skin and is absorbed and utilized, promotion skin metabolism, and macromolecular
The protein good film-forming property of amount can improve the sliding sense of skin, have significant nutrition moist and moisture-keeping efficacy, also, hydrolyze oat
Amino acid is abundant in albumen, can prevent oxidizing tyrosine, the release for preventing melanin is carried out, to have the function that whitening.
Aloe zymophyte powder: by carrying out fermentation process to aloe, the macromolecular egg being absorbed by the skin will be not easy in aloe
White matter, amino acid are decomposed into the small molecule amino acid and polypeptide being easily absorbed by the skin, and have good nutrition, taste to human skin
The hydrolysis royal jelly added when moistening, whitening function, while fermenting contains the amino acid that can be largely absorbed by the body, enzyme, hormone, dimension
Raw element and carbohydrate, there is the beautification function of nourishing skin care.
The deep-sea fish skin collagen, Chinese herbal medicine extract, yeast dextran, hydrolysis avenin and aloe zymophyte
Powder compounding, in conjunction with glycerol, 1,3-PD, glycerin monostearate, polyacrylic acid, cetanol palmitate, SIMMONDSIA CHINENSIS SEED OIL,
Carboxymethyl chitosan, algal polysaccharides, hyaluronic acid, tocopherol acetate, Symwhite-337, hydrolecithin, carbomer
Receive, the basic materials such as EDETATE SODIUM, Phenoxyethanol obtain whitening and moisturizing facial mask liquid of the invention, each component collaboration reaches this hair
Bright whitening and moisturizing facial mask liquid can be quickly by skin overall absorption, effective moisturizing, while depth water lock, long-acting moisturizing, meanwhile, whitening
Moisturizing obvious effect, and it is without any side effects.
The present invention also provides the preparation processes of above-mentioned whitening and moisturizing facial mask liquid, comprising the following steps:
(1) by the deionized water of formula ratio, 1,3- propylene glycol, glycerin monostearate, polyacrylic acid, cetanol palmitinic acid
Ester, SIMMONDSIA CHINENSIS SEED OIL after weighing in proportion, are added in the stainless steel kettle with stirring, heat under the stirring of revolving speed 30-50rpm
Dissolution is complete, and constant temperature disinfection 20min at a temperature of 80 DEG C, then adds the carboxymethyl chitosan and hyalomitome of formula ratio
Acid stirs evenly, and obtains the first mixture, for use；
(2) by the glycerol of formula ratio, algal polysaccharides, Marine fish collagen, Chinese herbal medicine extract, yeast dextran, water
Avenin, aloe zymophyte powder are solved, after weighing in proportion, is added in emulsion pot, is heated with stirring to 50-60 DEG C, Zhi Houtong
Filter screen is extracted into stainless steel homogeneous kettle, under the stirring of 30-40rpm, continues to be heated to 70-80 DEG C, and constant temperature disinfection 10-
20min obtains the second mixture, for use；
(3) triethanolamine is added in second mixture, is kept the temperature after stirring 2-4min under the conditions of 82-86 DEG C
15-20min obtains third mixture；
(4) the first mixture is slowly pumped into third mixture, and scrapes wall stirring, revolving speed increases to 60-70rpm, stirs
After mixing 3-5min, high speed homogenization device is started, the homogeneous 5-8min under the high speed of 3500-4500rpm will scrape wall revolving speed reduction of speed later
To 50-60rpm, and it is cooled to 50 DEG C under this revolving speed, the tocopherol acetate, Symwhite-337, hydrogen of formula ratio is added
Change lecithin, carbomer, EDETATE SODIUM, Phenoxyethanol, triethanolamine and essence, continuation stirs 20- under same revolving speed
30min is to get the whitening and moisturizing facial mask liquid.
Compared with prior art, the present invention it has the advantages that
(1) whitening moisturizing face masque liquid of the present invention contains the plant extractions ingredients such as Chinese herbal medicine extract, aloe protein hydrolysate, can
Go deep into skin bottom to keep the skin wet, can be quickly absorbed by the skin, meanwhile, Chinese herbal medicine extract is contained into whitening conditioning ingredients and reed
Whitening, antioxidant content in luxuriant growth zymophyte powder etc. organically combine, and functionally carry out balanced collocation, to guarantee
Reach efficient whitening and moistening skin effect under the premise of being perfectly safe, and the nutrients such as Marine fish collagen, hydrolysis avenin are fast
It speed and completely penetrates into skin bottom, repairs skin lines, that improves skin resists power.
(2) whitening and moisturizing facial mask liquid of the present invention contains yeast dextran, can promote skin and restores good barrier function, has
Effect reduces trans epidermal water loss, and keyed moisture plays the function of moisturizing water lock, and skin can be made tender pale, improves collagen egg
White and elastic fibers element synthesis, supplies various kinds of cell growth factor, to have the function that skin whitening.
(3) whitening and moisturizing facial mask liquid each component collaboration of the present invention, moistening effect is good, and safe and non-stimulating, while the present invention
The preparation method of whitening and moisturizing facial mask liquid is simple, can promote the use of.
Specific embodiment
To make the object, technical solutions and advantages of the present invention clearer, technical solution of the present invention will be carried out below
Clear, complete description.Obviously, the described embodiment is only a part of the embodiment of the present invention, instead of all the embodiments.
Based on the embodiments of the present invention, those of ordinary skill in the art obtained institute without making creative work
There are other embodiments, belongs to the range that the present invention is protected.
Embodiment 1
The whitening and moisturizing facial mask liquid of the present embodiment, is prepared from the following raw materials in parts by weight: 50 parts of deionized water, glycerol 2
Part, 2 parts of 1,3- propylene glycol, 4 parts of glycerin monostearate, 3 parts of polyacrylic acid, 2 parts of cetanol palmitate, 1 part of SIMMONDSIA CHINENSIS SEED OIL,
1 part of carboxymethyl chitosan, 0.5 part of algal polysaccharides, 0.3 part of hyaluronic acid, 0.6 part of deep-sea fish skin collagen, Chinese herbal medicine extract
0.8 part of object, 0.4 part of yeast dextran, hydrolysis 0.5 part of avenin, 0.4 part of aloe zymophyte powder, tocopherol acetate 0.2
Part, 0.3 part of Symwhite-337,0.1 part of hydrolecithin, carbomer receive 0.2 part, 0.1 part of vitamin, Phenoxyethanol 0.3
Part, 0.1 part of triethanolamine and 0.1 part of essence.
Wherein, the Chinese herbal medicine extract is the mixture of Herba Saussureae Involueratae extract, licorice and Rhizoma Atractylodis Macrocephalae root extract,
The weight ratio of the Herba Saussureae Involueratae extract, licorice and Rhizoma Atractylodis Macrocephalae root extract is 8:2:2.
Wherein, the Herba Saussureae Involueratae extract the preparation method is as follows: lanatechead saussurea herb with flower is cleaned up with drinking water, it is dry after powder
It is broken into coarse grain, 5 times 70% of lanatechead saussurea herb with flower of ethyl alcohol is added and carries out alcohol extracting, alcohol extracting 2 times, each 2h, merges alcohol extract, is concentrated into opposite
Density is 1.25 medicinal extract, lets cool, medicinal extract is put into rail mounted film drier, is dried, and after dry, is ground into fine powder,
And it sieves with 100 mesh sieve to get Herba Saussureae Involueratae extract.
The licorice the preparation method comprises the following steps: extracting liquorice, is extracted using 80%v/v alcohol reflux, extracting solution recycling
It after ethyl alcohol, then with AB-8 macroreticular resin carries out absorption passivation, and is eluted using 90%v/v ethyl alcohol, collect ethanol eluate,
Ethyl alcohol is recycled, concentration is dry to get licorice.
The Rhizoma Atractylodis Macrocephalae root extract the preparation method comprises the following steps: by coarse grain is ground into after the drinking water cleaning, drying of Rhizoma Atractylodis Macrocephalae root, add
Enter 8 times of purified waters of Rhizoma Atractylodis Macrocephalae root, decoct 2 times, decoct 2h every time, merge decoction liquor, being concentrated into relative density is 1.15 medicinal extract, is put
It is cold, 95%v/v ethyl alcohol is added and carries out alcohol precipitation, final alcohol precipitation degree is 70, it stands more than for 24 hours, extracts supernatant, be concentrated,
Being concentrated into relative density is 1.30, and medicinal extract is put into rail mounted film drier, is dried, and after dry, is ground into fine powder, and
It sieves with 100 mesh sieve to get Rhizoma Atractylodis Macrocephalae root extract.
Wherein, the hyaluronic acid is macromolecular Sodium Hyaluronate, middle numerator sodium hyaluronate and micromolecule hyaluronic acid
The mixture of sodium, and its weight ratio is 1:1:2.
Wherein, the aloe zymophyte powder is made of the substance of following parts by weight: 60 parts of aloe, hydrolysis 5 parts of royal jelly, egg
3 parts of white peptone, 0.3 part of phosphoric acid hydrogen dimethylamino potassium, 0.5 part of epsom salt；
Sufficiently being beaten the preparation method comprises the following steps: dry aloe is mixed with water 1:10 in mass ratio for the aloe zymophyte powder, makees
For basic liquid, hydrolysis royal jelly, peptone, phosphoric acid hydrogen dimethylamino potassium and the epsom salt of above-mentioned parts by weight are added into basal liquid
It sterilizes after mixing well, and microbe inoculation leavening, is kept for 25 DEG C of temperature, after the 48h that ferments, high-temperature sterilization, freeze-drying, i.e.,
Obtain aloe zymophyte powder.
Wherein, the microbe leaven is by Bacillus acidi lactici, bacillus licheniformis, Corynebacterium glutamicum 3:2 in mass ratio:
1 mixing gained.
Wherein, the vitamin is vitamin B, vitamin C and vitamin E, and weight ratio is 1:2:5.
The present invention also provides the preparation processes of above-mentioned whitening and moisturizing facial mask liquid, comprising the following steps:
(1) by the deionized water of formula ratio, 1,3- propylene glycol, glycerin monostearate, polyacrylic acid, cetanol palmitinic acid
Ester, SIMMONDSIA CHINENSIS SEED OIL after weighing in proportion, are added in the stainless steel kettle with stirring, dissolve by heating under the stirring of revolving speed 30rpm
Completely, the constant temperature disinfection 20min and at a temperature of 80 DEG C, then adds the carboxymethyl chitosan and hyaluronic acid of formula ratio, stirs
It mixes uniformly, obtains the first mixture, for use；
(2) by the glycerol of formula ratio, algal polysaccharides, Marine fish collagen, Chinese herbal medicine extract, yeast dextran, water
Avenin, aloe zymophyte powder are solved, after weighing in proportion, is added in emulsion pot, is heated with stirring to 50 DEG C, pass through filter later
Net is extracted into stainless steel homogeneous kettle, under the stirring of 30rpm, is continued to be heated to 70 DEG C, and constant temperature disinfection 10min, is obtained second
Mixture, for use；
(3) triethanolamine is added in second mixture, is kept the temperature after stirring 2min under the conditions of 82 DEG C
15min obtains third mixture；
(4) the first mixture is slowly pumped into third mixture, and scrapes wall stirring, revolving speed increases to 60rpm, stirs
After 3min, high speed homogenization device is started, the homogeneous 5min under the high speed of 3500rpm will scrape wall revolving speed reduction of speed to 50rpm later, and
It is cooled to 50 DEG C under this revolving speed, tocopherol acetate, Symwhite-337, hydrolecithin, the card wave of formula ratio is added
Nurse, EDETATE SODIUM, Phenoxyethanol, triethanolamine and essence continue to stir 20min under same revolving speed to get the beauty
White MASQUE APAISANT HYDRATANT liquid.
Embodiment 2
The whitening and moisturizing facial mask liquid of the present embodiment, is prepared from the following raw materials in parts by weight: 60 parts of deionized water, glycerol 5
Part, 5 parts of 1,3- propylene glycol, 8 parts of glycerin monostearate, 7 parts of polyacrylic acid, 6 parts of cetanol palmitate, 4 parts of SIMMONDSIA CHINENSIS SEED OIL,
3 parts of carboxymethyl chitosan, 1.5 parts of algal polysaccharides, 0.7 part of hyaluronic acid, 1.2 parts of deep-sea fish skin collagen, Chinese herbal medicine extract
1.6 parts of object, 0.8 part of yeast dextran, hydrolysis 1 part of avenin, 0.8 part of aloe zymophyte powder, 0.4 part of tocopherol acetate,
0.6 part of Symwhite-337,0.3 part of hydrolecithin, carbomer receive 0.4 part, 0.3 part of vitamin, 0.6 part of Phenoxyethanol,
0.5 part and 0.3 part of essence of triethanolamine.
Wherein, the Chinese herbal medicine extract is the mixture of Herba Saussureae Involueratae extract, licorice and Rhizoma Atractylodis Macrocephalae root extract,
The weight ratio of the Herba Saussureae Involueratae extract, licorice and Rhizoma Atractylodis Macrocephalae root extract is 3:5:2.
Wherein, the Herba Saussureae Involueratae extract the preparation method is as follows: lanatechead saussurea herb with flower is cleaned up with drinking water, it is dry after powder
It is broken into coarse grain, 5 times 70% of lanatechead saussurea herb with flower of ethyl alcohol is added and carries out alcohol extracting, alcohol extracting 2 times, each 2h, merges alcohol extract, is concentrated into opposite
Density is 1.25 medicinal extract, lets cool, medicinal extract is put into rail mounted film drier, is dried, and after dry, is ground into fine powder,
And it sieves with 100 mesh sieve to get Herba Saussureae Involueratae extract.
The licorice the preparation method comprises the following steps: extracting liquorice, is extracted using 80%v/v alcohol reflux, extracting solution recycling
It after ethyl alcohol, then with AB-8 macroreticular resin carries out absorption passivation, and is eluted using 90%v/v ethyl alcohol, collect ethanol eluate,
Ethyl alcohol is recycled, concentration is dry to get licorice.
The Rhizoma Atractylodis Macrocephalae root extract the preparation method comprises the following steps: by coarse grain is ground into after the drinking water cleaning, drying of Rhizoma Atractylodis Macrocephalae root, add
Enter 8 times of purified waters of Rhizoma Atractylodis Macrocephalae root, decoct 2 times, decoct 2h every time, merge decoction liquor, being concentrated into relative density is 1.15 medicinal extract, is put
It is cold, 95%v/v ethyl alcohol is added and carries out alcohol precipitation, final alcohol precipitation degree is 70, it stands more than for 24 hours, extracts supernatant, be concentrated,
Being concentrated into relative density is 1.30, and medicinal extract is put into rail mounted film drier, is dried, and after dry, is ground into fine powder, and
It sieves with 100 mesh sieve to get Rhizoma Atractylodis Macrocephalae root extract.
Wherein, the hyaluronic acid is macromolecular Sodium Hyaluronate, middle numerator sodium hyaluronate and micromolecule hyaluronic acid
The mixture of sodium, and its weight ratio is 1:1:2.
Wherein, the aloe zymophyte powder is made of the substance of following parts by weight: 80 parts of aloe, hydrolysis 10 parts of royal jelly,
6 parts of peptone, 0.7 part of phosphoric acid hydrogen dimethylamino potassium, 1.5 parts of epsom salt；
Sufficiently being beaten the preparation method comprises the following steps: dry aloe is mixed with water 1:15 in mass ratio for the aloe zymophyte powder, makees
For basic liquid, hydrolysis royal jelly, peptone, phosphoric acid hydrogen dimethylamino potassium and the epsom salt of above-mentioned parts by weight are added into basal liquid
It sterilizes after mixing well, and microbe inoculation leavening, is kept for 35 DEG C of temperature, after the 54h that ferments, high-temperature sterilization, freeze-drying, i.e.,
Obtain aloe zymophyte powder.
Wherein, the microbe leaven is by Bacillus acidi lactici, bacillus licheniformis, Corynebacterium glutamicum 3:2 in mass ratio:
1 mixing gained.
Wherein, the vitamin is vitamin B, vitamin C and vitamin E, and weight ratio is 1:2:5.
The present invention also provides the preparation processes of above-mentioned whitening and moisturizing facial mask liquid, comprising the following steps:
(1) by the deionized water of formula ratio, 1,3- propylene glycol, glycerin monostearate, polyacrylic acid, cetanol palmitinic acid
Ester, SIMMONDSIA CHINENSIS SEED OIL after weighing in proportion, are added in the stainless steel kettle with stirring, heat under the stirring of revolving speed 30-50rpm
Dissolution is complete, and constant temperature disinfection 20min at a temperature of 80 DEG C, then adds the carboxymethyl chitosan and hyalomitome of formula ratio
Acid stirs evenly, and obtains the first mixture, for use；
(2) by the glycerol of formula ratio, algal polysaccharides, Marine fish collagen, Chinese herbal medicine extract, yeast dextran, water
Avenin, aloe zymophyte powder are solved, after weighing in proportion, is added in emulsion pot, is heated with stirring to 60 DEG C, pass through filter later
Net is extracted into stainless steel homogeneous kettle, under the stirring of 40rpm, is continued to be heated to 80 DEG C, and constant temperature disinfection 20min, is obtained second
Mixture, for use；
(3) triethanolamine is added in second mixture, is kept the temperature after stirring 4min under the conditions of 86 DEG C
20min obtains third mixture；
(4) the first mixture is slowly pumped into third mixture, and scrapes wall stirring, revolving speed increases to 70rpm, stirs 3-
After 5min, high speed homogenization device is started, the homogeneous 8min under the high speed of 4500rpm will scrape wall revolving speed reduction of speed to 60rpm later, and
It is cooled to 50 DEG C under this revolving speed, tocopherol acetate, Symwhite-337, hydrolecithin, the card wave of formula ratio is added
Nurse, EDETATE SODIUM, Phenoxyethanol, triethanolamine and essence continue to stir 30min under same revolving speed to get the beauty
White MASQUE APAISANT HYDRATANT liquid.
Embodiment 3
The whitening and moisturizing facial mask liquid of the present embodiment, is prepared from the following raw materials in parts by weight: 55 parts of deionized water, glycerol
3.5 parts, 3.5 parts of 1,3- propylene glycol, 6 parts of glycerin monostearate, 5 parts of polyacrylic acid, 4 parts of cetanol palmitate, Jojoba
Oily 2.5 parts, 2 parts of carboxymethyl chitosan, 1 part of algal polysaccharides, 0.5 part of hyaluronic acid, 0.8 part of deep-sea fish skin collagen, medium-height grass
1.2 parts of medicament extract, 0.6 part of yeast dextran, hydrolysis 0.7 part of avenin, 0.6 part of aloe zymophyte powder, tocopheryl acetate
0.3 part of ester, 0.5 part of Symwhite-337,0.2 part of hydrolecithin, carbomer receive 0.3 part, 0.2 part of EDETATE SODIUM, benzene oxygen
0.4 part of ethyl alcohol, 0.3 part of triethanolamine and 0.2 part of essence.
Wherein, the Chinese herbal medicine extract is the mixture of Herba Saussureae Involueratae extract, licorice and Rhizoma Atractylodis Macrocephalae root extract,
The weight ratio of the Herba Saussureae Involueratae extract, licorice and Rhizoma Atractylodis Macrocephalae root extract is 5:3:6.
Wherein, the Herba Saussureae Involueratae extract the preparation method is as follows: lanatechead saussurea herb with flower is cleaned up with drinking water, it is dry after powder
It is broken into coarse grain, 5 times 70% of lanatechead saussurea herb with flower of ethyl alcohol is added and carries out alcohol extracting, alcohol extracting 2 times, each 2h, merges alcohol extract, is concentrated into opposite
Density is 1.25 medicinal extract, lets cool, medicinal extract is put into rail mounted film drier, is dried, and after dry, is ground into fine powder,
And it sieves with 100 mesh sieve to get Herba Saussureae Involueratae extract.
The licorice the preparation method comprises the following steps: extracting liquorice, is extracted using 80%v/v alcohol reflux, extracting solution recycling
It after ethyl alcohol, then with AB-8 macroreticular resin carries out absorption passivation, and is eluted using 90%v/v ethyl alcohol, collect ethanol eluate,
Ethyl alcohol is recycled, concentration is dry to get licorice.
The Rhizoma Atractylodis Macrocephalae root extract the preparation method comprises the following steps: by coarse grain is ground into after the drinking water cleaning, drying of Rhizoma Atractylodis Macrocephalae root, add
Enter 8 times of purified waters of Rhizoma Atractylodis Macrocephalae root, decoct 2 times, decoct 2h every time, merge decoction liquor, being concentrated into relative density is 1.15 medicinal extract, is put
It is cold, 95%v/v ethyl alcohol is added and carries out alcohol precipitation, final alcohol precipitation degree is 70, it stands more than for 24 hours, extracts supernatant, be concentrated,
Being concentrated into relative density is 1.30, and medicinal extract is put into rail mounted film drier, is dried, and after dry, is ground into fine powder, and
It sieves with 100 mesh sieve to get Rhizoma Atractylodis Macrocephalae root extract.
Wherein, the hyaluronic acid is macromolecular Sodium Hyaluronate, middle numerator sodium hyaluronate and micromolecule hyaluronic acid
The mixture of sodium, and its weight ratio is 1:1:2.
Wherein, the aloe zymophyte powder is made of the substance of following parts by weight: 70 parts of aloe, hydrolysis 7.5 parts of royal jelly,
4.5 parts of peptone, 0.5 part of phosphoric acid hydrogen dimethylamino potassium, 1 part of epsom salt；
Sufficiently being beaten the preparation method comprises the following steps: dry aloe is mixed with water 1:12 in mass ratio for the aloe zymophyte powder, makees
For basic liquid, hydrolysis royal jelly, peptone, phosphoric acid hydrogen dimethylamino potassium and the epsom salt of above-mentioned parts by weight are added into basal liquid
It sterilizes after mixing well, and microbe inoculation leavening, is kept for 30 DEG C of temperature, after the 51h that ferments, high-temperature sterilization, freeze-drying, i.e.,
Obtain aloe zymophyte powder.
Wherein, the microbe leaven is by Bacillus acidi lactici, bacillus licheniformis, Corynebacterium glutamicum 3:2 in mass ratio:
1 mixing gained.
Wherein, the vitamin is vitamin B, vitamin C and vitamin E, and weight ratio is 1:2:5.
The present invention also provides the preparation processes of above-mentioned whitening and moisturizing facial mask liquid, comprising the following steps:
(1) by the deionized water of formula ratio, 1,3- propylene glycol, glycerin monostearate, polyacrylic acid, cetanol palmitinic acid
Ester, SIMMONDSIA CHINENSIS SEED OIL after weighing in proportion, are added in the stainless steel kettle with stirring, dissolve by heating under the stirring of revolving speed 40rpm
Completely, the constant temperature disinfection 20min and at a temperature of 80 DEG C, then adds the carboxymethyl chitosan and hyaluronic acid of formula ratio, stirs
It mixes uniformly, obtains the first mixture, for use；
(2) by the glycerol of formula ratio, algal polysaccharides, Marine fish collagen, Chinese herbal medicine extract, yeast dextran, water
Avenin, aloe zymophyte powder are solved, after weighing in proportion, is added in emulsion pot, is heated with stirring to 55 DEG C, pass through filter later
Net is extracted into stainless steel homogeneous kettle, under the stirring of 35rpm, is continued to be heated to 75 DEG C, and constant temperature disinfection 15min, is obtained second
Mixture, for use；
(3) triethanolamine is added in second mixture, is kept the temperature after stirring 3min under the conditions of 84 DEG C
18min obtains third mixture；
(4) the first mixture is slowly pumped into third mixture, and scrapes wall stirring, revolving speed increases to 65rpm, stirs
After 4min, high speed homogenization device is started, the homogeneous 6.5min under the high speed of 4000rpm will scrape wall revolving speed reduction of speed to 55rpm later,
And 50 DEG C are cooled under this revolving speed, tocopherol acetate, Symwhite-337, hydrolecithin, the card of formula ratio is added
Wave nurse, EDETATE SODIUM, Phenoxyethanol, triethanolamine and essence continue to stir 25min under same revolving speed to get described
Whitening and moisturizing facial mask liquid.
Embodiment 4
The whitening and moisturizing facial mask liquid of the present embodiment, is prepared from the following raw materials in parts by weight: 52 parts of deionized water, glycerol 3
Part, 3 parts of 1,3- propylene glycol, 5 parts of glycerin monostearate, 4 parts of polyacrylic acid, 3 parts of cetanol palmitate, 2 parts of SIMMONDSIA CHINENSIS SEED OIL,
1.5 parts of carboxymethyl chitosan, 0.8 part of algal polysaccharides, 0.4 part of hyaluronic acid, 0.7 part of deep-sea fish skin collagen, Chinese herbal medicine mention
Take 1 part of object, 0.5 part of yeast dextran, hydrolysis 0.6 part of avenin, 0.5 part of aloe zymophyte powder, tocopherol acetate 0.2
Part, 0.4 part of Symwhite-337,0.2 part of hydrolecithin, carbomer receive 0.3 part, 0.2 part of vitamin, Phenoxyethanol 0.4
Part, 0.2 part of triethanolamine and 0.2 part of essence.
Wherein, the Chinese herbal medicine extract is the mixture of Herba Saussureae Involueratae extract, licorice and Rhizoma Atractylodis Macrocephalae root extract,
The weight ratio of the Herba Saussureae Involueratae extract, licorice and Rhizoma Atractylodis Macrocephalae root extract is 2:7:5.
Wherein, the Herba Saussureae Involueratae extract the preparation method is as follows: lanatechead saussurea herb with flower is cleaned up with drinking water, it is dry after powder
It is broken into coarse grain, 5 times 70% of lanatechead saussurea herb with flower of ethyl alcohol is added and carries out alcohol extracting, alcohol extracting 2 times, each 2h, merges alcohol extract, is concentrated into opposite
Density is 1.25 medicinal extract, lets cool, medicinal extract is put into rail mounted film drier, is dried, and after dry, is ground into fine powder,
And it sieves with 100 mesh sieve to get Herba Saussureae Involueratae extract.
The licorice the preparation method comprises the following steps: extracting liquorice, is extracted using 80%v/v alcohol reflux, extracting solution recycling
It after ethyl alcohol, then with AB-8 macroreticular resin carries out absorption passivation, and is eluted using 90%v/v ethyl alcohol, collect ethanol eluate,
Ethyl alcohol is recycled, concentration is dry to get licorice.
The Rhizoma Atractylodis Macrocephalae root extract the preparation method comprises the following steps: by coarse grain is ground into after the drinking water cleaning, drying of Rhizoma Atractylodis Macrocephalae root, add
Enter 8 times of purified waters of Rhizoma Atractylodis Macrocephalae root, decoct 2 times, decoct 2h every time, merge decoction liquor, being concentrated into relative density is 1.15 medicinal extract, is put
It is cold, 95%v/v ethyl alcohol is added and carries out alcohol precipitation, final alcohol precipitation degree is 70, it stands more than for 24 hours, extracts supernatant, be concentrated,
Being concentrated into relative density is 1.30, and medicinal extract is put into rail mounted film drier, is dried, and after dry, is ground into fine powder, and
It sieves with 100 mesh sieve to get Rhizoma Atractylodis Macrocephalae root extract.
Wherein, the hyaluronic acid is macromolecular Sodium Hyaluronate, middle numerator sodium hyaluronate and micromolecule hyaluronic acid
The mixture of sodium, and its weight ratio is 1:1:2.
Wherein, the aloe zymophyte powder is made of the substance of following parts by weight: 65 parts of aloe, hydrolysis 6 parts of royal jelly, egg
4 parts of white peptone, 0.4 part of phosphoric acid hydrogen dimethylamino potassium, 0.8 part of epsom salt；
The aloe zymophyte powder is sufficiently beaten the preparation method comprises the following steps: dry aloe is mixed with water 1:10-15 in mass ratio,
As basic liquid, hydrolysis royal jelly, peptone, phosphoric acid hydrogen dimethylamino potassium and the seven water sulfuric acid of above-mentioned parts by weight are added into basal liquid
Magnesium sterilizes after mixing well, and microbe inoculation leavening, is kept for 25-35 DEG C of temperature, ferments after 48-54h, high-temperature sterilization is cold
It is lyophilized dry to get aloe zymophyte powder.
Wherein, the microbe leaven is by Bacillus acidi lactici, bacillus licheniformis, Corynebacterium glutamicum 3:2 in mass ratio:
1 mixing gained.
Wherein, the vitamin is vitamin B, vitamin C and vitamin E, and weight ratio is 1:2:5.
The present invention also provides the preparation processes of above-mentioned whitening and moisturizing facial mask liquid, comprising the following steps:
(1) by the deionized water of formula ratio, 1,3- propylene glycol, glycerin monostearate, polyacrylic acid, cetanol palmitinic acid
Ester, SIMMONDSIA CHINENSIS SEED OIL after weighing in proportion, are added in the stainless steel kettle with stirring, heat under the stirring of revolving speed 30-50rpm
Dissolution is complete, and constant temperature disinfection 20min at a temperature of 80 DEG C, then adds the carboxymethyl chitosan and hyalomitome of formula ratio
Acid stirs evenly, and obtains the first mixture, for use；
(2) by the glycerol of formula ratio, algal polysaccharides, Marine fish collagen, Chinese herbal medicine extract, yeast dextran, water
Avenin, aloe zymophyte powder are solved, after weighing in proportion, is added in emulsion pot, is heated with stirring to 50-60 DEG C, Zhi Houtong
Filter screen is extracted into stainless steel homogeneous kettle, under the stirring of 30-40rpm, continues to be heated to 70-80 DEG C, and constant temperature disinfection 10-
20min obtains the second mixture, for use；
(3) triethanolamine is added in second mixture, is kept the temperature after stirring 2-4min under the conditions of 82-86 DEG C
15-20min obtains third mixture；
(4) the first mixture is slowly pumped into third mixture, and scrapes wall stirring, revolving speed increases to 60-70rpm, stirs
After mixing 3-5min, high speed homogenization device is started, the homogeneous 5-8min under the high speed of 3500-4500rpm will scrape wall revolving speed reduction of speed later
To 50-60rpm, and it is cooled to 50 DEG C under this revolving speed, the tocopherol acetate, Symwhite-337, hydrogen of formula ratio is added
Change lecithin, carbomer, EDETATE SODIUM, Phenoxyethanol, triethanolamine and essence, continuation stirs 20- under same revolving speed
30min is to get the whitening and moisturizing facial mask liquid.
Embodiment 5
The whitening and moisturizing facial mask liquid of the present embodiment, is prepared from the following raw materials in parts by weight: 58 parts of deionized water, glycerol 4
Part, 4 parts of 1,3- propylene glycol, 7 parts of glycerin monostearate, 6 parts of polyacrylic acid, 5 parts of cetanol palmitate, 3 parts of SIMMONDSIA CHINENSIS SEED OIL,
2.5 parts of carboxymethyl chitosan, 1.2 parts of algal polysaccharides, 0.6 part of hyaluronic acid, 1 part of deep-sea fish skin collagen, Chinese herbal medicine extract
1.4 parts of object, 0.7 part of yeast dextran, hydrolysis 0.8 part of avenin, 0.7 part of aloe zymophyte powder, tocopherol acetate 0.3
Part, 0.5 part of Symwhite-337,0.3 part of hydrolecithin, carbomer receive 0.3 part, 0.3 part of vitamin, Phenoxyethanol 0.5
0.2 part of part, 0.4 part of triethanolamine and essence
Wherein, the Chinese herbal medicine extract is the mixture of Herba Saussureae Involueratae extract, licorice and Rhizoma Atractylodis Macrocephalae root extract,
The weight ratio of the Herba Saussureae Involueratae extract, licorice and Rhizoma Atractylodis Macrocephalae root extract is 5:1:5.
Wherein, the Herba Saussureae Involueratae extract the preparation method is as follows: lanatechead saussurea herb with flower is cleaned up with drinking water, it is dry after powder
It is broken into coarse grain, 5 times 70% of lanatechead saussurea herb with flower of ethyl alcohol is added and carries out alcohol extracting, alcohol extracting 2 times, each 2h, merges alcohol extract, is concentrated into opposite
Density is 1.25 medicinal extract, lets cool, medicinal extract is put into rail mounted film drier, is dried, and after dry, is ground into fine powder,
And it sieves with 100 mesh sieve to get Herba Saussureae Involueratae extract.
The licorice the preparation method comprises the following steps: extracting liquorice, is extracted using 80%v/v alcohol reflux, extracting solution recycling
It after ethyl alcohol, then with AB-8 macroreticular resin carries out absorption passivation, and is eluted using 90%v/v ethyl alcohol, collect ethanol eluate,
Ethyl alcohol is recycled, concentration is dry to get licorice；
The Rhizoma Atractylodis Macrocephalae root extract the preparation method comprises the following steps: by coarse grain is ground into after the drinking water cleaning, drying of Rhizoma Atractylodis Macrocephalae root, add
Enter 8 times of purified waters of Rhizoma Atractylodis Macrocephalae root, decoct 2 times, decoct 2h every time, merge decoction liquor, being concentrated into relative density is 1.15 medicinal extract, is put
It is cold, 95%v/v ethyl alcohol is added and carries out alcohol precipitation, final alcohol precipitation degree is 70, it stands more than for 24 hours, extracts supernatant, be concentrated,
Being concentrated into relative density is 1.30, and medicinal extract is put into rail mounted film drier, is dried, and after dry, is ground into fine powder, and
It sieves with 100 mesh sieve to get Rhizoma Atractylodis Macrocephalae root extract.
Wherein, the hyaluronic acid is macromolecular Sodium Hyaluronate, middle numerator sodium hyaluronate and micromolecule hyaluronic acid
The mixture of sodium, and its weight ratio is 1:1:2.
Wherein, the aloe zymophyte powder is made of the substance of following parts by weight: 75 parts of aloe, hydrolysis 9 parts of royal jelly, egg
5 parts of white peptone, 0.6 part of phosphoric acid hydrogen dimethylamino potassium, 1.2 parts of epsom salt；
Sufficiently being beaten the preparation method comprises the following steps: dry aloe is mixed with water 1:14 in mass ratio for the aloe zymophyte powder, makees
For basic liquid, hydrolysis royal jelly, peptone, phosphoric acid hydrogen dimethylamino potassium and the epsom salt of above-mentioned parts by weight are added into basal liquid
It sterilizes after mixing well, and microbe inoculation leavening, is kept for 25-35 DEG C of temperature, after the 48-54h that ferments, high-temperature sterilization, freezing
Drying is to get aloe zymophyte powder.
Wherein, the microbe leaven is by Bacillus acidi lactici, bacillus licheniformis, Corynebacterium glutamicum 3:2 in mass ratio:
1 mixing gained.
Wherein, the vitamin is vitamin B, vitamin C and vitamin E, and weight ratio is 1:2:5.
The present invention also provides the preparation processes of above-mentioned whitening and moisturizing facial mask liquid, comprising the following steps:
(1) by the deionized water of formula ratio, 1,3- propylene glycol, glycerin monostearate, polyacrylic acid, cetanol palmitinic acid
Ester, SIMMONDSIA CHINENSIS SEED OIL after weighing in proportion, are added in the stainless steel kettle with stirring, dissolve by heating under the stirring of revolving speed 45rpm
Completely, the constant temperature disinfection 20min and at a temperature of 80 DEG C, then adds the carboxymethyl chitosan and hyaluronic acid of formula ratio, stirs
It mixes uniformly, obtains the first mixture, for use；
(2) by the glycerol of formula ratio, algal polysaccharides, Marine fish collagen, Chinese herbal medicine extract, yeast dextran, water
Avenin, aloe zymophyte powder are solved, after weighing in proportion, is added in emulsion pot, is heated with stirring to 58 DEG C, pass through filter later
Net is extracted into stainless steel homogeneous kettle, under the stirring of 38rpm, is continued to be heated to 78 DEG C, and constant temperature disinfection 18min, is obtained second
Mixture, for use；
(3) triethanolamine is added in second mixture, is kept the temperature after stirring 3.5min under the conditions of 85 DEG C
19min obtains third mixture；
(4) the first mixture is slowly pumped into third mixture, and scrapes wall stirring, revolving speed increases to 68rpm, stirs
After 4.5min, high speed homogenization device is started, the homogeneous 7min under the high speed of 4200rpm will scrape wall revolving speed reduction of speed to 58rpm later,
And 50 DEG C are cooled under this revolving speed, tocopherol acetate, Symwhite-337, hydrolecithin, the card of formula ratio is added
Wave nurse, EDETATE SODIUM, Phenoxyethanol, triethanolamine and essence continue to stir 28min under same revolving speed to get described
Whitening and moisturizing facial mask liquid.
Comparative example 1
In addition to no deep-sea fish skin collagen, material content and preparation step are consistent with embodiment 1
Comparative example 2
In addition to no Chinese herbal medicine extract, material content and preparation step are consistent with embodiment 1.
Comparative example 3
In addition to no yeast dextran, material content and preparation step are consistent with embodiment 1.
Comparative example 4
In addition to without hydrolysis avenin, material content and preparation step are consistent with embodiment 1.
Comparative example 5
In addition to no aloe zymophyte powder, material content and preparation step are consistent with embodiment 1.
Test example 1
Product Safety evaluates (experiment of human skin patch)
1, trial target: whitening and moisturizing facial mask liquid prepared by embodiment 1-5, comparative example 1-5
Tested crowd's number: 50 people
Age: between 20-50 years old
Gender: 35 people of female, male 15 people
Health status: subjects skin's health, no skin disease allergies meet subject and volunteer inclusion criteria.
2, patch method: qualified spot tester is selected, with closed patch experiment method, by tested material about 0.020ml-
For 0.025ml drop in spot tester, external application special adhesive tape is covered on subject back, and tested material is removed after 24 hours, is removed respectively
Observation dermoreaction in 0.5,6,12,24,48 hour afterwards, records it according to dermoreaction grade scale in " cosmetics health specification "
As a result.
3, experimental result: human skin patch test result is shown: 50 subjects pass through embodiment 1-5, comparative example 1-5
Moisture saver mask liquid patch test, in observation dermoreaction in 0.5,6,12,24,48 hour, wherein 0 skin occur bad anti-
It answers, it is safe to illustrate that whitening and moisturizing facial mask liquid of the invention uses.
Test example 2
Product moisturizing effect measuring
1,100 female volunteers are invited, are randomly divided into 10 groups, are tried out made from embodiment 1-5, comparative example 1-5 respectively
Whitening and moisturizing facial mask liquid.Volunteer is cleaned after face using clear water and is surveyed respectively using Fiss Kai Er SK-III skin moisture detector
The moisture content of forehead, left face, right face and chin skin is tried, and takes arithmetic mean of instantaneous value, volunteer reuses above-mentioned facial mask liquid,
It is even to be applied to face, it gently pats, with skin moisture tester test forehead, left face, right face and chin same location after 10min
Skin moisture content, and take arithmetic mean of instantaneous value, skin moisture tester reused after 12h and is tested one time.Every group of 10 aspirations
The result tested is taken arithmetic mean of instantaneous value by person, test result is as follows table 1.
Wherein, skin moisture content gradient after moisture retention water 10min=use skin average water after moisture retention water 10min is used
Point-use skin average moisture before moisture retention water.
Use skin moisture content gradient after moisture retention water 12h=use skin average moisture after moisture retention water 12h-use guarantor
Skin average moisture before wet water.
1 skin moisture content test result table of table
As shown in Table 1, the moisturizing of whitening and moisturizing facial mask liquid of the invention, moistening effect are good, can not only significantly mention after use
High skin moisture content can also lock moisture, reduce water loss, and skin is made to keep long-acting water profit.Wherein with the beauty of embodiment 3
The moisturizing of white MASQUE APAISANT HYDRATANT liquid, water lock effect are best, are highly preferred embodiment of the present invention.And by comparative example 1-5 it is found that passing through
Marine fish collagen, Chinese herbal medicine extract, yeast dextran, hydrolysis avenin and aloe are added in whitening and moisturizing facial mask
Zymophyte powder can effectively improve moisturizing, the water lock effect of whitening and moisturizing facial mask.
2, (one month) the feedback conclusive table on probation of whitening and moisturizing facial mask liquid
Gender number: female, 200 people
Age: between 20-40 years old
Health status: subjects skin's health, no skin disease allergies meet subject and volunteer inclusion criteria.
Grouping: being randomly divided into 10 groups, and every group of 20 people average age 28 ± 2 years old, try out embodiment 1-5, comparative example 1- respectively
Using effect is observed and experienced to whitening and moisturizing facial mask liquid made from 5
Test method: after volunteer cleans face, film cloth is unfolded inwardly to be lightly spread in face, flicking is bonded to complete, gently
It pats to beat to skin and all absorb, it is each using primary daily morning and evening, adhere to using one month, at least checks weekly once to understand
Whether there is or not whole body and local adverse reactions, and record result in detail.Test assessment result such as the following table 2:
2 whitening and moisturizing facial mask liquid of table tries out (one month) feedback conclusive table
The whitening and moisturizing facial mask liquid of 1-5 of the embodiment of the present invention liking and approving by volunteer on probation as shown in Table 2, examination
The mild pro-skin of moisture retention water is indicated with volunteer, is easily absorbed, and using the salubrious non-greasy of rear face, moistening effect is good, tries out one month
Feel afterwards dry skin, it is coarse, low and deep etc. be improved significantly, skin water profit is smooth, flexible.In embodiment 1-5, embodiment
The degree of recognition highest of 3 whitening and moisturizing facial mask liquids, therefore embodiment 3 is highly preferred embodiment of the present invention.And the use of comparative example 1-5
Effect is not so good as embodiment 1-5, it can be seen that, by the way that Marine fish collagen, Chinese herbal medicine are added in whitening and moisturizing facial mask liquid
The guarantor of whitening and moisturizing facial mask of the present invention can be improved in extract, yeast dextran, hydrolysis avenin and aloe zymophyte powder
Wet, water lock effect.
Test example 3
The whitening and moisturizing facial mask liquid of embodiment 1-5 and comparative example 1-5 are verified, trier uses 2-3 times weekly, even
Continuous to use one month, each embodiment is chosen 10 volunteers and is tried out, and whitening effect is divided into three grades:
Whitening effect is obvious: skin obviously bleaches, and is moistened with rear skin water, and white effect protects special a whole day；
Whitening effect is general: skin has that darkening is bright, is moistened with rear skin water, and white effect protects special half a day；
Whitening effect is unchanged: skin does not bleach, but the sign also deepened without black.
Application product result on trial of the present invention is as shown in table 3:
Table 3
As shown in Table 2, the whitening function that whitening and moisturizing facial mask liquid of the invention has had, and by comparative example 1-5 it is found that logical
Cross in whitening and moisturizing facial mask liquid be added Marine fish collagen, Chinese herbal medicine extract, yeast dextran, hydrolysis avenin and
The whitening effect of whitening and moisturizing facial mask liquid can be improved in aloe zymophyte powder.
In conclusion creativeness of the invention is concentrated mainly on the following aspects:
(1) whitening moisturizing face masque liquid of the present invention contains the plant extractions ingredients such as Chinese herbal medicine extract, aloe protein hydrolysate, can
Go deep into skin bottom to keep the skin wet, can be quickly absorbed by the skin, meanwhile, Chinese herbal medicine extract is contained into whitening conditioning ingredients and reed
Whitening, antioxidant content in luxuriant growth zymophyte powder etc. organically combine, and functionally carry out balanced collocation, to guarantee
Reach efficient whitening and moistening skin effect under the premise of being perfectly safe, and the nutrients such as Marine fish collagen, hydrolysis avenin are fast
It speed and completely penetrates into skin bottom, repairs skin lines, that improves skin resists power.
(2) whitening and moisturizing facial mask liquid of the present invention contains yeast dextran, can promote skin and restores good barrier function, has
Effect reduces trans epidermal water loss, and keyed moisture plays the function of moisturizing water lock, and skin can be made tender pale, improves collagen egg
White and elastic fibers element synthesis, supplies various kinds of cell growth factor, to have the function that skin whitening.
(3) whitening and moisturizing facial mask liquid each component collaboration of the present invention, moistening effect is good, and safe and non-stimulating, while the present invention
The preparation method of whitening and moisturizing facial mask liquid is simple, can promote the use of.
Specific embodiments of the present invention are described above.It is to be appreciated that the invention is not limited to above-mentioned
Particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims, this not shadow
Ring substantive content of the invention.
Claims (8)
1. a kind of whitening and moisturizing facial mask liquid, which is characterized in that be prepared from the following raw materials in parts by weight: 50-60 parts of deionized water,
2-5 parts of glycerol, 2-5 parts of 1,3- propylene glycol, 4-8 parts of glycerin monostearate, 3-7 parts of polyacrylic acid, cetanol palmitate 2-6
Part, 1-4 parts of SIMMONDSIA CHINENSIS SEED OIL, 1-3 parts of carboxymethyl chitosan, 0.5-1.5 parts of algal polysaccharides, 0.3-0.7 parts of hyaluronic acid, deep-sea fish
0.6-1.2 parts of collagen, 0.8-1.6 parts of Chinese herbal medicine extract, 0.4-0.8 parts of yeast dextran, hydrolysis avenin
0.5-1 parts, 0.4-0.8 parts of aloe zymophyte powder, 0.2-0.4 parts of tocopherol acetate, 0.3-0.6 parts of Symwhite-337,
0.1-0.3 parts of hydrolecithin, carbomer receive 0.2-0.4 parts, 0.1-0.3 parts of vitamin, 0.3-0.6 parts of Phenoxyethanol, three second
0.1-0.5 parts and essence 0.1-0.3 parts of hydramine；
Wherein, the Chinese herbal medicine extract is the mixture of Herba Saussureae Involueratae extract, licorice and Rhizoma Atractylodis Macrocephalae root extract, described
The weight ratio of Herba Saussureae Involueratae extract, licorice and Rhizoma Atractylodis Macrocephalae root extract is (0.5-10): (0.5-10): (0.5-10)；
Wherein, the Herba Saussureae Involueratae extract the preparation method is as follows: lanatechead saussurea herb with flower is cleaned up with drinking water, crushed after being dried at
Coarse grain is added 5 times 70% of lanatechead saussurea herb with flower of ethyl alcohol and carries out alcohol extracting, alcohol extracting 2 times, each 2h, merges alcohol extract, be concentrated into relative density
It for 1.25 medicinal extract, lets cool, medicinal extract is put into rail mounted film drier, is dried, after dry, be ground into fine powder, and mistake
100 meshes are to get Herba Saussureae Involueratae extract；
The licorice the preparation method comprises the following steps: extracting liquorice, is extracted using 80%v/v alcohol reflux, extracting solution recycles ethyl alcohol
Afterwards, then with AB-8 macroreticular resin absorption passivation is carried out, and is eluted using 90%v/v ethyl alcohol, collect ethanol eluate, recycling
Ethyl alcohol, concentration are dry to get licorice；
The Rhizoma Atractylodis Macrocephalae root extract the preparation method comprises the following steps: coarse grain will be ground into after the drinking water cleaning, drying of Rhizoma Atractylodis Macrocephalae root, be added white
8 times of purified waters of art root decoct 2 times, decoct 2h every time, merge decoction liquor, and being concentrated into relative density is 1.15 medicinal extract, let cool, add
Enter 95%v/v ethyl alcohol and carry out alcohol precipitation, final alcohol precipitation degree is 70, stands more than for 24 hours, extracts supernatant, be concentrated, be concentrated into
Relative density is 1.30, and medicinal extract is put into rail mounted film drier, is dried, and after dry, is ground into fine powder, and cross 100
Mesh is to get Rhizoma Atractylodis Macrocephalae root extract.
2. whitening and moisturizing facial mask liquid according to claim 1, which is characterized in that be prepared from the following raw materials in parts by weight:
55 parts of deionized water, 3.5 parts of glycerol, 3.5 parts of 1,3- propylene glycol, 6 parts of glycerin monostearate, 5 parts of polyacrylic acid, cetanol palm fibre
4 parts of glycerin monostearate, 2.5 parts of SIMMONDSIA CHINENSIS SEED OIL, 2 parts of carboxymethyl chitosan, 1 part of algal polysaccharides, 0.5 part of hyaluronic acid, deep-sea fish hide glue
0.8 part of former albumen, 1.2 parts of Chinese herbal medicine extract, 0.6 part of yeast dextran, hydrolysis 0.7 part of avenin, aloe zymophyte powder
0.6 part, 0.3 part of tocopherol acetate, 0.5 part of Symwhite-337,0.2 part of hydrolecithin, carbomer receive 0.3 part,
0.2 part of EDETATE SODIUM, 0.4 part of Phenoxyethanol, 0.3 part of triethanolamine and 0.2 part of essence.
3. whitening and moisturizing facial mask liquid according to claim 1, which is characterized in that the Herba Saussureae Involueratae extract, Radix Glycyrrhizae are extracted
The weight ratio of object and Rhizoma Atractylodis Macrocephalae root extract is (3-7): (3-7): (3-7).
4. whitening and moisturizing facial mask liquid according to claim 1, which is characterized in that the hyaluronic acid is macromolecular hyalomitome
The mixture of sour sodium, middle numerator sodium hyaluronate and micromolecule hyaluronic acid sodium, and its weight ratio is 1:1:2.
5. whitening and moisturizing facial mask liquid according to claim 1, which is characterized in that the aloe zymophyte powder is by following weight
Part substance be made: 60-80 part of aloe, hydrolyze royal jelly 5-10 parts, 3-6 parts of peptone, 0.3-0.7 parts of phosphoric acid hydrogen dimethylamino potassium,
0.5-1.5 parts of epsom salt；
The aloe zymophyte powder is sufficiently beaten the preparation method comprises the following steps: dry aloe is mixed with water 1:10-15 in mass ratio, as
Basal liquid, hydrolysis royal jelly, peptone, phosphoric acid hydrogen dimethylamino potassium and the epsom salt that above-mentioned parts by weight are added into basal liquid fill
Divide after mixing and sterilize, and microbe inoculation leavening, kept for 25-35 DEG C of temperature, after the 48-54h that ferments, high-temperature sterilization, freezing is done
It is dry to get aloe zymophyte powder.
6. whitening and moisturizing facial mask liquid according to claim 5, which is characterized in that the microbe leaven is by lactic acid bar
Bacterium, bacillus licheniformis, Corynebacterium glutamicum 3:2:1 in mass ratio mixing gained.
7. whitening and moisturizing facial mask liquid according to claim 1, which is characterized in that the vitamin is vitamin B, vitamin
C and vitamin E, and weight ratio is 1:2:5.
8. the preparation process of whitening and moisturizing facial mask liquid according to claim 1-7, which is characterized in that including following
Step:
(1) by the deionized water of formula ratio, 1,3- propylene glycol, glycerin monostearate, polyacrylic acid, cetanol palmitate,
SIMMONDSIA CHINENSIS SEED OIL after weighing in proportion, is added in the stainless steel kettle with stirring, dissolves by heating under the stirring of revolving speed 30-50rpm
Completely, the constant temperature disinfection 20min and at a temperature of 80 DEG C, then adds the carboxymethyl chitosan and hyaluronic acid of formula ratio, stirs
It mixes uniformly, obtains the first mixture, for use；
(2) by the glycerol of formula ratio, algal polysaccharides, Marine fish collagen, Chinese herbal medicine extract, yeast dextran, hydrolysis swallow
Aleuronat, aloe zymophyte powder, after weighing in proportion, are added in emulsion pot, are heated with stirring to 50-60 DEG C, pass through filter later
Net is extracted into stainless steel homogeneous kettle, under the stirring of 30-40rpm, continues to be heated to 70-80 DEG C, and constant temperature disinfection 10-20min,
The second mixture is obtained, for use；
(3) triethanolamine is added in second mixture, keeps the temperature 15- after stirring 2-4min under the conditions of 82-86 DEG C
20min obtains third mixture；
(4) the first mixture is slowly pumped into third mixture, and scrapes wall stirring, revolving speed increases to 60-70rpm, stirs 3-
After 5min, high speed homogenization device is started, the homogeneous 5-8min under the high speed of 3500-4500rpm will scrape wall revolving speed reduction of speed later and arrive
50-60rpm, and 50 DEG C are cooled under this revolving speed, the tocopherol acetate, Symwhite-337, hydrogenation of formula ratio is added
Lecithin, carbomer, EDETATE SODIUM, Phenoxyethanol, triethanolamine and essence, continuation stir 20- under same revolving speed
30min is to get the whitening and moisturizing facial mask liquid.
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Application publication date: 20181221 |